CN107510624A - A kind of adsorbed film - Google Patents
A kind of adsorbed film Download PDFInfo
- Publication number
- CN107510624A CN107510624A CN201710740819.5A CN201710740819A CN107510624A CN 107510624 A CN107510624 A CN 107510624A CN 201710740819 A CN201710740819 A CN 201710740819A CN 107510624 A CN107510624 A CN 107510624A
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- CN
- China
- Prior art keywords
- fulvic acid
- adsorbed film
- nano kaoline
- selenoprotein
- thioredoxin reductase
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/66—Enzymes
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/26—Aluminium; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/965—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of inanimate origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/008—Preparations for oily skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Dermatology (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a kind of adsorbed film, and it includes the composition of following mass percent：Fulvic acid 0.1%~2%, selenoprotein thioredoxin reductase 0.01%~0.4%, nano kaoline 0.02%~0.05%, ethanol 4~8%, polyvinyl alcohol 5~10%, acrylic acid (ester) analog copolymer 0.1~0.2%, propane diols 3~4%, allantoin 0.2~0.3%, the rilanit specials 1~5% of PEG 50, Bis(hydroxymethyl)imidazolidinyl urea 0.15~0.25%, Phenoxyethanol 0.2~0.5%, Sensiva SC50 0.4~0.8%, iodine propilolic alcohol butyl mephenesin Carbamate 0.01~0.05%, methyl hydroxybenzoate 0.05~0.25%, deionized water surplus.Long-term use of collapsible pore of the adsorbed film, while can also improve skin microcirculation, and be able to maintain that intracellular redox state, regulation cell growth, propagation, removes the peroxide inside human body, skin is got well state.
Description
Technical field
The present invention relates to cosmetic field, and in particular to a kind of adsorbed film.
Background technology
Humic acid material is a kind of natural macromolecular organic matter, including fulvic acid, humic acid or humic acid, humic acid,
It is widely present in water body and soil.Humus accounts for half of contained total amount of organic or so in general water body, and what is had is reachable
80%, wherein fulvic acid accounts for 83-90%, and humic acid or humic acid account for 3-4%, and humic acid accounts for 7-13%.Thus fulvic acid is water
The main body of humus in body.Fulvic acid surface includes substantial amounts of active group, and fulvic acid is based on aromatic group, containing a large amount of
Hydroxyl, carboxyl, carbonyl.These functional structures contribute to fulvic acid to be complexed with heavy metal ion.In addition, fulvic acid surface band
There is larger elecrtonegativity, the series reaction between fulvic acid and heavy metal ion can be promoted.By fulvic acid and selenoprotein-sulphur oxygen also
Reductase proteins, nano kaoline composite usage have the work(such as cleaning skin, regulation fat secretion, anti-oxidant in cosmetics
Effect.
The content of the invention
It is an object of the invention to provide a kind of adsorbed film, and it has the work(such as cleaning skin, regulation fat secretion, anti-oxidant
Effect, long-term use can make skin keep fit state.
To achieve the above object, the present invention adopts the following technical scheme that：
A kind of adsorbed film includes three kinds of fulvic acid, selenoprotein-thioredoxin reductase, nano kaoline compositions, its
Mass percent is as follows：
Fulvic acid：0.1%~2%
Selenoprotein-thioredoxin reductase：0.01%~0.4%
Nano kaoline：0.02%~0.05%.
Preferably, described fulvic acid, selenoprotein-thioredoxin reductase, nano kaoline mass percent such as
Under：
Fulvic acid：0.7%~1.5%
Selenoprotein-thioredoxin reductase：0.2%~0.3%
Nano kaoline：0.03%~0.04%.
It is optimal, described fulvic acid, selenoprotein-thioredoxin reductase, nano kaoline mass percent such as
Under：
Fulvic acid：1%
Selenoprotein-thioredoxin reductase：0.25%
Nano kaoline：0.04%.
Further, described fulvic acid is prepared as follows：The water body containing fulvic acid is gathered, by 1:1
Na4P207, NaOH mixed extract extract, and adjust pH to 7.5 after fully removing impurity and freeze-drying obtains fulvic acid.
Further, described nano kaoline is prepared as follows：Cryptocrystalline kaolinite clay raw material, add water and
Dispersant is stirred, and mud is made；Mud carries out magnetic separation by high gradient magnetic separator；By the mud adjustment pH value after magnetic separation extremely
2.5~4.8, add reducing agent and chelating agent is stirred, react after terminating through being dehydrated, washing and obtaining filter cake；By above-mentioned washing
Filter cake afterwards adds water that slurry is made, and then stirring adds surfactant；Broken up after drying, obtain nano kaoline, its pine
Bulk density is 0.04g/cm3~0.08g/cm3, and average thickness is 25 nanometers~65 nanometers, and average diameter is 450 nanometers~780
Nanometer.
Further, described adsorbed film also includes the composition of following mass percent：Ethanol 4~8%, polyvinyl alcohol 5
~10%, acrylic acid (ester) analog copolymer 0.1~0.2%, propane diols 3~4%, allantoin 0.2~0.3%, PEG-50 hydrogenations
Castor oil 1~5%, Bis(hydroxymethyl)imidazolidinyl urea 0.15~0.25%, Phenoxyethanol 0.2~0.5%, Sensiva SC50
0.4~0.8%, iodine propilolic alcohol butyl mephenesin Carbamate 0.01~0.05%, methyl hydroxybenzoate 0.05~0.25%, more than deionized water
Amount.
It is the device have the advantages that as follows：Adsorbed film of the present invention, mainly by fulvic acid, selenoprotein-thioredoxin
Reductase, nano kaoline form in specific proportions, toxin expelling, absorption heavy metal are carried out by fulvic acid, than common adsorbed film
With more adsorption capacity, while nano kaoline and can enough adsorbs skin surface dirt and fixed contents of many kinds of heavy metal ion, to sweat
The dirt and toxin of pore do deep layer cleaning, and can oil suction, draw the grease of skin hypersecretion, reduce pore；Selenium egg
The peroxide of internal body is capable of in the addition of in vain-thioredoxin reductase, can also with many protein bindings in cell,
Participate in the growth of regulating cell and suppress Apoptosis, so that skin and can during pore is reduced enough improves skin.
The collapsible pore of long-term use of adsorbed film, while skin microcirculation can also be improved, and it is able to maintain that intracellular oxidation also
Original state, regulation cell growth, propagation, removes the peroxide inside human body, skin is got well state.
Embodiment
Below in conjunction with specific embodiment, the present invention is further elaborated：
The adsorbed film embodiment 1~5 of the present invention is formulated, and is shown in Table 1.
Table 1
1st, the preparation method of the fulvic acid in the present invention is as follows：
The water body containing fulvic acid is gathered, by 1:1 Na4P207, NaOH mixed extracts extraction, fully remove impurity after
Adjust pH to 7.5 and be freeze-dried and obtain fulvic acid.
2nd, the preparation method of the nano kaoline in the present invention is as follows：
Cryptocrystalline kaolinite clay raw material, adds water and dispersant is stirred, and mud is made；Mud passes through High-gradient Magnetic
Machine is selected to carry out magnetic separation；Mud after magnetic separation is adjusted into pH value to 2.5~4.8, reducing agent is added and chelating agent is stirred, instead
Through being dehydrated, washing and obtaining filter cake after should terminating；Add water that slurry is made the filter cake after above-mentioned washing, then stirring adds surface-active
Agent；Broken up after drying, obtain nano kaoline, its loose thickness is 0.04g/cm3~0.08g/cm3, average thickness 25
Nanometer~65 nanometers, average diameter are 450 nanometers~780 nanometers.
Comparative example 1：
Difference with embodiment 3 is only to be free of fulvic acid, and remaining each group material addition, preparation does not change with technique.
Comparative example 2：
Only Selenonic protein-thioredoxin reductase, remaining each group material do not add for difference with embodiment 3, prepare
Do not changed with technique.
Comparative example 3：
Difference with embodiment 3 is only to be free of nano kaoline, and remaining each group material addition, preparation does not change with technique
Become.
Comparative example 4：
Difference with embodiment 3 is only to be free of 3 kinds of fulvic acid, selenoprotein-thioredoxin reductase and nano kaoline
Composition, the addition of remaining each group material, preparation do not change with technique.Efficacy validation：
Adsorb heavy metal plan-validation：The film liquid of embodiment 1-5 and comparative example 1-3 adsorbed film is prepared, by film liquid, sulfuric acid
Copper solution is with 0.1mg/L:10mmol/L proportioning is added in 10ml centrifuge tubes, and it is 7 to adjust its ph with PBS solution, is shaken at room temperature
12h is swung, is centrifuged, the lead nitrate solution of equivalent, nitric acid cadmium solution, nitric acid mercury solution is separately added into and carries out adsorption test,
20min, 40min, 60min measure absorption of the test agent for the adsorption capacity, the adsorption capacity of cadmium ion, mercury ion of lead ion
Ability, as a result such as table 2 below.
Table 2
From table 2 it can be seen that film liquid corresponding to embodiment 1-5 has the characteristic of adsorbing heavy metal cadmium, lead, mercury, comparative example 1-3
Because lacking fulvic acid, selenoprotein-thioredoxin reductase, nano kaoline any one therein, cause film liquid absorption affinity poor,
Comparative example 4 does not add 3 kinds of fulvic acid, selenoprotein-thioredoxin reductase, nano kaoline compositions, the absorption of heavy metal
For 0, illustrating the product heavy metal of the present invention plays the role of conspicuousness.
The effect of in order to further verify adsorbed film of the present invention, choose embodiment 1~5 and comparative example 1~4 carries out tune on probation
Look into and evaluation test.
Embodiment is as follows：Every group of 30 people are chosen to be tested.Product 22-24 every night corresponding to experimenter's use
Using corresponding trial target between point, each sampling phase is one month, and at the 30th day, experimenter was to absorption heavy metal effect
Fruit carries out self-appraisal, the cleannes of adsorbed film carry out self-appraisal, the improvement of pore carries out self-appraisal；Whole people complete whole during experiment
Individual experiment, other any skin-protection products must not be used in experimentation.
Object on probation：Trier's health is all right, without lactation or pregnancy period, shows as face after heavy metal poisoning
Allergy, long spot, redness, the thick crowd of pore.
Using the clinical evaluation of skin quality, the result of the test of heavy metal is adsorbed, cleannes are tested, pore improves result such as
Table 3 below.
Table 3
As can be seen from Table 3, for face's allergy caused by heavy metal, long spot, it is red and swollen the problem of, the composition of embodiment has
Obvious improvement result, and in comparative example because lack fulvic acid, selenoprotein-thioredoxin reductase, nano kaoline one
Kind is a variety of, causes DeGrain, or even to no effect, it is seen that functional component synergy of the present invention；Pore can be improved in addition
Environment, Sage Extract, effectively improves skin indirectly, maintains skin health.
Above example is merely to illustrate embodiment of the present invention, does not have any formal limit to the present invention
System；It is any to be engaged in professional and technical personnel, all have the ability using the technology contents having revealed that, some are made to it and changes or repaiies
Decorations, turn into the equivalent embodiment of equivalent variations.According to the technology of the present invention essence, simply modification, equivalent variations are carried out to the present invention
With modification, belong in the range of technical solution of the present invention.
Claims (6)
- A kind of 1. adsorbed film, it is characterised in that described adsorbed film include fulvic acid, selenoprotein-thioredoxin reductase, Three kinds of compositions of nano kaoline, its mass percent are as follows：Fulvic acid：0.1%~2%Selenoprotein-thioredoxin reductase：0.01%~0.4%Nano kaoline：0.02%~0.05%.
- 2. a kind of adsorbed film according to claim 1, it is characterised in that described fulvic acid, selenoprotein-thioredoxin Reductase, the mass percent of nano kaoline are as follows：Fulvic acid：0.7%~1.5%Selenoprotein-thioredoxin reductase：0.2%~0.3%Nano kaoline：0.03%~0.04%.
- 3. a kind of adsorbed film according to claim 2, it is characterised in that described fulvic acid, selenoprotein-thioredoxin Reductase, the mass percent of nano kaoline are as follows：Fulvic acid：1%Selenoprotein-thioredoxin reductase：0.25%Nano kaoline：0.04%.
- 4. a kind of adsorbed film according to any one of claims 1 to 3, it is characterised in that described fulvic acid presses such as lower section It is prepared by method：The water body containing fulvic acid is gathered, by 1:1 Na4P207, NaOH mixed extracts extraction, fully remove impurity after adjust Save pH to 7.5 and be freeze-dried and obtain fulvic acid.
- 5. a kind of adsorbed film according to any one of claims 1 to 3, it is characterised in that described nano kaoline is by such as It is prepared by lower section method：Cryptocrystalline kaolinite clay raw material, adds water and dispersant is stirred, and mud is made；Mud passes through high ladder Spend magnetic separator and carry out magnetic separation；Mud after magnetic separation is adjusted into pH value to 2.5~4.8, reducing agent is added and chelating agent is stirred Mix, react after terminating through being dehydrated, washing and obtaining filter cake；Add water that slurry is made the filter cake after above-mentioned washing, then stirring adds table Face activating agent；Broken up after drying, obtain nano kaoline, its loose thickness is 0.04g/cm3~0.08g/cm3, average thickness Spend for 25 nanometers~65 nanometers, average diameter is 450 nanometers~780 nanometers.
- 6. a kind of adsorbed film according to any one of Claims 1 to 5, it is characterised in that described adsorbed film is also included such as The composition of lower mass percent：Ethanol 4~8%, polyvinyl alcohol 5~10%, acrylic acid (ester) analog copolymer 0.1~0.2%, third Glycol 3~4%, allantoin 0.2~0.3%, PEG-50 rilanit specials 1~5%, Bis(hydroxymethyl)imidazolidinyl urea 0.15~ 0.25%th, Phenoxyethanol 0.2~0.5%, Sensiva SC50 0.4~0.8%, iodine propilolic alcohol butyl mephenesin Carbamate 0.01~ 0.05%th, methyl hydroxybenzoate 0.05~0.25%, deionized water surplus.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710740819.5A CN107510624A (en) | 2017-08-24 | 2017-08-24 | A kind of adsorbed film |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710740819.5A CN107510624A (en) | 2017-08-24 | 2017-08-24 | A kind of adsorbed film |
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| CN107510624A true CN107510624A (en) | 2017-12-26 |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1510088A (en) * | 2002-12-24 | 2004-07-07 | 中国矿业大学（北京校区） | Nanometer kaolinite powder and preparing method thereof |
| CN104684568A (en) * | 2012-11-13 | 2015-06-03 | 株式会社爱茉莉太平洋 | Composition for external use skin preparation, containing thioredoxin |
| CN105534872A (en) * | 2016-02-22 | 2016-05-04 | 太仓市荣德生物技术研究所 | Kaolin cleaning facial mask |
| CN106726655A (en) * | 2015-12-31 | 2017-05-31 | 营口富里泥炭科技有限公司 | A kind of nanoscale fulvic acid peat facial mask and preparation method thereof |
| CN106745020A (en) * | 2016-12-09 | 2017-05-31 | 湖南御家化妆品制造有限公司 | High oil-absorbing kaolin and its preparation method and application |
-
2017
- 2017-08-24 CN CN201710740819.5A patent/CN107510624A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1510088A (en) * | 2002-12-24 | 2004-07-07 | 中国矿业大学（北京校区） | Nanometer kaolinite powder and preparing method thereof |
| CN104684568A (en) * | 2012-11-13 | 2015-06-03 | 株式会社爱茉莉太平洋 | Composition for external use skin preparation, containing thioredoxin |
| CN106726655A (en) * | 2015-12-31 | 2017-05-31 | 营口富里泥炭科技有限公司 | A kind of nanoscale fulvic acid peat facial mask and preparation method thereof |
| CN105534872A (en) * | 2016-02-22 | 2016-05-04 | 太仓市荣德生物技术研究所 | Kaolin cleaning facial mask |
| CN106745020A (en) * | 2016-12-09 | 2017-05-31 | 湖南御家化妆品制造有限公司 | High oil-absorbing kaolin and its preparation method and application |
Non-Patent Citations (1)
| Title |
|---|
| 黄开勋 等: "《硒的化学、生物化学及其在生命科学中的应用 第二版》", 30 June 2009, 华中科技大学出版社 * |
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Application publication date: 20171226 |
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