CN107663413B - Repairing agent and preparation method and use method thereof - Google Patents
Repairing agent and preparation method and use method thereof Download PDFInfo
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- CN107663413B CN107663413B CN201610605334.0A CN201610605334A CN107663413B CN 107663413 B CN107663413 B CN 107663413B CN 201610605334 A CN201610605334 A CN 201610605334A CN 107663413 B CN107663413 B CN 107663413B
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- repairing agent
- silicone oil
- cooker
- water
- repairing
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- 238000000034 method Methods 0.000 title claims abstract description 22
- 238000002360 preparation method Methods 0.000 title abstract description 20
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 103
- 229920002545 silicone oil Polymers 0.000 claims abstract description 50
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 50
- 239000004094 surface-active agent Substances 0.000 claims abstract description 22
- 239000002562 thickening agent Substances 0.000 claims abstract description 22
- 239000003755 preservative agent Substances 0.000 claims abstract description 17
- 230000002335 preservative effect Effects 0.000 claims abstract description 17
- 230000001965 increasing effect Effects 0.000 claims abstract description 14
- 230000000694 effects Effects 0.000 claims abstract description 13
- 238000000576 coating method Methods 0.000 claims description 34
- 239000011248 coating agent Substances 0.000 claims description 31
- 238000003756 stirring Methods 0.000 claims description 27
- -1 fatty acid ester Chemical class 0.000 claims description 18
- 239000008367 deionised water Substances 0.000 claims description 17
- 229910021641 deionized water Inorganic materials 0.000 claims description 17
- 239000003921 oil Substances 0.000 claims description 15
- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 claims description 14
- 238000002156 mixing Methods 0.000 claims description 12
- 238000004945 emulsification Methods 0.000 claims description 11
- JXKPEJDQGNYQSM-UHFFFAOYSA-M sodium propionate Chemical compound [Na+].CCC([O-])=O JXKPEJDQGNYQSM-UHFFFAOYSA-M 0.000 claims description 11
- 239000004324 sodium propionate Substances 0.000 claims description 11
- 235000010334 sodium propionate Nutrition 0.000 claims description 11
- 229960003212 sodium propionate Drugs 0.000 claims description 11
- 238000010411 cooking Methods 0.000 claims description 10
- 239000004744 fabric Substances 0.000 claims description 9
- 239000011737 fluorine Substances 0.000 claims description 9
- 229910052731 fluorine Inorganic materials 0.000 claims description 9
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 claims description 8
- 230000008439 repair process Effects 0.000 claims description 8
- JLPULHDHAOZNQI-ZTIMHPMXSA-N 1-hexadecanoyl-2-(9Z,12Z-octadecadienoyl)-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCCCCCC\C=C/C\C=C/CCCCC JLPULHDHAOZNQI-ZTIMHPMXSA-N 0.000 claims description 7
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims description 7
- CHHHXKFHOYLYRE-UHFFFAOYSA-M 2,4-Hexadienoic acid, potassium salt (1:1), (2E,4E)- Chemical compound [K+].CC=CC=CC([O-])=O CHHHXKFHOYLYRE-UHFFFAOYSA-M 0.000 claims description 7
- 229920001817 Agar Polymers 0.000 claims description 7
- BCZXFFBUYPCTSJ-UHFFFAOYSA-L Calcium propionate Chemical compound [Ca+2].CCC([O-])=O.CCC([O-])=O BCZXFFBUYPCTSJ-UHFFFAOYSA-L 0.000 claims description 7
- 108010010803 Gelatin Proteins 0.000 claims description 7
- 239000008272 agar Substances 0.000 claims description 7
- 235000010419 agar Nutrition 0.000 claims description 7
- 239000004330 calcium propionate Substances 0.000 claims description 7
- 235000010331 calcium propionate Nutrition 0.000 claims description 7
- 238000004140 cleaning Methods 0.000 claims description 7
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 7
- 239000000194 fatty acid Substances 0.000 claims description 7
- 229930195729 fatty acid Natural products 0.000 claims description 7
- 239000008273 gelatin Substances 0.000 claims description 7
- 229920000159 gelatin Polymers 0.000 claims description 7
- 235000019322 gelatine Nutrition 0.000 claims description 7
- 235000011852 gelatine desserts Nutrition 0.000 claims description 7
- 229940075507 glyceryl monostearate Drugs 0.000 claims description 7
- 229920003063 hydroxymethyl cellulose Polymers 0.000 claims description 7
- 229940031574 hydroxymethyl cellulose Drugs 0.000 claims description 7
- 229920000609 methyl cellulose Polymers 0.000 claims description 7
- 239000001923 methylcellulose Substances 0.000 claims description 7
- 235000010981 methylcellulose Nutrition 0.000 claims description 7
- 239000000203 mixture Substances 0.000 claims description 7
- 239000001788 mono and diglycerides of fatty acids Substances 0.000 claims description 7
- 229950008882 polysorbate Drugs 0.000 claims description 7
- 229920000136 polysorbate Polymers 0.000 claims description 7
- 239000004302 potassium sorbate Substances 0.000 claims description 7
- 235000010241 potassium sorbate Nutrition 0.000 claims description 7
- 229940069338 potassium sorbate Drugs 0.000 claims description 7
- 235000010413 sodium alginate Nutrition 0.000 claims description 7
- 239000000661 sodium alginate Substances 0.000 claims description 7
- 229940005550 sodium alginate Drugs 0.000 claims description 7
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 claims description 7
- 239000004299 sodium benzoate Substances 0.000 claims description 7
- 235000010234 sodium benzoate Nutrition 0.000 claims description 7
- 229940083466 soybean lecithin Drugs 0.000 claims description 7
- 238000005303 weighing Methods 0.000 claims description 7
- 238000001816 cooling Methods 0.000 claims description 6
- 238000010438 heat treatment Methods 0.000 claims description 6
- 229920003216 poly(methylphenylsiloxane) Polymers 0.000 claims description 6
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 5
- 229920000223 polyglycerol Polymers 0.000 claims description 5
- 229910052710 silicon Inorganic materials 0.000 claims description 5
- 239000010703 silicon Substances 0.000 claims description 5
- 239000008399 tap water Substances 0.000 claims description 5
- 235000020679 tap water Nutrition 0.000 claims description 5
- 239000000263 2,3-dihydroxypropyl (Z)-octadec-9-enoate Substances 0.000 claims description 4
- RZRNAYUHWVFMIP-GDCKJWNLSA-N 3-oleoyl-sn-glycerol Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OC[C@H](O)CO RZRNAYUHWVFMIP-GDCKJWNLSA-N 0.000 claims description 4
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims description 4
- RZRNAYUHWVFMIP-UHFFFAOYSA-N monoelaidin Natural products CCCCCCCCC=CCCCCCCCC(=O)OCC(O)CO RZRNAYUHWVFMIP-UHFFFAOYSA-N 0.000 claims description 4
- 244000144730 Amygdalus persica Species 0.000 claims description 3
- 239000001856 Ethyl cellulose Substances 0.000 claims description 3
- ZZSNKZQZMQGXPY-UHFFFAOYSA-N Ethyl cellulose Chemical compound CCOCC1OC(OC)C(OCC)C(OCC)C1OC1C(O)C(O)C(OC)C(CO)O1 ZZSNKZQZMQGXPY-UHFFFAOYSA-N 0.000 claims description 3
- 239000004354 Hydroxyethyl cellulose Substances 0.000 claims description 3
- 229920000663 Hydroxyethyl cellulose Polymers 0.000 claims description 3
- 235000006040 Prunus persica var persica Nutrition 0.000 claims description 3
- 235000010489 acacia gum Nutrition 0.000 claims description 3
- 229940023476 agar Drugs 0.000 claims description 3
- 235000010418 carrageenan Nutrition 0.000 claims description 3
- 239000000679 carrageenan Substances 0.000 claims description 3
- 229920001525 carrageenan Polymers 0.000 claims description 3
- 229940113118 carrageenan Drugs 0.000 claims description 3
- 238000005524 ceramic coating Methods 0.000 claims description 3
- 235000019325 ethyl cellulose Nutrition 0.000 claims description 3
- 229920001249 ethyl cellulose Polymers 0.000 claims description 3
- 229940014259 gelatin Drugs 0.000 claims description 3
- 235000019447 hydroxyethyl cellulose Nutrition 0.000 claims description 3
- 239000001866 hydroxypropyl methyl cellulose Substances 0.000 claims description 3
- 235000010979 hydroxypropyl methyl cellulose Nutrition 0.000 claims description 3
- 229920003088 hydroxypropyl methyl cellulose Polymers 0.000 claims description 3
- UFVKGYZPFZQRLF-UHFFFAOYSA-N hydroxypropyl methyl cellulose Chemical compound OC1C(O)C(OC)OC(CO)C1OC1C(O)C(O)C(OC2C(C(O)C(OC3C(C(O)C(O)C(CO)O3)O)C(CO)O2)O)C(CO)O1 UFVKGYZPFZQRLF-UHFFFAOYSA-N 0.000 claims description 3
- 238000004519 manufacturing process Methods 0.000 claims description 3
- 229960003885 sodium benzoate Drugs 0.000 claims description 3
- UHVMMEOXYDMDKI-JKYCWFKZSA-L zinc;1-(5-cyanopyridin-2-yl)-3-[(1s,2s)-2-(6-fluoro-2-hydroxy-3-propanoylphenyl)cyclopropyl]urea;diacetate Chemical compound [Zn+2].CC([O-])=O.CC([O-])=O.CCC(=O)C1=CC=C(F)C([C@H]2[C@H](C2)NC(=O)NC=2N=CC(=CC=2)C#N)=C1O UHVMMEOXYDMDKI-JKYCWFKZSA-L 0.000 claims description 3
- LNAZSHAWQACDHT-XIYTZBAFSA-N (2r,3r,4s,5r,6s)-4,5-dimethoxy-2-(methoxymethyl)-3-[(2s,3r,4s,5r,6r)-3,4,5-trimethoxy-6-(methoxymethyl)oxan-2-yl]oxy-6-[(2r,3r,4s,5r,6r)-4,5,6-trimethoxy-2-(methoxymethyl)oxan-3-yl]oxyoxane Chemical compound CO[C@@H]1[C@@H](OC)[C@H](OC)[C@@H](COC)O[C@H]1O[C@H]1[C@H](OC)[C@@H](OC)[C@H](O[C@H]2[C@@H]([C@@H](OC)[C@H](OC)O[C@@H]2COC)OC)O[C@@H]1COC LNAZSHAWQACDHT-XIYTZBAFSA-N 0.000 claims description 2
- 239000008213 purified water Substances 0.000 claims description 2
- 239000001785 acacia senegal l. willd gum Substances 0.000 claims 1
- 230000002708 enhancing effect Effects 0.000 abstract description 2
- 239000004205 dimethyl polysiloxane Substances 0.000 description 8
- 235000013601 eggs Nutrition 0.000 description 8
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 description 8
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 6
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 5
- 239000000126 substance Substances 0.000 description 4
- RZRNAYUHWVFMIP-KTKRTIGZSA-N 1-oleoylglycerol Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OCC(O)CO RZRNAYUHWVFMIP-KTKRTIGZSA-N 0.000 description 3
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 3
- 230000000844 anti-bacterial effect Effects 0.000 description 3
- 239000003054 catalyst Substances 0.000 description 3
- 150000002148 esters Chemical class 0.000 description 3
- 229920002313 fluoropolymer Polymers 0.000 description 3
- RZRNAYUHWVFMIP-HXUWFJFHSA-N glycerol monolinoleate Natural products CCCCCCCCC=CCCCCCCCC(=O)OC[C@H](O)CO RZRNAYUHWVFMIP-HXUWFJFHSA-N 0.000 description 3
- 229920001343 polytetrafluoroethylene Polymers 0.000 description 3
- 244000215068 Acacia senegal Species 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 229920000084 Gum arabic Polymers 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 2
- 239000000205 acacia gum Substances 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- SZVJSHCCFOBDDC-UHFFFAOYSA-N ferrosoferric oxide Chemical compound O=[Fe]O[Fe]O[Fe]=O SZVJSHCCFOBDDC-UHFFFAOYSA-N 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000002736 nonionic surfactant Substances 0.000 description 2
- 239000000049 pigment Substances 0.000 description 2
- 239000004810 polytetrafluoroethylene Substances 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 description 2
- 239000002888 zwitterionic surfactant Substances 0.000 description 2
- WTUTXGGXSHMISM-UHFFFAOYSA-N 2-acetyloxyacetic acid;butanoic acid Chemical compound CCCC(O)=O.CC(=O)OCC(O)=O WTUTXGGXSHMISM-UHFFFAOYSA-N 0.000 description 1
- MTJGVAJYTOXFJH-UHFFFAOYSA-N 3-aminonaphthalene-1,5-disulfonic acid Chemical compound C1=CC=C(S(O)(=O)=O)C2=CC(N)=CC(S(O)(=O)=O)=C21 MTJGVAJYTOXFJH-UHFFFAOYSA-N 0.000 description 1
- 239000004925 Acrylic resin Substances 0.000 description 1
- 229920000178 Acrylic resin Polymers 0.000 description 1
- 239000004606 Fillers/Extenders Substances 0.000 description 1
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000002421 anti-septic effect Effects 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000004927 clay Substances 0.000 description 1
- 239000012459 cleaning agent Substances 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 239000003599 detergent Substances 0.000 description 1
- PKTOVQRKCNPVKY-UHFFFAOYSA-N dimethoxy(methyl)silicon Chemical compound CO[Si](C)OC PKTOVQRKCNPVKY-UHFFFAOYSA-N 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 230000008821 health effect Effects 0.000 description 1
- 125000001165 hydrophobic group Chemical group 0.000 description 1
- 239000002563 ionic surfactant Substances 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 239000010445 mica Substances 0.000 description 1
- 229910052618 mica group Inorganic materials 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 229910000077 silane Inorganic materials 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000008247 solid mixture Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- CPUDPFPXCZDNGI-UHFFFAOYSA-N triethoxy(methyl)silane Chemical compound CCO[Si](C)(OCC)OCC CPUDPFPXCZDNGI-UHFFFAOYSA-N 0.000 description 1
- JCVQKRGIASEUKR-UHFFFAOYSA-N triethoxy(phenyl)silane Chemical compound CCO[Si](OCC)(OCC)C1=CC=CC=C1 JCVQKRGIASEUKR-UHFFFAOYSA-N 0.000 description 1
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D183/00—Coating compositions based on macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon, with or without sulfur, nitrogen, oxygen, or carbon only; Coating compositions based on derivatives of such polymers
- C09D183/04—Polysiloxanes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D183/00—Coating compositions based on macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon, with or without sulfur, nitrogen, oxygen, or carbon only; Coating compositions based on derivatives of such polymers
- C09D183/04—Polysiloxanes
- C09D183/08—Polysiloxanes containing silicon bound to organic groups containing atoms other than carbon, hydrogen, and oxygen
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/08—Anti-corrosive paints
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Paints Or Removers (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Application Of Or Painting With Fluid Materials (AREA)
Abstract
The invention discloses a repairing agent capable of increasing or repairing the non-stick property of cookers, a preparation method and a use method thereof, the repairing agent contains silicone oil, a surfactant, a thickening agent, water and a preservative, particularly, the weight percentage of the silicone oil in the repairing agent is 10-50%, the weight percentage of the surfactant is 0.5-5%, the weight percentage of the thickening agent is 0.2-10%, the weight percentage of the water is 40-80%, the weight percentage of the preservative is 0.1-2%, and the viscosity of the repairing agent at 25 ℃ is 2000-8000 mPa s. The repairing agent has the advantages of repairing non-stick cookers and enhancing the non-stick performance of cookers, and the preparation method and the use method are simple and convenient, and the effect is excellent; the repairing agent of the invention is healthier and more environment-friendly in use and has good non-stick performance.
Description
Technical Field
The invention relates to a non-stick cooker repairing agent, in particular to a repairing agent capable of increasing or repairing the non-stick performance of cookers, and a preparation method and a use method thereof.
Background
Non-stick cookware has been widely used in modern life and is characterized by a non-stick characteristic because the cookware surface has a special coating. The coating compound has the advantages of high temperature resistance, low temperature resistance, self-lubricating property, chemical stability and the like, so that the non-stick cooker is different from common cooking tools. However, the longer the non-stick cookware is used, the more the non-stick performance decreases, and even the non-stick performance is lost. The prior art generally provides improvements in the preparation of utensils to achieve the non-stick characteristics of non-stick cookware, and does not provide a corresponding repair when there is a problem with the non-stick characteristics of the utensils. The invention provides a repairing agent, which is used for forming a non-stick coating on the surface of a cooker so that the cooker has non-stick performance again, thereby reducing the preparation cost and the use cost of a user. In addition, the repairing agent of the invention can make the cooker regain the non-stick property in a short time, and is more convenient to use.
The prior art CN101955697A discloses a ceramic non-stick coating with an antibacterial effect, and particularly discloses that the coating is prepared from A, B, C three components in a weight ratio of 2: 0.5-2: 0.1-2, wherein: the component A comprises: mixing the following components in percentage by mass: dispersing 50-100% of silica sol, 0-50% of temperature-resistant pigment, 0-20% of extender pigment, 0-2% of dispersing aid and 0-2% of leveling aid, and then grinding for more than 2 hours to obtain a component A; and B component: mixing 0.4-1.5% of acetic acid and the balance of at least one silane by mass; and C, component C: dispersing and dissolving 1-10% of alcohol-soluble acrylic resin, 0-30% of non-stick auxiliary agent and 1-50% of antibacterial material in 50-95% of isopropanol by mass to obtain a component C, wherein the addition amount of the antibacterial material is 1-25% of the total mass of solid components in A, B, C three components. The coating has various components, complex manufacturing process and higher production cost.
In addition, prior art CN102634278A discloses a high temperature resistant ceramic coating for non-stick cookware and a preparation method thereof, wherein the coating is prepared by mixing component a and component B at a weight ratio of 2.0-2.2:1.0-1.2, the component a is prepared from silica sol, alumina sol, zirconia sol, mica powder, iron oxide black, high temperature alumina, isopropanol, deionized water, cellulose carboxymethyl acetate butyrate, and fluorosilicone oil, and the component B is prepared from methyltriethoxysilane, ニ methyldimethoxysilane, phenyltriethoxysilane, isopropanol, and ethanol; the preparation method comprises the steps of mixing the component A and the component B of the coating according to the weight ratio of 2.0-2.2:1.0-1.2, and carrying out sealed stirring and curing for at least 3 hours at 35 ℃ and under the condition of 200rpm at 150 ℃ to obtain the coating, wherein the coating mainly utilizes the high-temperature resistance stability of-Si-O-bonds, so that the excellent high-temperature performance of the coating is ensured. However, because of the use of inorganic components such as iron oxide black and high temperature alumina, the coating uniformity is difficult to control, and the coating is easy to fall off.
The prior art CN97100857 discloses a non-stick coating with low fluorine release, the dry solid composition of which comprises fluorocarbon polymer less than 40% of the total weight, inorganic powder filler more than 10% of the total weight and part of binder. The coating can maintain low-density fluorine release level and reduce food contamination. However, the coating uses a fluorocarbon polymer such as polytetrafluoroethylene, which is a non-stick cookware that generally cannot be cooked at higher temperatures because the ptfe tends to be unstable above 260 c and begins to decompose and produce substances harmful to humans when the temperature is raised to about 310 c and above. In recent years, people pay more attention to the health effect of fluorine-containing substances released by non-stick cookware coatings, so that more healthy and environment-friendly non-stick cookware coatings are urgently needed.
Disclosure of Invention
The invention provides a repairing agent for increasing or repairing non-stick performance of cookers, a preparation method and a use method thereof, aiming at the defects that the non-stick performance cannot be repaired when the non-stick performance is in problem in the prior art. The repairing agent has the functions of repairing non-stick cookers, enhancing the non-stick performance of any cooker and the like, and has simple preparation method and use method and excellent effect.
The technical scheme of the invention is as follows:
a restoring agent for increasing or restoring the non-stick performance of cooking utensils contains silicon oil, surfactant, thickening agent, water and antiseptic, and the weight percentage of the silicon oil in the restoring agent is 10-50%.
In particular, the silicone oil is a silicone oil with non-stick effect.
In particular, the silicone oil with non-stick effect is selected from one or more of polydimethyl silicone oil, phenyl silicone oil, methyl phenyl silicone oil and fluorine modified silicone oil.
In particular, the surfactant is selected from one or more of soybean lecithin, polyglycerol fatty acid ester, polysorbate, glyceryl monostearate or glyceryl monooleate.
In particular, the thickener is water soluble.
In particular, the thickening agent is selected from one or more of methyl cellulose, ethyl cellulose, hydroxymethyl cellulose, hydroxyethyl cellulose, hydroxypropyl methyl cellulose, sodium alginate, gelatin, agar, carrageenan, gum arabic or peach gum.
In particular, the water is selected from tap water, pure water or deionized water.
In particular, the preservative is selected from one or more of calcium propionate, sodium propionate, potassium sorbate or sodium benzoate.
In particular, the surfactant is present in the repairing agent in an amount of 0.5 to 5% by weight.
In particular, the weight percentage of the thickening agent in the repairing agent is 0.2-10%.
Particularly, the water accounts for 40 to 80 percent of the weight of the repairing agent.
In particular, the preservative is present in the repairing agent in an amount of 0.1 to 2% by weight.
In particular, the viscosity of the repairing agent at 25 ℃ is 2000-8000 mPa s.
The preparation method of the repairing agent comprises the following steps:
weighing the silicone oil, the surfactant, the thickener, the water and the preservative according to the above dosage at room temperature, firstly stirring and mixing the silicone oil and the water by a stirrer at a stirring speed of 5-15 m/s, adding half of the surfactant to enable the mixture to generate an emulsification effect, stirring for 20min, then adding the thickener and the preservative, stirring for 10min at the same stirring speed until the thickener and the preservative are completely dissolved, then adding the other half of the surfactant, and adjusting the dosage of the thickener or the water according to viscosity requirements to obtain the repairing agent, wherein the viscosity of the obtained repairing agent at 25 ℃ is about 2000-8000 mPa s, preferably 3000mPa s.
Particularly, the silicone oil, the surfactant and the deionized water in the repairing agent are stirred and mixed to generate an emulsification effect, so that the silicone oil and the water are prevented from being separated, and the silicone oil floats on the surface of the repairing agent.
In particular, the thickener in the repairing agent functions to increase the viscosity of the repairing agent and to prevent the separation of silicone oil and water.
In particular, the deionized water in the repairing agent is used for adjusting the viscosity besides being matched with silicone oil and a surfactant to generate emulsification.
In particular, the preservative in the restorative acts to prevent decay of the restorative.
The using method of the repairing agent comprises the following steps:
coating a small amount of the repairing agent on the surface of a cooker, wiping the surface of the cooker coated with the repairing agent by cloth or paper towel until the surface is dry, dry-burning the cooker on a low-to-medium-fire cooking furnace at the temperature of 180 ℃ and 250 ℃ for 2-5 minutes, cooling the cooker to room temperature, and cleaning the cooker by clear water for later use.
If the repairing effect needs to be enhanced after cleaning, a small amount of the repairing agent can be coated on the surface of the cooker, the surface of the cooker coated with the repairing agent is wiped by cloth or paper towel, and then the cooker is treated by the dry burning method. The non-stick property of the surface of the cooker can be enhanced by the treatment of the method.
In the heating process, the silicone oil in the repairing agent forms a new non-stick coating due to heating, so that the cooker recovers the non-stick function.
In particular, the method is suitable for cooking utensils, ovens and the like in households and restaurants.
By using the repairing agent of the invention, the following beneficial effects are achieved: a new non-stick coating can be formed on the surface of the cooker, so that the cooker can obtain the non-stick characteristic again in a short time, the preparation cost and the use cost of a user are reduced, and the use is convenient; the repairing agent does not use fluorocarbon polymers which are easy to generate toxic decomposition products, such as polytetrafluoroethylene and the like commonly used in non-stick coatings, so that the repairing agent is healthier and more environment-friendly; the cookware repaired by the repairing agent has good non-stick performance.
Drawings
FIG. 1 shows a basic schematic of the reaction of the components of the repair agent according to the invention.
FIG. 2 shows a flow chart of the use of the repairing agent of the invention.
FIG. 3 shows a graph comparing the results of a non-stick property test without and with the repair agent of the present invention.
Detailed Description
The invention is further illustrated below with reference to specific examples. It is to be understood, however, that these examples are illustrative only and are not to be construed as limiting the scope of the present invention. The experimental procedures, in which specific conditions are not noted in the following examples, are generally carried out under conventional conditions or conditions recommended by the manufacturers. All percentages and parts are by weight unless otherwise indicated.
In order to solve the problems that the non-stick property in the prior art cannot be repaired when the problem occurs, the invention provides a repairing agent and a preparation method thereof, and the repairing agent specifically comprises the following steps: the method comprises the steps of mixing raw materials of silicone oil accounting for 10-50% of the repairing agent by weight, surfactant accounting for 0.5-5%, thickening agent accounting for 0.2-10%, water accounting for 40-80% of the repairing agent by weight and preservative accounting for 0.1-2% of the repairing agent by weight to prepare the repairing agent capable of increasing or repairing the non-stick property of the cooker, and only coating the repairing agent on an area to be repaired in the using process, so that the problems existing in the using process of the cooker can be solved.
In the technical scheme of the invention, the air conditioner is provided with a fan,
the silicone oil used in the present invention is a silicone oil having a non-stick effect, which is used to provide a repair agent with higher non-stick properties, good smooth touch, water repellency, and durability of a repair coating. The silicone oil used in the present invention is selected from commercially available polydimethyl silicone oil, phenyl silicone oil, methylphenyl silicone oil and fluorine modified silicone oil. Silicone oils increase in molecular weight and viscosity with the number of chain segments n, so silicone oils can have a variety of viscosities, from 0.65 centistokes up to millions of centistokes. The invention can adjust the preparation process of the silicone oil according to the viscosity requirement of the silicone oil. If silicone oil with low viscosity is to be prepared, acid clay is used as a catalyst and telomerization is carried out at the temperature of 180 ℃, or sulfuric acid is used as a catalyst and telomerization is carried out at the low temperature; an alkaline catalyst can be used if a high viscosity silicone oil is produced. According to the invention, silicone oil with the viscosity of 50-5000 centistokes is preferably used, the weight percentage of the silicone oil in the repairing agent is 10-50%, if the weight percentage is less than 10%, the durability of the repairing coating is poor, and exceeds 50%, and the difficulty of emulsification with water is increased.
The non-stick silicone oil used in the invention can react with the surface of the cooker to form a long-term non-stick coating, and the non-stick coating still exists even after being cleaned by using a cleaning agent.
The specific working principle is shown in fig. 1:
under the condition of heating, hydroxyl of silicon oil in the repairing agent can be condensed with hydroxyl on the surface of the ceramic coating, so that the repairing agent is tightly combined with the surface of the cooker, and the non-stick property of the surface of the coating can be repaired.
The surfactant is a substance which is added in a small amount and can cause the interface state of a solution system to change obviously. The molecular structure of the surfactant has amphipathy: one end is a hydrophilic group and the other end is a hydrophobic group. The surfactant is divided into ionic surfactant, non-ionic surfactant, zwitterionic surfactant, compound surfactant and the like. The surfactant used in the present invention may be soybean lecithin, which is a zwitterionic surfactant, and polyglycerin fatty acid ester, polysorbate, glyceryl monostearate or glyceryl monooleate, which is a nonionic surfactant. The surfactant in the repairing agent can be mixed with the silicone oil and the deionized water by stirring to generate an emulsification effect, so that the silicone oil and the deionized water can be prevented from being separated, and the silicone oil is prevented from floating on the surface of the repairing agent.
The thickener is used for increasing the viscosity of the repairing agent and preventing the silicon oil from being separated from water. The thickening agent of the present invention is water soluble and may be selected from the group consisting of methylcellulose, ethylcellulose, hydroxymethylcellulose, hydroxyethylcellulose, hydroxypropylmethylcellulose, sodium alginate, gelatin, agar, carrageenan, gum arabic, or peach gum. The content of the thickening agent has a remarkable influence on the stability of the repairing agent, and the thickening agent accounts for 0.2-10% of the weight percentage of the repairing agent, and preferably 1-5%.
The preservative can prevent the repairing agent from being rotten and increase the storage time of the repairing agent. The preservative can be selected from calcium propionate, sodium propionate, potassium sorbate or sodium benzoate, and the content of the preservative in the repairing agent is 0.1-2% by weight.
In order to make the objects, technical solutions and advantages of the present invention more apparent, embodiments of the present invention will be described in detail with reference to the accompanying drawings.
Example one
A repairing agent for increasing or repairing the non-stick property of cooker is prepared from polydimethyl silicone oil (50 wt.%), polysorbate (2), hydroxymethyl cellulose (1), deionized water (46.5) and sodium propionate (0.5).
The preparation method of the repairing agent comprises the following steps:
at room temperature, weighing the polydimethylsiloxane oil, the polysorbate ester, the hydroxymethyl cellulose, the deionized water and the sodium propionate according to the above dosage, firstly stirring and mixing the polydimethylsiloxane oil and the deionized water by a stirrer at a stirring speed of 5m/s, adding half of the polysorbate ester to enable the mixture to generate emulsification, then adding the hydroxymethyl cellulose and the sodium propionate, stirring until the hydroxymethyl cellulose and the sodium propionate are completely dissolved, and then adding the other half of the polysorbate ester to obtain the formula A.
The method of using the repairing agent is shown in figure 2:
for the cooker to be repaired or the cooker to be increased with non-stick performance, a proper amount of repairing agent is smeared on the surface of the position to be repaired, the surface of the cooker coated with the repairing agent is wiped to be dry by cloth or paper towel, and the cooker is dried and burned for 2 to 5 minutes in a cooking furnace with the temperature of 180 ℃ and 250 ℃ and the temperature of low to medium fire; if the repairing effect needs to be enhanced, a small amount of the repairing agent can be coated on the surface of the cooker, the surface of the cooker coated with the repairing agent is wiped by cloth or paper towels, the cooker is treated by the dry burning method, and finally the cooker is cooled and washed by clean water.
Example two
A restoring agent for increasing or restoring the non-sticking performance of cooker is prepared from phenyl silicone oil (30 wt.%), polyglycerin fatty acid ester (5), methylcellulose (2), purified water (61) and potassium sorbate (2).
The preparation method of the repairing agent comprises the following steps:
at room temperature, weighing the phenyl silicone oil, the polyglycerol fatty acid ester, the methyl cellulose, the pure water and the potassium sorbate according to the above dosage, firstly stirring and mixing the phenyl silicone oil and the pure water by a stirrer at a stirring speed of 10m/s, adding half of the polyglycerol fatty acid ester to enable the mixture to generate emulsification, then adding the methyl cellulose and the potassium sorbate, stirring until the methyl cellulose and the potassium sorbate are completely dissolved, and then adding the other half of the polyglycerol fatty acid ester to obtain the repairing agent.
The using method of the repairing agent comprises the following steps:
coating a small amount of the repairing agent on the surface of a cooker, wiping the surface of the cooker coated with the repairing agent by cloth until the surface is dry, dry-burning the cooker on a low-to-medium-fire cooking furnace at the temperature of 180-250 ℃ for 2-5 minutes, cooling the cooker to room temperature, and cleaning the cooker by clear water for later use.
EXAMPLE III
A restoring agent for increasing or restoring the non-sticking performance of cooker is prepared from methyl phenyl silicone oil (10 wt.%), soybean lecithin (0.5), sodium alginate (9.4), tap water (80) and sodium benzoate (0.1).
The preparation method of the repairing agent comprises the following steps:
weighing methyl phenyl silicone oil, soybean lecithin, sodium alginate, tap water and sodium benzoate according to the above dosage at room temperature, firstly stirring and mixing the methyl phenyl silicone oil and the tap water by a stirrer at a stirring speed of 15m/s, adding half of the dosage of the soybean lecithin to enable the mixture to generate emulsification, then adding the sodium alginate and the sodium benzoate, stirring until the sodium alginate and the sodium benzoate are completely dissolved, and then adding the other half of the dosage of the soybean lecithin to obtain the repairing agent.
The using method of the repairing agent comprises the following steps:
coating a small amount of the repairing agent on the surface of a cooker, wiping the surface of the cooker coated with the repairing agent by cloth until the surface is dry, dry-burning the cooker on a low-to-medium-fire cooking furnace at the temperature of 180-250 ℃ for 2-5 minutes, cooling the cooker to room temperature, and cleaning the cooker by clear water for later use.
Example four
A repairing agent for increasing or repairing the non-stick property of cooker contains fluorine modified silicon oil (50 wt.%), glyceryl monostearate (5), gelatin (3), deionized water (40) and calcium propionate (2).
The preparation method of the repairing agent comprises the following steps:
at room temperature, weighing the fluorine modified silicone oil, the glyceryl monostearate, the gelatin, the deionized water and the calcium propionate according to the above dosage, firstly stirring and mixing the fluorine modified silicone oil and the deionized water by a stirrer at a stirring speed of 15m/s, adding half of the dosage of the glyceryl monostearate to enable the mixture to generate emulsification, then adding the gelatin and the calcium propionate, stirring until the gelatin and the calcium propionate are completely dissolved, and then adding the other half of the dosage of the glyceryl monostearate to obtain the repairing agent.
The using method of the repairing agent comprises the following steps:
coating a small amount of the repairing agent on the surface of a cooker, wiping the surface of the cooker coated with the repairing agent by cloth until the surface is dry, dry-burning the cooker on a low-to-medium-fire cooking furnace at the temperature of 180-250 ℃ for 2-5 minutes, cooling the cooker to room temperature, and cleaning the cooker by clear water for later use.
EXAMPLE five
A repairing agent for increasing or repairing the non-stick property of cooker is prepared from polydimethyl silicone oil (50 wt.%), glyceryl monooleate (5), agar (0.2), deionized water (42.8) and sodium propionate (2).
The preparation method of the repairing agent comprises the following steps:
at room temperature, weighing the polydimethylsiloxane oil, the glycerol monooleate, the agar, the deionized water and the sodium propionate according to the above dosage, firstly stirring and mixing the polydimethylsiloxane oil and the deionized water by a stirrer at a stirring speed of 15m/s, adding half of the dosage of the glycerol monooleate to enable the mixture to generate an emulsification effect, then adding the agar and the sodium propionate, stirring until the agar and the sodium propionate are completely dissolved, and then adding the other half of the dosage of the glycerol monooleate to obtain the repairing agent.
The using method of the repairing agent comprises the following steps:
coating a small amount of the repairing agent on the surface of a cooker, wiping the surface of the cooker coated with the repairing agent by cloth until the surface is dry, dry-burning the cooker on a low-to-medium-fire cooking furnace at the temperature of 180-250 ℃ for 2-5 minutes, cooling the cooker to room temperature, and cleaning the cooker by clear water for later use.
Comparative examples
And (3) adjusting the contents of the polydimethylsiloxane oil and the deionized water according to the technical scheme of the first embodiment to obtain a formula B, C, D. The specific contents are shown in table 1:
TABLE 1
Non-stick property test
The non-stick property test method is as follows: mainly used for egg frying tests, as shown in figure 3, the frying pot is placed on a gas stove for heating, a far infrared ray thermometer is used for measuring the surface temperature of the frying pot, when the surface temperature reaches 170-190 ℃, eggs are thrown in, after the heating is carried out for 3-4 minutes, the eggs are shoveled by a shovel, and whether the eggs are left or not is observed. And if no residue exists, continuing to perform the fried egg test according to the method until the residue of the eggs appears, terminating the test and recording the number of the fried eggs.
Note: one egg is fried and cleaned by detergent once.
TABLE 2
When the percentage of the polydimethylsiloxane oil in the total amount of the repairing agent is 40% and 50%, the non-stick performance of the cooker is better, and when the content of the polydimethylsiloxane oil is 50%, the effect is best. With the reduction of the content of the polydimethylsiloxane oil, the non-stick property is weakened.
While the invention has been described with reference to a preferred embodiment, it will be understood by those skilled in the art that various changes in form and detail may be made therein without departing from the spirit and scope of the invention as defined by the appended claims.
Claims (5)
1. A repairing agent is used for increasing or repairing the non-stick performance of cookers, and is characterized in that the repairing agent consists of 10-50 wt% of silicone oil, 0.5-5 wt% of surfactant, 0.2-10 wt% of thickener, 40-80 wt% of water and 0.1-2 wt% of preservative, and the repairing agent has a viscosity of 2000-8000 mPa & s at 25 ℃;
wherein the silicone oil is selected from one or more of polydimethyl silicone oil, methyl phenyl silicone oil and fluorine modified silicone oil; the surfactant is selected from one or more of soybean lecithin, polyglycerol fatty acid ester, polysorbate, glyceryl monostearate or glyceryl monooleate; the thickening agent is water-soluble and is selected from one or more of methyl cellulose, ethyl cellulose, hydroxymethyl cellulose, hydroxyethyl cellulose, hydroxypropyl methyl cellulose, sodium alginate, gelatin, agar, carrageenan, Arabic gum or peach gum;
under the condition of heating, hydroxyl of silicon oil in the repairing agent is condensed with hydroxyl on the surface of the ceramic coating, so that the repairing agent is tightly combined with the surface of the cooker, and the non-stick property of the surface of the coating is repaired;
the using method of the repairing agent comprises the following steps: coating a small amount of the repairing agent on the surface of a cooker, wiping the surface of the cooker coated with the repairing agent by cloth or paper towel until the surface is dry, dry-burning the cooker on a low-to-medium-fire cooking furnace at the temperature of 180-250 ℃ for 2-5min, cooling the cooker to room temperature, and cleaning the cooker by clear water for later use.
2. The repair agent of claim 1 wherein the silicone oil is a non-stick silicone oil.
3. The repair kit of claim 1 wherein the water is selected from the group consisting of tap water, purified water, and deionized water.
4. The repair kit of claim 1 wherein the preservative is selected from one or more of calcium propionate, sodium propionate, potassium sorbate or sodium benzoate.
5. The method for producing a repairing agent according to any one of claims 1 to 4,
weighing the silicone oil, the surfactant, the thickener, the water and the preservative according to the above dosage at room temperature, firstly stirring and mixing the silicone oil and the water by using a stirrer at a stirring speed of 5-15 m/s, adding half of the dosage of the surfactant to enable the mixture to generate an emulsification effect, stirring for 20min, then adding the thickener and the preservative, stirring for 10min at the same stirring speed until the thickener and the preservative are completely dissolved, then adding the other half of the dosage of the surfactant, and adjusting the dosage of the thickener or the water according to viscosity requirements to obtain the repairing agent.
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GB1061556A (en) * | 1963-03-11 | 1967-03-15 | Oberschwaeb Metallwaren | Enamelled cooking,frying or roasting vessels |
JPH02169680A (en) * | 1988-12-22 | 1990-06-29 | Mitsubishi Kasei Corp | Polishing cleaner composition |
CN101117039A (en) * | 2006-07-31 | 2008-02-06 | Seb公司 | Culinary item with improved hydrophobic properties and method of producing such an item |
CN101663368A (en) * | 2007-04-18 | 2010-03-03 | Seb公司 | Non-sticky metallic coating with hydrophobic property of improvement |
KR20120139306A (en) * | 2011-06-17 | 2012-12-27 | (주)드림셰프 | Kitchen container coating composite |
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- 2016-07-28 CN CN201610605334.0A patent/CN107663413B/en active Active
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
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GB1061556A (en) * | 1963-03-11 | 1967-03-15 | Oberschwaeb Metallwaren | Enamelled cooking,frying or roasting vessels |
JPH02169680A (en) * | 1988-12-22 | 1990-06-29 | Mitsubishi Kasei Corp | Polishing cleaner composition |
CN101117039A (en) * | 2006-07-31 | 2008-02-06 | Seb公司 | Culinary item with improved hydrophobic properties and method of producing such an item |
CN101663368A (en) * | 2007-04-18 | 2010-03-03 | Seb公司 | Non-sticky metallic coating with hydrophobic property of improvement |
KR20120139306A (en) * | 2011-06-17 | 2012-12-27 | (주)드림셰프 | Kitchen container coating composite |
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Effective date of registration: 20210508 Address after: Ronghuashan industrial Group textile park Pucheng County Nanping City Fujian Province Patentee after: Fujian Kaitai Chemical Co.,Ltd. Address before: 2707, unit 1, building A1, Shengshi garden, Longhua Xinghe, Shenzhen, Guangdong Patentee before: Zhou Baoli |