CN205055994U - Multiple organic monomer ultrasonic dispersion polymeric reation kettle - Google Patents
Multiple organic monomer ultrasonic dispersion polymeric reation kettle Download PDFInfo
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- CN205055994U CN205055994U CN201520729307.5U CN201520729307U CN205055994U CN 205055994 U CN205055994 U CN 205055994U CN 201520729307 U CN201520729307 U CN 201520729307U CN 205055994 U CN205055994 U CN 205055994U
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- kettle body
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- reaction kettle
- reation kettle
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Abstract
The utility model relates to a control the reation kettle of multiple organic monomer polymerization temperature, reation kettle is external to be provided with the reation kettle body and to press from both sides the cover, and the reation kettle body presss from both sides the cover bottom and is provided with the reation kettle body and presss from both sides the cover water inlet, and the reation kettle body presss from both sides the cover top and is provided with the reation kettle body and presss from both sides the cover delivery port, have a reation kettle spirally twisted pipe in that reation kettle is internal, reation kettle spirally twisted socle portion is provided with reation kettle spirally twisted pipe water inlet, and reation kettle spirally twisted nose portion is provided with reation kettle spirally twisted pipe delivery port, be provided with the reation kettle sleeve between reation kettle spirally twisted pipe and the reation kettle body, be provided with reation kettle sleeve water inlet in reation kettle body bottom, personally experience sth. Part of the body the top at reation kettle and be provided with reation kettle sleeve delivery port, physically install ultrasonator in the top in reation kettle through reation kettle. The beneficial effects of the utility model are that: temperature in the controlled reaction cauldron effectively, the segregation of partial polymer reaction monomer has been avoided to homodisperse polymer monomer fully.
Description
Technical field
The utility model relates to a kind of reactor, is specifically related to the reactor of one kind of multiple organic monomer ultrasonic disperse polymerization.
Background technology
At present, the synthetic method of polymer generally adopts and several polymer reaction monomers used are put into reactor simultaneously carries out polymerisation.Polymer reaction monomer is meeting neither endothermic nor exothermic in polymerization process, and the control of temperature has great role to the selective of reactive material and yield.Polymer reaction monomer, in course of reaction, needs intensification induced reaction during beginning, enter a large amount of heat release again after course of reaction, need to remove heat fast.To control reaction temperature well, ensure reaction speed, stabilized product quality.Because general polymerization thing reaction monomers polymerization process is all continuous feed, and the course of reaction of adjoint very exothermic, conventional temperature control method generally adopts the method passing into steam or refrigerant in reacting kettle jacketing to carry out heating, cooling control, this method temperature control precision is poor, energy consumption is high, the cold and hot exchange of reacting kettle jacketing is too fast in addition, and variations in temperature is too large, has impact to the life-span of reactor.
Polymer reaction monomer polymerization reactions adds monomer continuously, and related auxiliaries is added in course of reaction, its reaction speed is very responsive to reaction temperature, and temperature is higher, react faster, heat release Shaoxing opera is strong, and more just, reaction is speed more for temperature, heat release is fewer, therefore control reaction temperature well, be control reaction speed, improve a key of the selective and yield of reactive material; Meanwhile, the Homogeneous phase mixing fully between several polymer monomer is also the key technical problem improving reaction efficiency.
For this reason, designer of the present utility model, because above-mentioned technological deficiency, by concentrating on studies and designing, is comprehensively engaged in experience and the achievement of related industry for a long time for many years, research and design goes out a kind of reactor controlling multiple organic monomer polymeric reaction temperature, to overcome above-mentioned technological deficiency.
Utility model content
The technical problems to be solved in the utility model is: the reactor designing the polymerization of one kind of multiple organic monomer ultrasonic disperse, can not control the technical problem of reaction temperature and reaction efficiency effectively to solve reactor in prior art.
In order to solve the problems of the technologies described above, the utility model have employed following technical scheme:
The reactor of one kind of multiple organic monomer ultrasonic disperse polymerization, is characterized in that: this reactor comprises reaction kettle body, charging aperture, discharging opening, ultrasonic generator, reaction kettle body chuck, reaction kettle body chuck water inlet, reaction kettle body chuck delivery port, temperature-measuring port, reactor coiled coil pipe, reactor coiled coil water inlet tube mouth, reactor coiled coil pipe delivery port, reactor sleeve, reactor sleeve water inlet and reactor sleeve delivery port; Described reaction kettle body top is provided with several charging apertures, bottom reaction kettle body, is provided with a discharging opening; Be outside equipped with reaction kettle body chuck at reaction kettle body, be provided with reaction kettle body chuck water inlet bottom reaction kettle body chuck, reaction kettle body chuck top is provided with reaction kettle body chuck delivery port, and temperature-measuring port is positioned at bottom reaction kettle body; In reaction kettle body with reaction kettle body center for axle is provided with reactor coiled coil pipe, be provided with reactor coiled coil water inlet tube mouth bottom reactor coiled coil pipe, reactor coiled coil pipe top is provided with reactor coiled coil pipe delivery port; Between described reactor coiled coil pipe and reaction kettle body, be provided with reactor sleeve, bottom reaction kettle body, be provided with reactor sleeve water inlet, be provided with reactor sleeve delivery port at reaction kettle body top; In reactor, be provided with ultrasonic generator by reaction kettle body top, described ultrasonic generator comprises supersonic generator and high-energy ultrasonic ultrasonic transformer, the high-energy ultrasonic ultrasonic transformer described in supersonic generator connects.
Above-mentioned high-energy ultrasonic ultrasonic transformer comprises the vertical high-energy ultrasonic ultrasonic transformer that is parallel to reactor central shaft and the horizontal high-energy ultrasonic ultrasonic transformer perpendicular to described vertical high-energy ultrasonic ultrasonic transformer, vertical high-energy ultrasonic ultrasonic transformer described in supersonic generator connects, described horizontal high-energy ultrasonic ultrasonic transformer and vertical high-energy ultrasonic ultrasonic transformer weld together.
Known by technique scheme, the reactor of one kind of multiple organic monomer ultrasonic disperse polymerization of the present utility model has following technique effect:
1, the reacting kettle jacketing arranged inside and outside reactor, reactor coiled coil pipe and reactor sleeve can control reaction temperature effectively, first effectively heat is passed to reactant to occur to impel reaction, once react certain one-phase after terminating to concentrate solar heat protection, heat can be taken away rapidly from reactor again, effectively control reaction temperature, drastically increase reaction efficiency.
2, the ultrasonic generator arranged can promote the Homogeneous phase mixing fully between multiple polymers monomer effectively, avoids a certain monomer component segregation, drastically increases reaction efficiency.
Detailed content of the present utility model obtains by following detailed description and Figure of description.
Accompanying drawing explanation
Fig. 1 is the structural representation of the reactor of one kind of multiple organic monomer ultrasonic disperse of the present utility model polymerization.
In figure: 1 is reaction kettle body, 2a, 2b and 2c is charging aperture, 3 is discharging opening, 4 is ultrasonic generator, 5 is reaction kettle body chuck, 6 is reaction kettle body chuck water inlet, 7 is reaction kettle body chuck delivery port, 8 is temperature-measuring port, 9 is reactor coiled coil pipe, 10 is reactor coiled coil water inlet tube mouth, 11 is reactor coiled coil pipe delivery port, 12 is horizontal high-energy ultrasonic ultrasonic transformer, 13 is vertical high-energy ultrasonic ultrasonic transformer, 15 is reactor sleeve, 16 is reactor sleeve water inlet, 17 is reactor sleeve delivery port.
Detailed description of the invention
The structural representation of the reactor of one kind of multiple organic monomer ultrasonic disperse of the present utility model polymerization is described in detail below in conjunction with Figure of description.
See Fig. 1, show the structural representation of the reactor of one kind of multiple organic monomer ultrasonic disperse of the present utility model polymerization.
Control a reactor for multiple organic monomer polymeric reaction temperature, this reactor comprises reaction kettle body 1, charging aperture 2, discharging opening 3, ultrasonic generator 4, reaction kettle body chuck 5, reaction kettle body chuck water inlet 6, reaction kettle body chuck delivery port 7, temperature-measuring port 8, reactor coiled coil pipe 9, reactor coiled coil water inlet tube mouth 10, reactor coiled coil pipe delivery port 11, reactor sleeve 15, reactor sleeve water inlet 16 and reactor sleeve delivery port 17; There are three charging apertures 2a, 2b and 2c at described reaction kettle body top, bottom reaction kettle body, have a discharging opening 3; Be outside equipped with reaction kettle body chuck 5 at reaction kettle body 1, respond bottom reaction kettle body chuck 5 kettle chuck water inlet 6, and reaction kettle body chuck 5 top responds kettle chuck delivery port 7; Temperature-measuring port 8 is positioned at bottom reaction kettle body 1; In reaction kettle body 1 with reaction kettle body center for axle is provided with reactor coiled coil pipe 9, respond bottom reactor coiled coil pipe 9 still coiled coil water inlet tube mouth 10, and reactor coiled coil pipe 9 top responds still coiled coil pipe delivery port 11; Between described reactor coiled coil pipe 9 and reaction kettle body 1, be provided with reactor sleeve 15, bottom reaction kettle body 1, be provided with reactor sleeve water inlet 16, reaction kettle body 1 top is provided with reactor sleeve delivery port 17; By reaction kettle body 1 top, ultrasonic generator 4 is installed in reactor, described ultrasonic generator 4 comprises supersonic generator, is parallel to the vertical high-energy ultrasonic ultrasonic transformer 12 of reactor central shaft and the horizontal high-energy ultrasonic ultrasonic transformer 13 perpendicular to described vertical high-energy ultrasonic ultrasonic transformer 12, vertical high-energy ultrasonic ultrasonic transformer 12 described in supersonic generator connects, described horizontal high-energy ultrasonic ultrasonic transformer 13 welds together with vertical high-energy ultrasonic ultrasonic transformer 12.
Known by said structure, a kind of reactor tool controlling multiple organic monomer polymeric reaction temperature of the present utility model has the following advantages:
1, the reacting kettle jacketing arranged inside and outside reactor, reactor coiled coil pipe and reactor sleeve can control reaction problem effectively, first effectively heat is passed to reactant to occur to impel reaction, once react certain one-phase after terminating to concentrate solar heat protection, heat can be taken away rapidly from reactor again, effectively control reaction temperature, drastically increase reaction efficiency.
2, the ultrasonic generator arranged can promote the Homogeneous phase mixing fully between multiple polymers monomer effectively, avoids a certain monomer component segregation, drastically increases reaction efficiency.
It is evident that, above description and record be only citing instead of in order to limit content disclosed in the utility model, application or use.Although described in an embodiment and described embodiment with reference to the accompanying drawings, but the utility model do not limit by accompanying drawing example and describe in an embodiment as the optimal mode thought at present to implement the specific examples of instruction of the present utility model, scope of the present utility model will comprise any embodiment of description and the appended claim fallen into above.
Claims (2)
1. the reactor of one kind of multiple organic monomer ultrasonic disperse polymerization, is characterized in that: this reactor comprises reaction kettle body, charging aperture, discharging opening, ultrasonic generator, reaction kettle body chuck, reaction kettle body chuck water inlet, reaction kettle body chuck delivery port, temperature-measuring port, reactor coiled coil pipe, reactor coiled coil water inlet tube mouth, reactor coiled coil pipe delivery port, reactor sleeve, reactor sleeve water inlet and reactor sleeve delivery port; Described reaction kettle body top is provided with several charging apertures, bottom reaction kettle body, is provided with a discharging opening; Be outside equipped with reaction kettle body chuck at reaction kettle body, be provided with reaction kettle body chuck water inlet bottom reaction kettle body chuck, reaction kettle body chuck top is provided with reaction kettle body chuck delivery port, and temperature-measuring port is positioned at bottom reaction kettle body; In reaction kettle body with reaction kettle body center for axle is provided with reactor coiled coil pipe, be provided with reactor coiled coil water inlet tube mouth bottom reactor coiled coil pipe, reactor coiled coil pipe top is provided with reactor coiled coil pipe delivery port; Between described reactor coiled coil pipe and reaction kettle body, be provided with reactor sleeve, bottom reaction kettle body, be provided with reactor sleeve water inlet, be provided with reactor sleeve delivery port at reaction kettle body top; In reactor, be provided with ultrasonic generator by reaction kettle body top, described ultrasonic generator comprises supersonic generator and high-energy ultrasonic ultrasonic transformer, the high-energy ultrasonic ultrasonic transformer described in supersonic generator connects.
2. the reactor of multiple organic monomer ultrasonic disperse polymerization as claimed in claim 1, it is characterized in that: described high-energy ultrasonic ultrasonic transformer comprises the vertical high-energy ultrasonic ultrasonic transformer that is parallel to reactor central shaft and the horizontal high-energy ultrasonic ultrasonic transformer perpendicular to described vertical high-energy ultrasonic ultrasonic transformer, vertical high-energy ultrasonic ultrasonic transformer described in supersonic generator connects, described horizontal high-energy ultrasonic ultrasonic transformer and vertical high-energy ultrasonic ultrasonic transformer weld together.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520729307.5U CN205055994U (en) | 2015-09-18 | 2015-09-18 | Multiple organic monomer ultrasonic dispersion polymeric reation kettle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520729307.5U CN205055994U (en) | 2015-09-18 | 2015-09-18 | Multiple organic monomer ultrasonic dispersion polymeric reation kettle |
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| Publication Number | Publication Date |
|---|---|
| CN205055994U true CN205055994U (en) | 2016-03-02 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201520729307.5U Expired - Fee Related CN205055994U (en) | 2015-09-18 | 2015-09-18 | Multiple organic monomer ultrasonic dispersion polymeric reation kettle |
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| CN (1) | CN205055994U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105126725A (en) * | 2015-09-18 | 2015-12-09 | 成都乐也科技有限公司 | Reaction kettle for ultrasonic dispersion polymerization of various organic monomers |
-
2015
- 2015-09-18 CN CN201520729307.5U patent/CN205055994U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105126725A (en) * | 2015-09-18 | 2015-12-09 | 成都乐也科技有限公司 | Reaction kettle for ultrasonic dispersion polymerization of various organic monomers |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160302 Termination date: 20160918 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |