CN107669569A - A kind of preparation method of whitening anti-acne facial cleanser - Google Patents
A kind of preparation method of whitening anti-acne facial cleanser Download PDFInfo
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- CN107669569A CN107669569A CN201711222634.1A CN201711222634A CN107669569A CN 107669569 A CN107669569 A CN 107669569A CN 201711222634 A CN201711222634 A CN 201711222634A CN 107669569 A CN107669569 A CN 107669569A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
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- Animal Behavior & Ethology (AREA)
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Abstract
The invention discloses a kind of preparation method of whitening anti-acne facial cleanser,The mildy wash harvests Qarnet hairpin extract solution with including,Extracting method harvests the parts by weight of fresh fruit 30 50 to clean the ground after removing surface irregularities,Clean the Qarnet hairpin parts by weight of fresh flower 10 15 after removing surface irregularities,It is subsequently placed in ultrasonic grinder and crushes 0.5h,Fruit purple fragrant plantain lily flower mixture is harvested into 45 times of volume mineral waters in ground after crushing,And harvest the sodium bicarbonate of fruit purple fragrant plantain lily flower mixture quality 0.01% with adding,5% white wine,Soak 24 36h,And every 1h stirrings once,Then 300 mesh screens obtain filtrate,Filtrate is concentrated under reduced pressure into proportion as 1.1 or so at 80 DEG C,Harvest Qarnet hairpin extract solution with producing contain a large number of nutrients,Not only cleaning skin effect is good,It also can be supplied to skin of face nutriment,It is long-term use of,Can skin whitening,And effectively dispel acne caused by a variety of causes,Anti-acne it is efficient up to 90%.
Description
Technical field
The present invention relates to beauty and skin care field, more particularly to a kind of preparation method of whitening anti-acne facial cleanser.
Background technology
Mildy wash is a kind of senior face washing agent, has the effect of cleaning, nutrition, protection skin.The general color and luster of mildy wash is pure
Just, fragrance is simple and elegant, quality is fine and smooth, has preferable mobility, ductility and permeability.The sweat of face can be removed by being washed one's face with it
Stain, grease, foundation cream, scurf etc., the mildy wash for having some special natures can also use in anhydrous conditions, can not only clean surface
Portion's skin, while also have the functions such as skin care, moisturizing, skin nutrition concurrently, face skin can be made tender bright and clean after.Due to washing one's face
Milk, which washes one's face to remove ornaments and formal dress, has fabulous clean skin health-care efficacy, has the advantage for using perfumed soap clean skin incomparable, therefore deep by consumer
Favor.
At present, the mildy wash of in the market is numerous in variety, and function is also varied.But mildy wash on the market is to change mostly
Study and be divided into main preparation, the ratio very little that natural component accounts for；On the one hand the enhancing with people's environmental consciousness and life water
Flat raising, containing a large amount of natural materials extracts can cleaning skin again have whitening, acne-removing mildy wash be undoubtedly
Best selection；On the other hand, many people chemical composition occur allergic phenomena, and applicability is poor.
In addition, current mildy wash, tends not to be provided simultaneously with whitening and acne-removal function.Moreover, possesses whitening, anti-acne work(
Can mildy wash it is often expensive, such as 100g mildy wash, its price is often more than 50 yuan, and whitening and anti-acne
Effect also unobvious.
The content of the invention
The purpose of the present invention, which is that, provides a kind of preparation method of whitening anti-acne facial cleanser.
Present inventor is by largely testing, and harvesting fruit uses special extracting method with finding, for mildy wash
Effect with significant whitening, anti-acne, it can mutually be cooperateed with purple fragrant plantain lily flower, is further improved whitening, the effect of anti-acne, is studied carefully
Its reason, it may be possible to because using the ground obtained by special extracting method harvest in Qarnet hairpin extract solution containing abundant vitamin C,
Reduced sugar, saponin(e, several amino acids include threonine, valine, methionine, leucine, isoleucine, phenylalanine, bad ammonia
The Multiple components such as acid, it effectively anti-oxidant, effective can dredge pilosebaceous duct and reduce dyssebacia, have to skin bright
The effect of aobvious whitening, anti-acne.
It can be used for being prepared into the skin care item such as mildy wash, exemplified by preparing mildy wash：
A kind of whitening anti-acne facial cleanser, the mildy wash harvest Qarnet hairpin extract solution with containing a large amount of natural extracts.
To achieve these goals, the technical solution adopted by the present invention is such：
A kind of whitening anti-acne facial cleanser, the mass fraction of each raw material is as follows in formula：
Harvest Qarnet hairpin extract solution 5-8 parts, sodium lauroyl glutamate 2-4 parts, ethylene glycol stearate 2-5 parts, palmitic acid isopropyl in ground
Ester 1.5-3 parts, glycerine 5-10 parts and deionized water 5-10 parts；
Above-mentioned raw materials are added in container, stirring, are gradually heating to 50-60 DEG C, and maintain this temperature even with 2500r/min
Matter 20-30min, it is subsequently cooled to 20-25 DEG C of discharging, packing.
It is as follows that Qarnet hairpin extract solution its preparation method is harvested of the present inventionly：Weigh and clean the ground after removing surface irregularities
Harvest fresh fruit 30-50 parts by weight, clean the Qarnet hairpin fresh flower 10-15 parts by weight after removing surface irregularities, be subsequently placed in ultrasonic wave powder
0.5h is crushed in broken machine, fruit purple fragrant plantain lily flower mixture is harvested into 4-5 times of volume mineral waters in the ground after crushing, and add ground
Harvest sodium bicarbonate, 5% white wine of fruit purple fragrant plantain lily flower mixture quality 0.01%（The percentage by volume of ethanol is 60%）, soak 24-
36h, and every 1h stirrings once, then 300 mesh screens obtain filtrate, and filtrate is concentrated under reduced pressure into proportion at 80 DEG C is
1.1 or so, harvest Qarnet hairpin extract solution with producing.
Fruit is harvested of the present inventionly to harvest for Melastomateae plants（Melastoma dodecandrum Lour.）Maturation
Fruit, using fresh herb；
Qarnet hairpin of the present invention（Hosta albo-marginata (Hook.) Ohwi）It is that Liliaceae, Hosta are perennial
The fresh flowers of herbaceous plant Qarnet hairpin.
Compared with prior art, the advantage of the invention is that：The main component of the present invention harvests purple for natural extract
Jade hairpin extract solution, there is the effect of obvious whitening, anti-acne to skin, anti-acne it is efficient up to 90%, and raw material are easy to get cost
Cheap, based on 100g mildy wash finished products, its cost is not higher than 10 yuan.
Embodiment
Below in conjunction with embodiment, the invention will be further described.
Embodiment 1：
A kind of whitening anti-acne facial cleanser, but following components in parts by weight forms：
Harvest 5 parts of extract solution of Qarnet hairpin, 2 parts of sodium lauroyl glutamate, 2 parts of ethylene glycol stearate, isopropyl palmitate 1.5 in ground
5 parts of part, 5 parts of glycerine and deionized water.
Harvest above-mentionedly Qarnet hairpin extract solution preparation method be：Weigh the ground cleaned after removing surface irregularities and harvest the weight of fresh fruit 35
Measure part, clean the Qarnet hairpin parts by weight of fresh flower 15 after removing surface irregularities, be subsequently placed in ultrasonic grinder and crush 0.5h,
Fruit purple fragrant plantain lily flower mixture is harvested into 4 times of volume mineral waters in ground after crushing, and harvest fruit purple fragrant plantain lily flower mixture with adding
The sodium bicarbonate of quality 0.01%, 5% white wine（The percentage by volume of ethanol is 60%）, 30h is soaked, and one is stirred every 1h
Secondary, then 300 mesh screens obtain filtrate, and it is 1.1 that filtrate is concentrated under reduced pressure into proportion at 80 DEG C, harvest Qarnet hairpin with producing carry
Take liquid；
Above-mentioned raw materials are added in container, stirring, are gradually heating to 60 DEG C, and maintain this temperature homogeneous with 2500r/min
30min, 20 DEG C of dischargings, packing are subsequently cooled to, produces " mildy wash A ".
Embodiment 2：
A kind of whitening anti-acne facial cleanser, but following components in parts by weight forms：
Ground harvest Qarnet hairpin 8 parts of extract solution, 4 parts of sodium lauroyl glutamate, 5 parts of ethylene glycol stearate, 3 parts of isopropyl palmitate,
10 parts of 10 parts of glycerine and deionized water；
The preparation method that Qarnet hairpin extract solution is harvested on ground is same as Example 1；
Above-mentioned raw materials are added in container, stirring, are gradually heating to 60 DEG C, and maintain this temperature homogeneous with 2500r/min
30min, 20 DEG C of dischargings, packing are subsequently cooled to, produces " mildy wash B ".
Embodiment 3：
A kind of whitening anti-acne facial cleanser, but following components in parts by weight forms：
Ground harvest Qarnet hairpin 6 parts of extract solution, 3 parts of sodium lauroyl glutamate, 4 parts of ethylene glycol stearate, 2 parts of isopropyl palmitate,
8 parts of 8 parts of glycerine and deionized water；
The preparation method that Qarnet hairpin extract solution is harvested on ground is same as Example 1；
Above-mentioned raw materials are added in container, stirring, are gradually heating to 50 DEG C, and maintain this temperature homogeneous with 2500r/min
20min, 25 DEG C of dischargings, packing are subsequently cooled to, produces " mildy wash C ".
Embodiment 4：Harvest 6 parts of fruit extract solution, 3 parts of sodium lauroyl glutamate, 4 parts of ethylene glycol stearate, isopropyl palmitate 2 in ground
8 parts of part, 8 parts of glycerine and deionized water；
Harvest the preparation method of fruit extract solution in ground：Weigh the ground cleaned after removing surface irregularities and harvest the parts by weight of fresh fruit 50, be subsequently placed in
0.5h is crushed in ultrasonic grinder, fruit is harvested into 4 times of volume mineral waters in the ground after crushing, and harvest fruit Qarnet with adding
Sodium bicarbonate, 5% white wine of hairpin flower mixture quality 0.01%（The percentage by volume of ethanol is 60%）, immersion 30h, and every
1h is stirred once, and then 300 mesh screens obtain filtrate, and it is 1.1 that filtrate is concentrated under reduced pressure into proportion at 80 DEG C, is harvested with producing
Fruit extract solution；
Above-mentioned raw materials are added in container, stirring, are gradually heating to 50 DEG C, and maintain this temperature homogeneous with 2500r/min
25min, 20 DEG C of dischargings, packing are subsequently cooled to, produces " mildy wash D ".
Embodiment 5：
It is purple 6 parts of fragrant plantain lily flower extract solution, 3 parts of sodium lauroyl glutamate, 4 parts of ethylene glycol stearate, 2 parts of isopropyl palmitate, sweet
8 parts of 8 parts of oil and deionized water；
The preparation method of purple fragrant plantain lily flower extract solution：Weigh and clean the Qarnet hairpin parts by weight of fresh flower 50 after removing surface irregularities, then
It is placed in ultrasonic grinder and crushes 0.5h, fruit is harvested into 4 times of volume mineral waters in the ground after crushing, and harvest fruit with adding
Sodium bicarbonate, 5% white wine of purple fragrant plantain lily flower mixture quality 0.01%（The percentage by volume of ethanol is 60%）, 30h is soaked, and
Every 1h stirrings once, then 300 mesh screens obtain filtrate, and it is 1.1 that filtrate is concentrated under reduced pressure into proportion at 80 DEG C, is produced
Harvest fruit extract solution in ground；
Above-mentioned raw materials are added in container, stirring, are gradually heating to 50 DEG C, and maintain this temperature homogeneous with 2500r/min
25min, 20 DEG C of dischargings, packing are subsequently cooled to, produces " mildy wash E ".
Embodiment 6
1. whitening effect clinical test：
Subject 120 is chosen, women, the age, the face of subject had different degrees of facial color between 18-40 year
It is plain calm, dull pitch-dark, it is randomly divided into four groups, every group of 30 people, use respectively " mildy wash B ", " mildy wash C ", " mildy wash D ",
" mildy wash E ", respectively wash once, at least massaged 2 minute in face during use sooner or later daily；Using two months,
Before use, use the melanin situation for using skinanalysis apparatus to test skin respectively after two months
As a result standard：
It is effective：Melanin value at least reduces 60%
Effectively：Melanin value at least reduces 20%
It is invalid：Melanin value does not change；
Experimental result is as shown in table 1
The face whitening clinical trial results of table 1（Numerical value unit：People）
2. anti-acne effect clinical test：
Acne is clinically divided into 3 degree, 4 grades according to acne lesions property and the order of severity：1 grade（Slightly）：Only acne；2 grades
（Moderate）：In addition to acne, there are some inflamed papules；3 grades（Moderate）：In addition to acne, also more inflamed papules or warts；
4 grades（Severe）：In addition to having acne, inflamed papules and warts, nodosity, tumour or scar are gone back.
The present invention is according to above-mentioned grade scale, and totally 120 people, age are male between 18-30 year by the subject of selection 1-3 levels
30 people of property, the people of women 90, wherein, 1 grade of 40 people, 2 grade of 40 people, 3 grade of 40 people be randomly divided into four groups, every group of 30 people, 1 grade of every group,
2 grades and 3 grades each 10 people, use respectively " mildy wash B ", " mildy wash C ", " mildy wash D ", " mildy wash E ", using two months, often
It is respectively washed once sooner or later, is at least massaged 2 minutes in face during use；Diet and other lives before not changing during use
Custom；Observe its effect；
Effect criterion：（1）Recovery from illness：Symptom is wholly absent；（2）Effectively, i.e., situation has clear improvement, and 2 grades at least become 1
Level, 3 grades at least become 2 grades；（3）Invalid, symptom is without any improvement；
It the results are shown in Table 2：
The anti-acne effect result of the test of table 2
Typical case
Lee, female, 21 years old, long whelk 2 years, it was classified as 3 grades, during which used Olay frosted anti-acne deep layer mildy wash half a year
More than, never positive effect, using the present invention " mildy wash C " 2 months, symptom is obviously improved, and reaches 1 grade.
3. the compliance test result test on whitening
In skin care field, ursin is the composition for being most commonly used for whitening, such as the white and moist Cleansing Foam that flesh is ground, and the inside just contains
There is ursin, to find out its cause, be that can substantially suppress tyrosinase because of ursin, and tyrosinase is the pass of B16 cell
Key enzyme, that is to say, that ursin can suppress the synthesis of melanin, and so as to reach skin whitening effect, the present invention uses ursin
As control, the effect for suppressing tyrosinase of the active ingredient in the Cleansing Foam of the present invention is verified；Experiment product is the He of embodiment 2
Qarnet hairpin extract solution is harvested on 3 worth ground, embodiment 4 harvests purple fragrant plantain lily flower extraction made from fruit extract solution and embodiment 5 obtainedly
Liquid；Tyrosinase and ursin are commercially available；
Test method is：
Qarnet hairpin extract solution is harvested on the worth ground of separately sampled ursin, embodiment 2 and 3, embodiment 4 harvests fruit extract solution obtainedly
With embodiment 5 made from purple fragrant plantain lily flower extract solution, be respectively labeled as 1#, 2#, 3#, 4# and 5#, using identical dosage and concentration,
10min is preheated in 37 oC, is then separately added into tyrosinase solution in each test tube, in 37 oC accurate response 5min, rapidly
It is transferred in cuvette, absorbance is surveyed at 475nm；
To cause tyrosinase vigor to decline 50% inhibitor concentration（IC50）The effect of to characterize inhibitor.Suppress tyrosine
Enzyme assay the results are shown in Table 3
Table 3 suppresses the concentration of tyrosinase activity（mg/ml）
From table 3 it can be seen that fruit extract solution is harvested on ground has the function that the definite tyrosinase activity that suppresses, and ground is harvested Qarnet hairpin and carried
Take the suppression tyrosinase activity of liquid suitable with ursin, even better than ursin.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all essences in the present invention
All any modification, equivalent and improvement made within refreshing and principle etc., should be included in the scope of the protection.
Claims (2)
1. a kind of preparation method of whitening anti-acne facial cleanser, it is characterised in that harvest Qarnet hairpin extract solution including ground, harvest purple describedly
Jade hairpin extract solution is that the Qarnet hairpin fresh flower that fresh fruit and 10-15 parts by weight are harvested using 30-50 parts by weight extracts what is obtained.
2. according to the method for claim 1, it is characterised in that extracting method is：Weigh after cleaning removing surface irregularities
Fresh fruit 30-50 parts by weight are harvested on ground, are cleaned the Qarnet hairpin fresh flower 10-15 parts by weight after removing surface irregularities, are subsequently placed in ultrasonic wave
0.5h is crushed in pulverizer, fruit purple fragrant plantain lily flower mixture is harvested into 4-5 times of volume mineral waters in the ground after crushing, and add
The sodium bicarbonate of fruit purple fragrant plantain lily flower mixture quality 0.01%, 5% white wine are harvested in ground, soak 24-36h, and stir one every 1h
Secondary, then 300 mesh screens obtain filtrate, and it is 1.1 or so that filtrate is concentrated under reduced pressure into proportion at 80 DEG C, harvests Qarnet with producing
Hairpin extract solution.
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