CN107557147A - A kind of extracting method of fruit-like flavour rapeseed oil - Google Patents
A kind of extracting method of fruit-like flavour rapeseed oil Download PDFInfo
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- CN107557147A CN107557147A CN201711003389.5A CN201711003389A CN107557147A CN 107557147 A CN107557147 A CN 107557147A CN 201711003389 A CN201711003389 A CN 201711003389A CN 107557147 A CN107557147 A CN 107557147A
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Abstract
The invention belongs to vegetable fat extractive technique field.A kind of extracting method of fruit-like flavour rapeseed oil, it is characterised in that comprise the following steps:1) vegetable seed screening cleaning, removal of impurities;2) vegetable seed decortication, separation are carried out using automatic peeling machine, obtains rapeseed dehulled;3) rapeseed dehulled is crushed, sieved, and obtains desquamated rapeseed powder;4) fruit slice of freeze-drying is crushed, sieving, obtains fruit freeze-dried powder;5) desquamated rapeseed powder and fruit jelly dry powder blend are uniform, using supercritical carbon dioxide extracting grease, obtain crude oil;6) after crude oil being carried out into centrifugal filtration, fruit-like flavour rapeseed oil is obtained.This method technological process is simple, and extraction efficiency is high, and Environmental Safety, grease obtained fruit-like flavour is pure, oxidation stability is good.
Description
Technical field
The invention belongs to vegetable fat extractive technique field, and in particular to a kind of extracting method of fruit-like flavour rapeseed oil.
Background technology
At present in the condiment in the market of salad and some other food, there is the tune with edible oil and various combinations of perfumes
Material, but most of directly blent with flavoring essence spices forms, it is lyophilized to there may be shoddy confusion, it is necessary to
Grease is extracted using safe and efficient method and retains good flavor.Grease is that a kind of fragrance well carries agent, Ke Yili
With " taste " principle, rapeseed meal and Fruit powder are compounded in flavor raw material, then it is same by supercritical carbon dioxide extracting
When extract grease and fruit-like flavour fragrance, the flavor grease produced there is the characteristics of green, safe and stable property is good.
The content of the invention
It is an object of the invention to provide a kind of extracting method of fruit-like flavour rapeseed oil, this method technological process is simple,
Extraction efficiency is high, and Environmental Safety, grease obtained fruit-like flavour is pure, oxidation stability is good.
To achieve these goals, the technical solution adopted in the present invention is:A kind of extraction side of fruit-like flavour rapeseed oil
Method, it is characterised in that comprise the following steps:
1) vegetable seed screening cleaning, removal of impurities;
2) vegetable seed decortication, separation are carried out using automatic peeling machine, obtains rapeseed dehulled;
3) rapeseed dehulled is crushed, sieve (sieve for crossing 60 mesh), obtains desquamated rapeseed powder;
4) fruit slice of freeze-drying is crushed, sieving (sieve for crossing 60 mesh), obtains fruit freeze-dried powder;
5) desquamated rapeseed powder and fruit jelly dry powder blend are uniform, using supercritical carbon dioxide extracting grease, obtain crude oil;
6) after crude oil being carried out into centrifugal filtration, fruit-like flavour rapeseed oil is obtained.
As the further scheme of the present invention:Impurity in vegetable seed (rapeseed, also referred to as brassicae chinensis,semen) in the step 1)
Rate is less than 10 (quality) %.
As the further scheme of the present invention:Vegetable seed sample size in the step 2) is 2-10kg, vegetable seed decortication power
For 800~4000W, the time is 2~20min.
As the further scheme of the present invention:Characterized in that, after rapeseed dehulled is crushed, sieved in the step 3)
Particle diameter is 0.5~5mm.
As the further scheme of the present invention:Characterized in that, fruit slice is orange piece, orange piece, lemon in the step 4)
One kind in lemon piece, shaddock piece etc..
As the further scheme of the present invention:Characterized in that, the fruit slice for the freeze-drying selected in the step 4)
Moisture content is less than 1 (quality) %, crushes, the particle diameter of sieving is 0.1~2mm.
As the further scheme of the present invention:Desquamated rapeseed powder is in mass ratio with fruit freeze-dried powder in the step 5)
15:1~1:1 mixing.
As the further scheme of the present invention:Supercritical carbon dioxide parameter is in the step 5):Extracting pressure be 7~
30MP, extraction temperature are 20~50 DEG C, and each extraction time is 20~150min, and extraction times are 1~5 time.Comprehensive oil yield
For 18%-30%.
As the further scheme of the present invention:Centrifugal rotational speed is 3000-10000rpm/min in the step 6).
The beneficial effects of the invention are as follows:Grease is that a kind of fragrance well carries agent, based on " taste " principle, prepares compounding
Fruit-like flavour rapeseed oil.Fruit freeze-dried powder mixes with rapeseed meal produces grease, can not only assign rapeseed oil pure and fresh fruit-like flavour,
The oxidation stability and Storage of rapeseed oil can also be obviously improved.Grease, hair are extracted using supercritical carbon dioxide extraction method
The filtered sedimentation of oil obtains fruit-like flavour rapeseed oil.With two major features:(1) using super critical CO 2 technology extraction
Flavor grease is green, safe and stable property is good;(2) freeze-drying fruit slice pure flavor and not easy oxidation discoloration, dish of peeling are selected
Seed chlorophyll content is low, therefore the flavor grease bright color produced.A kind of rapeseed oil for novel sapor that the present invention produces, tool
Have product safety, pure flavor, stability it is good, it is simple to operate, can be achieved industrialized production the characteristics of.
Embodiment
Example below illustrates to technical scheme.
Embodiment 1:
A kind of extracting method of fruit-like flavour rapeseed oil, comprises the following steps:
1) 2kg vegetable seed is cleared up, removal of impurities, percentage of admixture is less than 10 (quality) % in vegetable seed;2) carried out using automatic peeling machine
Vegetable seed decortication, separation, vegetable seed decortication power is 3000W, and the decortication time is 12min, and skin-containing rate is 10 (quality) % in benevolence, is obtained
Rapeseed dehulled;3) rapeseed dehulled is crushed, sieved, and particle diameter is 0.5mm after de-hulled rapeseed kernel powder crushes, and obtains desquamated rapeseed powder;4)
It is less than 1 (quality) % from the orange piece moisture content of freeze-drying, the orange piece of freeze-drying is crushed, sieving, the orange of freeze-drying
Particle diameter is 1mm after piece crushes, and obtains orange powder (i.e. fruit freeze-dried powder);5) it is than ratio in the quality of desquamated rapeseed powder and orange powder
10:1 mixing, using supercritical carbon dioxide extracting grease, supercritical carbon dioxide extracting pressure is 20MP, extraction temperature 40
DEG C, each extraction time is 60min, and it is 2 times to repeat extraction times, obtains crude oil;6) crude oil is subjected to centrifugal filtration, using height
Fast centrifuge 1 time, rotating speed 5000rmp/min, comprehensive oil yield is 24.6%, and obtaining fruit-like flavour rapeseed oil (has
The rapeseed oil of fruit-like flavour, i.e. fragrant citrus flavor rapeseed oil).By 20 people's sensory evaluation groups (12 women, 10 males form)
Preference degree evaluation is carried out to fragrant citrus flavor rapeseed oil, full marks are 10 points.Analyses Methods for Sensory Evaluation Results fragrant citrus flavor rapeseed oil comprehensive score
9.1 points, grease obtained fruit-like flavour is pure.Oxidation of Fat and Oils induction time (h) improves more than 20% at 110 DEG C.
Embodiment 2:
A kind of extracting method of fruit-like flavour rapeseed oil, comprises the following steps:
1) 8kg vegetable seed is cleared up, removal of impurities, percentage of admixture is less than 10 (quality) % in vegetable seed;2) carried out using automatic peeling machine
Vegetable seed decortication, separation, vegetable seed decortication power is 4000W, and the decortication time is 20min, and skin-containing rate is 9.5 (quality) % in benevolence, is obtained
To rapeseed dehulled;3) rapeseed dehulled is crushed, sieved, and particle diameter is 2mm after de-hulled rapeseed kernel powder crushes, and obtains desquamated rapeseed powder;4)
The orange piece of freeze-drying is crushed, sieving, particle diameter is 1.5mm after the orange piece crushing of freeze-drying, obtains tangerine powder (i.e. fruit
Freeze-dried powder);5) it is 4 than ratio in the quality of desquamated rapeseed powder and tangerine powder:1 mixing, using supercritical carbon dioxide extracting grease,
Supercritical carbon dioxide extracting pressure is 20MP, and extraction temperature is 30 DEG C, and each extraction time is 70min, repeats extraction times
For 3 times, crude oil is obtained;6) crude oil is subjected to centrifugal filtration, centrifuged 1 time, rotating speed 8000rmp/min using supercentrifuge,
Comprehensive oil yield is 21.3%, obtains fruit-like flavour rapeseed oil (i.e. fragrant tangerine flavor rapeseed oil).By 20 people's sensory evaluation groups (12
Name women, 10 male's compositions) preference degree evaluation is carried out to fragrant tangerine flavor rapeseed oil, full marks are 10 points.Analyses Methods for Sensory Evaluation Results is fragrant
Tangerine flavor rapeseed oil comprehensive score 8.9 is divided, and grease obtained fruit-like flavour is pure.Oxidation of Fat and Oils induction time (h) improves at 110 DEG C
20% with first-class.
Embodiment 3:
A kind of extracting method of fruit-like flavour rapeseed oil, comprises the following steps:
1) 5kg vegetable seed is cleared up, removal of impurities, percentage of admixture is less than 10 (quality) % in vegetable seed;2) carried out using automatic peeling machine
Vegetable seed decortication, separation, vegetable seed decortication power is 3000W, and the decortication time is 15min, and skin-containing rate is 8.5 (quality) % in benevolence, is obtained
To rapeseed dehulled;3) rapeseed dehulled is crushed, sieved, and particle diameter is 2mm after de-hulled rapeseed kernel powder crushes, and obtains desquamated rapeseed powder;4)
The lemon tablet of freeze-drying is crushed, sieving, particle diameter is 1.5mm after the lemon tablet crushing of freeze-drying, obtains lemon powder (i.e. water
Jelly dry powder);5) it is 8 than ratio in the quality of desquamated rapeseed powder and lemon powder:1 mixing, using supercritical carbon dioxide extracting
Grease, supercritical carbon dioxide extracting pressure are 15MP, and extraction temperature is 40 DEG C, and each extraction time is 40min, repeat to extract
Number is 2 times, obtains crude oil;6) crude oil is subjected to centrifugal filtration, centrifuged 1 time using supercentrifuge, rotating speed 10000rmp/
Min, comprehensive oil yield is 27.2%, obtains fruit-like flavour rapeseed oil (i.e. lemon flavor rapeseed oil).It is small by 20 people's sensory evaluations
Group (12 women, 10 male's compositions) carries out preference degree evaluation to lemon flavor rapeseed oil, and full marks are 10 points.Sensory evaluation knot
Fruit lemon flavor rapeseed oil comprehensive score 9.5 is divided, and grease obtained fruit-like flavour is pure.Oxidation of Fat and Oils induction time (h) at 110 DEG C
Improve more than 30%.
Embodiment 4:
A kind of extracting method of fruit-like flavour rapeseed oil, comprises the following steps:
1) 5kg vegetable seed is cleared up, removal of impurities, percentage of admixture is less than 10 (quality) % in vegetable seed;2) carried out using automatic peeling machine
Vegetable seed decortication, separation, vegetable seed decortication power is 3000W, and the decortication time is 15min, and skin-containing rate is 9.0 (quality) % in benevolence, is obtained
To rapeseed dehulled;3) rapeseed dehulled is crushed, sieved, and particle diameter is 2mm after de-hulled rapeseed kernel powder crushes, and obtains desquamated rapeseed powder;4)
The shaddock piece of freeze-drying is crushed, sieving, particle diameter is 1.5mm after the shaddock piece crushing of freeze-drying, obtains shaddock powder (i.e. water
Jelly dry powder);5) it is 6 than ratio in the quality of desquamated rapeseed powder and shaddock powder:1 mixing, using supercritical carbon dioxide extracting
Grease, supercritical carbon dioxide extracting pressure are 15MP, and extraction temperature is 50 DEG C, and each extraction time is 40min, repeat to extract
Number is 2 times, obtains crude oil;6) crude oil is subjected to centrifugal filtration, centrifuged 1 time using supercentrifuge, rotating speed 10000rmp/
Min, comprehensive oil yield is 24.6%, obtains fruit-like flavour rapeseed oil (i.e. fragrant shaddock flavor rapeseed oil).It is small by 20 people's sensory evaluations
Group (12 women, 10 male's compositions) carries out preference degree evaluation to fragrant shaddock flavor rapeseed oil, and full marks are 10 points.Sensory evaluation knot
Fruity shaddock flavor rapeseed oil comprehensive score 9.3 is divided, and grease obtained fruit-like flavour is pure.Oxidation of Fat and Oils induction time (h) at 110 DEG C
Improve more than 20%.
Embodiment 5:
A kind of extracting method of fruit-like flavour rapeseed oil, comprises the following steps:
By the cleaning of 2kg vegetable seed, clean, percentage of admixture is less than 10 (quality) % in vegetable seed;2) dish is carried out using automatic peeling machine
Seed decortication, separation, vegetable seed decortication power is 800W, and the decortication time is 20min, and skin-containing rate is 10 (quality) % in benevolence, obtains dish
Seed benevolence;3) rapeseed dehulled is crushed, sieved, and particle diameter is 0.5mm after de-hulled rapeseed kernel powder crushes, and obtains desquamated rapeseed powder;4) select
It is less than 1 (quality) % with the orange piece moisture content of freeze-drying, the orange piece of freeze-drying is crushed, sieving, the orange piece of freeze-drying
Particle diameter is 0.1mm after crushing, obtains orange powder (i.e. fruit freeze-dried powder);5) it is than ratio in the quality of desquamated rapeseed powder and orange powder
15:1 mixing, using supercritical carbon dioxide extracting grease, supercritical carbon dioxide extracting pressure is 7MP, extraction temperature 50
DEG C, each extraction time is 150min, and it is 1 time to repeat extraction times, obtains crude oil;6) crude oil is subjected to centrifugal filtration, used
Supercentrifuge centrifuges 1 time, rotating speed 3000rmp/min, and comprehensive oil yield is 20.5%, obtains fruit-like flavour rapeseed oil (tool
There are the rapeseed oil of fruit-like flavour, i.e. fragrant citrus flavor rapeseed oil).By 20 people's sensory evaluation groups (12 women, 10 male's groups
Into) preference degree evaluation is carried out to fragrant tangerine flavor rapeseed oil, full marks are 10 points.Analyses Methods for Sensory Evaluation Results fragrant citrus flavor rapeseed oil is comprehensive
Divide 9.0 points, grease obtained fruit-like flavour is pure.Oxidation of Fat and Oils induction time (h) improves more than 20% at 110 DEG C.
Embodiment 6:
A kind of extracting method of fruit-like flavour rapeseed oil, comprises the following steps:
1) 10kg vegetable seed is cleared up, removal of impurities, percentage of admixture is less than 10 (quality) % in vegetable seed;2) carried out using automatic peeling machine
Vegetable seed decortication, separation, vegetable seed decortication power is 4000W, and the decortication time is 2min, and skin-containing rate is 10 (quality) % in benevolence, is obtained
Rapeseed dehulled;3) rapeseed dehulled is crushed, sieved, and particle diameter is 5mm after de-hulled rapeseed kernel powder crushes, and obtains desquamated rapeseed powder;4) select
It is less than 1 (quality) % with the orange piece moisture content of freeze-drying, the orange piece of freeze-drying is crushed, sieving, the orange piece of freeze-drying
Particle diameter is 2mm after crushing, obtains orange powder (i.e. fruit freeze-dried powder);5) it is 1 than ratio in the quality of desquamated rapeseed powder and orange powder:1
Mixing, using supercritical carbon dioxide extracting grease, supercritical carbon dioxide extracting pressure is 30MP, and extraction temperature is 20 DEG C,
Each extraction time is 20min, and it is 5 times to repeat extraction times, obtains crude oil;6) crude oil is subjected to centrifugal filtration, using at a high speed
Centrifuge 1 time, rotating speed 10000rmp/min, comprehensive oil yield is 22.8%, and obtaining fruit-like flavour rapeseed oil (has water
The rapeseed oil of fruit flavor, i.e. fragrant citrus flavor rapeseed oil).It is right by 20 people's sensory evaluation groups (12 women, 10 males form)
Lemon flavor rapeseed oil carries out preference degree evaluation, and full marks are 10 points.Analyses Methods for Sensory Evaluation Results fragrant citrus flavor rapeseed oil comprehensive score 9.2
Point, grease obtained fruit-like flavour is pure.Oxidation of Fat and Oils induction time (h) improves more than 20% at 110 DEG C.
Each raw material cited by the present invention, and bound, the section value of each raw material of the present invention, and technological parameter
Bound, the section value of (such as temperature, time) can realize the present invention, embodiment numerous to list herein.
Above example is only to illustrative and not limiting technical scheme, although above-described embodiment enters to the present invention
Detailed description is gone, the person skilled of this area should be understood:The present invention can be modified or replaced on an equal basis, but
Any modification and local replacement for not departing from spirit and scope of the invention all should be covered in scope of the presently claimed invention.
Claims (9)
1. a kind of extracting method of fruit-like flavour rapeseed oil, it is characterised in that comprise the following steps:
1) vegetable seed screening cleaning, removal of impurities;
2) vegetable seed decortication, separation are carried out using automatic peeling machine, obtains rapeseed dehulled;
3) rapeseed dehulled is crushed, sieved, and obtains desquamated rapeseed powder;
4) fruit slice of freeze-drying is crushed, sieving, obtains fruit freeze-dried powder;
5) desquamated rapeseed powder and fruit jelly dry powder blend are uniform, using supercritical carbon dioxide extracting grease, obtain crude oil;
6) after crude oil being carried out into centrifugal filtration, fruit-like flavour rapeseed oil is obtained.
A kind of 2. extracting method of fruit-like flavour rapeseed oil according to claim 1, it is characterised in that:In the step 1)
Vegetable seed in percentage of admixture be less than 10 (quality) %.
A kind of 3. extracting method of fruit-like flavour rapeseed oil according to claim 1, it is characterised in that:The step 2)
In, vegetable seed decortication power is 800~4000W, and the time is 2~20min.
A kind of 4. extracting method of fruit-like flavour rapeseed oil according to claim 1, it is characterised in that:In the step 3)
Rapeseed dehulled crushed, sieve after particle diameter be 0.5~5mm.
A kind of 5. extracting method of fruit-like flavour rapeseed oil according to claim 1, it is characterised in that:In the step 4)
Fruit slice is one kind in orange piece, orange piece, lemon tablet, shaddock piece etc..
A kind of 6. extracting method of fruit-like flavour rapeseed oil according to claim 1, it is characterised in that:In the step 4)
The fruit slice moisture content of the freeze-drying of selection is less than 1 (quality) %, crushes, the particle diameter of sieving is 0.1~2mm.
A kind of 7. extracting method of fruit-like flavour rapeseed oil according to claim 1, it is characterised in that:In the step 5)
Desquamated rapeseed powder is 15 in mass ratio with fruit freeze-dried powder:1~1:1 mixing.
A kind of 8. extracting method of fruit-like flavour rapeseed oil according to claim 1, it is characterised in that:In the step 5)
Supercritical carbon dioxide parameter is:Extracting pressure is 7~30MP, and extraction temperature is 20~50 DEG C, each extraction time is 20~
150min, extraction times are 1~5 time.
A kind of 9. extracting method of fruit-like flavour rapeseed oil according to claim 1, it is characterised in that:In the step 6)
Centrifugal rotational speed is 3000-10000rpm/min.
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Citations (7)
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CN104877756A (en) * | 2015-05-26 | 2015-09-02 | 合肥工业大学 | Rapeseed peeling method used for making oil through cold pressing |
CN104957282A (en) * | 2015-06-24 | 2015-10-07 | 洛阳国花坊牡丹生物科技有限公司 | Preparation method for edible oil blended from peony seed oil and rapeseed oil |
CN105038975A (en) * | 2015-08-12 | 2015-11-11 | 查光圣 | Supercritical extraction process for rapeseed oil |
CN105038967A (en) * | 2015-08-12 | 2015-11-11 | 查光圣 | Production process of oil of decorticated rapeseeds |
CN105886112A (en) * | 2016-05-18 | 2016-08-24 | 蚌埠市九华油脂有限公司 | Fragrant nutrient healthcare peanut oil |
CN105886111A (en) * | 2016-05-18 | 2016-08-24 | 蚌埠市九华油脂有限公司 | Fragrant nutrient health-care sunflower seed oil |
CN105901164A (en) * | 2016-04-15 | 2016-08-31 | 合肥珠光粮油贸易有限公司 | Lemon fragrance nata de coco rice bran blend oil |
-
2017
- 2017-10-24 CN CN201711003389.5A patent/CN107557147B/en active Active
Patent Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104877756A (en) * | 2015-05-26 | 2015-09-02 | 合肥工业大学 | Rapeseed peeling method used for making oil through cold pressing |
CN104957282A (en) * | 2015-06-24 | 2015-10-07 | 洛阳国花坊牡丹生物科技有限公司 | Preparation method for edible oil blended from peony seed oil and rapeseed oil |
CN105038975A (en) * | 2015-08-12 | 2015-11-11 | 查光圣 | Supercritical extraction process for rapeseed oil |
CN105038967A (en) * | 2015-08-12 | 2015-11-11 | 查光圣 | Production process of oil of decorticated rapeseeds |
CN105901164A (en) * | 2016-04-15 | 2016-08-31 | 合肥珠光粮油贸易有限公司 | Lemon fragrance nata de coco rice bran blend oil |
CN105886112A (en) * | 2016-05-18 | 2016-08-24 | 蚌埠市九华油脂有限公司 | Fragrant nutrient healthcare peanut oil |
CN105886111A (en) * | 2016-05-18 | 2016-08-24 | 蚌埠市九华油脂有限公司 | Fragrant nutrient health-care sunflower seed oil |
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