CN107714550A - A kind of preparation method of antibacterial wet tissue - Google Patents
A kind of preparation method of antibacterial wet tissue Download PDFInfo
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- CN107714550A CN107714550A CN201711114159.6A CN201711114159A CN107714550A CN 107714550 A CN107714550 A CN 107714550A CN 201711114159 A CN201711114159 A CN 201711114159A CN 107714550 A CN107714550 A CN 107714550A
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- wet tissue
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- granatum
- antibacterial
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- 230000000844 anti-bacterial effect Effects 0.000 title claims abstract description 35
- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- 239000000463 material Substances 0.000 claims abstract description 58
- 238000005057 refrigeration Methods 0.000 claims abstract description 14
- 230000001954 sterilising effect Effects 0.000 claims abstract description 9
- 239000000203 mixture Substances 0.000 claims abstract description 8
- 238000000855 fermentation Methods 0.000 claims abstract description 6
- 230000004151 fermentation Effects 0.000 claims abstract description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 33
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 22
- 239000012530 fluid Substances 0.000 claims description 20
- 239000000284 extract Substances 0.000 claims description 19
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 14
- 239000006166 lysate Substances 0.000 claims description 14
- 239000007921 spray Substances 0.000 claims description 14
- GXCLVBGFBYZDAG-UHFFFAOYSA-N N-[2-(1H-indol-3-yl)ethyl]-N-methylprop-2-en-1-amine Chemical compound CN(CCC1=CNC2=C1C=CC=C2)CC=C GXCLVBGFBYZDAG-UHFFFAOYSA-N 0.000 claims description 12
- 239000012141 concentrate Substances 0.000 claims description 12
- 238000001035 drying Methods 0.000 claims description 12
- 239000000706 filtrate Substances 0.000 claims description 12
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 claims description 12
- 239000007788 liquid Substances 0.000 claims description 12
- 235000015097 nutrients Nutrition 0.000 claims description 12
- 238000002156 mixing Methods 0.000 claims description 9
- 238000000034 method Methods 0.000 claims description 8
- 239000001569 carbon dioxide Substances 0.000 claims description 7
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 7
- 229920001817 Agar Polymers 0.000 claims description 6
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims description 6
- 108091005804 Peptidases Proteins 0.000 claims description 6
- 239000004365 Protease Substances 0.000 claims description 6
- 102100037486 Reverse transcriptase/ribonuclease H Human genes 0.000 claims description 6
- 240000004808 Saccharomyces cerevisiae Species 0.000 claims description 6
- 239000008272 agar Substances 0.000 claims description 6
- 238000001914 filtration Methods 0.000 claims description 6
- 239000008103 glucose Substances 0.000 claims description 6
- 238000010438 heat treatment Methods 0.000 claims description 6
- 230000007062 hydrolysis Effects 0.000 claims description 6
- 238000006460 hydrolysis reaction Methods 0.000 claims description 6
- 238000007654 immersion Methods 0.000 claims description 6
- 239000004310 lactic acid Substances 0.000 claims description 6
- 235000014655 lactic acid Nutrition 0.000 claims description 6
- 229920002643 polyglutamic acid Polymers 0.000 claims description 6
- 238000004659 sterilization and disinfection Methods 0.000 claims description 6
- 238000000605 extraction Methods 0.000 claims description 4
- 239000004744 fabric Substances 0.000 claims description 4
- ULWHHBHJGPPBCO-UHFFFAOYSA-N propane-1,1-diol Chemical class CCC(O)O ULWHHBHJGPPBCO-UHFFFAOYSA-N 0.000 claims description 4
- 235000009508 confectionery Nutrition 0.000 claims description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims 1
- 241000790917 Dioxys <bee> Species 0.000 claims 1
- 229910052799 carbon Inorganic materials 0.000 claims 1
- 239000000126 substance Substances 0.000 abstract description 7
- 230000001580 bacterial effect Effects 0.000 abstract description 6
- 241000894006 Bacteria Species 0.000 abstract description 5
- 230000006378 damage Effects 0.000 abstract description 4
- 230000005059 dormancy Effects 0.000 abstract description 4
- 229920002521 macromolecule Polymers 0.000 abstract description 4
- WCGUUGGRBIKTOS-GPOJBZKASA-N (3beta)-3-hydroxyurs-12-en-28-oic acid Chemical compound C1C[C@H](O)C(C)(C)[C@@H]2CC[C@@]3(C)[C@]4(C)CC[C@@]5(C(O)=O)CC[C@@H](C)[C@H](C)[C@H]5C4=CC[C@@H]3[C@]21C WCGUUGGRBIKTOS-GPOJBZKASA-N 0.000 abstract description 2
- BJEPYKJPYRNKOW-REOHCLBHSA-N (S)-malic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O BJEPYKJPYRNKOW-REOHCLBHSA-N 0.000 abstract description 2
- OVSQVDMCBVZWGM-IDRAQACASA-N Hirsutrin Natural products O([C@H]1[C@H](O)[C@H](O)[C@H](O)[C@@H](CO)O1)C1=C(c2cc(O)c(O)cc2)Oc2c(c(O)cc(O)c2)C1=O OVSQVDMCBVZWGM-IDRAQACASA-N 0.000 abstract description 2
- FVQOMEDMFUMIMO-UHFFFAOYSA-N Hyperosid Natural products OC1C(O)C(O)C(CO)OC1OC1C(=O)C2=C(O)C=C(O)C=C2OC1C1=CC=C(O)C(O)=C1 FVQOMEDMFUMIMO-UHFFFAOYSA-N 0.000 abstract description 2
- BJEPYKJPYRNKOW-UHFFFAOYSA-N alpha-hydroxysuccinic acid Natural products OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 abstract description 2
- 230000000975 bioactive effect Effects 0.000 abstract description 2
- 238000003912 environmental pollution Methods 0.000 abstract description 2
- 229930187533 granatin Natural products 0.000 abstract description 2
- 230000010189 intracellular transport Effects 0.000 abstract description 2
- GXMWXESSGGEWEM-UHFFFAOYSA-N isoquercitrin Natural products OCC(O)C1OC(OC2C(Oc3cc(O)cc(O)c3C2=O)c4ccc(O)c(O)c4)C(O)C1O GXMWXESSGGEWEM-UHFFFAOYSA-N 0.000 abstract description 2
- 239000001630 malic acid Substances 0.000 abstract description 2
- 235000011090 malic acid Nutrition 0.000 abstract description 2
- OVSQVDMCBVZWGM-QSOFNFLRSA-N quercetin 3-O-beta-D-glucopyranoside Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1OC1=C(C=2C=C(O)C(O)=CC=2)OC2=CC(O)=CC(O)=C2C1=O OVSQVDMCBVZWGM-QSOFNFLRSA-N 0.000 abstract description 2
- 230000000452 restraining effect Effects 0.000 abstract description 2
- 239000000758 substrate Substances 0.000 abstract description 2
- 229940096998 ursolic acid Drugs 0.000 abstract description 2
- PLSAJKYPRJGMHO-UHFFFAOYSA-N ursolic acid Natural products CC1CCC2(CCC3(C)C(C=CC4C5(C)CCC(O)C(C)(C)C5CCC34C)C2C1C)C(=O)O PLSAJKYPRJGMHO-UHFFFAOYSA-N 0.000 abstract description 2
- FBPFZTCFMRRESA-KVTDHHQDSA-N D-Mannitol Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-KVTDHHQDSA-N 0.000 abstract 1
- 229930195725 Mannitol Natural products 0.000 abstract 1
- 235000010355 mannitol Nutrition 0.000 abstract 1
- 239000000594 mannitol Substances 0.000 abstract 1
- 239000002120 nanofilm Substances 0.000 abstract 1
- 210000001519 tissue Anatomy 0.000 description 39
- 210000003491 skin Anatomy 0.000 description 32
- 238000004140 cleaning Methods 0.000 description 9
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 8
- 239000004745 nonwoven fabric Substances 0.000 description 7
- 230000000694 effects Effects 0.000 description 5
- 230000002421 anti-septic effect Effects 0.000 description 4
- 235000011187 glycerol Nutrition 0.000 description 4
- 239000003755 preservative agent Substances 0.000 description 3
- FJKROLUGYXJWQN-UHFFFAOYSA-N 4-hydroxybenzoic acid Chemical compound OC(=O)C1=CC=C(O)C=C1 FJKROLUGYXJWQN-UHFFFAOYSA-N 0.000 description 2
- 241000282414 Homo sapiens Species 0.000 description 2
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 2
- 230000003115 biocidal effect Effects 0.000 description 2
- NUVBSKCKDOMJSU-UHFFFAOYSA-N ethylparaben Chemical compound CCOC(=O)C1=CC=C(O)C=C1 NUVBSKCKDOMJSU-UHFFFAOYSA-N 0.000 description 2
- 210000000245 forearm Anatomy 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 230000002335 preservative effect Effects 0.000 description 2
- 238000003825 pressing Methods 0.000 description 2
- QELSKZZBTMNZEB-UHFFFAOYSA-N propylparaben Chemical compound CCCOC(=O)C1=CC=C(O)C=C1 QELSKZZBTMNZEB-UHFFFAOYSA-N 0.000 description 2
- 239000007779 soft material Substances 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 229940090248 4-hydroxybenzoic acid Drugs 0.000 description 1
- 229920002955 Art silk Polymers 0.000 description 1
- 208000012657 Atopic disease Diseases 0.000 description 1
- 239000005711 Benzoic acid Substances 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- 206010012444 Dermatitis diaper Diseases 0.000 description 1
- 208000003105 Diaper Rash Diseases 0.000 description 1
- 206010014198 Eczema infantile Diseases 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 239000004743 Polypropylene Substances 0.000 description 1
- 244000294611 Punica granatum Species 0.000 description 1
- 235000014360 Punica granatum Nutrition 0.000 description 1
- 230000000172 allergic effect Effects 0.000 description 1
- 201000008937 atopic dermatitis Diseases 0.000 description 1
- 208000010668 atopic eczema Diseases 0.000 description 1
- 235000010233 benzoic acid Nutrition 0.000 description 1
- KDNLGZKGICMVBZ-UHFFFAOYSA-N butyl 3-iodoprop-2-ynyl carbonate Chemical compound CCCCOC(=O)OCC#CI KDNLGZKGICMVBZ-UHFFFAOYSA-N 0.000 description 1
- 230000003750 conditioning effect Effects 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 210000002615 epidermis Anatomy 0.000 description 1
- BEFDCLMNVWHSGT-UHFFFAOYSA-N ethenylcyclopentane Chemical compound C=CC1CCCC1 BEFDCLMNVWHSGT-UHFFFAOYSA-N 0.000 description 1
- 239000004403 ethyl p-hydroxybenzoate Substances 0.000 description 1
- 235000010228 ethyl p-hydroxybenzoate Nutrition 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 239000001963 growth medium Substances 0.000 description 1
- 239000010985 leather Substances 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 206010025482 malaise Diseases 0.000 description 1
- 239000002609 medium Substances 0.000 description 1
- 239000004292 methyl p-hydroxybenzoate Substances 0.000 description 1
- 235000010270 methyl p-hydroxybenzoate Nutrition 0.000 description 1
- LXCFILQKKLGQFO-UHFFFAOYSA-N methylparaben Chemical compound COC(=O)C1=CC=C(O)C=C1 LXCFILQKKLGQFO-UHFFFAOYSA-N 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 230000003020 moisturizing effect Effects 0.000 description 1
- 230000000474 nursing effect Effects 0.000 description 1
- 239000005022 packaging material Substances 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 229920000728 polyester Polymers 0.000 description 1
- -1 polypropylene Polymers 0.000 description 1
- 229920001155 polypropylene Polymers 0.000 description 1
- 230000003389 potentiating effect Effects 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 239000004405 propyl p-hydroxybenzoate Substances 0.000 description 1
- 235000010232 propyl p-hydroxybenzoate Nutrition 0.000 description 1
- 229960003415 propylparaben Drugs 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- DCKVNWZUADLDEH-UHFFFAOYSA-N sec-butyl acetate Chemical compound CCC(C)OC(C)=O DCKVNWZUADLDEH-UHFFFAOYSA-N 0.000 description 1
- 230000037380 skin damage Effects 0.000 description 1
- 230000005808 skin problem Effects 0.000 description 1
- 239000004334 sorbic acid Substances 0.000 description 1
- 235000010199 sorbic acid Nutrition 0.000 description 1
- 229940075582 sorbic acid Drugs 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 238000013112 stability test Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 210000004243 sweat Anatomy 0.000 description 1
- 208000024891 symptom Diseases 0.000 description 1
- 229920002994 synthetic fiber Polymers 0.000 description 1
- 239000012209 synthetic fiber Substances 0.000 description 1
- 229920003002 synthetic resin Polymers 0.000 description 1
- 239000000057 synthetic resin Substances 0.000 description 1
- 230000032258 transport Effects 0.000 description 1
- 230000002087 whitening effect Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/99—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from microorganisms other than algae or fungi, e.g. protozoa or bacteria
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0208—Tissues; Wipes; Patches
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/88—Polyamides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- Animal Behavior & Ethology (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Engineering & Computer Science (AREA)
- Dermatology (AREA)
- Biotechnology (AREA)
- Emergency Medicine (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Biomedical Technology (AREA)
- Tropical Medicine & Parasitology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of preparation method of antibacterial wet tissue, belong to wet tissue technical field.The present invention utilizes granatum cultivation and fermentation in the medium,Granatum is a kind of natural plant antibacterial substance simultaneously,Composition in granatum is mainly granatin,Ursolic acid,Isoquercitrin,Mannitol and malic acid bioactive substance play bacteriostasis,So as to provide a kind of new bacterial strain with antibacterial activity,The present invention causes bacterial strain dormancy using refrigeration,Because dormancy bacterial strain is also equipped with suction-operated,Adsorbable and bacterium surface,So as to play a part of restraining and sterilizing bacteria,Simultaneously one layer of degradable macromolecule material is laid in substrate surface,So as to form a floor height molecular film,Nutriment is prevented to intracellular transport,Degradable macromolecule material can allow wet tissue biodegradable simultaneously,Avoid causing environmental pollution,The present invention is additionally added NMF,Skin conditioner,So as to be preferably bonded with skin,The problem of avoiding the damage to epiderm skin.
Description
Technical field
The invention belongs to wet tissue technical field, and in particular to a kind of preparation method of antibacterial wet tissue.
Background technology
Wet tissue, be from wet strong soft fine high osmosis base material, through fold, humidify, pack made of disposable cleaning it is hygienic
Articles for use, because its have the characteristics that cleaning, moisturizing skin basic function and be easy to carry as common in people's daily life
Cleaning supplies.It was used for such as civil aviaton, hotel, restaurant, exhibition commercial affairs and reception place in the past, in recent years as people give birth to
The flat raising of running water, the personal consumption amount of wet tissue gradually increase.At present, wet tissue has been widely used in daily life, than
Such as using wet tissue come cleaning skin, removal sweat.The species of wet tissue is also very more, such as cleaning skin, for wiping
Leather shoes, have and aim at baby's design, have and aim at Ms's design, be also accompanied with whitening or radiation resistance.Wherein, baby
Used with wet tissue in the daily nursing of infant very extensive.Baby wipes are mainly used in cleaning baby's hip,
Or face is wiped, to prevent diaper rash, infantile eczema or allergic.Baby wipes, which can typically add antiseptic, makes it possess certain resist
Bacterium function.
Generally, disposable wet tissue is used for by nonspecific crowd in the various business such as restaurant, public transport and hospital or public place
Itself clean or cleaning paediatric faecal.When being commonly used by people for wiped clean skin, wet tissue must be able to protect skin and energy is potent
Remove the foreign matter on user's skin.Therefore, wet tissue is made using soft material such as non-woven fabrics such as paper, fabrics, and in quilt
Enclose or be cut into as specific shape before loading synthetic resin packaging material and add distilled water.The main original of wet tissue
Material non-woven fabrics is by the way that fabric is parallel or placed, without fixed-direction with reference to forming it into felt shape.Wet tissue raw material includes viscous
The synthetic fibers such as glue artificial silk, polyester, polypropylene, cotton and natural pulp.When manufacturing wet tissue, prepare in wet tissue water and lead to
NMF and surfactant can often be added.Wet tissue preservative, alcohol and perfume prevent that wet tissue is contaminated, may change attached
Feed property, and reduces niff.With expanding economy, growth in the living standard, people pursue a kind of user
Just, non-stimulated to skin and have antibacterial, conditioning improves skin properties, and the wet tissue of optimum efficiency is reached to skin-friendliness.
Antibacterial wet tissue on the market is all to add chemical preservative, antiseptic again such as using soft materials such as paper, fabrics at present
Benzoic acid, sorbic acid, methyl p-hydroxybenzoate, ethyl-para-hydroxybenzoate, propylparaben, P-hydroxybenzoic acid
Prepared by the iodo- 2-propynyl butyl carbonate of butyl ester, 3-, ethanol etc., but foregoing preservatives material is that skin stimuli can draw
Skin problem is sent out, it is likely to accumulate in vulnerable children's body, and as the inducement of Atopic disease of skin；
The antiseptic that wet tissue is added is generally artificial synthesized chemical material, does not reach the effect of antibiotic cleaning not only after a number of uses
Fruit, the damage to epiderm skin is caused on the contrary, the health of baby can be affected, it is not safe enough.Therefore, produce
A kind of wet tissue of safely and effectively antibacterial is a necessary thing.
The content of the invention
The technical problems to be solved by the invention：The antiseptic added for current wet tissue is generally artificial synthesized change
Material is learned, does not reach the effect of antibiotic cleaning not only after a number of uses, the damage to epiderm skin is caused on the contrary, to baby's
Health can affect, it is not safe enough the problem of, there is provided a kind of preparation method of antibacterial wet tissue.
In order to solve the above technical problems, the present invention is using technical scheme as described below：
A kind of preparation method of antibacterial wet tissue, it is characterised in that this method comprises the following steps：
（1）After granatum is washed with water, dried, the granatum after must drying, the granatum after drying is put into crushing
Crushed in machine, obtain crushed material, crushed material, ethanol solution are subjected to mixing 8 ~ 10h of immersion, recycle supercritical carbon dioxide fluid
Extraction, obtains extract solution；
（2）Count in parts by weight, take 30 ~ 40 parts of water, 13 ~ 17 parts of agar, 8 ~ 10 parts of malt extracts, 3 ~ 5 parts of dusty yeasts, 3 ~ 5
Part glucose is well mixed, and high-temperature sterilization, obtains nutrient solution, extract solution, nutrient solution are mixed, in 25 ~ 30 DEG C of temperature
Under carry out 2 ~ 3d of fermentation, obtain zymotic fluid, zymotic fluid be placed at 3 ~ 4 DEG C and refrigerated, obtain refrigeration liquid, it is standby；
（3）Count in parts by weight, take 30 ~ 40 parts of water, 10 ~ 15 parts of polyglutamic acids, 0.1 ~ 2 part of NMF, 0.1 ~ 1 portion of skin conditioner to enter
Row mixing, and be stirred, until all dissolvings, obtain lysate；
（4）First by step（2）Standby refrigeration liquid spray is shone on base material, is stood 5 ~ 8min, must be sprayed the base material after shining, after spray is shone
Base material, lysate mixed, obtain mixture, produce antibacterial wet tissue.
The step（1）The parameter of middle supercritical carbon dioxide fluid extraction is that pressure is 15 ~ 20MPa, and temperature is 55 ~ 65
℃。
The step（2）Middle malt extract is that malt is put into pulverizer to crush, and obtains crushed material, in mass ratio 1：3~
4：0.5~0.8：0.3 ~ 0.4, crushed material, water, lactic acid, protease are subjected to heating hydrolysis, are heated to 40 ~ 50 DEG C, hydrolyzes 2 ~ 4h,
Filtering, obtains filtrate, filtrate is concentrated in vacuo at vacuum -0.09 ~ -0.05MPa, 50 ~ 60 DEG C of temperature, obtains concentrate, will
Concentrate is dried in vacuo at 50 ~ 60 DEG C of temperature, obtains dried object, dried object is put into pulverizer and crushed again, is produced
Malt extract.
The step（3）Middle NMF be glycerine, propane diols it is therein any one.
The step（3）Middle skin conditioner is in mass ratio 1：0.8 ~ 1, suet, water are mixed, produce skin conditioner.
The step（4）Base material, the mass ratio of lysate after middle spray solarization are 1：2.5~3.5.
The step（4）Middle base material is non-woven fabrics.
Compared with other method, advantageous effects are the present invention：The present invention cultivates hair in the medium using granatum
Ferment, and malt extract contains abundant organic substance in culture medium, so as to promote the growth of microorganism in extract solution, while pomegranate
Skin is a kind of natural plant antibacterial substance, and the composition in granatum is mainly granatin, ursolic acid, Isoquercitrin, sweet
Dew alcohol and malic acid bioactive substance play bacteriostasis, so as to provide a kind of new bacterial strain with antibacterial activity, this
Invention causes bacterial strain dormancy using refrigeration, because dormancy bacterial strain is also equipped with suction-operated, adsorbable and bacterium surface, so as to play
The effect of restraining and sterilizing bacteria, while one layer of degradable macromolecule material is laid in substrate surface, so as to form a floor height molecule
Film, nutriment is prevented to intracellular transport, while degradable macromolecule material can allow wet tissue biodegradable, avoid making
Into environmental pollution, the present invention is additionally added NMF, skin conditioner, so as to be preferably bonded with skin, avoids to epiderm skin
Damage the problem of.
Embodiment
Malt extract is that malt is put into pulverizer to crush, and obtains crushed material, in mass ratio 1：3~4：0.5~0.8：0.3
~ 0.4, crushed material, water, lactic acid, protease are subjected to heating hydrolysis, are heated to 40 ~ 50 DEG C, 2 ~ 4h is hydrolyzed, filtering, obtains filtrate,
Filtrate is concentrated in vacuo at vacuum -0.09 ~ -0.05MPa, 50 ~ 60 DEG C of temperature, concentrate is obtained, by concentrate in temperature
It is dried in vacuo at 50 ~ 60 DEG C, obtains dried object, dried object is put into pulverizer and crushed again, produces malt extract.
NMF be glycerine, propane diols it is therein any one.
Skin conditioner is in mass ratio 1：0.8 ~ 1, suet, water are mixed, produce skin conditioner.
Base material is non-woven fabrics.
A kind of preparation method of antibacterial wet tissue, this method comprise the following steps：
（1）After granatum is washed with water, dried, the granatum after must drying, the granatum after drying is put into crushing
Crushed in machine, obtain crushed material, in mass ratio 1：3 ~ 4, crushed material, 1.0mol/L ethanol solutions are subjected to mixing 8 ~ 10h of immersion, then
It is 15 ~ 20MPa in pressure, temperature is to be extracted at 55 ~ 65 DEG C using supercritical carbon dioxide fluid, obtains extract solution；
（2）Count in parts by weight, take 30 ~ 40 parts of water, 13 ~ 17 parts of agar, 8 ~ 10 parts of malt extracts, 3 ~ 5 parts of dusty yeasts, 3 ~ 5
Part glucose is well mixed, and high-temperature sterilization, obtains nutrient solution, in mass ratio 1：3 ~ 4, extract solution, nutrient solution are mixed,
2 ~ 3d of fermentation is carried out at 25 ~ 30 DEG C of temperature, zymotic fluid is obtained, zymotic fluid is placed at 3 ~ 4 DEG C and refrigerated, obtain refrigeration liquid, it is standby；
（3）Count in parts by weight, take 30 ~ 40 parts of water, 10 ~ 15 parts of polyglutamic acids, 0.1 ~ 2 part of NMF, 0.1 ~ 1 portion of skin conditioner to enter
Row mixing, and be stirred, until all dissolvings, obtain lysate；
（4）First by step（2）Standby refrigeration liquid spray is shone on base material, is stood 5 ~ 8min, must be sprayed the base material after shining, after spray is shone
Base material, lysate mixed, obtain mixture, produce antibacterial wet tissue.
Example 1
Malt extract is that malt is put into pulverizer to crush, and obtains crushed material, in mass ratio 1：3：0.5：0.3, by crushed material,
Water, lactic acid, protease carry out heating hydrolysis, are heated to 40 DEG C, hydrolyze 2h, filtering, obtain filtrate, by filtrate vacuum-
0.09MPa, it is concentrated in vacuo under temperature 50 C, obtains concentrate, concentrate is dried in vacuo under temperature 50 C, obtained dry
Dry thing, dried object is put into pulverizer and crushed again, produces malt extract.
NMF is glycerine.
Skin conditioner is in mass ratio 1：0.8, suet, water are mixed, produce skin conditioner.
Base material is non-woven fabrics.
A kind of preparation method of antibacterial wet tissue, this method comprise the following steps：
（1）After granatum is washed with water, dried, the granatum after must drying, the granatum after drying is put into crushing
Crushed in machine, obtain crushed material, in mass ratio 1：3, crushed material, 1.0mol/L ethanol solutions are subjected to mixing immersion 8h, then pressing
Power is 15MPa, and temperature is to be extracted at 55 DEG C using supercritical carbon dioxide fluid, obtains extract solution；
（2）Count in parts by weight, take 30 parts of water, 13 parts of agar, 8 parts of malt extracts, 3 parts of dusty yeasts, 3 parts of glucose to be mixed
Close uniformly, high-temperature sterilization, obtain nutrient solution, in mass ratio 1：3, extract solution, nutrient solution are mixed, carried out at 25 DEG C of temperature
Ferment 2d, obtains zymotic fluid, zymotic fluid is placed at 3 DEG C and refrigerated, obtain refrigeration liquid, standby；
（3）Count in parts by weight, take 30 parts of water, 10 parts of polyglutamic acids, 0.1 part of NMF, 0.1 portion of skin conditioner to be mixed, and
It is stirred, until all dissolvings, obtain lysate；
（4）First by step（2）Standby refrigeration liquid spray is shone on base material, is stood 5min, must be sprayed the base material after shining, after spray is shone
Base material, lysate are mixed, and obtain mixture, produce antibacterial wet tissue.
Example 2
Malt extract is that malt is put into pulverizer to crush, and obtains crushed material, in mass ratio 1：4：0.8：0.4, by crushed material,
Water, lactic acid, protease carry out heating hydrolysis, are heated to 50 DEG C, hydrolyze 4h, filtering, obtain filtrate, by filtrate vacuum-
0.05MPa, it is concentrated in vacuo under temperature 60 C, obtains concentrate, concentrate is dried in vacuo under temperature 60 C, obtained dry
Dry thing, dried object is put into pulverizer and crushed again, produces malt extract.
NMF is propane diols.
Skin conditioner is in mass ratio 1：0.9, suet, water are mixed, produce skin conditioner.
Base material is non-woven fabrics.
A kind of preparation method of antibacterial wet tissue, this method comprise the following steps：
（1）After granatum is washed with water, dried, the granatum after must drying, the granatum after drying is put into crushing
Crushed in machine, obtain crushed material, in mass ratio 1：4, crushed material, 1.0mol/L ethanol solutions are subjected to mixing immersion 10h, then pressing
Power is 20MPa, and temperature is to be extracted at 65 DEG C using supercritical carbon dioxide fluid, obtains extract solution；
（2）Count in parts by weight, take 40 parts of water, 17 parts of agar, 10 parts of malt extracts, 5 parts of dusty yeasts, 5 parts of glucose to carry out
It is well mixed, high-temperature sterilization, obtain nutrient solution, in mass ratio 1：4, extract solution, nutrient solution are mixed, entered at 30 DEG C of temperature
Row fermentation 3d, obtains zymotic fluid, zymotic fluid is placed at 3 DEG C and refrigerated, obtain refrigeration liquid, standby；
（3）Count in parts by weight, take 35 parts of water, 12 parts of polyglutamic acids, 0.1 part of NMF, 0.8 portion of skin conditioner to be mixed, and
It is stirred, until all dissolvings, obtain lysate；
（4）First by step（2）Standby refrigeration liquid spray is shone on base material, is stood 6min, must be sprayed the base material after shining, after spray is shone
Base material, lysate are mixed, and obtain mixture, produce antibacterial wet tissue.
Example 3
Malt extract is that malt is put into pulverizer to crush, and obtains crushed material, in mass ratio 1：3.5：0.65：0.35, by powder
Mince, water, lactic acid, protease carry out heating hydrolysis, are heated to 45 DEG C, hydrolyze 3h, filtering, obtain filtrate, by filtrate vacuum-
0.07MPa, it is concentrated in vacuo at 55 DEG C of temperature, obtains concentrate, concentrate is dried in vacuo at 55 DEG C of temperature, obtained dry
Dry thing, dried object is put into pulverizer and crushed again, produces malt extract.
NMF is glycerine.
Skin conditioner is in mass ratio 1：1, suet, water are mixed, produce skin conditioner.
Base material is non-woven fabrics.
A kind of preparation method of antibacterial wet tissue, this method comprise the following steps：
（1）After granatum is washed with water, dried, the granatum after must drying, the granatum after drying is put into crushing
Crushed in machine, obtain crushed material, in mass ratio 1：3.5, by crushed material, 1.0mol/L ethanol solutions carry out mixing immersion 9h, then
Pressure is 17MPa, and temperature is to be extracted at 60 DEG C using supercritical carbon dioxide fluid, obtains extract solution；
（2）Count in parts by weight, take 35 parts of water, 15 parts of agar, 9 parts of malt extracts, 4 parts of dusty yeasts, 4 parts of glucose to be mixed
Close uniformly, high-temperature sterilization, obtain nutrient solution, in mass ratio 1：3.5, extract solution, nutrient solution are mixed, entered at 27 DEG C of temperature
Row fermentation 2.5d, obtains zymotic fluid, zymotic fluid is placed at 4 DEG C and refrigerated, obtain refrigeration liquid, standby；
（3）Count in parts by weight, take 40 parts of water, 15 parts of polyglutamic acids, 2 parts of NMFs, 1 portion of skin conditioner to be mixed, and carried out
Stirring, until all dissolvings, obtain lysate；
（4）First by step（2）Standby refrigeration liquid spray is shone on base material, is stood 8min, must be sprayed the base material after shining, after spray is shone
Base material, lysate are mixed, and obtain mixture, produce antibacterial wet tissue.
Reference examples：The antibacterial wet tissue of Baoding company production.
Reference《GB15979-2002 disposable sanitary articles sanitary standards》Appendix C《Product bactericidal property, bacteriostasis property with
Stability test method》Sterilizing rate experiment is carried out to wet tissue, action time is 5 minutes.Test result is shown in Table 1.
Table 1：
Security test：
Healthy volunteer 40 is chosen, male 20, women 20, the age was at 20 ~ 50 years old.In isoperibol（20~22℃）, phase
To humidity 50 ± 10%, rest after 1 hour, the sample that embodiment and reference examples is respectively adopted is coated in subject's left hand forearm
Side（3cm×3cm）With right forearm inner side（3cm×3cm）, wipe daily three times, Follow-up observation one month.After one month find by
There are skin malaise symptoms in none example of examination person, and epidermis also without any damage, illustrates that the antibacterial wet tissue of the present invention will not be to human body skin
Skin has undesirable effect.
Summary, antibacterial wet tissue antibacterial effect of the invention is more preferable and harmless, is worthy to be popularized.
Claims (7)
1. a kind of preparation method of antibacterial wet tissue, it is characterised in that this method comprises the following steps：
（1）After granatum is washed with water, dried, the granatum after must drying, the granatum after drying is put into crushing
Crushed in machine, obtain crushed material, crushed material, ethanol solution are subjected to mixing 8 ~ 10h of immersion, recycle supercritical carbon dioxide fluid
Extraction, obtains extract solution；
（2）Count in parts by weight, take 30 ~ 40 parts of water, 13 ~ 17 parts of agar, 8 ~ 10 parts of malt extracts, 3 ~ 5 parts of dusty yeasts, 3 ~ 5
Part glucose is well mixed, and high-temperature sterilization, obtains nutrient solution, extract solution, nutrient solution are mixed, in 25 ~ 30 DEG C of temperature
Under carry out 2 ~ 3d of fermentation, obtain zymotic fluid, zymotic fluid be placed at 3 ~ 4 DEG C and refrigerated, obtain refrigeration liquid, it is standby；
（3）Count in parts by weight, take 30 ~ 40 parts of water, 10 ~ 15 parts of polyglutamic acids, 0.1 ~ 2 part of NMF, 0.1 ~ 1 portion of skin conditioner to enter
Row mixing, and be stirred, until all dissolvings, obtain lysate；
（4）First by step（2）Standby refrigeration liquid spray is shone on base material, is stood 5 ~ 8min, must be sprayed the base material after shining, after spray is shone
Base material, lysate mixed, obtain mixture, produce antibacterial wet tissue.
2. the preparation method of antibacterial wet tissue according to claim 1, it is characterised in that the step（1）In overcritical dioxy
The parameter for changing carbon fluid extraction is that pressure is 15 ~ 20MPa, and temperature is 55 ~ 65 DEG C.
3. the preparation method of antibacterial wet tissue according to claim 1, it is characterised in that the step（2）Middle malt extract
It is that malt is put into pulverizer to crush, obtains crushed material, in mass ratio 1：3~4：0.5~0.8：0.3 ~ 0.4, by crushed material, water,
Lactic acid, protease carry out heating hydrolysis, are heated to 40 ~ 50 DEG C, hydrolyze 2 ~ 4h, filtering, filtrate are obtained, by filtrate in vacuum -0.09
~ -0.05MPa, it is concentrated in vacuo at 50 ~ 60 DEG C of temperature, obtains concentrate, concentrate is subjected to vacuum at 50 ~ 60 DEG C of temperature
Dry, obtain dried object, dried object is put into pulverizer and crushed again, produces malt extract.
4. the preparation method of antibacterial wet tissue according to claim 1, it is characterised in that the step（3）Middle NMF is sweet
Oil, propane diols it is therein any one.
5. the preparation method of antibacterial wet tissue according to claim 1, it is characterised in that the step（3）Middle skin conditioner be by
Mass ratio 1：0.8 ~ 1, suet, water are mixed, produce skin conditioner.
6. the preparation method of antibacterial wet tissue according to claim 1, it is characterised in that the step（4）Base after middle spray solarization
Material, the mass ratio of lysate are 1：2.5~3.5.
7. the preparation method of antibacterial wet tissue according to claim 1, it is characterised in that the step（4）Middle base material is nonwoven
Cloth.
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| CN108403534A (en) * | 2018-06-04 | 2018-08-17 | 上海克拉方今环保科技有限公司 | A kind of skin care wet tissue and its preparation method and application |
| CN110368346A (en) * | 2019-08-20 | 2019-10-25 | 上海潼舜日化用品有限公司 | A kind of antibacterial pro-skin moisture paper tissue papers and its production technology |
| CN112376164A (en) * | 2020-10-28 | 2021-02-19 | 东营俊富净化科技有限公司 | Melt-blown non-woven fabric for biomass antivirus and bacteriostatic mask and preparation method thereof |
| WO2023217004A1 (en) * | 2022-05-09 | 2023-11-16 | 萍乡小日科技有限公司 | Preparation method for antibacterial wet wipe |
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