CN107574292A - A kind of surface treatment method of cast iron seal - Google Patents

A kind of surface treatment method of cast iron seal Download PDF

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Publication number
CN107574292A
CN107574292A CN201710773436.8A CN201710773436A CN107574292A CN 107574292 A CN107574292 A CN 107574292A CN 201710773436 A CN201710773436 A CN 201710773436A CN 107574292 A CN107574292 A CN 107574292A
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China
Prior art keywords
seal
cast iron
iron seal
surface treatment
treatment method
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Pending
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CN201710773436.8A
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Chinese (zh)
Inventor
张文尧
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Ningguo Ning Sealing Parts Factory
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Ningguo Ning Sealing Parts Factory
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Priority to CN201710773436.8A priority Critical patent/CN107574292A/en
Publication of CN107574292A publication Critical patent/CN107574292A/en
Pending legal-status Critical Current

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Abstract

The invention mainly relates to sealing material field, discloses a kind of surface treatment method of cast iron seal, including:Clean, polish, rise again, quench, pack;Method is simple, and ultrasonic polishing is carried out to cleaning part, allantoin is added in carborundum suspension, quickly seal is polished comprehensively, roughness is down to 0.07 μm, avoids producing machinery the service life of abrasion, prolonged mechanical and seal;It is incubated after being slowly heated after polishing to seal; the nitrogen dioxide gas in heating furnace is promoted to penetrate into seal; protective layer is formed to seal; strengthen the corrosion resistance of seal; the grain size number of cast iron seal can be reduced; intensity, hardness and the toughness of seal are improved, avoids seal leakage;Seal is placed in ammonium nitrate solution after heating and quenched, diaphragm is formed in seal surface, improves the wearability and corrosion resistance of seal.

Description

A kind of surface treatment method of cast iron seal
Technical field
The invention mainly relates to sealing material field, more particularly to a kind of surface treatment method of cast iron seal.
Background technology
The seal used at present is mostly non-metallic seal, and wear resistance is poor, does not focus on maintenance somewhat and is easy for out Existing leakage phenomenon, it can be used for the mechanical system stood, run at high speed, the mechanical system that seal is often worn out just needs hardness Higher mechanical sealing member, cast iron seal are a kind of conventional metal seals, but current cast iron seal surface compared with It is coarse, damage, and the easy corrosion after friction repeatedly and oil immersion of cast iron seal are easily caused to machinery, causes sealing Decline.
The content of the invention
The defects of in order to make up prior art, it is an object of the invention to provide a kind of surface treatment side of cast iron seal Method.
A kind of surface treatment method of cast iron seal, comprises the following steps:
(1)Cleaning:Cast iron seal after casting is placed in sodium carbonate liquor, 30 ~ 32kHz ultrasounds 25 ~ 30 minutes, must be cleaned Part;
(2)Polishing:Cleaning part is placed in ultrasonic polishing machine, polishing suspension is carborundum suspension, in 31 ~ 33kHz polish 30 ~ 35 minutes, clean, obtain polished part;
(3)Rise again:Polished part is placed in heating furnace, is passed through nitrogen dioxide gas, is heated to temperature as 800 ~ 900 DEG C, insulation 80 ~ 90 minutes, must rise again part;
(4)Quenching:Part of rising again is placed in the ammonium nitrate solution that mass concentration is 1.1 ~ 1.3% and quenched, 360 ~ 400 DEG C of guarantors Temperature 30 ~ 40 minutes, is naturally cooling to room temperature, cast iron seal after must handling;
(5)Packaging:Oiling, packaging, obtains cast iron seal finished product.
The step(1)Carborundum suspension, also containing mass concentration be 2.2 ~ 2.4% allantoin.
The step(3)Nitrogen dioxide gas, volume fraction in heating furnace is 1.1 ~ 1.3%.
The step(3)Heating, heated up with 1.6 ~ 1.8 DEG C/min.
Cast iron seal finished product prepared by the surface treatment method of the cast iron seal.
It is an advantage of the invention that:The surface treatment method of cast iron seal provided by the invention, method is simple, after casting Cast iron seal cleaning after remove surface impurity, be easy to later stage uniform treatment;Ultrasonic polishing, carborundum are carried out to cleaning part Allantoin is added in suspension, quickly seal can comprehensively be polished, roughness is down to 0.07 μm, avoids producing machinery The service life of raw abrasion, prolonged mechanical and seal;It is incubated after being slowly heated after polishing to seal, promotes heating furnace Interior nitrogen dioxide gas penetrates into seal, forms protective layer to seal, strengthens the corrosion resistance of seal, can reduce casting The grain size number of iron seal, the intensity, hardness and toughness of seal are improved, avoids seal leakage;By seal after heating It is placed in ammonium nitrate solution and is quenched, forms diaphragm in seal surface, improve the wearability and corrosion resistance of seal.
Embodiment
Illustrate the present invention with specific embodiment below.
Embodiment 1
A kind of surface treatment method of cast iron seal, comprises the following steps:
(1)Cleaning:Cast iron seal after casting is placed in sodium carbonate liquor, 30kHz ultrasounds 25 minutes, obtains cleaning part;
(2)Polishing:Cleaning part is placed in ultrasonic polishing machine, polishing suspension is carborundum suspension, and 30 points are polished in 31kHz Clock, clean, obtain polished part;Described carborundum suspension, also containing the allantoin that mass concentration is 2.2%;
(3)Rise again:Polished part is placed in heating furnace, is passed through nitrogen dioxide gas, the volume fraction in heating furnace is 1.1%, Temperature is heated to as 800 DEG C using 1.6 DEG C/min, is incubated 80 minutes, must rise again part;
(4)Quenching:Part of rising again is placed in the ammonium nitrate solution that mass concentration is 1.1% and quenched, 360 DEG C are incubated 30 minutes, Room temperature is naturally cooling to, cast iron seal after must handling;
(5)Packaging:Oiling, packaging, obtains cast iron seal finished product.
Cast iron seal finished product prepared by the surface treatment method of the cast iron seal.
Embodiment 2
A kind of surface treatment method of cast iron seal, comprises the following steps:
(1)Cleaning:Cast iron seal after casting is placed in sodium carbonate liquor, 31kHz ultrasounds 28 minutes, obtains cleaning part;
(2)Polishing:Cleaning part is placed in ultrasonic polishing machine, polishing suspension is carborundum suspension, and 33 points are polished in 32kHz Clock, clean, obtain polished part;Described carborundum suspension, also containing the allantoin that mass concentration is 2.3%;
(3)Rise again:Polished part is placed in heating furnace, is passed through nitrogen dioxide gas, the volume fraction in heating furnace is 1.2%, Temperature is heated to as 850 DEG C using 1.7 DEG C/min, is incubated 85 minutes, must rise again part;
(4)Quenching:Part of rising again is placed in the ammonium nitrate solution that mass concentration is 1.2% and quenched, 380 DEG C are incubated 35 minutes, Room temperature is naturally cooling to, cast iron seal after must handling;
(5)Packaging:Oiling, packaging, obtains cast iron seal finished product.
Cast iron seal finished product prepared by the surface treatment method of the cast iron seal.
Embodiment 3
A kind of surface treatment method of cast iron seal, comprises the following steps:
(1)Cleaning:Cast iron seal after casting is placed in sodium carbonate liquor, 32kHz ultrasounds 30 minutes, obtains cleaning part;
(2)Polishing:Cleaning part is placed in ultrasonic polishing machine, polishing suspension is carborundum suspension, and 35 points are polished in 33kHz Clock, clean, obtain polished part;Described carborundum suspension, also containing the allantoin that mass concentration is 2.4%;
(3)Rise again:Polished part is placed in heating furnace, is passed through nitrogen dioxide gas, the volume fraction in heating furnace is 1.3%, Temperature is heated to as 900 DEG C using 1.8 DEG C/min, is incubated 90 minutes, must rise again part;
(4)Quenching:Part of rising again is placed in the ammonium nitrate solution that mass concentration is 1.3% and quenched, 400 DEG C are incubated 40 minutes, Room temperature is naturally cooling to, cast iron seal after must handling;
(5)Packaging:Oiling, packaging, obtains cast iron seal finished product.
Cast iron seal finished product prepared by the surface treatment method of the cast iron seal.
Comparative example 1
Existing traditional cast iron seal finished product.
The performance of embodiment and comparative example cast iron seal:
Each 8 of the cast iron seal finished product of selection example and comparative example respectively, at normal temperatures and pressures, each group selects 2 respectively The 6mol/L NaCl aqueous solution is placed in, selects 2 HCl/water solution for being placed in 6mol/L, selects 2 NaOH water for being placed in 6mol/L In solution, there is the time corroded in observation each group cast iron seal finished product, and selects 2 to be used for Surface testing, results averaged, Embodiment and the performance of comparative example cast iron seal are shown in Table 1.
Table 1:The performance of embodiment and comparative example cast iron seal
Project Roughness/(μm) Acidproof/(d) Alkaline-resisting/(d) Salt tolerant/(d) Wearability/(mm3
Embodiment 1 0.08 294 318 304 23
Embodiment 2 0.08 292 315 307 22
Embodiment 3 0.07 293 317 305 20
Comparative example 1 0.26 197 206 204 43
Show from the result of table 1, the cast iron seal finished product that the surface treatment method of the cast iron seal of embodiment obtains is coarse Degree is substantially small compared with comparative example, and acidproof, alkaline-resisting and salt tolerance is substantially strong compared with comparative example, and the Volume Loss amount after friction substantially relatively contrasts Example is small, and illustrating the surface treatment method of cast iron seal provided by the invention has good treatment effect.

Claims (5)

1. a kind of surface treatment method of cast iron seal, it is characterised in that comprise the following steps:
(1)Cleaning:Cast iron seal after casting is placed in sodium carbonate liquor, 30 ~ 32kHz ultrasounds 25 ~ 30 minutes, must be cleaned Part;
(2)Polishing:Cleaning part is placed in ultrasonic polishing machine, polishing suspension is carborundum suspension, in 31 ~ 33kHz polish 30 ~ 35 minutes, clean, obtain polished part;
(3)Rise again:Polished part is placed in heating furnace, is passed through nitrogen dioxide gas, is heated to temperature as 800 ~ 900 DEG C, insulation 80 ~ 90 minutes, must rise again part;
(4)Quenching:Part of rising again is placed in the ammonium nitrate solution that mass concentration is 1.1 ~ 1.3% and quenched, 360 ~ 400 DEG C of guarantors Temperature 30 ~ 40 minutes, is naturally cooling to room temperature, cast iron seal after must handling;
(5)Packaging:Oiling, packaging, obtains cast iron seal finished product.
2. the surface treatment method of cast iron seal according to claim 1, it is characterised in that the step(1)Carbonization Silicon suspension, also containing the allantoin that mass concentration is 2.2 ~ 2.4%.
3. the surface treatment method of cast iron seal according to claim 1, it is characterised in that the step(3)Dioxy Change nitrogen, the volume fraction in heating furnace is 1.1 ~ 1.3%.
4. the surface treatment method of cast iron seal according to claim 1, it is characterised in that the step(3)Heating, Heated up with 1.6 ~ 1.8 DEG C/min.
5. cast iron seal finished product prepared by a kind of surface treatment method of any one of claim 1 ~ 4 cast iron seal.
CN201710773436.8A 2017-08-31 2017-08-31 A kind of surface treatment method of cast iron seal Pending CN107574292A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710773436.8A CN107574292A (en) 2017-08-31 2017-08-31 A kind of surface treatment method of cast iron seal

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710773436.8A CN107574292A (en) 2017-08-31 2017-08-31 A kind of surface treatment method of cast iron seal

Publications (1)

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CN107574292A true CN107574292A (en) 2018-01-12

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TWI784694B (en) * 2021-08-31 2022-11-21 正修學校財團法人正修科技大學 Method for metal treating

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TWI784694B (en) * 2021-08-31 2022-11-21 正修學校財團法人正修科技大學 Method for metal treating

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Application publication date: 20180112