CN107626273A - A kind of horizontal reacting kettle of temperature-controllable - Google Patents
A kind of horizontal reacting kettle of temperature-controllable Download PDFInfo
- Publication number
- CN107626273A CN107626273A CN201711045269.1A CN201711045269A CN107626273A CN 107626273 A CN107626273 A CN 107626273A CN 201711045269 A CN201711045269 A CN 201711045269A CN 107626273 A CN107626273 A CN 107626273A
- Authority
- CN
- China
- Prior art keywords
- kettle
- cooling water
- temperature
- agitating device
- clip slot
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
Landscapes
- Physical Or Chemical Processes And Apparatus (AREA)
- Mixers Of The Rotary Stirring Type (AREA)
- Accessories For Mixers (AREA)
Abstract
The invention discloses a kind of horizontal reacting kettle of temperature-controllable,Including the support with pooling feature,The kettle being arranged on support,It is arranged on the control system of kettle side,It is arranged on the charging aperture of kettle roof center and is arranged on the discharging opening of autoclave body bottom,Also include the first agitating device,Second agitating device and along kettle outer wall outer rim set cooling water clip slot,Helical pipe is provided with described cooling water clip slot,The other end of the agitating shaft is provided with agitator frame,Electric boiling plate is provided with the inside of the agitator frame,The opposite side of the charging aperture and the first agitating device are symmetrically arranged with the second agitating device,Temperature inductor is provided with the kettle,By using the helical pipe for being connected with cooling water and it is arranged on electric boiling plate on the inside of agitator frame,Both can be that reactant heats,Can be the mixture cooling in course of reaction again,Realize the accurate temperature control to the inside and outside dual of polymerisation.
Description
Technical field
The present invention relates to the horizontal reacting kettle of a kind of reactor, more particularly to a kind of temperature-controllable.
Background technology
Reactor is widely used in oil, chemical industry, rubber, agricultural chemicals, dyestuff, medicine, food, for completing to vulcanize, nitrifying,
The pressure vessel of the technical process such as hydrogenation, hydrocarbonylation, polymerization, condensation.
At present, the synthetic method of polymer is typically used several polymer reaction monomers being put into reactor simultaneously and carried out
Polymerisation.Polymer reaction monomer in polymerization process can neither endothermic nor exothermic, the choosing of the control of temperature to reactive material
Selecting property and yield have great role.Polymer reaction monomer needs the induced reaction that heats up during the course of the reaction, during beginning, enters
It is again highly exothermic, it is necessary to quickly remove heat after course of reaction.Its reaction speed is very sensitive to reaction temperature, and temperature is higher,
Reaction is faster, and heat release is more violent, and temperature gets over height, and speed is got in reaction, and heat release is fewer, therefore controls reaction temperature, is control
Reaction speed, improve the selectivity of reactive material and a key of yield；Meanwhile between several polymer monomers fully
A uniformly key technical problem of mixing and raising reaction efficiency.
Therefore, the present invention is in view of above-mentioned technological deficiency, by concentrating on studies and designing, synthesis is engaged in related production for many years for a long time
The experience and achievement of industry, research and design goes out the inside and outside regulation thermotonus kettle of one kind, to overcome above-mentioned technological deficiency.
The content of the invention
It is an object of the invention to：The phenomenon of accurate temperature controlling is unable to for aforesaid reaction vessel, causes polymerisation reaction speed
The problem of rate is difficult to control, the present invention provide a kind of horizontal reacting kettle of temperature-controllable.
The technical solution adopted by the present invention is as follows：A kind of horizontal reacting kettle of temperature-controllable, including with pooling feature
Support, the kettle being arranged on support, the control system for being arranged on kettle side, the charging aperture for being arranged on kettle roof center
And the discharging opening of autoclave body bottom is arranged on, in addition to the first agitating device, the second agitating device and along kettle outer wall
The cooling water clip slot that outer rim is set, one end of the cooling water clip slot are provided with cooling water inlet, the cooling water clip slot it is another
One end is provided with coolant outlet, is provided with helical pipe in described cooling water clip slot, one end of the helical pipe with it is cold
But water inlet connects, and the other end of the helical pipe connects with coolant outlet, and first agitating device is located at charging aperture
Side, the first agitating device includes agitating shaft and motor, and one end of the agitating shaft extends to the outside of kettle and is connected with
Motor, the other end of the agitating shaft are provided with agitator frame, electric boiling plate, the charging are provided with the inside of the agitator frame
The opposite side and the first agitating device of mouth are symmetrically arranged with the second agitating device, and temperature inductor is provided with the kettle.
Reactant enters the inside of kettle by material inlet, and it is anti-to use the electric boiling plate being arranged on the inside of agitator frame
Thing is answered to heat, with the progress of polymerisation, substantial amounts of heat is released in reaction, when temperature inductor detects that the temperature of mixture is high
When a certain value, signal is passed to control system, what control system made that cooling water continues enters cold from cooling water inlet
But in the helical pipe in water clip slot, the mixture in kettle is cooled, then cooling water is flowed out from coolant outlet, it is cold
But water constant flow in helical pipe, the state of cooling can be made to keep optimal, so as to realize quick cooling, made in kettle
The mixture in portion is in temperature constant state, and after the completion of reaction, product flows out from discharging opening；By using the spiral shell for being connected with cooling water
Coil road and electric boiling plate on the inside of agitator frame is arranged on, both can be that reactant heats, can be mixed in course of reaction again
Compound cools, and realizes the accurate temperature control to the inside and outside dual of polymerisation；It can both increase by using helical pipe cold
But in water clip slot cooling water amount, so as to accelerate to cool, cooling water residence time can be improved again, make full use of cooling water；
By using the first agitating device and the second agitating device, material can be made sufficiently to mix, on the one hand can be to be mixed in kettle
The temperature of thing is uniform, on the other hand the heat of electric boiling plate can be made quickly to be dispersed into mixture；By using stirring frame
Frame, electric boiling plate is set to be on the inside of agitator frame, there is provided the high compactedness of whole device；By using with pooling feature
Support, the vibrations of horizontal kettle can be reduced, avoid horizontal kettle from damaging.
It is preferably located on the agitating shaft above agitator frame and is symmetrically arranged with paddle.By symmetrical on agitating shaft
Paddle is set, can further improve the effect of stirring.
Preferably, it is provided with decelerator on described motor.Pass through the rotating speed of decelerator regulation motor.
Preferably, support includes bottom plate and 3~4 legs being arranged on bottom plate, it is evenly arranged with 2 in the bottom plate~
3 elastomer blocks.By the inside of bottom plate set 3~4 elastomer blocks, can smaller horizontal reacting kettle vibrations.
In summary, by adopting the above-described technical solution, the beneficial effects of the invention are as follows：
Both can be anti-1. by using the helical pipe for being connected with cooling water and being arranged on electric boiling plate on the inside of agitator frame
Answer thing to heat, can be the mixture cooling in course of reaction again, realize the accurate control to the inside and outside dual of polymerisation
Temperature；
2. can both increase the amount of cooling water in cooling water clip slot by using helical pipe, so as to accelerate to cool, again may be used
To improve cooling water residence time, cooling water is made full use of；
3. by using the first agitating device and the second agitating device, material can be made sufficiently to mix, on the one hand can be with
The temperature of mixture is uniform in kettle, on the other hand the heat of electric boiling plate can be made quickly to be dispersed into mixture；
4. by using agitator frame, electric boiling plate is on the inside of agitator frame, there is provided high whole device it is compact
Property；
5. by using the support with pooling feature, the vibrations of horizontal kettle can be reduced, avoid horizontal kettle from damaging.
Brief description of the drawings
Examples of the present invention will be described by way of reference to the accompanying drawings, wherein：
Fig. 1 is the structural representation of the present invention；
Fig. 2 is the stereogram of helical pipe；
Reference：1- supports, 2- kettlies, 3- control systems, 4- charging apertures, 5- discharging openings, the agitating devices of 6- first, 7-
Second agitating device, 8- cooling water clip slots, 9- cooling water inlets, 10- coolant outlets, 11- helical pipes, 12- agitating shafts,
13- motors, 14- agitator frames, 15- electric boiling plates, 16- temperature inductors, 17- paddles, 18- decelerators, 19- bottom plates, 20-
Leg, 21- elastomer blocks.
Embodiment
All features disclosed in this specification, or disclosed all methods or during the step of, except mutually exclusive
Feature and/or step beyond, can combine in any way.
The present invention is elaborated with reference to Fig. 1, Fig. 2.
Embodiment 1
The technical solution adopted by the present invention is as follows：A kind of horizontal reacting kettle of temperature-controllable, including with pooling feature
Support 1, the kettle 2 being arranged on support 1, the control system 3 for being arranged on the side of kettle 2, it is arranged on the roof center of kettle 2
Charging aperture 4 and the discharging opening 5 for being arranged on the bottom of kettle 2, in addition to the first agitating device 6, the second agitating device 7 and along
The cooling water clip slot 8 that the outer rim of the outer wall of kettle 2 is set, one end of the cooling water clip slot 8 is provided with cooling water inlet 9, described
The other end of cooling water clip slot 8 is provided with coolant outlet 10, and helical pipe 11, institute are provided with described cooling water clip slot 8
The one end for stating helical pipe 11 connects with cooling water inlet 9, and the other end of the helical pipe 11 connects with coolant outlet 10,
First agitating device 6 is located at the side of charging aperture 4, and the first agitating device 6 includes agitating shaft 12 and motor 13, the stirring
One end of axle 12 extends to the outside of kettle 2 and is connected with motor 13, and the other end of the agitating shaft 12 is provided with agitator frame
14, the inner side of agitator frame 14 is provided with electric boiling plate 15, and the opposite side of the charging aperture 4 and the first agitating device 6 are symmetrical
Be provided with the second agitating device 7, be provided with temperature inductor 16 in the kettle 2.
Reactant enters the inside of kettle 2 by material inlet, using the electric boiling plate for being arranged on the inner side of agitator frame 14
15 be that reactant heats, and with the progress of polymerisation, substantial amounts of heat is released in reaction, when temperature inductor 16 detects mixture
Temperature when being higher than a certain value, signal is passed to control system 3, control system 3 makes what cooling water continued to enter from cooling water
Mouthfuls 9 are entered in the helical pipe 11 in cooling water clip slot 8, and the mixture in kettle 2 is cooled, then make cooling water from cold
But water out 10 flows out, cooling water constant flow in helical pipe 11, the state of cooling can be made to keep optimal, so as to realize
Quickly cooling, makes the mixture inside kettle 2 be in temperature constant state, after the completion of reaction, product flows out from discharging opening 5；
By using the helical pipe 11 for being connected with cooling water and the inner side electric boiling plate 15 of agitator frame 14 is arranged on, both can be reactant
Heating, it can be the mixture cooling in course of reaction again, realize the accurate temperature control to the inside and outside dual of polymerisation；It is logical
The amount of cooling water in cooling water clip slot 8 can both have been increased using helical pipe 11 by crossing, and so as to accelerate to cool, can improve cooling again
Water residence time, makes full use of cooling water；By using the first agitating device 6 and the second agitating device 7, material can be filled
The mixing divided, on the one hand can make the temperature of mixture in kettle 2 uniform, the heat of electric boiling plate 15 on the other hand can be made fast
Speed is dispersed into mixture；By using agitator frame 14, electric boiling plate 15 is set to be in the inner side of agitator frame 14, there is provided Gao Liao
The compactedness of whole device；By using the support 1 with pooling feature, the vibrations of horizontal kettle 2 can be reduced, avoided horizontal
Kettle 2 damages.
Embodiment 2
On the basis of embodiment 1, paddle 17 is symmetrically arranged with the agitating shaft 12 above agitator frame 14.It is logical
Cross on agitating shaft 12 and be symmetrical arranged paddle 17, can further improve the effect of stirring.
Embodiment 3
On the basis of embodiment 1, decelerator 18 is provided with described motor 13.Pass through the regulation motor 13 of decelerator 18
Rotating speed.
Embodiment 4
On the basis of embodiment 1, support 1 includes bottom plate 19 and 3~4 legs 20 being arranged on bottom plate 19, described
2~3 elastomer blocks 21 are evenly arranged with bottom plate 19., can be compared with by setting 3~4 elastomer blocks 21 in the inside of bottom plate 19
The vibrations of small horizontal reacting kettle.
Claims (4)
1. a kind of horizontal reacting kettle of temperature-controllable, including the support with pooling feature, the kettle being arranged on support, setting
Control system in kettle side, it is arranged on the charging aperture of kettle roof center and is arranged on the discharging opening of autoclave body bottom,
Characterized in that, also include the first agitating device, the second agitating device and the cooling water set along the outer rim of kettle outer wall
Clip slot, one end of the cooling water clip slot are provided with cooling water inlet, and the other end of the cooling water clip slot is provided with cooling water
Export, be provided with helical pipe in described cooling water clip slot, one end of the helical pipe connects with cooling water inlet, described
The other end of helical pipe connects with coolant outlet, and first agitating device is located at the side of charging aperture, the first stirring dress
Put including agitating shaft and motor, one end of the agitating shaft extends to the outside of kettle and is connected with motor, the agitating shaft
The other end is provided with agitator frame, and electric boiling plate, the opposite side of the charging aperture and first are provided with the inside of the agitator frame
Agitating device is symmetrically arranged with the second agitating device, and temperature inductor is provided with the kettle.
2. the horizontal reacting kettle of a kind of temperature-controllable according to claim 1, it is characterised in that above agitator frame
Agitating shaft on be symmetrically arranged with paddle.
3. the horizontal reacting kettle of a kind of temperature-controllable according to claim 1, it is characterised in that set on described motor
There is decelerator.
4. the horizontal reacting kettle of a kind of temperature-controllable according to claims 1 to 4, it is characterised in that support includes bottom plate
With 3~4 legs being arranged on bottom plate, 2~3 elastomer blocks are evenly arranged with the bottom plate.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711045269.1A CN107626273A (en) | 2017-10-31 | 2017-10-31 | A kind of horizontal reacting kettle of temperature-controllable |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711045269.1A CN107626273A (en) | 2017-10-31 | 2017-10-31 | A kind of horizontal reacting kettle of temperature-controllable |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107626273A true CN107626273A (en) | 2018-01-26 |
Family
ID=61106511
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711045269.1A Withdrawn CN107626273A (en) | 2017-10-31 | 2017-10-31 | A kind of horizontal reacting kettle of temperature-controllable |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107626273A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108786658A (en) * | 2018-06-27 | 2018-11-13 | 安徽科幂机械科技有限公司 | A kind of high-temperature vacuum tubular type stove carrying out light-catalyzed reaction |
-
2017
- 2017-10-31 CN CN201711045269.1A patent/CN107626273A/en not_active Withdrawn
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108786658A (en) * | 2018-06-27 | 2018-11-13 | 安徽科幂机械科技有限公司 | A kind of high-temperature vacuum tubular type stove carrying out light-catalyzed reaction |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US8066954B2 (en) | Plug flow reactor and polymers prepared therewith | |
| CN107837772A (en) | A kind of reactor of temperature-controllable | |
| CN208218740U (en) | Propylene polymerization combination evaluation device | |
| JP2009057564A (en) | Olefin polymerization method | |
| TW201244815A (en) | Continuous polymerization apparatus and process for producing polymer composition | |
| CN107626273A (en) | A kind of horizontal reacting kettle of temperature-controllable | |
| CN107670620A (en) | A kind of horizontal reacting kettle of temperature-controllable | |
| US9901894B2 (en) | Energy recovery system and method and polymerization plant with such a recovery system | |
| CN106669574A (en) | Chemical reaction kettle | |
| CN110624487A (en) | Poly alpha-olefin reaction equipment and method | |
| CN202322675U (en) | 2-acrylamide-2-methylacrylsulfonate continuous synthesis reaction device | |
| CN206731104U (en) | Leather with temperature control equipment polyurethane resin agitator tank | |
| CN104650265B (en) | A kind of solution polymerization process synthetic rubber polyreaction removes by the use of thermal means | |
| CN204865829U (en) | Cinnamic acid accuse temperature condensation reaction cauldron | |
| CN105771858A (en) | Reactor with adjustable interior and exterior temperatures | |
| CN105771867A (en) | Efficient polymeric reactor | |
| CN204768728U (en) | Agitated reactor | |
| CN205700539U (en) | A kind of built-in heat exchange reactor | |
| CN207786572U (en) | A kind of reaction kettle with inside and outside temperature controlling function | |
| CN105008405B (en) | The manufacture method of continuous polymerization unit and polymer composition | |
| CN208097941U (en) | A kind of New agitator | |
| CN205700538U (en) | A kind of inside and outside regulation thermotonus still | |
| CN205055994U (en) | Multiple organic monomer ultrasonic dispersion polymeric reation kettle | |
| CN206613483U (en) | A kind of highly effective reaction device | |
| CN109894070A (en) | A kind of dynamic respons kettle |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WW01 | Invention patent application withdrawn after publication | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20180126 |