CN107714554A - A kind of natural plants toner and its extraction and deep process - Google Patents
A kind of natural plants toner and its extraction and deep process Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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- A61K2800/59—Mixtures
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/81—Preparation or application process involves irradiation
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Abstract
The invention discloses a kind of natural plants toner and its extraction and deep process, it is related to cosmetic technical field.Wherein natural plants toner includes the component of following parts by weight：13 parts of coixan extract；13 parts of coix seed protein extract；0.5 1.5 parts of Chondrus crispus extract；15 parts of NMF；6 10 parts of film forming agent；0.1 1 parts of anti-sensitizer；0.1 0.5 parts of preservative；Water complements to 100 parts.Chondrus crispus extract and coixan extract, coix seed protein extract compounding use, Synergistic, are obviously improved moisturizing, whitening and repairing effect in the present invention；By adding aloe barbadensis Miller leaf extract, close Luo Mu leaves/stem extraction, ginkgo biloba p.e, the further moisturizing for improving toner, moist, whitening, nti-freckle, wrinkle-dispelling function；Impurity is removed by degreasing, the protein added in protease hydrolyzed coix seed so that polysaccharide is easier dissolution, then coordinates microwave and pressurised extraction technique, improves the leaching velocity and recovery rate of polysaccharide.
Description
Technical field
The present invention relates to cosmetic technical field, more specifically, it relates to a kind of natural plants toner and its extraction
With deep process.
Background technology
Recently as there is pigment on the aging of population, environmental pollution, the increasing people's skin of global warning
Imbalance is formed, foxiness, freckle, the wrinkle of skin have turned into serious skin and perplexed.Particularly skin after foxiness, freckle and Exposure to Sunlight
Black pigment calmness on skin can increase with the age and produce, increase, while be increasingly difficult to eliminate, thus can not as people
The worry avoided.
Disclosed in Publication No. CN106389257A Chinese invention patent a kind of basil anti-acne opsonic water and its
Preparation method, it includes Semen Coicis extract, and the preparation method of Semen Coicis extract is：Coix seed is weighed, adds coix seed weight 5
The deionized water of~15 times of volumes, extraction 3 times is decocted, after being heated to boiling, starts agitator once every half an hour, maintain boiling
Rise state 1~4 hour, obtain coix seed aqueous extract, cross 100~400 mesh filter clothes, filter residue adds the water of 4~12 times of volumes, stirred again
Heating is mixed, maintains fluidized state 1~3 hour, takes coix seed aqueous extract, crosses 100~400 mesh filter clothes, filter residue adds 4~12 times again
The water boiling and extraction of volume once, merges extract solution three times, is concentrated into the coix seed that 20 DEG C of relative densities are about 1.0~1.03
Concentrate, appropriate beta-schardinger dextrin or/and maltodextrin are then added, after stirring, spray drying, obtain coix seed extraction
Thing.
Using water extraction method extraction Semen Coicis extract, the problem of being primarily present, has above-mentioned patent：The rate of recovery is low, efficiency is low
And high temperature causes the destruction of heat-sensitive ingredients, and without tools such as proline, alanine and the leucines in extraction coix seed
There is the aminoacid ingredient of repair, cause the skin effects such as extract moisturizing, whitening and reparation bad.
The content of the invention
In view of the deficienciess of the prior art, the purpose of the present invention one is to provide a kind of natural plants toner, pass through
The compounding use of coixan extract, coix seed protein extract and Chondrus crispus extract, to solve above-mentioned ask
Topic, it has the advantages of moisturizing, whitening and repairing effect are good.
To achieve the above object one, the invention provides following technical scheme：
A kind of natural plants toner, include the component of following parts by weight：
Coixan extract 1-3 parts；
Coix seed protein extract 1-3 parts；
Chondrus crispus extract 0.5-1.5 parts；
NMF 1-5 parts；
Film forming agent 6-10 parts；
Anti-sensitizer 0.1-1 parts；
Preservative 0.1-0.5 parts；
Water complements to 100 parts.
Pass through above-mentioned technical proposal, in coixan extract containing mannose, galactolipin, rhamnose, arabinose,
6 kinds of monose such as glucose, xylose, it has been investigated that, coixan extract removes hydroxyl radical free radical and superoxide anion certainly
It is stronger by the ability of base, and the activity of antioxidase with anti-lipid peroxidation, can be improved, so as to reach the effect of anti-aging
Fruit；Contain proline, alanine and leucine in coix seed protein extract, these amino acid can repair muscle, connective
The damage of tissue and skin.
Chondrus crispus contains higher vitamin, mineral matter and amino acid, has the function that to supplement mineral matter and mediation.
Contain floridoside and taurine in Chondrus crispus extract, floridoside and taurine are NMF and regulation cell
The material of infiltration, skin NMF NMF synthesis can be promoted, promote skin smooth, soft, recovered epidermis and naturally shield
Hinder function, contained tax is living in Chondrus crispus and protection composition, can give skin cell moisturizing, makes skin water moisten and is full of pool.
Found through experiment, Chondrus crispus extract and coixan extract, coix seed protein extract compounding use, collaboration
Synergy, it is obviously improved moisturizing, whitening and repairing effect.
Further, the natural plants toner also includes 0.5-2.5 part aloe barbadensis Miller leaf extracts.
Pass through above-mentioned technical proposal, aloe barbadensis Miller leaf extract can be in skins while being permeated to deep skin
Top layer forms one layer of very thin ventilated membrane, stops the evaporation of moisture of skin, polysaccharide component, the amino acids material penetrated into after skin
With obviously moisturizing, moist and softening effect, strengthen the adsorptivity of cuticula and bearing water property, make the skin to follow the string
With the effect that dry cuticula is rapidly reached activation, moisture fills, recover original smooth, the soft and moist and good bullet of skin
Property, coordinate Chondrus crispus extract, coixan extract and coix seed protein extract, Synergistic, also have
The multiple efficacies such as whitening, nti-freckle, anti-wrinkle, natural sun-prevention and reparation, bactericidal antiphlogistic, anti-acne.
Further, the natural plants toner also includes the close Luo Mu leaves/stem extraction of 1-2 parts.
Pass through above-mentioned technical proposal, close Luo Mu leaves/stem extraction is natural cell activator, is had and hyalomitome acids
As efficient water lock power, but molecule is smaller than hyaluronic acid 500 times, possesses potent activation and reproducibility, can strengthen cell work
Power and metabolism, activating and regenerating Skin Cell, the inoxidizability of enhancing Skin Cell, type i collagen egg in accelerated ageing cell
The synthesis of Cynanchum glaucescens body, increase skin moisture retention, elasticity and slickness, repair skin, and with aloe barbadensis Miller leaf extract, wrinkle
Ripple chondrus extract, coixan extract and coix seed protein extract compounding use, Synergistic.
Further, the natural plants toner also includes 1-2 part ginkgo biloba p.es.
Pass through above-mentioned technical proposal, the flavones contained by ginkgo biloba p.e have strong oxygen radical removing effect,
Skin Cell can be protected not influenceed by oxygen radical over oxidation, so as to extend the life-span of Skin Cell, it coordinates coix seed
Polyoses extract can strengthen the ability of anti-aging.Lactone in ginkgo biloba p.e can also accelerate metabolism, improve blood and follow
Ring, strengthen cell viability, moisturizing, also with high-efficiency broad spectrum bactericidal action, with close Luo Mu leaves/stem extraction, Aloe Barbadensis Miller
Extract, Chondrus crispus extract, coixan extract and coix seed protein extract compounding use, collaboration increase
Effect.
The purpose of the present invention two is extraction and the deep process for providing a kind of natural plants toner, using the technique
The natural plants toner of preparation has the advantages of moisturizing, whitening and repairing effect are good.
To achieve the above object two, the invention provides following technical scheme：
A kind of extraction of natural plants toner and deep process, comprise the following steps：
Step 1, prepare coixan extract：
A, crushed after coix seed is dried, cross 50 mesh sieves, with petroleum ether or ethyl acetate degreasing, after being filtrated to get filter residue drying
It is standby；
B, filter residue and water are placed in into heated constant temperature in water-bath to extract, solid-liquid ratio 1：40, protease hydrolyzed is added, microwave adds
Hot enzyme deactivation；
C, the solution after enzyme deactivation is placed in pressurised extraction device, after sealing under 2-2.5kg/cm2 pressure pressurised extraction 1-
3h, then extract solution is filtered by vacuum, supernatant is taken, is precipitated standby；
D, the precipitation for obtaining step c repeats extraction twice, and extracting method is identical with step c；
E, it supernatant will merge three times, and be concentrated in vacuo to 0.2-0.3 times of original volume, add 90% ethanol solution of 2 times of volumes,
10h is stood, it is coixan extract that centrifugation, which obtains sediment,；
Step 2, prepare coix seed protein extract：
F, crushed after coix seed is dried, cross 50 mesh sieves, and water is placed in water-bath is heated to 60-80 DEG C together, solid-liquid ratio is
1：20, regulation system pH to alkalescence, add amylase enzymolysis starch, and extracting at constant temperature obtains leaching liquor；
G, leaching liquor is centrifuged, obtained supernatant is coix seed protein extract；
Step 3, all components are added in agitated kettle and are mixed evenly, each component is uniformly dispersed and is completely dissolved to be formed
Mixed solution, obtain natural plants toner.
Pass through above-mentioned technical proposal, before being extracted with water, degreasing removes impurity；The egg added in protease hydrolyzed coix seed
White matter so that polysaccharide is easier dissolution；Microwave has four features such as high frequency, fluctuation, thermal characteristics and non-thermal characteristics, and it is former
Reason fast steering and is aligned in microwave electromagnetic field using polar molecule in heated material, so as to produce tear and phase
Mutual friction and generate heat, have compared with traditional extraction process extraction efficiency it is high, it is quick, save solvent, save the time and the energy
Advantage.
Because coix seed quality is solid, compactness is strong, the more difficult infiltration of solvent, after applying certain pressure during extraction, can make
Some cell membranes inside coix seed are destroyed, and are advantageous to the diffusion of solvent, are accelerated the impregnation process of coix seed, are made coix seed
Quickly hydraulically full solvent in pore, improve the leaching velocity and recovery rate of polysaccharide.But pressure too Gao Shihui makes crushing
Coix seed particle aggregation afterwards together, hinders solvent fully to be contacted with it.
Further, 65-75 DEG C is heated in the step b, extraction time 7-9h.
Pass through above-mentioned technical proposal, due to the too high activity that may destroy polysaccharide of extraction temperature, therefore select relatively low temperature
Degree and longer extraction time, lost with fully extracting polysaccharide and reducing.
Further, the addition of protease is 10000-20000U, enzymolysis time 1-3h in the step b.
Pass through above-mentioned technical proposal, protein is hydrolyzed into small-molecular peptides and free amino acid with protease, reduces polysaccharide
Loss late.
Further, microwave power is 560-600W in the step b, and the microwave time is 3-6min.
Pass through above-mentioned technical proposal, being found through experiment, microwave has a significant impact to the yield of coixan extract, when
When other conditions are constant, microwave power is too low to cause coixan to be fully dissolved out, and microwave power is too high and can be certain
Coixan is set to degrade in degree；Similarly, the selection of microwave time also has an impact to the yield of coixan extract.
Further, system pH is 8-11 in the step f.
Pass through above-mentioned technical proposal, found through experiment, alkaline environment is advantageous to the extraction of coix seed protein, and pH is in 8-11
When, the extraction rate of protein is significantly improved.
Further, the addition of amylase is 5000-10000U, extraction time 1-3h in the step f.
Pass through above-mentioned technical proposal, when being extracted due to heating, starch can produce gelatinization, influence the extraction of protein, pass through
Amylase enzymolysis starch is added, reduces its gelatinization degree.
Natural plants toner in the present invention is rich in natural plant composition adlay elite, being capable of skin care, adjustment flesh
Skin state, moisten without sticky, dry position can be permeated rapidly, only need to gently pat wetting skin can keep skin smooth soft
It is soft；Also cotton pads or paper handkerchief can be used to permeate enough this product and make moisture saver mask, soak 5 minutes is better；And it can press down
System shine after burning heat sensation, ice is ice-cold cool tightens up skin；Face and whole body can be used, and can be used for moistening whole body after shower is bathed
Skin, it is safe to the human body non-stimulated without spices and pigment.
In summary, compared with prior art, the invention has the advantages that：
(1) Chondrus crispus extract and coixan extract, coix seed protein extract compounding use, collaboration increase
Effect, is obviously improved moisturizing, whitening and repairing effect；
(2) by adding aloe barbadensis Miller leaf extract, close Luo Mu leaves/stem extraction, ginkgo biloba p.e, Synergistic, enter
The moisturizing of one step raising toner, moist, whitening, nti-freckle, wrinkle-dispelling function；
(3) impurity being removed by degreasing, the protein added in protease hydrolyzed coix seed so that polysaccharide is easier dissolution, then
Coordinate microwave and pressurised extraction technique, improve the leaching velocity and recovery rate of polysaccharide.
Brief description of the drawings
Fig. 1 is the process chart of the present invention.
Embodiment
With reference to the accompanying drawings and examples, the present invention will be described in detail.
Embodiment 1：A kind of natural plants toner, each component and its corresponding parts by weight are as shown in table 1, its technique stream
Journey reference picture 1, and prepared by following steps：
Step 1, prepare coixan extract：
A, crushed after coix seed is dried, cross 50 mesh sieves, with petroleum ether or ethyl acetate degreasing, after being filtrated to get filter residue drying
It is standby；
B, filter residue and water are placed in water-bath and are heated to 65 DEG C, extracting at constant temperature, extraction time 7h, solid-liquid ratio 1：40, then
10000U protease hydrolyzeds are added, enzymolysis time 1h, microwave heating enzyme deactivation, microwave power 560W, the microwave time is 3min；
C, the solution after enzyme deactivation is placed in pressurised extraction device, after sealing under 2kg/cm2 pressure pressurised extraction 1h, then will
Extract solution is filtered by vacuum, and takes supernatant, is precipitated standby；
D, the precipitation for obtaining step c repeats extraction twice, and extracting method is identical with step c；
E, it supernatant will merge three times, and be concentrated in vacuo to 0.2-0.3 times of original volume, add 90% ethanol solution of 2 times of volumes,
10h is stood, it is coixan extract that centrifugation, which obtains sediment,；
Step 2, prepare coix seed protein extract：
F, crushed after coix seed is dried, cross 50 mesh sieves, and water is placed in water-bath and is heated to 60 DEG C together, solid-liquid ratio 1：
20, regulation system pH are 8, add 5000U amylase enzymolysis starch, extracting at constant temperature, extraction time 1h, obtain leaching liquor；
G, leaching liquor is centrifuged, obtained supernatant is coix seed protein extract；
Step 3, all components are added in agitated kettle and are mixed evenly, each component is uniformly dispersed and is completely dissolved to be formed
Mixed solution, obtain natural plants toner.
Wherein NMF is dipropylene glycol or glycerine, and film forming agent is styrene/acrylic (ester) analog copolymer, anti-sensitizer
For dipotassium glycyrrhizinate, preservative is methyl hydroxybenzoate or Nipasol.
Embodiment 2-8：A kind of natural plants toner, is with the difference of embodiment 1, each component and its corresponding
Parts by weight are as shown in table 1.
Each component and its parts by weight in the embodiment 1-8 of table 1
Embodiment 9-15：A kind of natural plants toner, is with the difference of embodiment 1, each component and its corresponding weight
It is as shown in table 2 to measure number.
Each component and its parts by weight in the embodiment 9-15 of table 2
| Component | 9 | 10 | 11 | 12 | 13 | 14 | 15 |
| Coixan extract | 1 | 1 | 1 | 1 | 1 | 1 | 1 |
| Coix seed protein extract | 1 | 1 | 1 | 1 | 1 | 1 | 1 |
| Chondrus crispus extract | 0.5 | 0.5 | 0.5 | 0.5 | 0.5 | 0.5 | 0.5 |
| NMF | 5 | 5 | 5 | 5 | 5 | 5 | 5 |
| Film forming agent | 6 | 6 | 6 | 6 | 6 | 6 | 6 |
| Anti-sensitizer | 0.1 | 0.1 | 0.1 | 0.1 | 0.1 | 0.1 | 0.1 |
| Preservative | 0.1 | 0.1 | 0.1 | 0.1 | 0.1 | 0.1 | 0.1 |
| Water | 86.3 | 86.3 | 86.3 | 86.3 | 86.3 | 86.3 | 86.3 |
| Aloe barbadensis Miller leaf extract | 0 | 0 | 0 | 0 | 0 | 0 | 0.5 |
| Close Luo Mu leaves/stem extraction | 1 | 1.5 | 2 | 0 | 0 | 0 | 1 |
| Ginkgo biloba p.e | 0 | 0 | 0 | 1 | 1.5 | 2 | 1 |
Embodiment 16：A kind of natural plants toner, is with the difference of embodiment 1, is placed in filter residue and water in step b
70 DEG C are heated in water-bath.
Embodiment 17：A kind of natural plants toner, is with the difference of embodiment 1, by filter residue and water in step b
It is placed in water-bath and is heated to 75 DEG C.
Embodiment 18：A kind of natural plants toner, it is, extraction time is in step b with the difference of embodiment 1
8h。
Embodiment 19：A kind of natural plants toner, it is, extraction time is in step b with the difference of embodiment 1
9h。
Embodiment 20：A kind of natural plants toner, is with the difference of embodiment 1, and protease adds in step b
It is 15000U to enter amount.
Embodiment 21：A kind of natural plants toner, is with the difference of embodiment 1, and protease adds in step b
It is 20000U to enter amount.
Embodiment 22：A kind of natural plants toner, it is, enzymolysis time is in step b with the difference of embodiment 1
2h。
Embodiment 23：A kind of natural plants toner, it is, enzymolysis time is in step b with the difference of embodiment 1
3h。
Embodiment 24：A kind of natural plants toner, it is, microwave power is in step b with the difference of embodiment 1
580W。
Embodiment 25：A kind of natural plants toner, it is, microwave power is in step b with the difference of embodiment 1
600W。
Embodiment 26：A kind of natural plants toner, is with the difference of embodiment 1, in step b the microwave time be
4.5min。
Embodiment 27：A kind of natural plants toner, is with the difference of embodiment 1, in step b the microwave time be
6min。
Embodiment 28：A kind of natural plants toner, is with the difference of embodiment 1, and pressurised extraction fills in step c
The pressure put is 2.25kg/cm2.
Embodiment 29：A kind of natural plants toner, is with the difference of embodiment 1, and pressurised extraction fills in step c
The pressure put is 2.5kg/cm2.
Embodiment 30：A kind of natural plants toner, is with the difference of embodiment 1, pressurised extraction in step c
2h。
Embodiment 31：A kind of natural plants toner, is with the difference of embodiment 1, pressurised extraction in step c
3h。
Embodiment 32：A kind of natural plants toner, is with the difference of embodiment 1, and 70 are heated in step f
℃。
Embodiment 33：A kind of natural plants toner, is with the difference of embodiment 1, and 80 are heated in step f
℃。
Embodiment 34：A kind of natural plants toner, is with the difference of embodiment 1, and pH is 9 in step f.
Embodiment 35：A kind of natural plants toner, is with the difference of embodiment 1, and pH is 11 in step f.
Embodiment 36：A kind of natural plants toner, is with the difference of embodiment 1, and amylase adds in step f
Dosage is 7500U.
Embodiment 37：A kind of natural plants toner, is with the difference of embodiment 1, and amylase adds in step f
Dosage is 10000U.
Embodiment 38：A kind of natural plants toner, it is, extraction time is in step f with the difference of embodiment 1
2h。
Embodiment 39：A kind of natural plants toner, it is, extraction time is in step f with the difference of embodiment 1
3h。
Comparative example 1：A kind of natural plants toner, is with the difference of embodiment 1, does not add coix seed protein
Extract and Chondrus crispus extract.
Comparative example 2：A kind of natural plants toner, is with the difference of embodiment 1, does not add coixan and carries
Take thing and Chondrus crispus extract.
Comparative example 3：A kind of natural plants toner, is with the difference of embodiment 1, does not add coixan and carries
Take thing and coix seed protein extract.
Comparative example 4：A kind of natural plants toner, is with the difference of embodiment 1, does not add coixan and carries
Take thing.
Comparative example 5：A kind of natural plants toner, is with the difference of embodiment 6, does not add coixan and carries
Take thing, coix seed protein extract and Chondrus crispus extract.
Comparative example 6：A kind of natural plants toner, is with the difference of embodiment 9, does not add coixan and carries
Take thing, coix seed protein extract and Chondrus crispus extract.
Comparative example 7：A kind of natural plants toner, is with the difference of embodiment 12, does not add coixan
Extract, coix seed protein extract and Chondrus crispus extract.
Comparative example 8：A kind of natural plants toner, is with the difference of embodiment 12, does not add coix seed albumen
Matter extract and Chondrus crispus extract.
Comparative example 9：A kind of natural plants toner, is with the difference of embodiment 1, is prepared and obtained by following steps
：
Step 1, prepare coixan extract：
A, crushed after coix seed is dried, cross 50 mesh sieves, with petroleum ether or ethyl acetate degreasing, after being filtrated to get filter residue drying
It is standby；
B, filter residue and water are placed in water-bath and are heated to 65 DEG C, extracting at constant temperature, extraction time 7h, solid-liquid ratio 1：40, then
10000U protease hydrolyzeds are added, enzymolysis time 1h, microwave heating enzyme deactivation, microwave power 560W, the microwave time is 3min；
C, extract solution is filtered by vacuum, takes supernatant, precipitated standby；
Supernatant is concentrated in vacuo to 0.2-0.3 times of original volume, add 90% ethanol solution of 2 times of volumes e, stands 10h,
It is coixan extract that centrifugation, which obtains sediment,；
Step 2, prepare coix seed protein extract：
F, crushed after coix seed is dried, cross 50 mesh sieves, and water is placed in water-bath and is heated to 60 DEG C together, solid-liquid ratio 1：
20, regulation system pH are 8, add 5000U amylase enzymolysis starch, extracting at constant temperature, extraction time 1h, obtain leaching liquor；
G, leaching liquor is centrifuged, obtained supernatant is coix seed protein extract；
Step 3, all components are added in agitated kettle and are mixed evenly, each component is uniformly dispersed and is completely dissolved to be formed
Mixed solution, obtain natural plants toner.
Comparative example 10：A kind of natural plants toner, is with the difference of embodiment 1, is prepared by following steps
Obtain：
Step 1, prepare coixan extract：
A, crushed after coix seed is dried, cross 50 mesh sieves, with petroleum ether or ethyl acetate degreasing, after being filtrated to get filter residue drying
It is standby；
B, filter residue and water are placed in water-bath and are heated to 65 DEG C, extracting at constant temperature, extraction time 7h, solid-liquid ratio 1：40；
C, the solution after extraction is placed in pressurised extraction device, after sealing under 2kg/cm2 pressure pressurised extraction 1h, then will
Extract solution is filtered by vacuum, and takes supernatant, is precipitated standby；
D, the precipitation for obtaining step c repeats extraction twice, and extracting method is identical with step c；
E, it supernatant will merge three times, and be concentrated in vacuo to 0.2-0.3 times of original volume, add 90% ethanol solution of 2 times of volumes,
10h is stood, it is coixan extract that centrifugation, which obtains sediment,；
Step 2, prepare coix seed protein extract：
F, crushed after coix seed is dried, cross 50 mesh sieves, and water is placed in water-bath and is heated to 60 DEG C together, solid-liquid ratio 1：
20, regulation system pH are 8, add 5000U amylase enzymolysis starch, extracting at constant temperature, extraction time 1h, obtain leaching liquor；
G, leaching liquor is centrifuged, obtained supernatant is coix seed protein extract；
Step 3, all components are added in agitated kettle and are mixed evenly, each component is uniformly dispersed and is completely dissolved to be formed
Mixed solution, obtain natural plants toner.
Comparative example 11：A kind of natural plants toner, each component and its corresponding parts by weight are as shown in table 1, and pass through
Following steps prepare：
Step 1, prepare coixan extract：
A, crushed after coix seed is dried, cross 50 mesh sieves, with petroleum ether or ethyl acetate degreasing, after being filtrated to get filter residue drying
It is standby；
B, filter residue and water are placed in water-bath and are heated to 65 DEG C, extracting at constant temperature, extraction time 7h, solid-liquid ratio 1：40, then
10000U protease hydrolyzeds are added, enzymolysis time 1h, microwave heating enzyme deactivation, microwave power 560W, the microwave time is 3min；
C, the solution after enzyme deactivation is placed in pressurised extraction device, after sealing under 2kg/cm2 pressure pressurised extraction 1h, then will
Extract solution is filtered by vacuum, and takes supernatant, is precipitated standby；
D, the precipitation for obtaining step c repeats extraction twice, and extracting method is identical with step c；
E, it supernatant will merge three times, and be concentrated in vacuo to 0.2-0.3 times of original volume, add 90% ethanol solution of 2 times of volumes,
10h is stood, it is coixan extract that centrifugation, which obtains sediment,；
Step 2, prepare coix seed protein extract：
F, crushed after coix seed is dried, cross 50 mesh sieves, and water is placed in water-bath and is heated to 60 DEG C together, solid-liquid ratio 1：
20, extracting at constant temperature, extraction time 1h, obtain leaching liquor；
G, leaching liquor is centrifuged, obtained supernatant is coix seed protein extract；
Step 3, all components are added in agitated kettle and are mixed evenly, each component is uniformly dispersed and is completely dissolved to be formed
Mixed solution, obtain natural plants toner.
A whitening is tested to test with moistening effect
Test specimen：Using the natural plants toner obtained in embodiment 1-39 as test specimen 1-39, using comparative example
The natural plants toner obtained in 1-11 is as control sample 1-11.
Test method：The healthy women crowd case 500 for randomly selecting 20-40 year of areal is used as subject,
The face of subject has the pigmentations such as color spot, chloasma, is divided into 50 groups, 1-50 group subject pers are washed one's face with warm water
Afterwards, to permeate enough this product using cotton pads and make moisture saver mask, soak is removed after 5 minutes, once in the morning and once at night, continuous use
2 months, determine and record the preceding change with test rear face color spot area of subject's test, and calculate color spot and reduce degree
(%), and subject is recorded using use feeling after two months and moistening effect, give up every group of maximum and minimum value,
It is remaining to take its average value.
Result of the test：1-50 group subject whitenings and moistening effect result of the test are as shown in table 3.As shown in Table 3, use
The color spot of test specimen 1-39 subject reduces level average values (%) and moisturizing water lock effect is far above control sample 1-
11, and use the color spot reduction level average values (%) of the subject of test specimen 1 and moisturizing water lock effect to be above compareing
Sample 1-3 summation, reduce level average values (%) using the color spot of the subject of test specimen 15 and moisturizing water lock effect is equal
Higher than control sample 1-3 and control sample 5-7 summation；Illustrate ginkgo biloba p.e in the present invention, close Luo Mu leaves/stem extraction
Thing, aloe barbadensis Miller leaf extract, Chondrus crispus extract, coixan extract and coix seed protein extract are answered
With use, then coordinate the extraction in the present invention and deep process, Synergistic, be obviously improved the guarantor of natural plants toner
Wet, whitening effect.
The 1-50 group subject whitenings of table 3 and moistening effect result of the test
Test the experiment of two anti-wrinkle
Test specimen：Using the natural plants toner obtained in embodiment 1-39 as test specimen 1-39, using comparative example
The natural plants toner obtained in 1-11 is as control sample 1-11.
Test method：The healthy women crowd case 500 for randomly selecting 25-40 year of areal is used as subject,
Stochastic averagina is divided into 50 groups, and the eye circumference skin of subject has the symptoms such as microgroove or wrinkle, and 1-50 group subjects make respectively
With test specimen 1-39 and control sample 1-11, application method：After being washed one's face every time with warm water, enough this product are permeated using cotton pads
Moisture saver mask is made, soak is removed after 5 minutes, twice a day.Record before subject uses and using face wrinkle after two months
The data of line quantity and depth.Give up every group of maximum and minimum value, it is remaining to take its average value, calculate wrinkle quantity and
The reduction percentage of depth.
Result of the test：1-50 group subject's anti-wrinkle test results are as shown in table 4.As shown in Table 4, using test specimen 1-
The wrinkle quantity and depth of 39 subject reduces percentage and is far above control sample 1-11, and uses test specimen 1
The wrinkle quantity and depth of subject reduces the summation that percentage is above control sample 1-3, uses the tested of test specimen 15
The wrinkle quantity and depth of person reduces the summation that percentage is above control sample 1-3 and control sample 5-7；Illustrate in the present invention
Ginkgo biloba p.e, close Luo Mu leaves/stem extraction, aloe barbadensis Miller leaf extract, Chondrus crispus extract, coixan
Extract and coix seed protein extract compounding use, then coordinate the extraction in the present invention and deep process, Synergistic,
It is obviously improved the anti-wrinkle repairing effect of natural plants toner.
The 1-50 group subject's smoothing wrinkle test results of table 4
Described above is only the preferred embodiment of the present invention, and protection scope of the present invention is not limited merely to above-described embodiment,
All technical schemes belonged under thinking of the present invention belong to protection scope of the present invention.It should be pointed out that for the art
For those of ordinary skill, some improvements and modifications without departing from the principles of the present invention, these improvements and modifications also should
It is considered as protection scope of the present invention.
Claims (10)
1. a kind of natural plants toner, it is characterised in that include the component of following parts by weight：
Coixan extract 1-3 parts；
Coix seed protein extract 1-3 parts；
Chondrus crispus extract 0.5-1.5 parts；
NMF 1-5 parts；
Film forming agent 6-10 parts；
Anti-sensitizer 0.1-1 parts；
Preservative 0.1-0.5 parts；
Water complements to 100 parts.
2. natural plants toner according to claim 1, it is characterised in that the natural plants toner also includes
0.5-2.5 part aloe barbadensis Miller leaf extracts.
3. natural plants toner according to claim 1, it is characterised in that the natural plants toner also includes 1-
2 parts of close Luo Mu leaves/stem extractions.
4. natural plants toner according to claim 1, it is characterised in that the natural plants toner also includes 1-
2 parts of ginkgo biloba p.es.
5. extraction and the deep process of a kind of natural plants toner, it is characterised in that comprise the following steps：
Step 1, prepare coixan extract：
A, crushed after coix seed is dried, cross 50 mesh sieves, with petroleum ether or ethyl acetate degreasing, after being filtrated to get filter residue drying
It is standby；
B, filter residue and water are placed in into heated constant temperature in water-bath to extract, solid-liquid ratio 1：40, protease hydrolyzed is added, microwave adds
Hot enzyme deactivation；
C, the solution after enzyme deactivation is placed in pressurised extraction device, after sealing under 2-2.5kg/cm2 pressure pressurised extraction 1-
3h, then extract solution is filtered by vacuum, supernatant is taken, is precipitated standby；
D, the precipitation for obtaining step c repeats extraction twice, and extracting method is identical with step c；
E, it supernatant will merge three times, and be concentrated in vacuo to 0.2-0.3 times of original volume, add 90% ethanol solution of 2 times of volumes,
10h is stood, it is coixan extract that centrifugation, which obtains sediment,；
Step 2, prepare coix seed protein extract：
F, crushed after coix seed is dried, cross 50 mesh sieves, and water is placed in water-bath is heated to 60-80 DEG C together, solid-liquid ratio is
1：20, regulation system pH to alkalescence, add amylase enzymolysis starch, and extracting at constant temperature obtains leaching liquor；
G, leaching liquor is centrifuged, obtained supernatant is coix seed protein extract；
Step 3, all components are added in agitated kettle and are mixed evenly, each component is uniformly dispersed and is completely dissolved to be formed
Mixed solution, obtain natural plants toner.
6. extraction and the deep process of natural plants toner according to claim 5, it is characterised in that the step
65-75 DEG C is heated in b, extraction time 7-9h.
7. extraction and the deep process of natural plants toner according to claim 5, it is characterised in that the step
The addition of protease is 10000-20000U, enzymolysis time 1-3h in b.
8. extraction and the deep process of natural plants toner according to claim 5, it is characterised in that the step
Microwave power is 560-600W in b, and the microwave time is 3-6min.
9. extraction and the deep process of natural plants toner according to claim 5, it is characterised in that the step
System pH is 8-11 in f.
10. extraction and the deep process of natural plants toner according to claim 5, it is characterised in that the step
The addition of amylase is 5000-10000U, extraction time 1-3h in rapid f.
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| CN111529416A (en) * | 2020-05-12 | 2020-08-14 | 广州怡嘉生物科技有限公司 | Powerful skin cleansing cream |
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| CN102578463A (en) * | 2012-03-20 | 2012-07-18 | 杨军 | Methods for preparing raw juice of coix seed, and preparing oral liquid, granules and buccal tablets by using raw juice of coix seed |
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Application publication date: 20180223 |