CN107523263A - A kind of anti-sticking increasing stick damping glue and preparation method thereof - Google Patents
A kind of anti-sticking increasing stick damping glue and preparation method thereof Download PDFInfo
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- CN107523263A CN107523263A CN201710871990.XA CN201710871990A CN107523263A CN 107523263 A CN107523263 A CN 107523263A CN 201710871990 A CN201710871990 A CN 201710871990A CN 107523263 A CN107523263 A CN 107523263A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J195/00—Adhesives based on bituminous materials, e.g. asphalt, tar, pitch
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/04—Non-macromolecular additives inorganic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/08—Macromolecular additives
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J161/00—Adhesives based on condensation polymers of aldehydes or ketones; Adhesives based on derivatives of such polymers
- C09J161/04—Condensation polymers of aldehydes or ketones with phenols only
- C09J161/06—Condensation polymers of aldehydes or ketones with phenols only of aldehydes with phenols
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J193/00—Adhesives based on natural resins; Adhesives based on derivatives thereof
- C09J193/04—Rosin
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/24—Acids; Salts thereof
- C08K3/26—Carbonates; Bicarbonates
- C08K2003/265—Calcium, strontium or barium carbonate
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Inorganic Chemistry (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
A kind of anti-sticking increasing stick damping glue and preparation method thereof, is related to damping material production field.A kind of anti-sticking increasing stick damping glue, mainly it is kneaded and is formed by raw material, raw material includes:The parts by weight of pitch 30 40, the parts by weight of softening agent 5 12, the parts by weight of inorganic filler 15 25 and the parts by weight of tackifying resin 32 40.Anti-sticking increasing stick damping glue has anti-sticking effect before heating melts, and has preferably viscosity after heating, can be snugly fine with other objects.
Description
Technical field
The present invention relates to damping material production field, and more particularly to a kind of anti-sticking increasing stick damping glue and preparation method thereof.
Background technology
Damping material is the material that mechanical vibrational energy can be changed into heat energy and dissipated.It is mainly used in control vibration and makes an uproar
Sound.The damping and amortization of material can be weighed according to the ability of its dissipation vibrational energy.Car is during traveling, because the vibration meeting of car
Larger noise is produced, mainly controls noise with automobile-used damp film at present.But existing damp film generally exist into
It is easy to stick after type, during use viscosity it is insufficient the defects of.
The content of the invention
It is an object of the invention to provide a kind of anti-sticking increasing stick damping glue, and it has anti-sticking effect before heating melts,
There is preferably viscosity after heating, can be snugly fine with other objects.
Another object of the present invention is to provide a kind of preparation method of anti-sticking increasing stick damping glue, its technique is simple, operation
It is easy.
The present invention is solved its technical problem and realized using following technical scheme.
The present invention proposes a kind of anti-sticking increasing stick damping glue, is mainly kneaded and formed by raw material, raw material includes:Pitch 30-40 weights
Measure part, softening agent 5-12 parts by weight, inorganic filler 15-25 parts by weight and tackifying resin 32-40 parts by weight.
A kind of preparation method of anti-sticking increasing stick damping glue described above, including:Raw material is blended in 75-90 DEG C of temperature strip
10-60min is kneaded under part.
The beneficial effect of the embodiment of the present invention is:The drip of 30-40 parts by weight is contained in the raw material of anti-sticking increasing stick damping glue
Green grass or young crops, the softening agent of 5-12 parts by weight, the tackifying resin of the inorganic filler of 15-25 parts by weight and 32-40 parts by weight, it is each in raw material
Component proportion is suitable, material based on pitch, ensure that the stickiness of anti-sticking increasing stick damping glue, and tackifying resin causes anti-sticking increasing stick
The stickiness of damping glue is more preferable, and inorganic filler agent can improve the case hardness and bending strength of anti-sticking increasing stick damping glue, improve it
The function of anti-sticking increasing stick.Softening agent, it can be uniformly dispersed between each raw material for anti-sticking increasing stick damping glue, reduce mixing
Power consumption, the plasticity, mobility and adherence of sizing material can be increased.Last obtained anti-sticking increasing stick damping glue heating melting
There is anti-sticking effect before, there is preferably viscosity after heating, can be snugly fine with other objects.
A kind of preparation method of anti-sticking increasing stick damping glue, including:Raw material is blended under 75-90 DEG C of temperature conditionss and be kneaded
10-60min.The technique of the preparation method is simple, easy to operate.
Embodiment
, below will be in the embodiment of the present invention to make the purpose, technical scheme and advantage of the embodiment of the present invention clearer
Technical scheme be clearly and completely described.Unreceipted actual conditions person, builds according to normal condition or manufacturer in embodiment
The condition of view is carried out.Agents useful for same or the unreceipted production firm person of instrument, it is the conventional production that can be obtained by commercially available purchase
Product.
A kind of anti-sticking increasing stick damping glue of the embodiment of the present invention and preparation method thereof is specifically described below.
A kind of anti-sticking increasing stick damping glue, mainly it is kneaded and is formed by raw material, raw material includes:Pitch 30-40 parts by weight, softening agent
5-12 parts by weight, inorganic filler 15-25 parts by weight and tackifying resin 32-40 parts by weight.
Pitch, the dark brown COMPLEX MIXED being made up of the hydrocarbon and its non metallic derivatives of different molecular weight
Thing, it is one kind of high viscosity organic liquid, is in a liquid state, surface is in black.Raw material by the use of pitch as anti-sticking increasing stick damping glue, tool
Having increases the sticky function of anti-sticking increasing stick damping glue.
Softening agent, it can be uniformly dispersed between each raw material for anti-sticking increasing stick damping glue, the power for reducing mixing disappears
Consumption, the plasticity, mobility and adherence of sizing material can be increased.In addition, softening agent, also cry filling oil, processing oil, operation it is oily,
Rubber oil, friction oil.
Further, softening agent includes at least one of coumarone indene resin and silicone oil.
Coumarone indene resin, it is thick liquid or solid.Coumarone indene resin is compounded with pitch, and anti-sticking increasing stick can be caused to hinder
Buddhist nun's glue has preferably viscosity.Meanwhile coumarone indene resin can play softening, reinforcement, scattered work for anti-sticking increasing stick damping glue
With so as to improve the processing characteristics of anti-sticking increasing stick damping glue.
Silicone oil, refer to keeping the linear polysiloxanes product of liquid condition at room temperature.It has higher heat resistance,
Water resistance and less surface tension.It can improve the mobility and plasticity of anti-sticking increasing stick damping glue, improve its processability
Energy.
In some embodiments of the invention, it is 1 that softening agent, which includes weight ratio,:1-3 coumarone indene resin and silicone oil.
Compounded by the coumarone indene resin and silicone oil of the ratio, can make it that the performance of anti-sticking increasing stick damping glue is more preferable.
Inorganic filler is used for anti-sticking increasing stick damping glue, is mainly used in improving the performance of anti-sticking increasing stick damping glue.It can be improved
The case hardness of anti-sticking increasing stick damping glue, and improve the bending strength of anti-sticking increasing stick damping glue.
In some embodiments of the invention, inorganic filler includes coarse whiting, coarse whiting namely powdered whiting, powdered whiting
The volume of anti-sticking increasing stick damping glue can be increased, reduce cost, improve the shrinkage factor of anti-sticking increasing stick damping glue, improve dimensionally stable
Property.Improve anti-slotting wound property, the smoothness of anti-sticking increasing stick damping glue.To the toughening effect of notched Izod impact hit intensity and it was kneaded simultaneously
There is obvious effect in terms of viscosity flow in journey.
Further, in some embodiments of the invention, inorganic filler also includes talcum powder.
The main component of talcum powder is water magnesium silicate, and the crystal structure of talcum powder is in stratiform, has special lubricity.Separately
Outside, talcum powder have it is anti-sticking, help the characteristics of stream, fire resistance, acid-resisting, insulating properties soft and strong adsorption force.Talcum powder is used as anti-
The filler of viscous increasing stick damping glue can increase the function of its anti-sticking increasing stick, and can improve the hardness and chi of anti-sticking increasing stick damping glue
Very little stability, prevents high-temerature creep.
Further, in some embodiments of the invention, the weight of talcum powder and coarse whiting ratio is 3-6:1.
Inorganic filler of the talcum powder and coarse whiting of the ratio as anti-sticking increasing stick damping glue, anti-sticking increasing stick can be caused to damp
The performance of glue is more preferable.
Tackifying resin, it is mainly used in improving the stickiness of the inorganic filler of anti-sticking increasing stick damping glue.For example, it may be rosin,
Alkyl phenolic resin and xylene resin etc..
The anti-sticking increasing stick damping glue of the present invention, the softening of the pitch, 5-12 parts by weight of 30-40 parts by weight is contained in raw material
The tackifying resin of agent, the inorganic filler of 15-25 parts by weight and 32-40 parts by weight, each group distribution ratio is suitable in raw material, and pitch is made
Based on material, ensure that the stickiness of anti-sticking increasing stick damping glue, tackifying resin make it that the stickiness of anti-sticking increasing stick damping glue is more preferable, nothing
Machine packing agent can improve the case hardness and bending strength of anti-sticking increasing stick damping glue, improve the function of its anti-sticking increasing stick.Softening
Agent, it can be uniformly dispersed between each raw material for anti-sticking increasing stick damping glue, reduce the power consumption of mixing, glue can be increased
Plasticity, mobility and the adherence of material.There is anti-sticking effect before last obtained anti-sticking increasing stick damping glue heating melting,
There is preferably viscosity after heating, can be snugly fine with other objects.
The present invention also provides a kind of preparation method of anti-sticking increasing stick damping glue, including:Raw material is blended in 75-90 DEG C of temperature
10-60min is kneaded under the conditions of degree.The technique of the preparation method is simple, easy to operate.
The feature and performance of the present invention are described in further detail with reference to embodiments.
Embodiment 1
The present embodiment provides a kind of anti-sticking increasing stick damping glue, and it is mainly kneaded by raw material and formed.Wherein, raw material includes:Drip
Blue or green 35 parts by weight, the parts by weight of softening agent 10, the parts by weight of coarse whiting 20 and the parts by weight of tackifying resin 35.
The preparation method of the anti-sticking increasing stick damping glue, including:Peace weighs raw material according to above-mentioned parts by weight, then by pitch, soft
Agent, coarse whiting and tackifying resin are blended under 85 DEG C of temperature conditionss and are kneaded 30min.
Embodiment 2
The present embodiment provides a kind of anti-sticking increasing stick damping glue, and it is mainly kneaded by raw material and formed, wherein, raw material includes:Drip
Blue or green 32 parts by weight, the parts by weight of coumarone indene resin 5, the parts by weight of coarse whiting 15 and the parts by weight of tackifying resin 32.
The preparation method of the anti-sticking increasing stick damping glue, including:Peace weighs raw material according to above-mentioned parts by weight, then by pitch, Gu
The grand resin of horse, coarse whiting and tackifying resin are blended under 80 DEG C of temperature conditionss and are kneaded 40min.
Embodiment 3
The present embodiment provides a kind of anti-sticking increasing stick damping glue, and it is mainly kneaded by raw material and formed, and raw material includes:The weight of pitch 34
Measure part, the parts by weight of coumarone indene resin 2, the parts by weight of silicone oil 4, the parts by weight of talcum powder 18 and the parts by weight of tackifying resin 34.
The preparation method of the anti-sticking increasing stick damping glue, including:Peace weighs raw material according to above-mentioned parts by weight, then by pitch, Gu
The grand resin of horse, silicone oil, talcum powder and tackifying resin are blended under 75 DEG C of temperature conditionss and are kneaded 60min.
Embodiment 4
The present embodiment provides a kind of anti-sticking increasing stick damping glue, and it is mainly kneaded by raw material and formed, and raw material includes:The weight of pitch 38
Measure part, the parts by weight of silicone oil 7, the parts by weight of coarse whiting 12, the parts by weight of talcum powder 4 and the parts by weight of tackifying resin 36.
The preparation method of the anti-sticking increasing stick damping glue, including:Peace weighs raw material according to above-mentioned parts by weight, then by pitch, silicon
Oil, coarse whiting, talcum powder and tackifying resin are blended under 75 DEG C of temperature conditionss and are kneaded 60min.
Embodiment 5
The present embodiment provides a kind of anti-sticking increasing stick damping glue, and it is mainly kneaded by raw material and formed, and raw material includes:The weight of pitch 35
Measure part, the parts by weight of coumarone indene resin 5, the parts by weight of silicone oil 5, the parts by weight of coarse whiting 25 and the parts by weight of tackifying resin 38.
The preparation method of the anti-sticking increasing stick damping glue, including:Peace weighs raw material according to above-mentioned parts by weight, then by pitch, Gu
The grand resin of horse, silicone oil, coarse whiting and tackifying resin are blended under 90 DEG C of temperature conditionss and are kneaded 10min.
Embodiment 6
The present embodiment provides a kind of anti-sticking increasing stick damping glue, and it is mainly kneaded by raw material and formed, and raw material includes:The weight of pitch 30
Measure part, the parts by weight of coumarone indene resin 2, the parts by weight of silicone oil 6, the parts by weight of coarse whiting 16, the parts by weight of talcum powder 4 and the weight of tackifying resin 33
Measure part.
The preparation method of the anti-sticking increasing stick damping glue, including:Peace weighs raw material according to above-mentioned parts by weight, then by pitch, Gu
The grand resin of horse, silicone oil, coarse whiting, talcum powder and tackifying resin are blended under 85 DEG C of temperature conditionss and are kneaded 40min.
Embodiment 7
The present embodiment provides a kind of anti-sticking increasing stick damping glue, and it is mainly kneaded by raw material and formed, and raw material includes:The weight of pitch 40
Measure part, the parts by weight of coumarone indene resin 3, the parts by weight of silicone oil 9, the parts by weight of coarse whiting 20, the parts by weight of talcum powder 4 and the weight of tackifying resin 37
Measure part.
The preparation method of the anti-sticking increasing stick damping glue, including:Peace weighs raw material according to above-mentioned parts by weight, then by pitch, Gu
The grand resin of horse, silicone oil, coarse whiting, talcum powder and tackifying resin are blended under 83 DEG C of temperature conditionss and are kneaded 20min.
Embodiment 8
The present embodiment provides a kind of anti-sticking increasing stick damping glue, and it is mainly kneaded by raw material and formed, and raw material includes:The weight of pitch 37
Measure part, the parts by weight of silicone oil 9, the parts by weight of coarse whiting 18, the parts by weight of talcum powder 3 and the parts by weight of tackifying resin 40.
The preparation method of the anti-sticking increasing stick damping glue, including:Peace weighs raw material according to above-mentioned parts by weight, then by pitch, silicon
Oil, coarse whiting, talcum powder and tackifying resin are blended under 78 DEG C of temperature conditionss and are kneaded 45min.
Embodiment 9
The present embodiment provides a kind of anti-sticking increasing stick damping glue, and it is mainly kneaded by raw material and formed, and raw material includes:The weight of pitch 36
Measure part, the parts by weight of coumarone indene resin 4, the parts by weight of silicone oil 7, the parts by weight of coarse whiting 17, the parts by weight of talcum powder 5 and the weight of tackifying resin 39
Measure part.
The preparation method of the anti-sticking increasing stick damping glue, including:Peace weighs raw material according to above-mentioned parts by weight, then by pitch, Gu
The grand resin of horse, silicone oil, coarse whiting, talcum powder and tackifying resin are blended under 88 DEG C of temperature conditionss and are kneaded 20min.
In summary, a kind of anti-sticking increasing stick damping glue of the embodiment of the present invention, 30-40 parts by weight are contained in its raw material
Pitch, the softening agent of 5-12 parts by weight, the tackifying resin of the inorganic filler of 15-25 parts by weight and 32-40 parts by weight, in raw material
Each group distribution ratio is suitable, material based on pitch, ensure that the stickiness of anti-sticking increasing stick damping glue, and tackifying resin causes anti-sticking increasing
The stickiness of glutinous damping glue is more preferable, and inorganic filler agent can improve the case hardness and bending strength of anti-sticking increasing stick damping glue, improves
The function of its anti-sticking increasing stick.It softening agent, can be uniformly dispersed between each raw material for anti-sticking increasing stick damping glue, reduce and be kneaded
Power consumption, the plasticity, mobility and adherence of sizing material can be increased.Last obtained anti-sticking increasing stick damping glue heating is molten
There is anti-sticking effect before melting, there is preferably viscosity after heating, can be snugly fine with other objects.
Embodiments described above is part of the embodiment of the present invention, rather than whole embodiments.The reality of the present invention
The detailed description for applying example is not intended to limit the scope of claimed invention, but is merely representative of the selected implementation of the present invention
Example.Based on the embodiment in the present invention, what those of ordinary skill in the art were obtained under the premise of creative work is not made
Every other embodiment, belongs to the scope of protection of the invention.
Claims (10)
1. a kind of anti-sticking increasing stick damping glue, it is characterised in that be mainly kneaded and formed by raw material, the raw material includes:Pitch 30-40
Parts by weight, softening agent 5-12 parts by weight, inorganic filler 15-25 parts by weight and tackifying resin 32-40 parts by weight.
2. anti-sticking increasing stick damping glue according to claim 1, it is characterised in that the pitch is 32-38 parts by weight, described
Softening agent is 6-10 parts by weight, and the inorganic filler is 18-24 parts by weight, and the tackifying resin is 35-38 parts by weight.
3. anti-sticking increasing stick damping glue according to claim 2, it is characterised in that the pitch is 35 parts by weight, described soft
Agent is 10 parts by weight, and the inorganic filler is 20 parts by weight, and the tackifying resin is 35 parts by weight.
4. the anti-sticking increasing stick damping glue according to claim any one of 1-3, it is characterised in that the softening agent includes ancient horse
At least one of grand resin and silicone oil.
5. anti-sticking increasing stick damping glue according to claim 4, it is characterised in that it is 1 that the softening agent, which includes weight ratio,:1-
3 coumarone indene resin and silicone oil.
6. the anti-sticking increasing stick damping glue according to claim any one of 1-3, it is characterised in that the inorganic filler includes weight
Calcium.
7. anti-sticking increasing stick damping glue according to claim 6, it is characterised in that the inorganic filler also includes talcum powder.
8. anti-sticking increasing stick damping glue according to claim 7, it is characterised in that the weight of the talcum powder and the coarse whiting
Than for 3-6:1.
A kind of 9. preparation method of anti-sticking increasing stick damping glue as described in claim any one of 1-8, it is characterised in that including:
The raw material is blended under 75-90 DEG C of temperature conditionss and is kneaded 10-60min.
10. the preparation method of anti-sticking increasing stick damping glue according to claim 9, it is characterised in that melting temperature 80-85
℃。
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN108753247A (en) * | 2018-05-29 | 2018-11-06 | 滁州君越高分子新材料有限公司 | A kind of preparation method of insulating cement |
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WO2008078856A2 (en) * | 2006-12-27 | 2008-07-03 | Industry-University Cooperation Foundation, Hanyang University | Damping composition for reducing of light and heavy impact sound through between stories and a method of preparation thereof |
CN104194367A (en) * | 2014-09-12 | 2014-12-10 | 广州市恩威曲新材料有限公司 | Damping, shock-absorption and acoustic-damping material as well as preparation method and application thereof |
CN107141824A (en) * | 2017-05-31 | 2017-09-08 | 马鞍山联洪合成材料有限公司 | A kind of composite hot-melt damping piece and its processing method |
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2017
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Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2008078856A2 (en) * | 2006-12-27 | 2008-07-03 | Industry-University Cooperation Foundation, Hanyang University | Damping composition for reducing of light and heavy impact sound through between stories and a method of preparation thereof |
CN104194367A (en) * | 2014-09-12 | 2014-12-10 | 广州市恩威曲新材料有限公司 | Damping, shock-absorption and acoustic-damping material as well as preparation method and application thereof |
CN107141824A (en) * | 2017-05-31 | 2017-09-08 | 马鞍山联洪合成材料有限公司 | A kind of composite hot-melt damping piece and its processing method |
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