CN107653013A - 一种改性洗油水煤浆添加剂的制备方法 - Google Patents
一种改性洗油水煤浆添加剂的制备方法 Download PDFInfo
- Publication number
- CN107653013A CN107653013A CN201710862181.2A CN201710862181A CN107653013A CN 107653013 A CN107653013 A CN 107653013A CN 201710862181 A CN201710862181 A CN 201710862181A CN 107653013 A CN107653013 A CN 107653013A
- Authority
- CN
- China
- Prior art keywords
- washing oil
- parts
- additive agent
- slurries additive
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000002002 slurry Substances 0.000 title claims abstract description 53
- 238000005406 washing Methods 0.000 title claims abstract description 50
- 239000003795 chemical substances by application Substances 0.000 title claims abstract description 49
- 239000000654 additive Substances 0.000 title claims abstract description 48
- 230000000996 additive effect Effects 0.000 title claims abstract description 48
- 238000002360 preparation method Methods 0.000 title claims abstract description 32
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 claims abstract description 32
- BNKAXGCRDYRABM-UHFFFAOYSA-N ethenyl dihydrogen phosphate Chemical compound OP(O)(=O)OC=C BNKAXGCRDYRABM-UHFFFAOYSA-N 0.000 claims abstract description 15
- 238000001816 cooling Methods 0.000 claims abstract description 11
- QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims abstract description 11
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 24
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 24
- CHQMHPLRPQMAMX-UHFFFAOYSA-L sodium persulfate Chemical compound [Na+].[Na+].[O-]S(=O)(=O)OOS([O-])(=O)=O CHQMHPLRPQMAMX-UHFFFAOYSA-L 0.000 claims description 20
- 238000010438 heat treatment Methods 0.000 claims description 11
- 239000002994 raw material Substances 0.000 claims description 11
- 238000003756 stirring Methods 0.000 claims description 10
- DYUWTXWIYMHBQS-UHFFFAOYSA-N n-prop-2-enylprop-2-en-1-amine Chemical compound C=CCNCC=C DYUWTXWIYMHBQS-UHFFFAOYSA-N 0.000 claims description 8
- 239000003999 initiator Substances 0.000 abstract description 14
- 238000000034 method Methods 0.000 abstract description 8
- 150000003839 salts Chemical class 0.000 abstract description 8
- 239000003431 cross linking reagent Substances 0.000 abstract description 7
- 238000006243 chemical reaction Methods 0.000 abstract description 3
- 239000000463 material Substances 0.000 abstract description 3
- 230000008569 process Effects 0.000 abstract description 3
- 229910019142 PO4 Inorganic materials 0.000 abstract description 2
- 125000003368 amide group Chemical group 0.000 abstract description 2
- 125000002791 glucosyl group Chemical group C1([C@H](O)[C@@H](O)[C@H](O)[C@H](O1)CO)* 0.000 abstract description 2
- 230000000977 initiatory effect Effects 0.000 abstract description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 abstract description 2
- 239000010452 phosphate Substances 0.000 abstract description 2
- 238000006068 polycondensation reaction Methods 0.000 abstract description 2
- ROOXNKNUYICQNP-UHFFFAOYSA-N ammonium persulfate Chemical compound [NH4+].[NH4+].[O-]S(=O)(=O)OOS([O-])(=O)=O ROOXNKNUYICQNP-UHFFFAOYSA-N 0.000 description 34
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 21
- 229910001870 ammonium persulfate Inorganic materials 0.000 description 17
- 239000003245 coal Substances 0.000 description 17
- 239000000203 mixture Substances 0.000 description 14
- 238000010792 warming Methods 0.000 description 9
- 238000002156 mixing Methods 0.000 description 8
- 239000003250 coal slurry Substances 0.000 description 7
- VICFASWPTIXXIR-UHFFFAOYSA-N ethenyl dihydrogen phosphate;sodium Chemical compound [Na].OP(O)(=O)OC=C VICFASWPTIXXIR-UHFFFAOYSA-N 0.000 description 7
- VPYJNCGUESNPMV-UHFFFAOYSA-N triallylamine Chemical compound C=CCN(CC=C)CC=C VPYJNCGUESNPMV-UHFFFAOYSA-N 0.000 description 6
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 4
- USHAGKDGDHPEEY-UHFFFAOYSA-L potassium persulfate Chemical compound [K+].[K+].[O-]S(=O)(=O)OOS([O-])(=O)=O USHAGKDGDHPEEY-UHFFFAOYSA-L 0.000 description 4
- 235000019394 potassium persulphate Nutrition 0.000 description 4
- QKSNQGHULIFUML-UHFFFAOYSA-N ethenyl dihydrogen phosphate;potassium Chemical compound [K].OP(O)(=O)OC=C QKSNQGHULIFUML-UHFFFAOYSA-N 0.000 description 3
- 230000004048 modification Effects 0.000 description 3
- 238000012986 modification Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 2
- 239000012530 fluid Substances 0.000 description 2
- 239000000446 fuel Substances 0.000 description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
- 229910000027 potassium carbonate Inorganic materials 0.000 description 2
- 229910000029 sodium carbonate Inorganic materials 0.000 description 2
- LWIHDJKSTIGBAC-UHFFFAOYSA-K tripotassium phosphate Chemical compound [K+].[K+].[K+].[O-]P([O-])([O-])=O LWIHDJKSTIGBAC-UHFFFAOYSA-K 0.000 description 2
- 125000003903 2-propenyl group Chemical group [H]C([*])([H])C([H])=C([H])[H] 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000003610 charcoal Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000002817 coal dust Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 239000012847 fine chemical Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 239000003077 lignite Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000003345 natural gas Substances 0.000 description 1
- 229910000160 potassium phosphate Inorganic materials 0.000 description 1
- 235000011009 potassium phosphates Nutrition 0.000 description 1
- 239000013049 sediment Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 238000006277 sulfonation reaction Methods 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 1
- 229920002554 vinyl polymer Polymers 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/32—Liquid carbonaceous fuels consisting of coal-oil suspensions or aqueous emulsions or oil emulsions
- C10L1/326—Coal-water suspensions
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F240/00—Copolymers of hydrocarbons and mineral oils, e.g. petroleum resins
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F8/00—Chemical modification by after-treatment
- C08F8/28—Condensation with aldehydes or ketones
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/10—Liquid carbonaceous fuels containing additives
- C10L1/14—Organic compounds
- C10L1/26—Organic compounds containing phosphorus
- C10L1/2666—Organic compounds containing phosphorus macromolecular compounds
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L2250/00—Structural features of fuel components or fuel compositions, either in solid, liquid or gaseous state
- C10L2250/04—Additive or component is a polymer
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Detergent Compositions (AREA)
- Lubricants (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
- Emulsifying, Dispersing, Foam-Producing Or Wetting Agents (AREA)
Abstract
Description
Claims (1)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201710862181.2A CN107653013B (zh) | 2016-01-23 | 2016-01-23 | 一种改性洗油水煤浆添加剂的制备方法 |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201610046676.3A CN105647604B (zh) | 2016-01-23 | 2016-01-23 | 一种改性洗油水煤浆添加剂及其制备方法 |
CN201710862181.2A CN107653013B (zh) | 2016-01-23 | 2016-01-23 | 一种改性洗油水煤浆添加剂的制备方法 |
Related Parent Applications (1)
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CN201610046676.3A Division CN105647604B (zh) | 2016-01-23 | 2016-01-23 | 一种改性洗油水煤浆添加剂及其制备方法 |
Publications (2)
Publication Number | Publication Date |
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CN107653013A true CN107653013A (zh) | 2018-02-02 |
CN107653013B CN107653013B (zh) | 2019-10-18 |
Family
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Family Applications (4)
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CN201710862181.2A Active CN107653013B (zh) | 2016-01-23 | 2016-01-23 | 一种改性洗油水煤浆添加剂的制备方法 |
CN201610046676.3A Active CN105647604B (zh) | 2016-01-23 | 2016-01-23 | 一种改性洗油水煤浆添加剂及其制备方法 |
CN201710694047.6A Active CN107267238B (zh) | 2016-01-23 | 2016-01-23 | 一种改性洗油水煤浆添加剂的制备方法 |
CN201710862189.9A Active CN107488473B (zh) | 2016-01-23 | 2016-01-23 | 一种改性洗油水煤浆添加剂的制备方法 |
Family Applications After (3)
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CN201610046676.3A Active CN105647604B (zh) | 2016-01-23 | 2016-01-23 | 一种改性洗油水煤浆添加剂及其制备方法 |
CN201710694047.6A Active CN107267238B (zh) | 2016-01-23 | 2016-01-23 | 一种改性洗油水煤浆添加剂的制备方法 |
CN201710862189.9A Active CN107488473B (zh) | 2016-01-23 | 2016-01-23 | 一种改性洗油水煤浆添加剂的制备方法 |
Country Status (1)
Country | Link |
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CN (4) | CN107653013B (zh) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110804141A (zh) * | 2019-11-19 | 2020-02-18 | 安徽鑫固环保股份有限公司 | 一种利用焦化洗油合成水煤浆分散剂的方法 |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108456283A (zh) * | 2016-07-15 | 2018-08-28 | 刘碧霞 | 一种萘系陶瓷分散剂及其制备方法 |
CN108795517B (zh) * | 2018-06-23 | 2021-11-09 | 泉州市联政信息科技有限公司 | 一种高分子水煤浆添加剂及其制备方法 |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4457762A (en) * | 1983-01-07 | 1984-07-03 | Diamond Shamrock Chemicals Company | Stabilized water slurries of carbonaceous materials |
CN1067259A (zh) * | 1991-05-28 | 1992-12-23 | 华煤水煤浆技术联合中心 | 焦油型高浓度水煤浆添加剂和生产工艺 |
CN101735870A (zh) * | 2009-12-16 | 2010-06-16 | 北京海淀华煤水煤浆技术开发中心 | 一种水煤浆添加剂及其制备方法与应用 |
CN105154151A (zh) * | 2015-10-20 | 2015-12-16 | 陈文水 | 一种水煤浆添加剂及其制备方法 |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101613256B (zh) * | 2009-07-01 | 2012-04-18 | 新奥科技发展有限公司 | 一种由煤制取酚类产品的方法 |
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2016
- 2016-01-23 CN CN201710862181.2A patent/CN107653013B/zh active Active
- 2016-01-23 CN CN201610046676.3A patent/CN105647604B/zh active Active
- 2016-01-23 CN CN201710694047.6A patent/CN107267238B/zh active Active
- 2016-01-23 CN CN201710862189.9A patent/CN107488473B/zh active Active
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4457762A (en) * | 1983-01-07 | 1984-07-03 | Diamond Shamrock Chemicals Company | Stabilized water slurries of carbonaceous materials |
CN1067259A (zh) * | 1991-05-28 | 1992-12-23 | 华煤水煤浆技术联合中心 | 焦油型高浓度水煤浆添加剂和生产工艺 |
CN101735870A (zh) * | 2009-12-16 | 2010-06-16 | 北京海淀华煤水煤浆技术开发中心 | 一种水煤浆添加剂及其制备方法与应用 |
CN105154151A (zh) * | 2015-10-20 | 2015-12-16 | 陈文水 | 一种水煤浆添加剂及其制备方法 |
Non-Patent Citations (2)
Title |
---|
吴晓华等: ""聚羧酸系水煤浆添加剂的合成研究"", 《洁净煤技术》 * |
王方: "《国际通用离子交换技术手册》", 31 May 2000, 科学技术文献出版社 * |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110804141A (zh) * | 2019-11-19 | 2020-02-18 | 安徽鑫固环保股份有限公司 | 一种利用焦化洗油合成水煤浆分散剂的方法 |
Also Published As
Publication number | Publication date |
---|---|
CN107267238B (zh) | 2019-10-01 |
CN107653013B (zh) | 2019-10-18 |
CN107267238A (zh) | 2017-10-20 |
CN107488473A (zh) | 2017-12-19 |
CN107488473B (zh) | 2019-07-26 |
CN105647604B (zh) | 2017-08-04 |
CN105647604A (zh) | 2016-06-08 |
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SE01 | Entry into force of request for substantive examination | ||
CB03 | Change of inventor or designer information | ||
CB03 | Change of inventor or designer information |
Inventor after: Si Chuanyu Inventor after: Li Qiao Inventor before: Li Qiao |
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TA01 | Transfer of patent application right | ||
TA01 | Transfer of patent application right |
Effective date of registration: 20190919 Address after: 273500 Taiping Town Industrial Park, Zoucheng City, Jining City, Shandong Province Applicant after: Si Chuan Yu Address before: 362700 R&D Center, Science and Technology Incubation Base on both sides of the Straits, Shihu Avenue, Shishi City, Quanzhou City, Fujian Province Applicant before: Li Qiao |
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CP02 | Change in the address of a patent holder |
Address after: No. 58, Xinfu Road, Xinjie community, yonganzhou Town, Gaogang District, Taizhou City, Jiangsu Province Patentee after: Si Chuanyu Address before: 273500 Taiping Town Industrial Park, Zoucheng City, Jining City, Shandong Province Patentee before: Si Chuanyu |
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CP02 | Change in the address of a patent holder | ||
CP02 | Change in the address of a patent holder |
Address after: 273500 Taiping Town Industrial Park, Zoucheng City, Jining City, Shandong Province Patentee after: Si Chuanyu Address before: No. 58, Xinfu Road, Xinjie community, yonganzhou Town, Gaogang District, Taizhou City, Jiangsu Province Patentee before: Si Chuanyu |
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CP02 | Change in the address of a patent holder | ||
CP02 | Change in the address of a patent holder |
Address after: No.438 Diaozhuang, Xulong administrative village, Huangji Township, yuncheng county, Heze City, Shandong Province Patentee after: Si Chuanyu Address before: 273500 Taiping Town Industrial Park, Zoucheng City, Jining City, Shandong Province Patentee before: Si Chuanyu |