CN107714550A - A kind of preparation method of antibacterial wet tissue - Google Patents
A kind of preparation method of antibacterial wet tissue Download PDFInfo
- Publication number
- CN107714550A CN107714550A CN201711114159.6A CN201711114159A CN107714550A CN 107714550 A CN107714550 A CN 107714550A CN 201711114159 A CN201711114159 A CN 201711114159A CN 107714550 A CN107714550 A CN 107714550A
- Authority
- CN
- China
- Prior art keywords
- wet tissue
- parts
- preparation
- granatum
- antibacterial
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/99—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from microorganisms other than algae or fungi, e.g. protozoa or bacteria
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0208—Tissues; Wipes; Patches
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/88—Polyamides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
Abstract
The invention discloses a kind of preparation method of antibacterial wet tissue, belong to wet tissue technical field.The present invention utilizes granatum cultivation and fermentation in the medium,Granatum is a kind of natural plant antibacterial substance simultaneously,Composition in granatum is mainly granatin,Ursolic acid,Isoquercitrin,Mannitol and malic acid bioactive substance play bacteriostasis,So as to provide a kind of new bacterial strain with antibacterial activity,The present invention causes bacterial strain dormancy using refrigeration,Because dormancy bacterial strain is also equipped with suction-operated,Adsorbable and bacterium surface,So as to play a part of restraining and sterilizing bacteria,Simultaneously one layer of degradable macromolecule material is laid in substrate surface,So as to form a floor height molecular film,Nutriment is prevented to intracellular transport,Degradable macromolecule material can allow wet tissue biodegradable simultaneously,Avoid causing environmental pollution,The present invention is additionally added NMF,Skin conditioner,So as to be preferably bonded with skin,The problem of avoiding the damage to epiderm skin.
Description
Technical field
The invention belongs to wet tissue technical field, and in particular to a kind of preparation method of antibacterial wet tissue.
Background technology
Wet tissue, be from wet strong soft fine high osmosis base material, through fold, humidify, pack made of disposable cleaning it is hygienic
Articles for use, because its have the characteristics that cleaning, moisturizing skin basic function and be easy to carry as common in people's daily life
Cleaning supplies.It was used for such as civil aviaton, hotel, restaurant, exhibition commercial affairs and reception place in the past, in recent years as people give birth to
The flat raising of running water, the personal consumption amount of wet tissue gradually increase.At present, wet tissue has been widely used in daily life, than
Such as using wet tissue come cleaning skin, removal sweat.The species of wet tissue is also very more, such as cleaning skin, for wiping
Leather shoes, have and aim at baby's design, have and aim at Ms's design, be also accompanied with whitening or radiation resistance.Wherein, baby
Used with wet tissue in the daily nursing of infant very extensive.Baby wipes are mainly used in cleaning baby's hip,
Or face is wiped, to prevent diaper rash, infantile eczema or allergic.Baby wipes, which can typically add antiseptic, makes it possess certain resist
Bacterium function.
Generally, disposable wet tissue is used for by nonspecific crowd in the various business such as restaurant, public transport and hospital or public place
Itself clean or cleaning paediatric faecal.When being commonly used by people for wiped clean skin, wet tissue must be able to protect skin and energy is potent
Remove the foreign matter on user's skin.Therefore, wet tissue is made using soft material such as non-woven fabrics such as paper, fabrics, and in quilt
Enclose or be cut into as specific shape before loading synthetic resin packaging material and add distilled water.The main original of wet tissue
Material non-woven fabrics is by the way that fabric is parallel or placed, without fixed-direction with reference to forming it into felt shape.Wet tissue raw material includes viscous
The synthetic fibers such as glue artificial silk, polyester, polypropylene, cotton and natural pulp.When manufacturing wet tissue, prepare in wet tissue water and lead to
NMF and surfactant can often be added.Wet tissue preservative, alcohol and perfume prevent that wet tissue is contaminated, may change attached
Feed property, and reduces niff.With expanding economy, growth in the living standard, people pursue a kind of user
Just, non-stimulated to skin and have antibacterial, conditioning improves skin properties, and the wet tissue of optimum efficiency is reached to skin-friendliness.
Antibacterial wet tissue on the market is all to add chemical preservative, antiseptic again such as using soft materials such as paper, fabrics at present
Benzoic acid, sorbic acid, methyl p-hydroxybenzoate, ethyl-para-hydroxybenzoate, propylparaben, P-hydroxybenzoic acid
Prepared by the iodo- 2-propynyl butyl carbonate of butyl ester, 3-, ethanol etc., but foregoing preservatives material is that skin stimuli can draw
Skin problem is sent out, it is likely to accumulate in vulnerable children's body, and as the inducement of Atopic disease of skin；
The antiseptic that wet tissue is added is generally artificial synthesized chemical material, does not reach the effect of antibiotic cleaning not only after a number of uses
Fruit, the damage to epiderm skin is caused on the contrary, the health of baby can be affected, it is not safe enough.Therefore, produce
A kind of wet tissue of safely and effectively antibacterial is a necessary thing.
The content of the invention
The technical problems to be solved by the invention：The antiseptic added for current wet tissue is generally artificial synthesized change
Material is learned, does not reach the effect of antibiotic cleaning not only after a number of uses, the damage to epiderm skin is caused on the contrary, to baby's
Health can affect, it is not safe enough the problem of, there is provided a kind of preparation method of antibacterial wet tissue.
In order to solve the above technical problems, the present invention is using technical scheme as described below：
A kind of preparation method of antibacterial wet tissue, it is characterised in that this method comprises the following steps：
（1）After granatum is washed with water, dried, the granatum after must drying, the granatum after drying is put into crushing
Crushed in machine, obtain crushed material, crushed material, ethanol solution are subjected to mixing 8 ~ 10h of immersion, recycle supercritical carbon dioxide fluid
Extraction, obtains extract solution；
（2）Count in parts by weight, take 30 ~ 40 parts of water, 13 ~ 17 parts of agar, 8 ~ 10 parts of malt extracts, 3 ~ 5 parts of dusty yeasts, 3 ~ 5
Part glucose is well mixed, and high-temperature sterilization, obtains nutrient solution, extract solution, nutrient solution are mixed, in 25 ~ 30 DEG C of temperature
Under carry out 2 ~ 3d of fermentation, obtain zymotic fluid, zymotic fluid be placed at 3 ~ 4 DEG C and refrigerated, obtain refrigeration liquid, it is standby；
（3）Count in parts by weight, take 30 ~ 40 parts of water, 10 ~ 15 parts of polyglutamic acids, 0.1 ~ 2 part of NMF, 0.1 ~ 1 portion of skin conditioner to enter
Row mixing, and be stirred, until all dissolvings, obtain lysate；
（4）First by step（2）Standby refrigeration liquid spray is shone on base material, is stood 5 ~ 8min, must be sprayed the base material after shining, after spray is shone
Base material, lysate mixed, obtain mixture, produce antibacterial wet tissue.
The step（1）The parameter of middle supercritical carbon dioxide fluid extraction is that pressure is 15 ~ 20MPa, and temperature is 55 ~ 65
℃。
The step（2）Middle malt extract is that malt is put into pulverizer to crush, and obtains crushed material, in mass ratio 1：3~
4：0.5~0.8：0.3 ~ 0.4, crushed material, water, lactic acid, protease are subjected to heating hydrolysis, are heated to 40 ~ 50 DEG C, hydrolyzes 2 ~ 4h,
Filtering, obtains filtrate, filtrate is concentrated in vacuo at vacuum -0.09 ~ -0.05MPa, 50 ~ 60 DEG C of temperature, obtains concentrate, will
Concentrate is dried in vacuo at 50 ~ 60 DEG C of temperature, obtains dried object, dried object is put into pulverizer and crushed again, is produced
Malt extract.
The step（3）Middle NMF be glycerine, propane diols it is therein any one.
The step（3）Middle skin conditioner is in mass ratio 1：0.8 ~ 1, suet, water are mixed, produce skin conditioner.
The step（4）Base material, the mass ratio of lysate after middle spray solarization are 1：2.5~3.5.
The step（4）Middle base material is non-woven fabrics.
Compared with other method, advantageous effects are the present invention：The present invention cultivates hair in the medium using granatum
Ferment, and malt extract contains abundant organic substance in culture medium, so as to promote the growth of microorganism in extract solution, while pomegranate
Skin is a kind of natural plant antibacterial substance, and the composition in granatum is mainly granatin, ursolic acid, Isoquercitrin, sweet
Dew alcohol and malic acid bioactive substance play bacteriostasis, so as to provide a kind of new bacterial strain with antibacterial activity, this
Invention causes bacterial strain dormancy using refrigeration, because dormancy bacterial strain is also equipped with suction-operated, adsorbable and bacterium surface, so as to play
The effect of restraining and sterilizing bacteria, while one layer of degradable macromolecule material is laid in substrate surface, so as to form a floor height molecule
Film, nutriment is prevented to intracellular transport, while degradable macromolecule material can allow wet tissue biodegradable, avoid making
Into environmental pollution, the present invention is additionally added NMF, skin conditioner, so as to be preferably bonded with skin, avoids to epiderm skin
Damage the problem of.
Embodiment
Malt extract is that malt is put into pulverizer to crush, and obtains crushed material, in mass ratio 1：3~4：0.5~0.8：0.3
~ 0.4, crushed material, water, lactic acid, protease are subjected to heating hydrolysis, are heated to 40 ~ 50 DEG C, 2 ~ 4h is hydrolyzed, filtering, obtains filtrate,
Filtrate is concentrated in vacuo at vacuum -0.09 ~ -0.05MPa, 50 ~ 60 DEG C of temperature, concentrate is obtained, by concentrate in temperature
It is dried in vacuo at 50 ~ 60 DEG C, obtains dried object, dried object is put into pulverizer and crushed again, produces malt extract.
NMF be glycerine, propane diols it is therein any one.
Skin conditioner is in mass ratio 1：0.8 ~ 1, suet, water are mixed, produce skin conditioner.
Base material is non-woven fabrics.
A kind of preparation method of antibacterial wet tissue, this method comprise the following steps：
（1）After granatum is washed with water, dried, the granatum after must drying, the granatum after drying is put into crushing
Crushed in machine, obtain crushed material, in mass ratio 1：3 ~ 4, crushed material, 1.0mol/L ethanol solutions are subjected to mixing 8 ~ 10h of immersion, then
It is 15 ~ 20MPa in pressure, temperature is to be extracted at 55 ~ 65 DEG C using supercritical carbon dioxide fluid, obtains extract solution；
（2）Count in parts by weight, take 30 ~ 40 parts of water, 13 ~ 17 parts of agar, 8 ~ 10 parts of malt extracts, 3 ~ 5 parts of dusty yeasts, 3 ~ 5
Part glucose is well mixed, and high-temperature sterilization, obtains nutrient solution, in mass ratio 1：3 ~ 4, extract solution, nutrient solution are mixed,
2 ~ 3d of fermentation is carried out at 25 ~ 30 DEG C of temperature, zymotic fluid is obtained, zymotic fluid is placed at 3 ~ 4 DEG C and refrigerated, obtain refrigeration liquid, it is standby；
（3）Count in parts by weight, take 30 ~ 40 parts of water, 10 ~ 15 parts of polyglutamic acids, 0.1 ~ 2 part of NMF, 0.1 ~ 1 portion of skin conditioner to enter
Row mixing, and be stirred, until all dissolvings, obtain lysate；
（4）First by step（2）Standby refrigeration liquid spray is shone on base material, is stood 5 ~ 8min, must be sprayed the base material after shining, after spray is shone
Base material, lysate mixed, obtain mixture, produce antibacterial wet tissue.
Example 1
Malt extract is that malt is put into pulverizer to crush, and obtains crushed material, in mass ratio 1：3：0.5：0.3, by crushed material,
Water, lactic acid, protease carry out heating hydrolysis, are heated to 40 DEG C, hydrolyze 2h, filtering, obtain filtrate, by filtrate vacuum-
0.09MPa, it is concentrated in vacuo under temperature 50 C, obtains concentrate, concentrate is dried in vacuo under temperature 50 C, obtained dry
Dry thing, dried object is put into pulverizer and crushed again, produces malt extract.
NMF is glycerine.
Skin conditioner is in mass ratio 1：0.8, suet, water are mixed, produce skin conditioner.
Base material is non-woven fabrics.
A kind of preparation method of antibacterial wet tissue, this method comprise the following steps：
（1）After granatum is washed with water, dried, the granatum after must drying, the granatum after drying is put into crushing
Crushed in machine, obtain crushed material, in mass ratio 1：3, crushed material, 1.0mol/L ethanol solutions are subjected to mixing immersion 8h, then pressing
Power is 15MPa, and temperature is to be extracted at 55 DEG C using supercritical carbon dioxide fluid, obtains extract solution；
（2）Count in parts by weight, take 30 parts of water, 13 parts of agar, 8 parts of malt extracts, 3 parts of dusty yeasts, 3 parts of glucose to be mixed
Close uniformly, high-temperature sterilization, obtain nutrient solution, in mass ratio 1：3, extract solution, nutrient solution are mixed, carried out at 25 DEG C of temperature
Ferment 2d, obtains zymotic fluid, zymotic fluid is placed at 3 DEG C and refrigerated, obtain refrigeration liquid, standby；
（3）Count in parts by weight, take 30 parts of water, 10 parts of polyglutamic acids, 0.1 part of NMF, 0.1 portion of skin conditioner to be mixed, and
It is stirred, until all dissolvings, obtain lysate；
（4）First by step（2）Standby refrigeration liquid spray is shone on base material, is stood 5min, must be sprayed the base material after shining, after spray is shone
Base material, lysate are mixed, and obtain mixture, produce antibacterial wet tissue.
Example 2
Malt extract is that malt is put into pulverizer to crush, and obtains crushed material, in mass ratio 1：4：0.8：0.4, by crushed material,
Water, lactic acid, protease carry out heating hydrolysis, are heated to 50 DEG C, hydrolyze 4h, filtering, obtain filtrate, by filtrate vacuum-
0.05MPa, it is concentrated in vacuo under temperature 60 C, obtains concentrate, concentrate is dried in vacuo under temperature 60 C, obtained dry
Dry thing, dried object is put into pulverizer and crushed again, produces malt extract.
NMF is propane diols.
Skin conditioner is in mass ratio 1：0.9, suet, water are mixed, produce skin conditioner.
Base material is non-woven fabrics.
A kind of preparation method of antibacterial wet tissue, this method comprise the following steps：
（1）After granatum is washed with water, dried, the granatum after must drying, the granatum after drying is put into crushing
Crushed in machine, obtain crushed material, in mass ratio 1：4, crushed material, 1.0mol/L ethanol solutions are subjected to mixing immersion 10h, then pressing
Power is 20MPa, and temperature is to be extracted at 65 DEG C using supercritical carbon dioxide fluid, obtains extract solution；
（2）Count in parts by weight, take 40 parts of water, 17 parts of agar, 10 parts of malt extracts, 5 parts of dusty yeasts, 5 parts of glucose to carry out
It is well mixed, high-temperature sterilization, obtain nutrient solution, in mass ratio 1：4, extract solution, nutrient solution are mixed, entered at 30 DEG C of temperature
Row fermentation 3d, obtains zymotic fluid, zymotic fluid is placed at 3 DEG C and refrigerated, obtain refrigeration liquid, standby；
（3）Count in parts by weight, take 35 parts of water, 12 parts of polyglutamic acids, 0.1 part of NMF, 0.8 portion of skin conditioner to be mixed, and
It is stirred, until all dissolvings, obtain lysate；
（4）First by step（2）Standby refrigeration liquid spray is shone on base material, is stood 6min, must be sprayed the base material after shining, after spray is shone
Base material, lysate are mixed, and obtain mixture, produce antibacterial wet tissue.
Example 3
Malt extract is that malt is put into pulverizer to crush, and obtains crushed material, in mass ratio 1：3.5：0.65：0.35, by powder
Mince, water, lactic acid, protease carry out heating hydrolysis, are heated to 45 DEG C, hydrolyze 3h, filtering, obtain filtrate, by filtrate vacuum-
0.07MPa, it is concentrated in vacuo at 55 DEG C of temperature, obtains concentrate, concentrate is dried in vacuo at 55 DEG C of temperature, obtained dry
Dry thing, dried object is put into pulverizer and crushed again, produces malt extract.
NMF is glycerine.
Skin conditioner is in mass ratio 1：1, suet, water are mixed, produce skin conditioner.
Base material is non-woven fabrics.
A kind of preparation method of antibacterial wet tissue, this method comprise the following steps：
（1）After granatum is washed with water, dried, the granatum after must drying, the granatum after drying is put into crushing
Crushed in machine, obtain crushed material, in mass ratio 1：3.5, by crushed material, 1.0mol/L ethanol solutions carry out mixing immersion 9h, then
Pressure is 17MPa, and temperature is to be extracted at 60 DEG C using supercritical carbon dioxide fluid, obtains extract solution；
（2）Count in parts by weight, take 35 parts of water, 15 parts of agar, 9 parts of malt extracts, 4 parts of dusty yeasts, 4 parts of glucose to be mixed
Close uniformly, high-temperature sterilization, obtain nutrient solution, in mass ratio 1：3.5, extract solution, nutrient solution are mixed, entered at 27 DEG C of temperature
Row fermentation 2.5d, obtains zymotic fluid, zymotic fluid is placed at 4 DEG C and refrigerated, obtain refrigeration liquid, standby；
（3）Count in parts by weight, take 40 parts of water, 15 parts of polyglutamic acids, 2 parts of NMFs, 1 portion of skin conditioner to be mixed, and carried out
Stirring, until all dissolvings, obtain lysate；
（4）First by step（2）Standby refrigeration liquid spray is shone on base material, is stood 8min, must be sprayed the base material after shining, after spray is shone
Base material, lysate are mixed, and obtain mixture, produce antibacterial wet tissue.
Reference examples：The antibacterial wet tissue of Baoding company production.
Reference《GB15979-2002 disposable sanitary articles sanitary standards》Appendix C《Product bactericidal property, bacteriostasis property with
Stability test method》Sterilizing rate experiment is carried out to wet tissue, action time is 5 minutes.Test result is shown in Table 1.
Table 1：
Security test：
Healthy volunteer 40 is chosen, male 20, women 20, the age was at 20 ~ 50 years old.In isoperibol（20~22℃）, phase
To humidity 50 ± 10%, rest after 1 hour, the sample that embodiment and reference examples is respectively adopted is coated in subject's left hand forearm
Side（3cm×3cm）With right forearm inner side（3cm×3cm）, wipe daily three times, Follow-up observation one month.After one month find by
There are skin malaise symptoms in none example of examination person, and epidermis also without any damage, illustrates that the antibacterial wet tissue of the present invention will not be to human body skin
Skin has undesirable effect.
Summary, antibacterial wet tissue antibacterial effect of the invention is more preferable and harmless, is worthy to be popularized.
Claims (7)
1. a kind of preparation method of antibacterial wet tissue, it is characterised in that this method comprises the following steps：
（1）After granatum is washed with water, dried, the granatum after must drying, the granatum after drying is put into crushing
Crushed in machine, obtain crushed material, crushed material, ethanol solution are subjected to mixing 8 ~ 10h of immersion, recycle supercritical carbon dioxide fluid
Extraction, obtains extract solution；
（2）Count in parts by weight, take 30 ~ 40 parts of water, 13 ~ 17 parts of agar, 8 ~ 10 parts of malt extracts, 3 ~ 5 parts of dusty yeasts, 3 ~ 5
Part glucose is well mixed, and high-temperature sterilization, obtains nutrient solution, extract solution, nutrient solution are mixed, in 25 ~ 30 DEG C of temperature
Under carry out 2 ~ 3d of fermentation, obtain zymotic fluid, zymotic fluid be placed at 3 ~ 4 DEG C and refrigerated, obtain refrigeration liquid, it is standby；
（3）Count in parts by weight, take 30 ~ 40 parts of water, 10 ~ 15 parts of polyglutamic acids, 0.1 ~ 2 part of NMF, 0.1 ~ 1 portion of skin conditioner to enter
Row mixing, and be stirred, until all dissolvings, obtain lysate；
（4）First by step（2）Standby refrigeration liquid spray is shone on base material, is stood 5 ~ 8min, must be sprayed the base material after shining, after spray is shone
Base material, lysate mixed, obtain mixture, produce antibacterial wet tissue.
2. the preparation method of antibacterial wet tissue according to claim 1, it is characterised in that the step（1）In overcritical dioxy
The parameter for changing carbon fluid extraction is that pressure is 15 ~ 20MPa, and temperature is 55 ~ 65 DEG C.
3. the preparation method of antibacterial wet tissue according to claim 1, it is characterised in that the step（2）Middle malt extract
It is that malt is put into pulverizer to crush, obtains crushed material, in mass ratio 1：3~4：0.5~0.8：0.3 ~ 0.4, by crushed material, water,
Lactic acid, protease carry out heating hydrolysis, are heated to 40 ~ 50 DEG C, hydrolyze 2 ~ 4h, filtering, filtrate are obtained, by filtrate in vacuum -0.09
~ -0.05MPa, it is concentrated in vacuo at 50 ~ 60 DEG C of temperature, obtains concentrate, concentrate is subjected to vacuum at 50 ~ 60 DEG C of temperature
Dry, obtain dried object, dried object is put into pulverizer and crushed again, produces malt extract.
4. the preparation method of antibacterial wet tissue according to claim 1, it is characterised in that the step（3）Middle NMF is sweet
Oil, propane diols it is therein any one.
5. the preparation method of antibacterial wet tissue according to claim 1, it is characterised in that the step（3）Middle skin conditioner be by
Mass ratio 1：0.8 ~ 1, suet, water are mixed, produce skin conditioner.
6. the preparation method of antibacterial wet tissue according to claim 1, it is characterised in that the step（4）Base after middle spray solarization
Material, the mass ratio of lysate are 1：2.5~3.5.
7. the preparation method of antibacterial wet tissue according to claim 1, it is characterised in that the step（4）Middle base material is nonwoven
Cloth.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711114159.6A CN107714550A (en) | 2017-11-13 | 2017-11-13 | A kind of preparation method of antibacterial wet tissue |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711114159.6A CN107714550A (en) | 2017-11-13 | 2017-11-13 | A kind of preparation method of antibacterial wet tissue |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107714550A true CN107714550A (en) | 2018-02-23 |
Family
ID=61214613
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711114159.6A Pending CN107714550A (en) | 2017-11-13 | 2017-11-13 | A kind of preparation method of antibacterial wet tissue |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107714550A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108403534A (en) * | 2018-06-04 | 2018-08-17 | 上海克拉方今环保科技有限公司 | A kind of skin care wet tissue and its preparation method and application |
| CN110368346A (en) * | 2019-08-20 | 2019-10-25 | 上海潼舜日化用品有限公司 | A kind of antibacterial pro-skin moisture paper tissue papers and its production technology |
| CN112376164A (en) * | 2020-10-28 | 2021-02-19 | 东营俊富净化科技有限公司 | Melt-blown non-woven fabric for biomass antivirus and bacteriostatic mask and preparation method thereof |
| WO2023217004A1 (en) * | 2022-05-09 | 2023-11-16 | 萍乡小日科技有限公司 | Preparation method for antibacterial wet wipe |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20120092229A (en) * | 2011-02-11 | 2012-08-21 | 장문식 | Cosmetic composition comprising the fermented extracts of tissue cultures of brassica napus l, punica granatum and panax ginseng) |
| CN104998163A (en) * | 2015-08-01 | 2015-10-28 | 张进 | Antibacterial wet tissue paper and manufacturing method thereof |
| CN106333887A (en) * | 2016-08-30 | 2017-01-18 | 陈燕兰 | Plant extract having acne removal function and preparation method and application thereof |
| CN106478229A (en) * | 2016-09-27 | 2017-03-08 | 青岛海之源智能技术有限公司 | A kind of oil balanced in nutrition Paeonia suffruticosa special nutrient fluid and preparation method thereof |
| CN106916649A (en) * | 2015-12-25 | 2017-07-04 | 山东龙力生物科技股份有限公司 | A kind of washing product |
-
2017
- 2017-11-13 CN CN201711114159.6A patent/CN107714550A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20120092229A (en) * | 2011-02-11 | 2012-08-21 | 장문식 | Cosmetic composition comprising the fermented extracts of tissue cultures of brassica napus l, punica granatum and panax ginseng) |
| CN104998163A (en) * | 2015-08-01 | 2015-10-28 | 张进 | Antibacterial wet tissue paper and manufacturing method thereof |
| CN106916649A (en) * | 2015-12-25 | 2017-07-04 | 山东龙力生物科技股份有限公司 | A kind of washing product |
| CN106333887A (en) * | 2016-08-30 | 2017-01-18 | 陈燕兰 | Plant extract having acne removal function and preparation method and application thereof |
| CN106478229A (en) * | 2016-09-27 | 2017-03-08 | 青岛海之源智能技术有限公司 | A kind of oil balanced in nutrition Paeonia suffruticosa special nutrient fluid and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 鲁耀邦等: "《中药学》", 31 December 2015, 中国农业大学出版社 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108403534A (en) * | 2018-06-04 | 2018-08-17 | 上海克拉方今环保科技有限公司 | A kind of skin care wet tissue and its preparation method and application |
| CN110368346A (en) * | 2019-08-20 | 2019-10-25 | 上海潼舜日化用品有限公司 | A kind of antibacterial pro-skin moisture paper tissue papers and its production technology |
| CN112376164A (en) * | 2020-10-28 | 2021-02-19 | 东营俊富净化科技有限公司 | Melt-blown non-woven fabric for biomass antivirus and bacteriostatic mask and preparation method thereof |
| WO2023217004A1 (en) * | 2022-05-09 | 2023-11-16 | 萍乡小日科技有限公司 | Preparation method for antibacterial wet wipe |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN107714550A (en) | A kind of preparation method of antibacterial wet tissue | |
| CN102112106A (en) | Cosmetic composition for anti-aging of the skin comprising phaseolus radiatus seed extracts by fermentation and enzyme treatment | |
| KR102006708B1 (en) | Soap composition using wood-cultivated ginseng and soap comprising the same | |
| CN106222883A (en) | A kind of have the inner lining of automobile material that sterilization eliminates the unusual smell | |
| CN103053738A (en) | Tea-processing herba cistanche and preparation method thereof | |
| CN105534372B (en) | It is a kind of with antibacterial, disinfection towel and preparation method thereof of going to the lavatory | |
| CN112618440A (en) | Mite-removing cleaning wet tissue and preparation method thereof | |
| CN102973479A (en) | Manufacturing method of facial mask paper | |
| KR101681638B1 (en) | A method for preparing an mask-pack sheet added with the fermented extract of at least one herb consisting of Salvia miltiorrhiza B, Persicaria tinctoria H. and Siegesbeckia glabrescens Makino showing potent skin beauty treatment effect and the mask-pack sheet prepared thereby | |
| CN104783966A (en) | Method for producing antibacterial sanitary towel | |
| WO2023217004A1 (en) | Preparation method for antibacterial wet wipe | |
| CN103520032B (en) | Violet essential antibacterial wet tissue and preparation method thereof | |
| CN105640409B (en) | It is a kind of with antibacterial, disinfection towel and preparation method thereof of going to the lavatory | |
| KR102111058B1 (en) | A cosmetic composition for skin moisturizing comprising an extract of plant-derived lactobacillus brevis (ami-1109) femented barley | |
| CN103520034B (en) | Herba Lysimachiae foenum-graeci quintessence oil antibacterial wet tissue and preparation method thereof | |
| JP2021532283A (en) | Biocellulose sheet and its manufacturing method | |
| CN103494744B (en) | Anti-bacterial pogostemon cablin essential oil wet tissue and preparation method thereof | |
| KR101681639B1 (en) | A method for preparing an mask-pack sheet added with the fermented extract of at least one herb consisting of Poncirus Fructus, Torilis japonica DC and Plantaginis Semen showing potent skin beauty treatment effect and the mask-pack sheet prepared thereby | |
| CN104783970A (en) | Manufacturing method of ecological diapers | |
| CN105411987A (en) | Silk peptide moisture retention skin care product suitable for babies and preparation method therefor | |
| KR101797548B1 (en) | Mask pack composition containing velvet-extract | |
| CN104224659A (en) | Facial mask containing periplaneta americana cosmetic ingredients and preparing method thereof | |
| CN107088235A (en) | The application of soapberry and its extract in amenities is prepared | |
| KR102661205B1 (en) | Cosmetic compostion for improving skin immune system, and its preparation method | |
| CN107693482A (en) | A kind of special anti-bacteria wet keeping wet tissue of infant |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20180425 Address after: 213000 Room 502, unit 54, Lihua three village, Tianning District, Changzhou, Jiangsu, China Applicant after: Zhou Rong Address before: 213102 Changzhou, Jiangsu Tianning District, Li Hua three village 61 Ding unit 102 room Applicant before: Changzhou Kai Heng Textile Co., Ltd. |
|
| TA01 | Transfer of patent application right | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180223 |
|
| RJ01 | Rejection of invention patent application after publication |