CN107700239A - A kind of preparation method of dried peppermint leaf powder print paste - Google Patents
A kind of preparation method of dried peppermint leaf powder print paste Download PDFInfo
- Publication number
- CN107700239A CN107700239A CN201711142278.2A CN201711142278A CN107700239A CN 107700239 A CN107700239 A CN 107700239A CN 201711142278 A CN201711142278 A CN 201711142278A CN 107700239 A CN107700239 A CN 107700239A
- Authority
- CN
- China
- Prior art keywords
- leaf powder
- peppermint leaf
- dried peppermint
- print paste
- thickener
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/445—Use of auxiliary substances before, during or after dyeing or printing
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The present invention relates to a kind of preparation method of dried peppermint leaf powder print paste, belong to technical field of textile printing.The present invention substitutes conventional pigment using dried peppermint leaf powder and prepares print paste, paste formula is made up of dried peppermint leaf powder, adhesive UDT, the thickener that particle diameter is 100 200nm, it is blended according to the ratio that mass percent is respectively 4 8%, 90 95.5%, 0.5 2%, under conditions of environment temperature is 22 24 DEG C, 19 29min are first stirred with 110 210r/min rotating speed in mixer, dried peppermint leaf powder and thickener is set to be dispersed in adhesive, 60 80min are stirred with 600 800r/min rotating speed again, stand, form print paste.Dried peppermint leaf powder print paste is prepared using the inventive method, technological process is short, and production cost is low, can both keep the original slow-release function of peppermint, pollution problem caused by and can from root solution pigment use.Stamp is carried out to fabric using print paste prepared by the above method, the pattern boundaries obtained are clear, and fastness is good, can be widely applied in the printing technology of textile.
Description
Technical field
The present invention relates to a kind of preparation method of dried peppermint leaf powder print paste, belong to technical field of textile printing.
Background technology
Stamp is one of textile dyeing method, typically prepares print paste using synthetic dyestuff, adhesive and thickener,
Such as Chinese public publication《Printing and dyeing》, at 2005 publication date, article name is " pigment printing of cotton fabric ", and the document describes
Pigment printing technology, the technology screening go out part coatings print paste and auxiliary aid product, and wherein auxiliary aid product includes
Adhesive, thickener and ammoniacal liquor, product good hand touch, the fastness printed are good, weak point be as Environmental Protection Situation is increasingly serious,
The preparation of synthetic dyestuff and using can cause certain environmental pollution.
Mentha Labiatae Mentha herbaceos perennial, with driveing, wind-heat, solution thermal sweating, head clearing etc. are medicinal
Effect.Peppermint stem and leaf has peat-reek, has good sustained release performance.In addition, peppermint can be used for extracting natural dye, such as China
Public publication《China brewages》, in May, 2012 publication date, article name is the " extraction of Xinjiang peppermint pigment and its stably
Journal of Sex Research ", the document describe the extraction process of Xinjiang peppermint pigment, the technology using alcohol steep method obtain it is fast light,
Heat-resisting pigment, and it shows stabilization in the range of pH is 4~8.Chinese public publication《Chinese Journal of Health Laboratory Technology》,
Publication date in August, 2013, article name are " extraction and its physicochemical property research of Guangxi Zhuang medicine peppermint pigment ", and the document is situated between
Continue and pigment is extracted from peppermint using distillation water extraction method, the technology is soaked at room temperature using distilled water to crushing peppermint
24h extracts peppermint pigment, and obtained pigment has stronger resistance to oxidation and reproducibility.Above two technology is disadvantageous in that
Not high in the peppermint natural dye stability of extraction, highly acid, strong alkaline condition are larger to peppermint pigment stability influence, simultaneously
The extraction of peppermint pigment destroys the original structure of peppermint, so as to destroy the slow-release function of peppermint.
The content of the invention
For above-mentioned problem, conventional pigment is substituted using dried peppermint leaf powder it is an object of the invention to provide one kind
The method for preparing print paste.To achieve the above object, the technical scheme is that：
A kind of preparation method of dried peppermint leaf powder print paste, by dried peppermint leaf powder, the adhesive that particle diameter is 100-200nm
UDT, thickener are respectively 4-8%, 90-95.5%, 0.5-2% ratio mixing by mass percentage, in environment temperature after mixing
Spend under conditions of 22-24 DEG C, first to stir 19-29min with 110-210r/min rotating speed in mixer, making dried peppermint leaf powder
It is dispersed in thickener in adhesive, then 60-80min is stirred with 600-800r/min rotating speed, stood, forms stamp color
Slurry.
As a result of above technical scheme, because the dried peppermint leaf powder used is Nano grade, still containing volatilization inside it
Oil component, peppermint possessed slow-release function can be kept, and the color of dried peppermint leaf powder itself institute band then assigns mill base color.This
Invention, instead of traditional granules of pigments, is prepared using the dried peppermint leaf powder of Nano grade after being mixed with adhesive UDT and thickener
Go out dried peppermint leaf powder print paste, pollution problem caused by can solving pigment use from source.
Environment temperature be 22-24 DEG C under the conditions of, dried peppermint leaf powder, adhesive UDT, thickener stirring at low speed process
Middle mixing, dried peppermint leaf powder and thickener are scattered in adhesive UDT, after disperseing fully, are improved mixing speed, are made dried peppermint leaf
Powder and the water molecules in adhesive UDT, the swelling of appropriate degree occurs, volume becomes big, beneficial to dried peppermint leaf powder granule
It is uniformly dispersed between particle, so that adhesive UDT is easier dried peppermint leaf powder granule being coated in binder film.This
Outside, dried peppermint leaf powder belongs to the granular materials containing cellulose components, has more reactive groups compared with conventional pigment particle
, the hydroxyl in strand can chemically react with adhesive UDT, enhance between dried peppermint leaf powder granule and adhesive
Active force.The present invention prepares print paste using dried peppermint leaf powder, and technological process is short, and production cost is low.Made using the present invention
Standby wormwood powder print paste carries out stamp to fabric, and the pattern boundaries obtained are clear, and fastness is good, can be widely applied to
In the printing technology of textile.
Embodiment
With reference to specific embodiment, the present invention is described in further detail：
A kind of preparation method of dried peppermint leaf powder print paste, dry peppermint is processed using superfine powder process equipment
Into the dried peppermint leaf powder that particle diameter is 100-200nm, it is respectively by mass percentage by dried peppermint leaf powder, adhesive UDT, thickener
4-8%, 90-95.5%, 0.5-2% ratio mixing, after mixing under conditions of environment temperature is 22-24 DEG C, in mixer
19-29min stirs with 110-210r/min rotating speed in interior elder generation, dried peppermint leaf powder and thickener is dispersed in adhesive,
60-80min is stirred with 600-800r/min rotating speed again, stood, forms print paste.Using the print paste prepared pure
Surface of cotton fabric stamp, re-test stamp color depth and dry, fastness to wet rubbing.
Specific embodiment
Embodiment 1
By particle diameter be 300nm dried peppermint leaf powder, adhesive UDT, thickener be respectively 4% by mass percentage,
95.5%th, 0.5% ratio mixing, after mixing under conditions of environment temperature is 22 DEG C, first with 110r/min in mixer
Rotating speed stirring 29min, be mixed uniformly, then 80min is stirred with 600r/min rotating speed, stand, form print paste.Will
A kind of dried peppermint leaf powder print paste prepared by the above method, stamp is carried out on pure cotton fabric surface.
Embodiment 2
By particle diameter be 15nm dried peppermint leaf powder, adhesive UDT, thickener be respectively 6% by mass percentage, 93%,
1% ratio mixing, after mixing under conditions of environment temperature is 23 DEG C, is first stirred in mixer with 160r/min rotating speed
24min, dried peppermint leaf powder and thickener is dispersed in adhesive, then 70min is stirred with 700r/min rotating speed, it is quiet
Put, form print paste.A kind of dried peppermint leaf powder print paste prepared by the above method, is printed on pure cotton fabric surface
Flower.
Embodiment 3
By particle diameter be 200nm dried peppermint leaf powder, adhesive UDT, thickener be respectively 8% by mass percentage, 90%,
2% ratio mixing, after mixing under conditions of environment temperature is 24 DEG C, is first stirred in mixer with 210r/min rotating speed
19min, dried peppermint leaf powder and thickener is dispersed in adhesive, then 60min is stirred with 800r/min rotating speed, it is quiet
Put, form print paste.A kind of dried peppermint leaf powder print paste prepared by the above method, is printed on pure cotton fabric surface
Flower.
The Apparent Depth and fastness of the PRINTED FABRIC of table 1
As shown in Table 1, synthetic dyestuff is substituted using coloured dried peppermint leaf powder, PRINTED FABRIC can be assigned with full
Color, embody environmental-protecting performance.With the increase of dried peppermint leaf powder quality percentage in print paste, the Apparent Depth of PRINTED FABRIC
Gradually increase, do, wet fastness of rubbing it is preferable, more than 3 grades.
Claims (1)
- A kind of 1. preparation method of dried peppermint leaf powder print paste, it is characterised in that：Described preparation method refers to 100-200nm dried peppermint leaf powder, adhesive UDT, thickener is respectively 4-8%, 90-95.5%, 0.5- by mass percentage 2% ratio mixing, after mixing under conditions of environment temperature is 22-24 DEG C, first with 110-210r/min's in mixer Rotating speed stirs 19-29min, dried peppermint leaf powder and thickener is dispersed in adhesive, then is turned with 600-800r/min Speed stirring 60-80min, stands, forms print paste.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711142278.2A CN107700239A (en) | 2017-11-17 | 2017-11-17 | A kind of preparation method of dried peppermint leaf powder print paste |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711142278.2A CN107700239A (en) | 2017-11-17 | 2017-11-17 | A kind of preparation method of dried peppermint leaf powder print paste |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107700239A true CN107700239A (en) | 2018-02-16 |
Family
ID=61180287
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711142278.2A Pending CN107700239A (en) | 2017-11-17 | 2017-11-17 | A kind of preparation method of dried peppermint leaf powder print paste |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107700239A (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102127868A (en) * | 2010-12-07 | 2011-07-20 | 江南大学 | Preparation method of ultraviolet-fluorescence-visible printing color paste for fabric |
| CN102978975A (en) * | 2012-12-07 | 2013-03-20 | 绍兴市天基印刷材料厂 | Printing paste preparation and printing process thereof |
| CN105350355A (en) * | 2015-11-30 | 2016-02-24 | 无锡新德印染制品有限公司 | Preparation method of printing color paste |
-
2017
- 2017-11-17 CN CN201711142278.2A patent/CN107700239A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102127868A (en) * | 2010-12-07 | 2011-07-20 | 江南大学 | Preparation method of ultraviolet-fluorescence-visible printing color paste for fabric |
| CN102978975A (en) * | 2012-12-07 | 2013-03-20 | 绍兴市天基印刷材料厂 | Printing paste preparation and printing process thereof |
| CN105350355A (en) * | 2015-11-30 | 2016-02-24 | 无锡新德印染制品有限公司 | Preparation method of printing color paste |
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| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180216 |
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| RJ01 | Rejection of invention patent application after publication |