CN107549205A - A kind of composite sterilization agent and preparation method thereof - Google Patents
A kind of composite sterilization agent and preparation method thereof Download PDFInfo
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- CN107549205A CN107549205A CN201710727364.3A CN201710727364A CN107549205A CN 107549205 A CN107549205 A CN 107549205A CN 201710727364 A CN201710727364 A CN 201710727364A CN 107549205 A CN107549205 A CN 107549205A
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- sterilization agent
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- nitrate
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Abstract
The invention discloses a kind of composite sterilization agent, it is prepared by the raw material of following mass parts:10 20 parts of active botanical, 5 10 parts of nitrate, 30 40 parts of cationic surfactant, 30 40 parts of composite enzyme and can 60 80 parts of sublimated compound template, also disclose the preparation method of the composite sterilization agent, advantage is:The bacterium in closed environment can be quickly eliminated, sterilization is efficiently and lasting, may be reused.
Description
Technical field
The present invention relates to a kind of bacteria remover, more particularly to a kind of composite sterilization agent and preparation method thereof.
Background technology
Refrigerator usage time is grown, and meeting breed bacteria, influences food hygiene and original flavor in refrigerator, meanwhile, in refrigerator doors
Rubber weather strip easily accumulates dirt and bacterium, also should periodic cleaning, so on the one hand can prevent the bacterium on door from passing through
Various approach enter refrigerator inside, on the other hand can also extend the service life of sealing strip.
Refrigerator is not " safety box ", and its low temperature can not thoroughly freeze to death bacterium, simply make bacterial growth more slowly;Cold
During jelly, some " psychrophiles " are the very strong bacterium of freezing tolerance, can be survived in 0 DEG C or so of environment.It is most common " thermophilic
Cold bacterium ", there are yersinia enterocolitica and listeria yersinia enterocolitica to cause a variety of diseases, most commonly enterocolitis.Simultaneously can be with
Cause skin to form erythema, erythema nodosa and arthritis more.It can cause people that septicemia, meningitis, pulmonary abscess, liver purulence occurs when serious
Swollen, osteomyelitis.
The content of the invention
Goal of the invention:The first object of the present invention is to provide a kind of composite sterilization agent of high-efficient and lasting, and the second purpose is to carry
For the preparation method of the bacteria remover.
Technical scheme:Composite sterilization agent of the present invention, is prepared by the raw material of following mass parts:Active plant carries
Take thing 10-20 parts, nitrate 5-10 parts, cationic surfactant 30-40 parts, composite enzyme (purchase of ferment Co., Ltd. of South Korea)
30-40 parts and can sublimated compound template 60-80 parts.
Wherein, the active botanical is prepared by following steps:
(1) plant leaves are chosen and is ground broken wall, obtained broken wall and plant leaf A;
(2) after broken wall plant leaf A is rinsed with NaOH solution, then it is multiple with clear water flushing, obtain broken wall and plant leaf B;
(3) broken wall plant leaf B is immersed in the tincture of iodine after 10-12h, filtering air-dries to obtain active botanical.
Plant is the mixing of leaf of Cortex cinnamomi camphorae or Poplar leaves or both in step (1).
The nitrate is the one or more in sodium nitrate, potassium nitrate and ammonium nitrate.
The cationic surfactant is quaternary ammonium compound.
It is described can sublimated compound template be melamine, hexa and metaformaldehyde in one or more.
The preparation method of described composite sterilization agent, comprises the following steps:
(1) active botanical, nitrate, cationic surfactant are mixed mixed in deionized water
Close solution A;
(2) can sublimated compound template add mixed solution A in, stirring reaction 20-24h, product is centrifuged
To mixed sols;
(3) gained mixed sols is mixed with composite enzyme and be dissolved in deionized water, mixed solution is obtained after ultrasonic disperse
B;
(4) mixed solution B is distilled, then the heat-treated sublimable compound template of removing, produce compound remove
Microbial inoculum.
Wherein, the mass ratio of the mixture and deionized water of mixed sols and composite enzyme is 1 in the step (3):10-
12。
Beneficial effect:Compared with prior art, advantages of the present invention is:Can quickly it eliminate thin in closed environment
Bacterium, sterilization is efficiently and lasting, may be reused.
Embodiment
Embodiment 1
A kind of composite sterilization agent, is prepared by the raw material of following mass parts:10 parts of active botanical, nitrate 5
Part, 30 parts of cationic surfactant, 30 parts of composite enzyme and can 60 parts of sublimated compound template.
Wherein, the active botanical is prepared by following steps:
(1) plant leaves are chosen and is ground broken wall, obtained broken wall and plant leaf A;
(2) after broken wall plant leaf A is rinsed with NaOH solution, then rinsed 3 times with clear water, obtain broken wall and plant leaf B;
(3) broken wall plant leaf B is immersed in the tincture of iodine after 10h, filtering air-dries to obtain active botanical.
Plant is leaf of Cortex cinnamomi camphorae in step (1).
The nitrate is sodium nitrate.
The cationic surfactant is quaternary ammonium compound.
It is described can sublimated compound template be melamine.
The preparation method of described composite sterilization agent, comprises the following steps:
(1) active botanical, nitrate, cationic surfactant are mixed mixed in deionized water
Close solution A;
(2) can sublimated compound template add mixed solution A in, stirring reaction 20h, product is centrifugally separating to obtain mixed
Close colloidal sol;
(3) gained mixed sols is mixed with composite enzyme and be dissolved in deionized water, mixed solution is obtained after ultrasonic disperse
B;
(4) mixed solution B is distilled, then the heat-treated sublimable compound template of removing, produce compound remove
Microbial inoculum.
Wherein, the mass ratio of the mixture and deionized water of mixed sols and composite enzyme is 1 in the step (3):10.
Embodiment 2
A kind of composite sterilization agent, is prepared by the raw material of following mass parts:15 parts of active botanical, nitrate 7
Part, 35 parts of cationic surfactant, 35 parts of composite enzyme and can 70 parts of sublimated compound template.
Wherein, the active botanical is prepared by following steps:
(1) plant leaves are chosen and is ground broken wall, obtained broken wall and plant leaf A;
(2) after broken wall plant leaf A is rinsed with NaOH solution, then rinsed 4 times with clear water, obtain broken wall and plant leaf B;
(3) broken wall plant leaf B is immersed in the tincture of iodine after 11h, filtering air-dries to obtain active botanical.
Plant is Poplar leaves in step (1).
The nitrate is potassium nitrate.
The cationic surfactant is quaternary ammonium compound.
It is described can sublimated compound template be hexa.
The preparation method of described composite sterilization agent, comprises the following steps:
(1) active botanical, nitrate, cationic surfactant are mixed mixed in deionized water
Close solution A;
(2) can sublimated compound template add mixed solution A in, stirring reaction 22h, product is centrifugally separating to obtain mixed
Close colloidal sol;
(3) gained mixed sols is mixed with composite enzyme and be dissolved in deionized water, mixed solution is obtained after ultrasonic disperse
B;
(4) mixed solution B is distilled, then the heat-treated sublimable compound template of removing, produce compound remove
Microbial inoculum.
Wherein, the mass ratio of the mixture and deionized water of mixed sols and composite enzyme is 1 in the step (3):11.
Embodiment 3
A kind of composite sterilization agent, is prepared by the raw material of following mass parts:20 parts of active botanical, nitrate 10
Part, 40 parts of cationic surfactant, 40 parts of composite enzyme and can 80 parts of sublimated compound template.
Wherein, the active botanical is prepared by following steps:
(1) plant leaves are chosen and is ground broken wall, obtained broken wall and plant leaf A;
(2) after broken wall plant leaf A is rinsed with NaOH solution, then rinsed 2 times with clear water, obtain broken wall and plant leaf B;
(3) broken wall plant leaf B is immersed in the tincture of iodine after 12h, filtering air-dries to obtain active botanical.
Plant is leaf of Cortex cinnamomi camphorae and Poplar leaves in step (1).
The nitrate is ammonium nitrate.
The cationic surfactant is quaternary ammonium compound.
It is described can sublimated compound template be metaformaldehyde.
The preparation method of described composite sterilization agent, comprises the following steps:
(1) active botanical, nitrate, cationic surfactant are mixed mixed in deionized water
Close solution A;
(2) can sublimated compound template add mixed solution A in, stirring reaction 24h, product is centrifugally separating to obtain mixed
Close colloidal sol;
(3) gained mixed sols is mixed with composite enzyme and be dissolved in deionized water, mixed solution is obtained after ultrasonic disperse
B;
(4) mixed solution B is distilled, then the heat-treated sublimable compound template of removing, produce compound remove
Microbial inoculum.
Wherein, the mass ratio of the mixture and deionized water of mixed sols and composite enzyme is 1 in the step (3):12.
Claims (8)
1. a kind of composite sterilization agent, it is characterised in that be prepared by the raw material of following mass parts:Active botanical 10-20
Part, nitrate 5-10 parts, cationic surfactant 30-40 parts, composite enzyme 30-40 parts and can sublimated compound template 60-
80 parts.
2. composite sterilization agent according to claim 1, it is characterised in that:The active botanical is by following steps system
It is standby to form:
(1) plant leaves are chosen and is ground broken wall, obtained broken wall and plant leaf A;
(2) after broken wall plant leaf A is rinsed with NaOH solution, then it is multiple with clear water flushing, obtain broken wall and plant leaf B;
(3) broken wall plant leaf B is immersed in the tincture of iodine after 10-12h, filtering air-dries to obtain active botanical.
3. composite sterilization agent according to claim 1, it is characterised in that:Plant is leaf of Cortex cinnamomi camphorae or poplar in step (1)
The mixing of leaf or both.
4. composite sterilization agent according to claim 1, it is characterised in that:The nitrate is sodium nitrate, potassium nitrate and nitre
One or more in sour ammonium.
5. composite sterilization agent according to claim 1, it is characterised in that:The cationic surfactant is quaternized
Thing.
6. composite sterilization agent according to claim 1, it is characterised in that:It is described can sublimated compound template be melamine
One or more in amine, hexa and metaformaldehyde.
7. the preparation method of the composite sterilization agent described in claim 1, it is characterised in that comprise the following steps:
(1) active botanical, nitrate, cationic surfactant are mixed to obtain in deionized water mix it is molten
Liquid A;
(2) can sublimated compound template add mixed solution A in, stirring reaction 20-24h, product is centrifugally separating to obtain mixed
Close colloidal sol;
(3) gained mixed sols is mixed with composite enzyme and be dissolved in deionized water, mixed solution B is obtained after ultrasonic disperse;
(4) mixed solution B is distilled, then the heat-treated sublimable compound template of removing, produce composite sterilization agent.
8. the preparation method of composite sterilization agent according to claim 7, it is characterised in that:Mixing is molten in the step (3)
The mass ratio of the mixture and deionized water of glue and composite enzyme is 1:10-12.
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Cited By (1)
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