CN107550780A - A kind of plant essence and preparation method thereof - Google Patents
A kind of plant essence and preparation method thereof Download PDFInfo
- Publication number
- CN107550780A CN107550780A CN201710869026.3A CN201710869026A CN107550780A CN 107550780 A CN107550780 A CN 107550780A CN 201710869026 A CN201710869026 A CN 201710869026A CN 107550780 A CN107550780 A CN 107550780A
- Authority
- CN
- China
- Prior art keywords
- parts
- extract
- plant essence
- selaginella tamariscina
- spikemoss
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Cosmetics (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The present invention relates to a kind of plant essence and preparation method thereof, wherein plant essence, including the component represented below with parts by weight：58 63 parts of distilled water；8 12 parts of Sodium Hyaluronate；Biological 15 8 parts of carbohydrate gum；8 12 parts of butanediol；25 parts of trehalose；23 parts of hydroxyethyl cellulose；1,2 8 10 parts of hexylene glycols；0.5 1 parts of spikemoss extract；0.5 2 parts of pepper extract；58 parts of acetyl chitosamine；24 parts of dipotassium glycyrrhizinate；0.01 0.05 parts of parahydroxyacet-ophenone；12 parts of methyl hydroxybenzoate.As more than match made from plant essence have releive, conditioning skin, keep moisture of skin the advantages of.
Description
Technical field
The present invention relates to cosmetic skin field, and in particular, it is related to a kind of plant essence and preparation method thereof.
Background technology
In autumn and winter weather relatively dry season, in order to ensure skin comfort, it usually needs additionally keep the skin wet.It is facial clear
It is clean finish after, it is necessary to coat toner in face, be coated with essence afterwards to keep moisture of skin.
At present, grease is included in conventional essence, one layer of oil reservoir can be formed coated in face, its amalgamation with water
It is poor, skin pore can be blocked.The applying date is 2011.6.8, and application publication number is that CN102198071A patent discloses one kind
The preparation technology of Pearl skin-caring oil-controlling essence.Pearl skin-caring oil-controlling essence mainly includes pearl powder, starch octenyl succinic
Sour aluminium, acrylic copolymer, mixture, dipotassium glycyrrhizinate and the methyl methacrylate cross-linked polymer of magnesium carbonate composition.
Wherein starch ocentyl succinic aluminium, acrylic copolymer, carbonic acid magnesium compound have the function that to absorb skin surface grease.
Human body skin coats Pearl skin-caring oil-controlling essence, after it absorbs the grease of human secretory, easily in skin surface
Floating powder is formed, influences cutaneous respiration.
The content of the invention
It is an object of the invention to provide a kind of plant essence, its have releive, conditioning skin, keep moisture of skin
Advantage.
The present invention above-mentioned technical purpose technical scheme is that：A kind of plant essence, including
The component represented below with parts by weight：
Preferably, including below the component represented with parts by weight：
Using above technical scheme, Sodium Hyaluronate, biological carbohydrate gum -1, butanediol, trehalose, hydroxyethyl cellulose and 1,
For 2- hexylene glycols as main moisturizing and composition of releiving, the excitant of each component is smaller, and is imitated with good moisturizing
Fruit.Spikemoss extract has the effect of repairing skin, and skin keeps water to moisten state for a long time；Also there is deep water supplement and water lock work(
Can, long-acting moisturizing.Pepper extract contains abundant vitamin C, and it has compact skin and antioxidation, improves skin
Bright property.Acetyl chitosamine aids in spikemoss extract and pepper extract, improves cutaneous immunisation power, has work of releiving well
With.Dipotassium glycyrrhizinate, parahydroxyacet-ophenone and methyl hydroxybenzoate have good inhibiting bacteria and diminishing inflammation effect, can additionally improve skin
Permeability, promote to absorb.
Preferably, spikemoss extract is prepared in accordance with the following methods：Selaginella tamariscina is crushed, and 24- is stood in 80%-95% ethanol
48h, keeping temperature are 60-80 DEG C；Extract to obtain Selaginella tamariscina extract using 70%-85% ethanol, Selaginella tamariscina extract makes successively
Use 5%NaHCO3, 0.2%NaOH, chloroform-methanol mixed solvent and ethyl acetate-acetone-water as eluant, eluent, collect Selaginella tamariscina
Extract solution；It is evaporated under reduced pressure and removes eluant, eluent, obtained spikemoss extract is dried at 50-60 DEG C.
Selaginella tamariscina is handled according to as above method, beneficial to fat-soluble pigments such as the chlorophyll removed in Selaginella tamariscina, can also effectively be divided
From the flavone aglycone and flavonoid glycoside in Selaginella tamariscina, the yield of active ingredient in spikemoss extract is improved.
Preferably, pepper extract is prepared in accordance with the following methods：Capsicum crushing, with 65%-75% alcohol steeps, keep temperature
Spend and obtain capsicum extract for 70 DEG C；Capsicum extract is successively using petroleum ether, 50%-60% ethanol, 65%-75% ethanol
Elution, capsicum extract is collected, be evaporated under reduced pressure and remove the obtained pepper extract of eluant, eluent.
Using above technical scheme, the fat-soluble pigments such as carrotene are can remove, the capsaicine etc. in capsicum can also be retained
Active ingredient.
Further, the volume ratio of chloroform-methanol in the mixed solvent chloroform and methanol is (8-9)：1.
Further, the volume ratio of ethyl acetate, acetone and water is 7 in ethyl acetate-acetone-water:2.5:2.5.
Chloroform-methanol and ethyl acetate-acetone-water made from proportioning is as eluant, eluent more than, spikemoss extract
Active ingredient dissolution rate is higher.
Another object of the present invention is to provide a kind of preparation method of plant essence, it, which has, improves plant essence
Dispersion effect, the advantages of promoting each component well mixed.
The above-mentioned purpose of the present invention is achieved by the following technical programs：A kind of preparation method of plant essence, bag
Include following steps：
The steaming of Sodium Hyaluronate, biological carbohydrate gum -1, butanediol, trehalose, hydroxyethyl cellulose, 1,2- hexylene glycols and 1/2 volume
Distilled water is mixed to prepare the first homogenizing fluid at 30-40 DEG C；
Spikemoss extract, pepper extract, acetyl chitosamine, dipotassium glycyrrhizinate, parahydroxyacet-ophenone, methyl hydroxybenzoate and surplus are steamed
Distilled water is stirred obtained second homogenizing fluid at 40-50 DEG C；
First homogenizing fluid and the second homogenizing fluid carry out homogeneous stirring in emulsion tank and plant essence is made in vacuum outgas.
Further, the mixing speed of the first homogenizing fluid and the second homogenizing fluid in emulsion tank is 500-600r/min.
Using above technical scheme, Sodium Hyaluronate, biological carbohydrate gum -1, butanediol, trehalose, hydroxyethyl cellulose, 1,
2- hexylene glycols have preferable hydrophily, and these components mix with water in advance, improve the dissolubility of each component.Spikemoss extract,
Pepper extract, acetyl chitosamine, dipotassium glycyrrhizinate, parahydroxyacet-ophenone, methyl hydroxybenzoate and water mix, in acetyl chitose
In the presence of amine and dipotassium glycyrrhizinate, dissolving each other for spikemoss extract and pepper extract and water is better, improves each component
Homogenizing effect.Finally, then by the first homogenizing fluid and the second homogenizing fluid stirring is emulsified in emulsion tank, improves whole plant essence
Mixing uniformity, in order to avoid be layered.
In summary, the invention has the advantages that：
1st, plant essence produced by the present invention has a good moistening effect, Sodium Hyaluronate, butanediol, 1,2- hexylene glycols and
Hydroxyethyl cellulose has preferable water conservation moisturizing effect, has the effect of skin care；Trehalose mixes with hydroxyethyl cellulose
Conjunction forms layer of gel film, in case skin water loss, has preferable Water-saving effect；
2nd, plant essence produced by the present invention has effect of preferably releiving, biological carbohydrate gum -1, spikemoss extract, glycyrrhizic acid two
Potassium and trehalose mixing avoid skin tight, keep skin permeation, sustainable absorption moisture, keep skin oil-water balance；
3rd, plant essence produced by the present invention has preferable long-acting moisturizing and repair function, spikemoss extract, capsicum extraction
Thing, hydroxyethyl cellulose, biological carbohydrate gum -1 and the mixing of acetyl chitosamine, improve the self-repairing capability of skin；Hydroxy ethyl fiber
The sustainable gel network that plain, biological carbohydrate gum -1 and acetyl chitosamine are formed is skin moisturizing, in case skin is dark yellow.
Embodiment
The present invention is described in further detail with reference to embodiments.It should be understood that described in the embodiment of the present invention
Preparation method is only used for the explanation present invention, rather than limitation of the present invention, to this hair under the concept thereof of the present invention
The simple modifications of bright preparation method belong to the scope of protection of present invention.
The raw materials used producer of the present invention is as shown in table 1.
The raw materials used producer of the present invention of table 1
Embodiment one：A kind of preparation method of plant essence, comprises the following steps：
1st, the preparation method of spikemoss extract：Selaginella tamariscina is crushed, and 24h, keeping temperature are stood in the ethanol that volume fraction is 80%
For 60 DEG C, Selaginella tamariscina is 1 with the volume ratio that volume fraction is 80% ethanol：3, obtain Selaginella tamariscina leachate；
Use volume fraction to extract above-mentioned Selaginella tamariscina again for 70% ethanol, and Selaginella tamariscina extraction is mixed to get with Selaginella tamariscina leachate
Thing；
Load silica gel in chromatographic column, Selaginella tamariscina extract is poured into chromatographic column, and use 5%NaHCO successively3, 0.2%NaOH,
(volume ratio of chloroform and methanol is 8 to chloroform-methanol mixed solvent:1) and ethyl acetate-acetone-water (ethyl acetate, acetone and
The volume ratio of water is 7:2.5:2.5) eluant, eluent is used as, Selaginella tamariscina extract solution is collected below chromatographic column；
Selaginella tamariscina extract solution dries obtained spikemoss extracts at 50 DEG C afterwards using removal eluant, eluent is evaporated under reduced pressure.
2nd, the preparation method of pepper extract：Capsicum crushing, using volume fraction as 65% alcohol steep, keeping temperature 70
DEG C obtain capsicum extract；
Load silica gel in chromatographic column, capsicum extract is poured into chromatographic column, and successively using petroleum ether, volume fraction 50%
Ethanol, volume fraction be 65% ethanol elution, capsicum extract is collected below chromatographic column；
Pepper extract is made using removal eluant, eluent is evaporated under reduced pressure in capsicum extract.
3rd, Sodium Hyaluronate, biological carbohydrate gum -1, butanediol, trehalose, hydroxyethyl cellulose, 1,2- hexylene glycols and 1/2 body
Long-pending distilled water is mixed to prepare the first homogenizing fluid at 30 DEG C；
Spikemoss extract, pepper extract, acetyl chitosamine, dipotassium glycyrrhizinate, parahydroxyacet-ophenone, methyl hydroxybenzoate and surplus are steamed
Distilled water is stirred obtained second homogenizing fluid at 40 DEG C；
First homogenizing fluid and the second homogenizing fluid carries out homogeneous stirring (mixing speed 500r/min) in emulsion tank and vacuum takes off
Plant essence is made in gas.
Embodiment two：A kind of preparation method of plant essence, comprises the following steps：
1st, the preparation method of spikemoss extract：Selaginella tamariscina is crushed, and 48h, keeping temperature are stood in the ethanol that volume fraction is 95%
For 80 DEG C, Selaginella tamariscina is 1 with the volume ratio that volume fraction is 95% ethanol：3, obtain Selaginella tamariscina leachate；
Use volume fraction to extract above-mentioned Selaginella tamariscina again for 85% ethanol, and Selaginella tamariscina extraction is mixed to get with Selaginella tamariscina leachate
Thing；
Load silica gel in chromatographic column, Selaginella tamariscina extract is poured into chromatographic column, and use 5%NaHCO successively3, 0.2%NaOH,
(volume ratio of chloroform and methanol is 9 to chloroform-methanol mixed solvent:1) and ethyl acetate-acetone-water (ethyl acetate, acetone and
The volume ratio of water is 7:2.5:2.5) eluant, eluent is used as, Selaginella tamariscina extract solution is collected below chromatographic column；
Selaginella tamariscina extract solution dries obtained spikemoss extracts at 60 DEG C afterwards using removal eluant, eluent is evaporated under reduced pressure.
2nd, the preparation method of pepper extract：Capsicum crushing, using volume fraction as 75% alcohol steep, keeping temperature 70
DEG C obtain capsicum extract；
Load silica gel in chromatographic column, capsicum extract is poured into chromatographic column, and successively using petroleum ether, volume fraction 60%
Ethanol, volume fraction be 75% ethanol elution, capsicum extract is collected below chromatographic column；
Pepper extract is made using removal eluant, eluent is evaporated under reduced pressure in capsicum extract.
3rd, Sodium Hyaluronate, biological carbohydrate gum -1, butanediol, trehalose, hydroxyethyl cellulose, 1,2- hexylene glycols and 1/2 body
Long-pending distilled water is mixed to prepare the first homogenizing fluid at 40 DEG C；
Spikemoss extract, pepper extract, acetyl chitosamine, dipotassium glycyrrhizinate, parahydroxyacet-ophenone, methyl hydroxybenzoate and surplus are steamed
Distilled water is stirred obtained second homogenizing fluid at 50 DEG C；
First homogenizing fluid and the second homogenizing fluid carries out homogeneous stirring (mixing speed 600r/min) in emulsion tank and vacuum takes off
Plant essence is made in gas.
Embodiment three：A kind of preparation method of plant essence, comprises the following steps：
1st, the preparation method of spikemoss extract：Selaginella tamariscina is crushed, and 30h, keeping temperature are stood in the ethanol that volume fraction is 90%
For 70 DEG C, Selaginella tamariscina is 1 with the volume ratio that volume fraction is 90% ethanol：3, obtain Selaginella tamariscina leachate；
Use volume fraction to extract above-mentioned Selaginella tamariscina again for 75% ethanol, and Selaginella tamariscina extraction is mixed to get with Selaginella tamariscina leachate
Thing；
Load silica gel in chromatographic column, Selaginella tamariscina extract is poured into chromatographic column, and use 5%NaHCO successively3, 0.2%NaOH,
(volume ratio of chloroform and methanol is 9 to chloroform-methanol mixed solvent:1) and ethyl acetate-acetone-water (ethyl acetate, acetone and
The volume ratio of water is 7:2.5:2.5) eluant, eluent is used as, Selaginella tamariscina extract solution is collected below chromatographic column；
Selaginella tamariscina extract solution dries obtained spikemoss extracts at 55 DEG C afterwards using removal eluant, eluent is evaporated under reduced pressure.
2nd, the preparation method of pepper extract：Capsicum crushing, using volume fraction as 70% alcohol steep, keeping temperature 70
DEG C obtain capsicum extract；
Load silica gel in chromatographic column, capsicum extract is poured into chromatographic column, and successively using petroleum ether, volume fraction 55%
Ethanol, volume fraction be 70% ethanol elution, capsicum extract is collected below chromatographic column；
Pepper extract is made using removal eluant, eluent is evaporated under reduced pressure in capsicum extract.
3rd, Sodium Hyaluronate, biological carbohydrate gum -1, butanediol, trehalose, hydroxyethyl cellulose, 1,2- hexylene glycols and 1/2 body
Long-pending distilled water is mixed to prepare the first homogenizing fluid at 35 DEG C；
Spikemoss extract, pepper extract, acetyl chitosamine, dipotassium glycyrrhizinate, parahydroxyacet-ophenone, methyl hydroxybenzoate and surplus are steamed
Distilled water is stirred obtained second homogenizing fluid at 45 DEG C；
First homogenizing fluid and the second homogenizing fluid carries out homogeneous stirring (mixing speed 600r/min) in emulsion tank and vacuum takes off
Plant essence is made in gas.
Example IV：A kind of preparation method of plant essence, comprises the following steps：
1st, the preparation method of spikemoss extract：Selaginella tamariscina is crushed, and 40h, keeping temperature are stood in the ethanol that volume fraction is 85%
For 75 DEG C, Selaginella tamariscina is 1 with the volume ratio that volume fraction is 85% ethanol：3, obtain Selaginella tamariscina leachate；
Use volume fraction to extract above-mentioned Selaginella tamariscina again for 70% ethanol, and Selaginella tamariscina extraction is mixed to get with Selaginella tamariscina leachate
Thing；
Load silica gel in chromatographic column, Selaginella tamariscina extract is poured into chromatographic column, and use 5%NaHCO successively3, 0.2%NaOH,
(volume ratio of chloroform and methanol is 8 to chloroform-methanol mixed solvent:1) and ethyl acetate-acetone-water (ethyl acetate, acetone and
The volume ratio of water is 7:2.5:2.5) eluant, eluent is used as, Selaginella tamariscina extract solution is collected below chromatographic column；
Selaginella tamariscina extract solution dries obtained spikemoss extracts at 60 DEG C afterwards using removal eluant, eluent is evaporated under reduced pressure.
2nd, the preparation method of pepper extract：Capsicum crushing, using volume fraction as 65% alcohol steep, keeping temperature 70
DEG C obtain capsicum extract；
Load silica gel in chromatographic column, capsicum extract is poured into chromatographic column, and successively using petroleum ether, volume fraction 55%
Ethanol, volume fraction be 75% ethanol elution, capsicum extract is collected below chromatographic column；
Pepper extract is made using removal eluant, eluent is evaporated under reduced pressure in capsicum extract.
3rd, Sodium Hyaluronate, biological carbohydrate gum -1, butanediol, trehalose, hydroxyethyl cellulose, 1,2- hexylene glycols and 1/2 body
Long-pending distilled water is mixed to prepare the first homogenizing fluid at 35 DEG C；
Spikemoss extract, pepper extract, acetyl chitosamine, dipotassium glycyrrhizinate, parahydroxyacet-ophenone, methyl hydroxybenzoate and surplus are steamed
Distilled water is stirred obtained second homogenizing fluid at 50 DEG C；
First homogenizing fluid and the second homogenizing fluid carries out homogeneous stirring (mixing speed 550r/min) in emulsion tank and vacuum takes off
Plant essence is made in gas.
Embodiment five：A kind of preparation method of plant essence, comprises the following steps：
1st, the preparation method of spikemoss extract：Selaginella tamariscina is crushed, and 36h, keeping temperature are stood in the ethanol that volume fraction is 80%
For 75 DEG C, Selaginella tamariscina is 1 with the volume ratio that volume fraction is 80% ethanol：3, obtain Selaginella tamariscina leachate；
Use volume fraction to extract above-mentioned Selaginella tamariscina again for 85% ethanol, and Selaginella tamariscina extraction is mixed to get with Selaginella tamariscina leachate
Thing；
Load silica gel in chromatographic column, Selaginella tamariscina extract is poured into chromatographic column, and use 5%NaHCO successively3, 0.2%NaOH,
(volume ratio of chloroform and methanol is 9 to chloroform-methanol mixed solvent:1) and ethyl acetate-acetone-water (ethyl acetate, acetone and
The volume ratio of water is 7:2.5:2.5) eluant, eluent is used as, Selaginella tamariscina extract solution is collected below chromatographic column；
Selaginella tamariscina extract solution dries obtained spikemoss extracts at 50 DEG C afterwards using removal eluant, eluent is evaporated under reduced pressure.
2nd, the preparation method of pepper extract：Capsicum crushing, using volume fraction as 70% alcohol steep, keeping temperature 70
DEG C obtain capsicum extract；
Load silica gel in chromatographic column, capsicum extract is poured into chromatographic column, and successively using petroleum ether, volume fraction 55%
Ethanol, volume fraction be 75% ethanol elution, capsicum extract is collected below chromatographic column；
Pepper extract is made using removal eluant, eluent is evaporated under reduced pressure in capsicum extract.
3rd, Sodium Hyaluronate, biological carbohydrate gum -1, butanediol, trehalose, hydroxyethyl cellulose, 1,2- hexylene glycols and 1/2 body
Long-pending distilled water is mixed to prepare the first homogenizing fluid at 35 DEG C；
Spikemoss extract, pepper extract, acetyl chitosamine, dipotassium glycyrrhizinate, parahydroxyacet-ophenone, methyl hydroxybenzoate and surplus are steamed
Distilled water is stirred obtained second homogenizing fluid at 50 DEG C；
First homogenizing fluid and the second homogenizing fluid carries out homogeneous stirring (mixing speed 500r/min) in emulsion tank and vacuum takes off
Plant essence is made in gas.
Concrete component in embodiment one to embodiment five is as shown in table 2.
The component and proportioning of 2 each embodiment of table
Comparative example：
The difference of comparative example one and embodiment three is to be not added with spikemoss extract.
The difference of comparative example two and embodiment three is to be not added with pepper extract.
The difference of comparative example three and embodiment three is to be not added with acetyl chitosamine.
Comparative example four is the aloe moisture-keeping essence of market purchase.
The plant essence as made from various embodiments above and comparative example does evaluation test：
First, subjective appreciation
Estimated under room temperature and non-direct sunlight whether fine and smooth, uniform.
2nd, pH is tested
Use the pH value of pH meter detection plant essence.
3rd, heat-resisting, cold tolerance test
Respectively in 40 DEG C and -10 DEG C of difference constant temperature 24h, whether observation of plant essence be layered plant essence, precipitates or water outlet.
4th, hydroscopicity is tested
Quality m is taken respectively0=5g samples, at 25 DEG C, relative humidity is respectively to place 8h in 43% and 75% environment, every
2h weighs a sample and records sample quality m1.Hydroscopicity=(m1-m0)/m0。
The evaluation test of plant essence made from 3 each embodiment of table and comparative example
Example one and the product of comparative example four do human body skin experiment on probation.
The subject 50 of all ages and classes layer is randomly selected, respectively using the back of the hand of left hand and the right hand as tested area, is implemented
Plant essence made from example one is coated on left hand the back of the hand, and the aloe moisture-keeping essence of comparative example four is coated on right hand the back of the hand.Point
It is other that sensory evaluation is done to two product：
Moisturizing effect (10 points)：It is non-greasy, salubrious；
Effect of releiving (10 points)：Non-stimulated, skin permeation；
24h continues moistening effect (10 points)：Skin is moist, non-greasy, persistently keeps penetrating.
Specific evaluation result is as shown in table 4.
The skin test results of product are made in the embodiment one of table 4 and each comparative example
| Embodiment one | Comparative example one | Comparative example two | Comparative example three | Comparative example four | |
| Moisturizing effect | 9.8 | 9.2 | 9.3 | 9.3 | 8.4 |
| Releive effect | 9.8 | 9.0 | 9.2 | 9.3 | 8.6 |
| 24h continues moistening effect | 9.7 | 9.2 | 9.2 | 9.1 | 8.5 |
From data above, subject is preferable using moist and effect of releiving after product made from embodiment one, and can have
There is long-acting moistening effect.Using the product of comparative example four, in short term with certain moistening effect, but after 24h, dry skin,
Moistening effect is bad.Comparative example one, comparative example two and product made from comparative example three moisturizing effect, relax compared with embodiment one
Slow fruit and moistening effect be not good enough.
Claims (8)
1. a kind of plant essence, it is characterised in that including the component represented below with parts by weight：
Distilled water 58-63 parts；
Sodium Hyaluronate 8-12 parts；
The biological 5-8 of carbohydrate gum -1 parts；
Butanediol 8-12 parts；
Trehalose 2-5 parts；
Hydroxyethyl cellulose 2-3 parts；
1,2- hexylene glycol 8-10 parts；
Spikemoss extract 0.5-1 parts；
Pepper extract 0.5-2 parts；
Acetyl chitosamine 5-8 parts；
Dipotassium glycyrrhizinate 2-4 parts；
Parahydroxyacet-ophenone 0.01-0.05 parts；
Methyl hydroxybenzoate 1-2 parts.
2. plant essence according to claim 1, it is characterised in that including the component represented below with parts by weight：
Distilled water 60-63 parts；
Sodium Hyaluronate 10-12 parts；
The biological 5-8 of carbohydrate gum -1 parts；
Butanediol 8-10 parts；
Trehalose 2-3 parts；
Hydroxyethyl cellulose 2-3 parts；
1,2- hexylene glycol 8-10 parts；
Spikemoss extract 0.5-1 parts；
Pepper extract 0.5-2 parts；
Acetyl chitosamine 5-8 parts；
Dipotassium glycyrrhizinate 2-4 parts；
Parahydroxyacet-ophenone 0.01-0.05 parts；
Methyl hydroxybenzoate 1-2 parts.
3. according to the plant essence described in any one of claim 1 or 2, it is characterised in that spikemoss extract is according to lower section
It is prepared by method：Selaginella tamariscina is crushed, and 24-48h is stood in 80%-95% ethanol, and keeping temperature is 60-80 DEG C；Using 70%-85% second
Alcohol extracting obtains Selaginella tamariscina extract, and Selaginella tamariscina extract uses 5%NaHCO successively3, 0.2%NaOH, chloroform-methanol mixed solvent and
Ethyl acetate-acetone-water collects Selaginella tamariscina extract solution as eluant, eluent；It is evaporated under reduced pressure and removes eluant, eluent, system is dried at 50-60 DEG C
Obtain spikemoss extract.
4. according to the plant essence described in any one of claim 1 or 2, it is characterised in that pepper extract is according to lower section
It is prepared by method：Capsicum crushing, with 65%-75% alcohol steeps, keeping temperature is 70 DEG C and obtains capsicum extract；Capsicum extract is successively
Using petroleum ether, 50%-60% ethanol, 65%-75% ethanol elutions, capsicum extract is collected, is evaporated under reduced pressure the eluant, eluent system of removing
Obtain pepper extract.
5. plant essence according to claim 3, it is characterised in that chloroform-methanol in the mixed solvent chloroform and methanol
Volume ratio be（8-9）：1.
6. plant essence according to claim 3, it is characterised in that ethyl acetate, third in ethyl acetate-acetone-water
The volume ratio of ketone and water is 7：2.5：2.5.
A kind of 7. preparation method of the plant essence described in any one of claim 1-6, it is characterised in that：Including following step
Suddenly：
The steaming of Sodium Hyaluronate, biological carbohydrate gum -1, butanediol, trehalose, hydroxyethyl cellulose, 1,2- hexylene glycols and 1/2 volume
Distilled water is mixed to prepare the first homogenizing fluid at 30-40 DEG C；
Spikemoss extract, pepper extract, acetyl chitosamine, dipotassium glycyrrhizinate, parahydroxyacet-ophenone, methyl hydroxybenzoate and surplus are steamed
Distilled water is stirred obtained second homogenizing fluid at 40-50 DEG C；
First homogenizing fluid and the second homogenizing fluid carry out homogeneous stirring in emulsion tank and plant essence is made in vacuum outgas.
8. the preparation method of plant essence according to claim 7, it is characterised in that：First homogenizing fluid and the second homogeneous
Mixing speed of the liquid in emulsion tank is 500-600r/min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710869026.3A CN107550780A (en) | 2017-09-22 | 2017-09-22 | A kind of plant essence and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710869026.3A CN107550780A (en) | 2017-09-22 | 2017-09-22 | A kind of plant essence and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107550780A true CN107550780A (en) | 2018-01-09 |
Family
ID=60982232
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710869026.3A Pending CN107550780A (en) | 2017-09-22 | 2017-09-22 | A kind of plant essence and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107550780A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108066245A (en) * | 2018-02-09 | 2018-05-25 | 广州御延堂生物科技有限公司 | A kind of skin whitening, moisturizing stoste and preparation method thereof |
| CN108078886A (en) * | 2018-02-09 | 2018-05-29 | 广州重生化妆品实业有限公司 | A kind of compound Thief zone moisturizing elite and its preparation process |
| CN113081892A (en) * | 2021-04-08 | 2021-07-09 | 珠海朗祺生物科技有限公司 | Composition containing acetyl chitosamine and having moisturizing effect as well as preparation method and application of composition |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1985859A (en) * | 2005-12-23 | 2007-06-27 | 广州白云山制药股份有限公司 | Method of identifying Rock lily plant and its preparation |
| CN102964264A (en) * | 2012-11-16 | 2013-03-13 | 上海太昊生物科技(周口)医药有限公司 | Preparation method of natural general alkaloids of capsicum annuum |
-
2017
- 2017-09-22 CN CN201710869026.3A patent/CN107550780A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1985859A (en) * | 2005-12-23 | 2007-06-27 | 广州白云山制药股份有限公司 | Method of identifying Rock lily plant and its preparation |
| CN102964264A (en) * | 2012-11-16 | 2013-03-13 | 上海太昊生物科技(周口)医药有限公司 | Preparation method of natural general alkaloids of capsicum annuum |
Non-Patent Citations (4)
| Title |
|---|
| 北京汉方淑华美容化妆品有限公司: ""淑美华康体丽肤精华"", 《国产非特殊用途化妆品备案服务平台》 * |
| 王建新主编: "《化妆品植物原料大全》", 30 June 2012 * |
| 田建霞等: ""辣椒抗氧化活性成分提取工艺研究"", 《农技服务》 * |
| 魏丽娜: ""卷柏中穗花杉双黄酮的提取和分离纯化研究"", 《中国优秀硕士学位论文全文数据库》 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108066245A (en) * | 2018-02-09 | 2018-05-25 | 广州御延堂生物科技有限公司 | A kind of skin whitening, moisturizing stoste and preparation method thereof |
| CN108078886A (en) * | 2018-02-09 | 2018-05-29 | 广州重生化妆品实业有限公司 | A kind of compound Thief zone moisturizing elite and its preparation process |
| CN110882203A (en) * | 2018-02-09 | 2020-03-17 | 广州重生化妆品实业有限公司 | Compound high-permeability moisturizing essence and preparation process thereof |
| CN113081892A (en) * | 2021-04-08 | 2021-07-09 | 珠海朗祺生物科技有限公司 | Composition containing acetyl chitosamine and having moisturizing effect as well as preparation method and application of composition |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN107550780A (en) | A kind of plant essence and preparation method thereof | |
| CN100402555C (en) | White fungus heteropolysaccharide and its extract, preparation method and uses | |
| CN106726646B (en) | A kind of clarity oil-control matifying lotion and preparation method thereof | |
| CN102525855B (en) | Preparation process for peach gum aqueous solution and prepared skin care products | |
| JP2003212776A (en) | Nanoemulsion comprising ginseng saponin metabolite as active ingredient, method for producing the same and cosmetic composition for preventing skin aging containing the same | |
| CN109394653A (en) | A kind of stoste and preparation method thereof | |
| CN110192985A (en) | A kind of care agent and preparation method thereof for skin moisture-keeping reparation | |
| CN104800124B (en) | It is a kind of to prevent the cosmetic material composition of skin aging and the cosmetics containing the cosmetic material composition | |
| CN108938498B (en) | Anti-allergy repair composition capable of inhibiting histamine release and preparation method and application thereof | |
| Kasipandi et al. | Effects of in vitro simulated gastrointestinal digestion on the antioxidant, α-glucosidase and α-amylase inhibitory activities of water-soluble polysaccharides from Opilia amentacea roxb fruit | |
| CN106418670B (en) | A kind of preparation and its application of compound tobacco humectant | |
| Hu et al. | Polysaccharides from pineapple pomace: new insight into ultrasonic-cellulase synergistic extraction and hypoglycemic activities | |
| CN108309833A (en) | A kind of lasting lip glaze of natural moisture preserving and preparation method thereof | |
| CN105968383A (en) | Low-molecular-weight polyglutamic acid, and preparation method and application thereof | |
| CN118059011A (en) | Rosa wood extract | |
| CN105662984A (en) | Moisturizing emulsion and preparation method thereof | |
| CN111297756B (en) | Essence with moistening and moisturizing and anti-allergy effects and preparation method thereof | |
| CN107349167B (en) | Cosmetic composition, preparation method and application thereof | |
| CN105250158A (en) | Body moistening lotion and preparation method thereof | |
| CN104814912A (en) | Hand cream containing camellia oil | |
| CN107041863A (en) | A kind of anti-wrinkle emulsion and preparation method thereof | |
| CN107997988A (en) | A kind of high moisturizing thickener blend composition and its application in cosmetics | |
| CN101565422A (en) | Method for extracting and refining sanggenon C and application thereof | |
| CN105708759A (en) | Pure natural antioxidant whitening multi-effect face cream with peony seed oil and preparation method thereof | |
| Chen et al. | Amylase-assisted extraction alters nutritional and physicochemical properties of polysaccharides and saponins isolated from Ganoderma spp. |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180109 |
|
| RJ01 | Rejection of invention patent application after publication |