CN107541941A - A kind of preparation method of Multifunctional composite fabric - Google Patents
A kind of preparation method of Multifunctional composite fabric Download PDFInfo
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- CN107541941A CN107541941A CN201710648892.XA CN201710648892A CN107541941A CN 107541941 A CN107541941 A CN 107541941A CN 201710648892 A CN201710648892 A CN 201710648892A CN 107541941 A CN107541941 A CN 107541941A
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Abstract
The present invention relates to a kind of preparation method of Multifunctional composite fabric, belong to function fabric technical field.The present invention utilizes dopamine itself high-adhesiveness,Tea Polyphenols is adsorbed on cotton fiber surface,The absorption of in-situ reducing nano copper particle is on cotton fiber surface again,Simultaneously because the dopamine surface of solution and internal oxygen concentration difference during autohemagglutination is stood make its polymerization speed different,Cause the particle shape size and film thickness difference that top layer generates with interior polymeric,So as to obtain the schemochrome material fiber of special duplicature refraction catoptric arrangement,Finally fiber interweaving is molded,It is and compound with TPUE,It is functional fabric with inside and outside two layers,Intermediate layer is the structure of TPUE,Multifunctional composite fabric is made,The present invention passes through Tea Polyphenols ortho position phenolic hydroxyl group,Easy dehydrogenation is converted into carbonyl and bacterial action,Eliminate harmful free radicals,Antibacterial and deodouring,Anti-aging and enhancing body's immunity,Synergic nano copper reaches efficient sterilizing deodorizing effect.
Description
Technical field
The present invention relates to a kind of preparation method of Multifunctional composite fabric, belong to function fabric technical field.
Background technology
As people gradually step up to new textile requirement, as assign fabric multifunctional main approach,
The surface that sight has been gathered in fabric by many researchers is modified.The method that various surfaces are modified is used on textile,
Textile is set to possess the excellent properties of high added value, mainly including colour-fast discoloration, high intensity, high-modulus, electric conductivity, heat conduction
Property, antibiotic property, hydrophobic, super hydrophilic, antistatic, radiation proof etc..
Multifunctional textile product are increasingly developed and launched, and receive what the favor people of consumer lived to high-quality
Pursuit and the raising of scientific and technological level, have promoted the development process of the functional ecological textile such as health care to a certain extent.My god
Right plant extract agent has lot of advantages compared with the function additive of chemical synthesis：1) security.To skin without anaphylaxis and cause
It is carcinous, there is preferable biodegradability and Environmental compatibility；2) healthcare function.Many medicinal plants are that China is with a long history
Chinese medicine, there are a variety of antibacterial desinsection effects of curing the wound；3) function is dyed.Natural pigment and plant fragrance and medicine during dyeing
Reason composition is absorbed by fiber together, reaches a kind of naturally special health care Color.Therefore, entered using natural plant function agent
Row health care, comfortable processing are favored by consumer, and cause many country's researchs and the concern of application device, still, at present
The antibacterial textile deodorizing effect that natural plant function agent is modified is undesirable, governs natural plant always the problem of colourity effect difference
The textile that thing functional agent is modified.
The content of the invention
The technical problems to be solved by the invention：Imitated for the antibacterial textile deodorization that current natural plant function agent is modified
Fruit is undesirable, and the problem of colourity effect difference, the invention provides a kind of preparation method of Multifunctional composite fabric.It is above-mentioned to solve
Technical problem, the technical solution adopted by the present invention are：
A kind of preparation method of Multifunctional composite fabric, it is characterised in that specifically preparation process is：
（1）Filtered after heating washing cotton fiber 3~5 times with absolute ether, washing and drying must pre-process cotton fiber；
（2）Take Dopamine hydrochloride to add in the tris-HCI buffer that pH is 7.5~8.5 to be well mixed, then
30~35 DEG C are heated to, and cotton fiber is taken out after 8~12h of dipping pretreatment cotton fiber, washes to obtain modified cotton fiber；
（3）Take Tea Polyphenols add deionized water in be well mixed, be again heated to 35~40 DEG C, and impregnate modified cotton fiber 50~
60min, washed after taking out cotton fiber, obtain impregnation cotton fiber；
（4）Impregnation cotton fiber is immersed in the copper-bath that mass fraction is 0.2%, at 30~35 DEG C, vibration is anti-
12~15h is answered, washing and drying after cotton fiber is taken out, obtains functional fibre；
（5）3~5 root functionality fiber plies are taken, then take 3~5 tencel plying, and with 50/50 intertexture ratio, by latitude plain group
Structure intertexture shaping is knitted, baking handles to obtain functional fabric；
（6）Functional fabric is compound with TPUE, it is functional fabric with inside and outside two layers, intermediate layer is thermoplasticity
The structure of polyurethane elastomer, compound 2~3min is heated with the compound pressure of 1~2MPa at 140~150 DEG C, obtained multi-functional multiple
Close fabric.
Step（2）Described in the mass ratio of Dopamine hydrochloride and tris-HCI buffer be 1：100,
The mass ratio for pre-processing cotton fiber and Dopamine hydrochloride is 10：1.
Step（3）Described in Tea Polyphenols dosage be the 6% of modified cotton fiber quality, modified cotton fiber and Tea Polyphenols solution
Bath raio is 1：30.
Step（4）Described in copper sulphate dosage be the 6% of impregnation cotton quality, impregnation cotton fiber and sulfuric acid
The bath raio of copper solution is 1：30.
Step（5）Described in baking processing be by fabric at 120~130 DEG C 30~40s of preliminary drying, then at 100~110 DEG C
30~40s of lower baking shapes.
Step（6）Described in the mass ratio of functional fabric and TPUE be 1：1.
The method have the benefit that：
（1）The present invention utilizes dopamine itself high-adhesiveness, and Tea Polyphenols is adsorbed on cotton fiber surface, then in-situ reducing Nanometer Copper
Granular absorption is on cotton fiber surface, simultaneously because dopamine surface of solution during autohemagglutination is stood is different with internal oxygen concentration
Make its polymerization speed different, cause particle shape size and film thickness difference that top layer generates with interior polymeric, so as to obtain spy
Fiber interweaving, is finally molded by the schemochrome material fiber of different duplicature refraction catoptric arrangement, and with thermoplastic polyurethane bullet
Property bluk recombination, with inside and outside two layers for functional fabric, intermediate layer be TPUE structure, be made it is multi-functional compound
Fabric；
（2）The present invention is stronger using ortho position phenolic hydroxyl group activity in chief active molecule catechin molecule in Tea Polyphenols, easy dehydrogenation
Carbonyl and bacterial action are converted into, so as to reach the effect of antibacterial, eliminates harmful free radicals, antibacterial and deodouring, anti-aging and enhancing
The characteristics of body's immunity, synergic nano copper reach efficient sterilizing deodorizing effect.
Embodiment
Taking cotton fiber is completely submerged in absolute ether and is fitted into apparatus,Soxhlet's, is heated to 80~90 DEG C, circulation cleaning
Filter residue is filtered to obtain after washing 3~5 times, is placed in after filter residue 2~3 times is washed with deionized in drying box, is done at 105~110 DEG C
It is dry to constant weight, obtain pretreatment cotton fiber；10~20g Dopamine hydrochlorides are taken to add the trihydroxy methyl ammonia that 1~2LpH is 7.5~8.5
In methylmethane-hydrochloride buffer, 20~30min is stirred with 300~400r/min, obtains modification liquid, modification liquid is heated to 30~
35 DEG C, then take 100~200g pretreatment cotton fibers to be immersed in modification liquid, cotton fiber is taken out after continuing 8~12h of stirring, is spent
Ion water washing 3~5 times, obtains modified cotton fiber；6~12g Tea Polyphenols is taken, is added in 3~6L deionized waters, with 300~400r/
Min stirs 20~30min, is again heated to 35~40 DEG C, and impregnates 100~200g, 50~60min of modified cotton fiber, and it is fine to take out cotton
It is washed with deionized after dimension 3~5 times, obtains impregnation cotton fiber；100~200g impregnation cotton fibers are immersed in 3~
6L mass fractions are in 0.2% copper-bath, at 30~35 DEG C, 12~15h of oscillating reactions, are spent after taking out cotton fiber
Ion water washing 3~5 times, then be placed in drying box, dried at 105~110 DEG C to constant weight, obtain functional fibre；Take 3 root functionalitys
Fiber plies, then take 3 tencels plying, and with 50/50 intertexture ratio, interweave by latitude plain construction and be molded, obtain fabric,
By fabric at 120~130 DEG C 30~40s of preliminary drying, then at 100~110 DEG C toast 30~40s sizing, obtain functional fabric；Will
100~200g functional fabrics and 100~200g TPUEs are compound, are functional fabric with inside and outside two layers, middle
Layer is the structure of TPUE, and compound 2~3min is heated with the compound pressure of 1~2MPa at 140~150 DEG C,
Obtain Multifunctional composite fabric.
Example 1
Taking cotton fiber is completely submerged in absolute ether and is fitted into apparatus,Soxhlet's, is heated to 80 DEG C, mistake after wash cycles 3 times
Filter residue is filtered to obtain, is placed in after filter residue 2 times is washed with deionized in drying box, is dried at 105 DEG C to constant weight, it is fine must pre-process cotton
Dimension；Take 10g Dopamine hydrochlorides to add in the tris-HCI buffer that 1LpH is 7.5, stirred with 300r/min
20min, modification liquid is obtained, modification liquid is heated to 30 DEG C, then take 100g pretreatment cotton fibers to be immersed in modification liquid, continue to stir
Cotton fiber is taken out after 8h, is washed with deionized 3 times, obtains modified cotton fiber；6g Tea Polyphenols is taken, is added in 3L deionized waters, with
300r/min stirs 20min, is again heated to 35 DEG C, and impregnates 100g modified cotton fiber 50min, and deionization is used after taking out cotton fiber
Water washing 3 times, obtains impregnation cotton fiber；100g impregnation cotton fibers are immersed in the copper sulphate that 3L mass fractions are 0.2%
In solution, at 30 DEG C, oscillating reactions 12h, it is washed with deionized 3 times, then is placed in drying box after taking out cotton fiber,
Dried at 105 DEG C to constant weight, obtain functional fibre；3 root functionality fiber plies are taken, then take 3 tencel plying, and with 50/50 friendship
Knit ratio, interweave by latitude plain construction and be molded, obtain fabric, by fabric at 120 DEG C preliminary drying 30s, then toasted at 100 DEG C
30s shapes, and obtains functional fabric；100g functional fabrics and 100g TPUEs is compound, it is work(with inside and outside two layers
Energy fabric, intermediate layer are the structure of TPUE, and compound 2min is heated with the compound pressure of 1MPa at 140 DEG C,
Obtain Multifunctional composite fabric.
Example 2
Taking cotton fiber is completely submerged in absolute ether and is fitted into apparatus,Soxhlet's, is heated to 85 DEG C, mistake after wash cycles 4 times
Filter residue is filtered to obtain, is placed in after filter residue 2 times is washed with deionized in drying box, is dried at 105 DEG C to constant weight, it is fine must pre-process cotton
Dimension；Take 15g Dopamine hydrochlorides to add in the tris-HCI buffer that 1.5LpH is 8.0, stirred with 350r/min
25min is mixed, obtains modification liquid, modification liquid is heated to 32 DEG C, then takes 150g pretreatment cotton fibers to be immersed in modification liquid, continues to stir
Cotton fiber is taken out after mixing 10h, is washed with deionized 4 times, obtains modified cotton fiber；9g Tea Polyphenols is taken, is added in 4L deionized waters,
25min is stirred with 300r/min, is again heated to 38 DEG C, and impregnate 150g modified cotton fiber 55min, take out spend after cotton fiber from
Sub- water washing 4 times, obtains impregnation cotton fiber；150g impregnation cotton fibers are immersed in the sulfuric acid that 4L mass fractions are 0.2%
In copper solution, at 32 DEG C, oscillating reactions 13h, it is washed with deionized 4 times, then is placed in drying box after taking out cotton fiber,
Dried at 108 DEG C to constant weight, obtain functional fibre；3 root functionality fiber plies are taken, then take 3 tencel plying, and with 50/50 friendship
Knit ratio, interweave by latitude plain construction and be molded, obtain fabric, by fabric at 125 DEG C preliminary drying 35s, then toasted at 105 DEG C
35s shapes, and obtains functional fabric；150g functional fabrics and 150g TPUEs is compound, it is work(with inside and outside two layers
Energy fabric, intermediate layer are the structure of TPUE, compound with the compound pressure hot melts of 1.5MPa at 145 DEG C
2min, obtain Multifunctional composite fabric.
Example 3
Taking cotton fiber is completely submerged in absolute ether and is fitted into apparatus,Soxhlet's, is heated to 90 DEG C, mistake after wash cycles 5 times
Filter residue is filtered to obtain, is placed in after filter residue 3 times is washed with deionized in drying box, is dried at 110 DEG C to constant weight, it is fine must pre-process cotton
Dimension；Take 20g Dopamine hydrochlorides to add in the tris-HCI buffer that 2LpH is 8.5, stirred with 400r/min
30min, modification liquid is obtained, modification liquid is heated to 35 DEG C, then take 200g pretreatment cotton fibers to be immersed in modification liquid, continue to stir
Cotton fiber is taken out after 12h, is washed with deionized 5 times, obtains modified cotton fiber；12g Tea Polyphenols is taken, is added in 6L deionized waters,
30min is stirred with 400r/min, is again heated to 40 DEG C, and impregnate 200g modified cotton fiber 60min, take out spend after cotton fiber from
Sub- water washing 5 times, obtains impregnation cotton fiber；200g impregnation cotton fibers are immersed in the sulfuric acid that 6L mass fractions are 0.2%
In copper solution, at 35 DEG C, oscillating reactions 15h, it is washed with deionized 5 times, then is placed in drying box after taking out cotton fiber,
Dried at 110 DEG C to constant weight, obtain functional fibre；3 root functionality fiber plies are taken, then take 3 tencel plying, and with 50/50 friendship
Knit ratio, interweave by latitude plain construction and be molded, obtain fabric, by fabric at 130 DEG C preliminary drying 40s, then toasted at 110 DEG C
40s shapes, and obtains functional fabric；200g functional fabrics and 200g TPUEs is compound, it is work(with inside and outside two layers
Energy fabric, intermediate layer are the structure of TPUE, and compound 3min is heated with the compound pressure of 2MPa at 150 DEG C,
Obtain Multifunctional composite fabric.
Reference examples：The Tea Polyphenols healthcare function textile fabric of Anhui company generation.
Multifunctional composite fabric obtained by above-described embodiment and the Tea Polyphenols healthcare function textile fabric of reference examples are carried out
Detection, specific detection are as follows：
The color feature value and case depth K/S values of fabric：Using D65 light sources, 10 ° of visual fields, by smooth 4 layers of cloth specimen doubling,
Color feature value L* (lightness), a* (red green ,+expression is partially red, and-expression is partially green), b* (champac ,+table are tested on color measurement and color match instrument
Show it is partially yellow ,-represent partially blue), C* (gorgeous degree), h (form and aspect), K/S values, survey 4 times, average.
The deodorization of fabric：With reference to Japan (society) estimation of fibres technological associations SEK mark fibre certification benchmark
21.Smelly eliminating is tested:Gas detecting tube method, the test of commission Shanghai Entry-Exit Inspection and Quarantine bureau.Foul smell is ammonia, and initial volume divides
Number is 0.01%, experimental period 2h.
The bacteriostasis rate of fabric：By GB/T20944.3-2008《The evaluation third portion of antibacterial textile performance:Succusion》
Tested, strain is Escherichia coli, staphylococcus aureus, Candida albicans.
As a result it is as shown in table 1：
Table 1
| Detection project | Example 1 | Example 2 | Example 3 | Reference examples |
| L* | 68.01 | 65.86 | 64.21 | 74.65 |
| a* | 3.14 | 3.21 | 3.40 | 1.45 |
| b* | 17.39 | 17.43 | 17.49 | 24.81 |
| C* | 17.59 | 17.77 | 17.79 | 24.88 |
| h | 80.84 | 79.59 | 79.45 | 85.11 |
| K/S values | 1.5627 | 1.6062 | 1.6489 | 1.1377 |
| Bacteriostasis rate % | 98.9 | 99.5 | 99.8 | 92.2 |
| Smelly eliminating rate % | 99.9 | 99.9 | 99.9 | 90.0 |
As seen from the above table, Multifunctional composite fabric antibiosis and deodorization effects of the present invention are good, the color feature value and case depth of fabric
K/S values are outstanding, are worthy to be popularized and use.
Claims (6)
1. a kind of preparation method of Multifunctional composite fabric, it is characterised in that specifically preparation process is：
（1）Filtered after heating washing cotton fiber 3~5 times with absolute ether, washing and drying must pre-process cotton fiber；
（2）Take Dopamine hydrochloride to add in the tris-HCI buffer that pH is 7.5~8.5 to be well mixed, then
30~35 DEG C are heated to, and cotton fiber is taken out after 8~12h of dipping pretreatment cotton fiber, washes to obtain modified cotton fiber；
（3）Take Tea Polyphenols add deionized water in be well mixed, be again heated to 35~40 DEG C, and impregnate modified cotton fiber 50~
60min, washed after taking out cotton fiber, obtain impregnation cotton fiber；
（4）Impregnation cotton fiber is immersed in the copper-bath that mass fraction is 0.2%, at 30~35 DEG C, vibration is anti-
12~15h is answered, washing and drying after cotton fiber is taken out, obtains functional fibre；
（5）3~5 root functionality fiber plies are taken, then take 3~5 tencel plying, and with 50/50 intertexture ratio, by latitude plain group
Structure intertexture shaping is knitted, baking handles to obtain functional fabric；
（6）Functional fabric is compound with TPUE, it is functional fabric with inside and outside two layers, intermediate layer is thermoplasticity
The structure of polyurethane elastomer, compound 2~3min is heated with the compound pressure of 1~2MPa at 140~150 DEG C, obtained multi-functional multiple
Close fabric.
A kind of 2. preparation method of Multifunctional composite fabric as claimed in claim 1, it is characterised in that step（2）Described in
The mass ratio of Dopamine hydrochloride and tris-HCI buffer is 1：100, pre-process cotton fiber and hydrochloric acid DOPA
The mass ratio of amine is 10：1.
A kind of 3. preparation method of Multifunctional composite fabric as claimed in claim 1, it is characterised in that step（3）Described in
Tea Polyphenols dosage is the 6% of modified cotton fiber quality, and the bath raio of modified cotton fiber and Tea Polyphenols solution is 1：30.
A kind of 4. preparation method of Multifunctional composite fabric as claimed in claim 1, it is characterised in that step（4）Described in
Copper sulphate dosage is the 6% of impregnation cotton quality, and the bath raio of impregnation cotton fiber and copper-bath is 1：30.
A kind of 5. preparation method of Multifunctional composite fabric as claimed in claim 1, it is characterised in that step（5）Described in
Baking processing be by fabric at 120~130 DEG C 30~40s of preliminary drying, then at 100~110 DEG C toast 30~40s sizing.
A kind of 6. preparation method of Multifunctional composite fabric as claimed in claim 1, it is characterised in that step（6）Described in
The mass ratio of functional fabric and TPUE is 1：1.
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Cited By (5)
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| CN110158315A (en) * | 2019-05-27 | 2019-08-23 | 安徽工程大学 | A kind of preparation method of poly-dopamine schemochrome film |
| CN110629552A (en) * | 2019-09-30 | 2019-12-31 | 韩建华 | Dopamine applied to antibacterial fabric and method for preparing antibacterial fabric |
| CN112267298A (en) * | 2020-10-28 | 2021-01-26 | 苏州健雄职业技术学院 | Preparation method of hydrophobic cotton fabric and hydrophobic cotton |
| CN114959999A (en) * | 2022-06-07 | 2022-08-30 | 东华大学 | Preparation method of antibacterial spring and summer elastic fabric containing Porel fibers |
| CN115247307A (en) * | 2022-08-29 | 2022-10-28 | 安徽东锦服饰有限公司 | Preparation method of breathable blended fabric |
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| CN110629552A (en) * | 2019-09-30 | 2019-12-31 | 韩建华 | Dopamine applied to antibacterial fabric and method for preparing antibacterial fabric |
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| CN114959999A (en) * | 2022-06-07 | 2022-08-30 | 东华大学 | Preparation method of antibacterial spring and summer elastic fabric containing Porel fibers |
| CN114959999B (en) * | 2022-06-07 | 2023-10-20 | 东华大学 | Preparation method of antibacterial spring Xia Danli fabric containing Portel fibers |
| CN115247307A (en) * | 2022-08-29 | 2022-10-28 | 安徽东锦服饰有限公司 | Preparation method of breathable blended fabric |
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Effective date of registration: 20180423 Address after: 213000 Room 201, unit 62, 62 new cool village, Tianning District, Jiangsu Applicant after: Li Zhang Address before: 213102 No. 3, blue harbour garden, Xinbei District, Changzhou, Jiangsu, China 305 Applicant before: Changzhou Tong Biao Trading Co., Ltd. |
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