CN107586189A - A kind of preparation method of the special damp-proof urea of Blending Fertilizer - Google Patents

A kind of preparation method of the special damp-proof urea of Blending Fertilizer Download PDF

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Publication number
CN107586189A
CN107586189A CN201710587757.9A CN201710587757A CN107586189A CN 107586189 A CN107586189 A CN 107586189A CN 201710587757 A CN201710587757 A CN 201710587757A CN 107586189 A CN107586189 A CN 107586189A
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CN
China
Prior art keywords
urea
fertilizer
special
preparation
proof
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710587757.9A
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Chinese (zh)
Inventor
王仁宗
操素芬
刘裕
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Hubei Forbon Technology Co Ltd
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Hubei Forbon Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
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Application filed by Hubei Forbon Technology Co Ltd filed Critical Hubei Forbon Technology Co Ltd
Priority to CN201710587757.9A priority Critical patent/CN107586189A/en
Priority to PCT/CN2017/102066 priority patent/WO2019015067A1/en
Priority to MA47625A priority patent/MA47625B1/en
Publication of CN107586189A publication Critical patent/CN107586189A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05DINORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
    • C05D9/00Other inorganic fertilisers
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/90Mixtures of one or more fertilisers with additives not having a specially fertilising activity for affecting the nitrification of ammonium compounds or urea in the soil

Abstract

The present invention relates to a kind of preparation method of the special damp-proof urea of Blending Fertilizer, it is characterised in that:Granular urea is put into coating drum front end, disk or in the blender with mixed function, in one layer of special anti-blushing agent of granular urea surface spraying;Then in coating roller rear end, disk or in the blender with mixed function, then one layer of modified magnesium powder end is sprayed, that is, the special damp-proof urea of Blending Fertilizer is made.The advantage of the invention is that:Urea made from this method can stablize mix with acidic fertiliziers such as general calciums, nonhygroscopic, constant tide, not lump.

Description

A kind of preparation method of the special damp-proof urea of Blending Fertilizer
Technical field
The present invention relates to Blending Fertilizer manufacturing field.The preparation method of mainly a kind of special damp-proof urea of Blending Fertilizer.
Background technology
China is a large agricultural country, and various fertilizer, especially chemical fertilizer play indelible tribute to China's grain security Offer.
The demand of grain drives the explosive growth of Chinese chemical fertilizer, past 10 years, all kinds of fertilizer enterprises up to 6000 of China More families, mostly compound fertilizer enterprise, they use granular urea, phosphorus ammonium, potassium chloride or potassium sulfate again after carrying out break process Steam dram is granulated, or high-tower granulation after melting, is zero for fertilizer nutrient contribution.With our Chinese fertilizer patterns completely The different U.S., then be based on Blending Fertilizer, Blending Fertilizer be exactly by granular urea, particle phosphorus ammonium and granular potash fertilizer physical mixed and Into eliminating the secondary operation of composite fertilizer, therefore Blending Fertilizer (also referred to as BB fertilizer) more low-carbon and economy.
In recent years, the Northeast of China also slowly started to apply Blending Fertilizer, and peasant household buys various straight fertilizers, common nitrogen Fertilizer is such as:Granular urea, conventional phosphate fertilizer is such as:The particle Diammonium phosphate (DAP) of high concentration, particle MAP and rich in phosphorus and calcium, Micro- general calcium and coarse whiting in magnesium, sulphur etc., conventional potash fertilizer are exactly granule potassium chloride, potassium sulfate.In these fertilizer, general calcium A kind of cost-effective phosphate fertilizer, its price is much lower compared with MAP and Diammonium phosphate (DAP) and middle micro-element nutrition more comprehensively, Because the production of general calcium is made with sulfuric acid and ground phosphate rock directly reaction, it is a kind of fertilizer of slant acidity, is providing phosphorus nutrient Meanwhile all keep down various metal trace elements in ground phosphate rock and moderate-element, plus the slant acidity of general calcium, also may be used To promote in soil by fixed nutrient again by crop utilization, thus it is better using the crop growing state of general calcium, it is also deep Approved by peasant.
But the acidic character of general calcium, cause it to be contacted with urea, because the sulfuric acid meeting remained in general calcium and urea Reaction forms ureasulfuric acid, in liquid, also result in peasant and is being mixed with Blending Fertilizer by the use of general calcium as phosphorus source and urea, potash fertilizer When, there is fertilizer and get wet, it is agglomerating, the problem of can not applying fertilizer.
Because this problem, the development of Blending Fertilizer is also constrained to a certain extent.
Therefore, in this context, prepare a kind of using general calcium and urea as the Blending Fertilizer tailored version urea of raw material, turn into The task of top priority.
The content of the invention
The invention reside in providing a kind of preparation method of the special damp-proof urea of Blending Fertilizer, urea made from this method can be with Stablize mixing with acidic fertiliziers such as general calciums, nonhygroscopic, constant tide, greatly widened the material fertilizer species of Blending Fertilizer.
A kind of preparation method of the special damp-proof urea of Blending Fertilizer, it is characterised in that:In coating drum front end, disk or Granular urea is put into blender with mixed function, in one layer of special anti-blushing agent of granular urea surface spraying;Then wrapping In membrane cylinder rear end, disk or in the blender with mixed function, then one layer of modified magnesium powder end is sprayed, that is, be made and mix The special damp-proof urea of complex fertilizer.
Described granular urea is granular urea, fluidized bed prilling prepared by granular urea, drum equipment prepared by high tower One or two or more kinds of mixtures in granular urea prepared by the granular urea of preparation, extrusion technique.
Described special anti-blushing agent for Hubei Forbon Technology Co., Ltd. product HISOFT FA130, by weight hundred Divide than meter, composition is the mixture of 10-30% dextrin, 5-50% Macrogol 4000 and 30-80% water.
The preparation method at described modified magnesium powder end is:By magnesia original powder and quality be magnesia quality 0.5- One or two or more kinds of mixtures in 10% paraffin, vegetable oil or mineral oil are well mixed, and are ground to 200-2000 Mesh, that is, modified magnesium powder body is made.
Described melting point of paraffin wax is 20 DEG C -120 DEG C.
The advantage of the invention is that:
1st, it is simple and quick.The system of the special damp-proof urea of Blending Fertilizer can be achieved in spraying in existing fertilizer pack roller It is standby;
2nd, without returning charge.Packing and storing system is directly entered after parcel;
3rd, with anti-caking function.Urea granules are loose made from this method, it is no longer necessary to extra addition fertilizer anti-caking Agent;
4th, efficiently moistureproof isolation.Two layers of efficient moistureproof isolation processing, urea and general calcium can be avoided completely or other are aqueous High fertilizer medium contact is measured, realizes preferable isolation effect.
Embodiment
With reference to embodiment, the invention will be further described.Embodiment is as follows.
Case study on implementation 1
On urea pack roller front end, 1 ton of urea granules, the limited public affairs of Hubei richness nation science and technology share of 0.5 kilogram of spraying Take charge of production HISOFT FA 130 (by weight percentage, composition be 20% dextrin, 20% Macrogol 4000 and The mixture of 60% water).In coating roller rear end, the modified magnesium powder prepared of 10 kilograms of spraying, that is, Blending Fertilizer is obtained Special damp-proof urea.Described modified magnesium powder body formula:Magnesia original powder, add and account for the 60 of magnesia original powder total amount 5% The paraffin grinding of DEG C fusing point, is 600 mesh to powder mesh number.
Urea through above-mentioned processing, general calcium superphosphate mass ratio 1:1, place 3 months completely loosely;
The not urea Jing Guo above-mentioned processing, general calcium superphosphate mass ratio 1:1, place 5 minutes, fertiliser mixtures separate out big Moisture is measured, material moisturizes, sticky, and fertilizer finally lumps, and presentation becomes a monoblock.
Case study on implementation 2
In disk, on 1 ton of urea granules, Hubei Forbon Technology Co., Ltd.'s production of 1 kilogram of spraying (by weight percentage, composition is 10% dextrin to HISOFT FA 130,30% Macrogol 4000 and 60% water Mixture), in disk, then 30 kilograms of the modified magnesium powder prepared is sprayed, that is, obtain the special damp-proof urine of Blending Fertilizer Element.Described modified magnesium powder body formula:Magnesia original powder, add the bean plant oil grinding for accounting for magnesia original powder total amount 3%, It is 500 mesh to powder mesh number.
Urea through above-mentioned processing, general calcium superphosphate mass ratio 1:1, place 4 months completely loosely;
The not urea Jing Guo above-mentioned processing, general calcium superphosphate mass ratio 1:1, place 5 minutes, fertiliser mixtures separate out big Moisture is measured, material moisturizes, sticky, and fertilizer finally lumps, and presentation becomes a monoblock.
Case study on implementation 3
In disk, on 1 ton of urea granules, Hubei Forbon Technology Co., Ltd.'s production of 1 kilogram of spraying HISOFT FA 130 (by weight percentage, composition be 30% dextrin, the mixing of 5% Macrogol 4000 and 65% water Thing), in disk, then 30 kilograms of the modified magnesium powder prepared is sprayed, that is, obtain the special damp-proof urea of Blending Fertilizer.Institute The modified magnesium powder body formula stated:Magnesia original powder, adds the intermixture for accounting for magnesia original powder total amount 3%, and fusing point is 70 DEG C Paraffin:Bean plant oil:Mineral oil (mineral oil of the carbochain in C16-C35) presses 1:1:1 ratio modulation and when into grinding changes Property, it is 200 mesh to powder mesh number.
Urea through above-mentioned processing, general calcium superphosphate mass ratio 1:1, place 3 months completely loosely;
The not urea Jing Guo above-mentioned processing, general calcium superphosphate mass ratio 1:1, place 5 minutes, fertiliser mixtures separate out big Moisture is measured, material moisturizes, sticky, and fertilizer finally lumps, and presentation becomes a monoblock.
Case study on implementation 4
In blender, on 1 ton of urea granules, Hubei Forbon Technology Co., Ltd.'s production of 1 kilogram of spraying (by weight percentage, composition is 10% dextrin to HISOFT FA 130,50% Macrogol 4000 and 40% water Mixture), in blender, then 30 kilograms of the modified magnesium powder prepared is sprayed, that is, obtain the special damp-proof of Blending Fertilizer Urea.Described modified magnesium powder body formula:Magnesia original powder, add the intermixture for accounting for magnesia original powder total amount 10%, soybean Vegetable oil:Mineral oil (mineral oil of the carbochain in C16-C35) presses 1:1 ratio modulation and when into, grinding be modified, to powder mesh number For 1000 mesh.
Urea through above-mentioned processing, general calcium superphosphate mass ratio 1:1, place 5 months completely loosely;
The not urea Jing Guo above-mentioned processing, general calcium superphosphate mass ratio 1:1, place 5 minutes, fertiliser mixtures separate out big Moisture is measured, material moisturizes, sticky, and fertilizer finally lumps, and presentation becomes a monoblock.

Claims (5)

  1. A kind of 1. preparation method of the special damp-proof urea of Blending Fertilizer, it is characterised in that:In coating drum front end, disk or have Have and put into granular urea in the blender of mixed function, in one layer of special anti-blushing agent of granular urea surface spraying;Then in coating In roller rear end, disk or in the blender with mixed function, then one layer of modified magnesium powder end is sprayed, that is, blending is made The special damp-proof urea of fertilizer.
  2. A kind of 2. preparation method of the special damp-proof urea of Blending Fertilizer as claimed in claim 1, it is characterised in that:Described Grain urea be high tower prepare granular urea, drum equipment prepare granular urea, fluidized bed prilling prepare granular urea, squeeze One or two or more kinds of mixtures in granular urea prepared by platen press technique.
  3. A kind of 3. preparation method of the special damp-proof urea of Blending Fertilizer as claimed in claim 1, it is characterised in that:Described is special With the product HISOFT FA 130 that anti-blushing agent is Hubei Forbon Technology Co., Ltd., by weight percentage, composition is The mixture of 10-30% dextrin, 5-50% Macrogol 4000 and 30-80% water.
  4. A kind of 4. preparation method of the special damp-proof urea of Blending Fertilizer as claimed in claim 1, it is characterised in that:Described changes The preparation method of property magnesium oxide powder is:Paraffin, vegetable oil by magnesia original powder with quality for magnesia quality 0.5-10% Or one or two or more kinds of mixtures in mineral oil are well mixed, and are ground to 200-2000 mesh, that is, modified oxidized magnesium is made Powder.
  5. A kind of 5. preparation method of the special damp-proof urea of Blending Fertilizer as claimed in claim 4, it is characterised in that:Described stone The fusing point of wax is 20 DEG C -120 DEG C.
CN201710587757.9A 2017-07-18 2017-07-18 A kind of preparation method of the special damp-proof urea of Blending Fertilizer Pending CN107586189A (en)

Priority Applications (3)

Application Number Priority Date Filing Date Title
CN201710587757.9A CN107586189A (en) 2017-07-18 2017-07-18 A kind of preparation method of the special damp-proof urea of Blending Fertilizer
PCT/CN2017/102066 WO2019015067A1 (en) 2017-07-18 2017-09-18 Method of preparing moisture-proof urea specifically for blended fertilizer
MA47625A MA47625B1 (en) 2017-07-18 2017-09-18 Method for preparing moisture resistant urea specifically for mixed fertilizer

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710587757.9A CN107586189A (en) 2017-07-18 2017-07-18 A kind of preparation method of the special damp-proof urea of Blending Fertilizer

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WO2019140724A1 (en) * 2018-01-19 2019-07-25 湖北富邦科技股份有限公司 Coating method for moisture-proof, anticaking, and anti-chalking granular fertilizer added with micronutrients
CN111825421A (en) * 2020-07-29 2020-10-27 襄阳市政建设集团有限公司 Preparation method of active phosphogypsum micro powder based on heat insulation material

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CN111825421A (en) * 2020-07-29 2020-10-27 襄阳市政建设集团有限公司 Preparation method of active phosphogypsum micro powder based on heat insulation material

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MA47625B1 (en) 2020-11-30
MA47625A1 (en) 2020-02-28

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