CN107503164A - Seamless fine nonwoven fabric base wall paper of length and preparation method thereof - Google Patents
Seamless fine nonwoven fabric base wall paper of length and preparation method thereof Download PDFInfo
- Publication number
- CN107503164A CN107503164A CN201710722137.1A CN201710722137A CN107503164A CN 107503164 A CN107503164 A CN 107503164A CN 201710722137 A CN201710722137 A CN 201710722137A CN 107503164 A CN107503164 A CN 107503164A
- Authority
- CN
- China
- Prior art keywords
- wall paper
- nonwoven fabric
- base wall
- fabric base
- length
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
- D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
- D06N3/04—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D—PROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D1/00—Processes for applying liquids or other fluent materials
- B05D1/16—Flocking otherwise than by spraying
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
- D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
- D06N3/0002—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof characterised by the substrate
- D06N3/0011—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof characterised by the substrate using non-woven fabrics
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
- D06N2209/00—Properties of the materials
- D06N2209/10—Properties of the materials having mechanical properties
- D06N2209/103—Resistant to mechanical forces, e.g. shock, impact, puncture, flexion, shear, compression, tear
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
- D06N2209/00—Properties of the materials
- D06N2209/16—Properties of the materials having other properties
- D06N2209/1671—Resistance to bacteria, mildew, mould, fungi
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
- D06N2211/00—Specially adapted uses
- D06N2211/06—Building materials
- D06N2211/063—Wall coverings
Abstract
The invention discloses a kind of seamless fine nonwoven fabric base wall paper of length and preparation method thereof, this is seamless long fine nonwoven fabric base wall paper includes from top to bottom compound nonwoven layer, adhesive layer successively, and the surface of adhesive layer is implanted with long fibre；Wherein, adhesive layer is dried by adhesive and formed, and adhesive is made up of polyvinyl alcohol, starch, urea, methyl methacrylate, polyacrylamide, nano silicon oxide, nano diatomite, APES, ethylene glycol, water, thickener and defoamer；Long stapled length is 55 70mm.There is excellent mechanical property and antifungi effect by the seamless fine nonwoven fabric base wall paper of length made from preparation method.
Description
Technical field
The present invention relates to wall paper, in particular it relates to a kind of seamless fine nonwoven fabric base wall paper of length and preparation method thereof.
Background technology
Very common material in the existing interior decoration of wall paper, mainly it is arranged at wall by way of gluing and splicing
On, although the quality of existing wall paper is more excellent, still suffer from weak point：More easy to change, not scrubbing resistance, the easy moisture absorption
With go mouldy, effect is poor especially in terms of its antifungi.Due to it is above-mentioned the defects of, significantly limit decoration pushing away in decoration
Extensively, in order to which wallpaper industry brings great industry obstacle.
The content of the invention
It is an object of the invention to provide a kind of seamless fine nonwoven fabric base wall paper of length and preparation method thereof, by preparation method system
The seamless fine nonwoven fabric base wall paper of length obtained has excellent mechanical property and antifungi effect.
To achieve these goals, the invention provides a kind of seamless fine nonwoven fabric base wall paper of length, including from top to bottom according to
Secondary compound nonwoven layer, adhesive layer, the surface of adhesive layer are implanted with long fibre；Wherein, adhesive layer is dried by adhesive and formed,
Adhesive is by polyvinyl alcohol, starch, urea, methyl methacrylate, polyacrylamide, nano silicon oxide, nano diatomite, alkane
Base phenol polyethenoxy ether, ethylene glycol, water, thickener and defoamer composition；Long stapled length is 55-70mm.
Present invention also offers a kind of preparation method of the seamless fine nonwoven fabric base wall paper of length described above, the preparation method bag
Include：
1) adhesive is coated on to the surface of nonwoven layer, then carries out preliminarily dried；
2) long fibre is laid in the surface of adhesive, then carries out redrying so that head product is made；
3) head product is subjected to compaction treatment so that the seamless fine nonwoven fabric base wall paper of length is made.
In the above-mentioned technical solutions, the present invention is compound by the way that adhesive is carried out long fibre with nonwoven layer, wherein viscous
Mixture can not only play a part of bonding, while also act as the effect of disinfecting mouldproof；It is further advanced by long fibre, adhesive layer
Collective effect can play a part of improve wall paper mechanical strength so that the wall paper have excellent mechanical property with
And antifungi effect.The preparation method has process simple and the advantages of raw material is easy to get simultaneously.
Other features and advantages of the present invention will be described in detail in subsequent specific embodiment part.
Embodiment
The embodiment of the present invention is described in detail below.It is it should be appreciated that described herein specific
Embodiment is merely to illustrate and explain the present invention, and is not intended to limit the invention.
The invention provides a kind of seamless fine nonwoven fabric base wall paper of length, including from top to bottom successively compound nonwoven layer,
Adhesive layer, the surface of adhesive layer are implanted with long fibre；Wherein, adhesive layer by adhesive dry form, adhesive by polyvinyl alcohol,
Starch, urea, methyl methacrylate, polyacrylamide, nano silicon oxide, nano diatomite, APES, second
Glycol, water, thickener and defoamer composition；Long stapled length is 55-70mm.
In the above-mentioned seamless fine nonwoven fabric base wall paper of length, the content of each component of adhesive can be selected in wide scope
Select, but in order that wall paper has the antifungi effect of more excellent mechanics, it is preferable that in adhesive, polyvinyl alcohol, shallow lake
Powder, urea, methyl methacrylate, polyacrylamide, nano silicon oxide, nano diatomite, APES, second two
Alcohol, water, the weight ratio of thickener and defoamer are 100：25-36：8-10：35-40：45-56：15-23：5-10：7-9：200-
300：50-80：2-4：1-3.
In the above-mentioned seamless fine nonwoven fabric base wall paper of length, the specific species of thickener can select in wide scope, but
It is in order that wall paper has the antifungi effect of more excellent mechanics, it is preferable that thickener is methylcellulose, carboxymethyl cellulose
At least one of element, hydroxyethyl cellulose and hydroxypropyl methyl cellulose.
In the above-mentioned seamless fine nonwoven fabric base wall paper of length, the specific species of defoamer can select in wide scope, but
It is in order that wall paper has the antifungi effect of more excellent mechanics, it is preferable that defoamer is polyoxyethylene polyoxypropylene season penta
At least one in four alcohol ethers, polyoxyethylene polyoxy propyl alcohol amidogen ether, polypropylene glycerol aether and polyoxyethylene polyoxypropylene glycerin ether
Person.
In the above-mentioned seamless fine nonwoven fabric base wall paper of length, long stapled specific species can select in wide scope, but
Be in order that wall paper have more excellent mechanics antifungi effect, it is preferable that long fibre be selected from polyester fiber, acrylic fiber,
At least one of nylon fibre, polypropylene fiber, vinylon fibre and polyvinyl chloride fibre fiber.
In the above-mentioned seamless fine nonwoven fabric base wall paper of length, long stapled specific species can select in wide scope, but
It is in order that wall paper has the antifungi effect of more excellent mechanics, it is preferable that the thickness of nonwoven layer is 20-30 silks, bonding
The thickness of layer is 25-40 silks, and the thickness of long fibre layer is 10-15 silks.
In the above-mentioned seamless fine nonwoven fabric base wall paper of length, the coverage density of fiber can be selected in wide scope in adhesive layer
Select, but in order that wall paper has the antifungi effect of more excellent mechanics, it is preferable that the coverage density of fiber is in adhesive layer
20-30 areas %.
In the above-mentioned seamless fine nonwoven fabric base wall paper of length, nano silicon oxide, nano diatomite average grain diameter can be in width
In the range of select, but in order that wall paper have more excellent mechanics antifungi effect, it is preferable that nano silicon oxide, receive
The diatomaceous average grain diameter of rice is 15-25nm.
Present invention also offers a kind of preparation method of the seamless fine nonwoven fabric base wall paper of length described above, the preparation method bag
Include：
1) adhesive is coated on to the surface of nonwoven layer, then carries out preliminarily dried；
2) long fibre is laid in the surface of adhesive, then carries out redrying so that head product is made；
3) head product is subjected to compaction treatment so that the seamless fine nonwoven fabric base wall paper of length is made.
In the step 1) of above-mentioned preparation method, the actual conditions of preliminarily dried can select in wide condition, still
In order that obtained wall paper has the antifungi effect of more excellent mechanics, it is preferable that in step 1), preliminarily dried is at least full
It is enough lower condition：Drying temperature is 50-70 DEG C, drying time 0.5-1h.
In the step 2) of above-mentioned preparation method, the actual conditions of redrying can select in wide condition, still
In order that obtained wall paper has the antifungi effect of more excellent mechanics, it is preferable that in step 2), redrying is at least full
It is enough lower condition：Drying temperature is 80-100 DEG C, drying time 12-24h.
In the step 3) of above-mentioned preparation method, the actual conditions of compaction treatment can select in wide condition, still
In order that obtained wall paper has the antifungi effect of more excellent mechanics, it is preferable that in step 3), compaction treatment is at least full
It is enough lower condition：Compaction pressure is 2-4MPa, and the compacting time is 8-12h.
The present invention will be described in detail by way of examples below.
Preparation example 1
1) by polyvinyl alcohol, urea, methyl methacrylate, polyacrylamide, APES, ethylene glycol and
Water is stirred 1h and mixture I is made；
2) starch, nano silicon oxide (average grain diameter 20nm), nano diatomite (average grain diameter 20nm) are added to
In the mixture I and 30min is stirred so that mixtures II is made；
3) by thickener (methylcellulose) and defoamer (polyoxyethylene polyoxypropylene pentaerythrite ether) described in
In mixtures II and 30min is stirred so that adhesive A 1 is made；Wherein, polyvinyl alcohol, starch, urea, methyl methacrylate, poly-
Acrylamide, nano silicon oxide, nano diatomite, APES, ethylene glycol, water, the weight of thickener and defoamer
Amount is than being 100：30：9：38：50：20：8：8：250：70：3：2.
Preparation example 2
1) by polyvinyl alcohol, urea, methyl methacrylate, polyacrylamide, APES, ethylene glycol and
Water is stirred 1h and mixture I is made；
2) starch, nano silicon oxide (average grain diameter 15nm), nano diatomite (average grain diameter 15nm) are added to
In the mixture I and 30min is stirred so that mixtures II is made；
3) thickener (hydroxyethyl cellulose) and defoamer (polypropylene glycerol aether) are added in the mixtures II
And 30min is stirred so that adhesive A 2 is made；Wherein, polyvinyl alcohol, starch, urea, methyl methacrylate, polyacrylamide,
Nano silicon oxide, nano diatomite, APES, ethylene glycol, water, the weight ratio of thickener and defoamer are 100：
25：8：35：45：15：5：7：200：50：2：1.
Preparation example 3
1) by polyvinyl alcohol, urea, methyl methacrylate, polyacrylamide, APES, ethylene glycol and
Water is stirred 1h and mixture I is made；
2) starch, nano silicon oxide (average grain diameter 25nm), nano diatomite (average grain diameter 25nm) are added to
In the mixture I and 30min is stirred so that mixtures II is made；
3) thickener (hydroxypropyl methyl cellulose) and defoamer (polyoxyethylene polyoxypropylene glycerin ether) are added to institute
State in mixtures II and stir 30min so that adhesive A 3 is made；Wherein, polyvinyl alcohol, starch, urea, methyl methacrylate,
Polyacrylamide, nano silicon oxide, nano diatomite, APES, ethylene glycol, water, thickener and defoamer
Weight ratio is 100：36：10：40：56：23：10：9：300：80：4：3.
Preparation example 4
Method according to preparation example 1 carries out that adhesive A 4 is made, except that nano silicon oxide is not used.
Preparation example 5
Method according to preparation example 1 carries out that adhesive A 5 is made, except that nano diatomite is not used.
Embodiment 1
1) by surface of the adhesive A 1 coated on nonwoven layer (thickness is 25), then carry out preliminarily dried and (dry temperature
Spend for 60 DEG C, drying time 0.8h) form adhesive phase (thickness is 30)；
2) by long fibre (polyester fiber；Length is 55-70mm) it is laid in the surface formation fibrous layer (thickness of adhesive phase
For 13, coverage density is 25 area %), redrying (drying temperature is 90 DEG C, drying time 20h) is then carried out with system
Obtain head product；
3) head product is subjected to compaction treatment (compaction pressure 3MPa, compacting time are 10h) so that the seamless fine nothing of length is made
Spin cloth foundation wall cloth B1.
Embodiment 2
1) by surface of the adhesive A 2 coated on nonwoven layer (thickness is 20), then carry out preliminarily dried and (dry temperature
Spend for 50 DEG C, drying time 0.5h) form adhesive phase (thickness is 25)；
2) by long fibre (nylon fibre；Length is 55mm) surface that is laid in adhesive phase forms fibrous layer (thickness is
10, coverage density is 20 area %), redrying (drying temperature is 80 DEG C, drying time 12h) is then carried out to be made
Head product；
3) head product is subjected to compaction treatment (compaction pressure 2MPa, compacting time are 8h) so that the seamless fine nonwoven of length is made
Cloth foundation wall cloth B2.
Embodiment 3
1) by surface of the adhesive A 3 coated on nonwoven layer (thickness is 30), then carry out preliminarily dried and (dry temperature
Spend for 70 DEG C, drying time 1h) form adhesive phase (thickness is 40)；
2) by long fibre (vinylon fibre；Length is 55-70mm) it is laid in the surface formation fibrous layer (thickness of adhesive phase
For 15, coverage density is 30 area %), then carry out redrying (drying temperature be 100 DEG C, drying time 24h) with
Head product is made；
3) head product is subjected to compaction treatment (compaction pressure 4MPa, compacting time are 12h) so that the seamless fine nothing of length is made
Spin cloth foundation wall cloth B3.
Comparative example 1
Method according to preparation example 1 carries out that the seamless fine nonwoven fabric base wall paper C1 of length is made, except that adhesive A 1 changes
For adhesive A 4.
Comparative example 2
Method according to preparation example 1 carries out that the seamless fine nonwoven fabric base wall paper C2 of length is made, except that adhesive A 1 changes
For adhesive A 5.
Comparative example 3
Method according to preparation example 1 carries out that the seamless fine nonwoven fabric base wall paper C3 of length is made, except that step 2) does not make
Use long fibre.
Detect example 1
1) above-mentioned wall paper is placed in the environment that humidity is 60%, temperature is 35 DEG C one week, then detects 1m2Interior mildew
Quantity；
2) and then by instron GP-6113 (Instrument Ltd. is surveyed in the high product examine in Suzhou City) above-mentioned wall is detected
The tensile strength of cloth；Concrete outcome is shown in Table 1.
Table 1
By above-described embodiment, comparative example and detection example, wall paper provided by the invention has excellent mechanics and resisted
Mould effect.
The preferred embodiment of the present invention described in detail above, still, the present invention are not limited in above-mentioned embodiment
Detail, in the range of the technology design of the present invention, a variety of simple variants can be carried out to technical scheme, this
A little simple variants belong to protection scope of the present invention.
It is further to note that each particular technique feature described in above-mentioned embodiment, in not lance
In the case of shield, can be combined by any suitable means, in order to avoid unnecessary repetition, the present invention to it is various can
The combination of energy no longer separately illustrates.
In addition, various embodiments of the present invention can be combined randomly, as long as it is without prejudice to originally
The thought of invention, it should equally be considered as content disclosed in this invention.
Claims (10)
- A kind of 1. seamless fine nonwoven fabric base wall paper of length, it is characterised in that including from top to bottom successively compound nonwoven layer, bond Layer, the surface of the adhesive layer is implanted with long fibre；Wherein, the adhesive layer by adhesive dry form, described adhesive by Polyvinyl alcohol, starch, urea, methyl methacrylate, polyacrylamide, nano silicon oxide, nano diatomite, alkyl phenol polyoxy Vinethene, ethylene glycol, water, thickener and defoamer composition；The long stapled length is 55-70mm.
- 2. the fine nonwoven fabric base wall paper of seamless length according to claim 1, wherein, in described adhesive, the polyethylene Alcohol, starch, urea, methyl methacrylate, polyacrylamide, nano silicon oxide, nano diatomite, alkylphenol-polyethenoxy Ether, ethylene glycol, water, the weight ratio of thickener and defoamer are 100：25-36：8-10：35-40：45-56：15-23：5-10：7- 9：200-300：50-80：2-4：1-3.
- 3. the fine nonwoven fabric base wall paper of seamless length according to claim 1, wherein, the thickener is methylcellulose, carboxylic At least one of methylcellulose, hydroxyethyl cellulose and hydroxypropyl methyl cellulose；The defoamer gathers for polyoxyethylene Oxypropylene pentaerythrite ether, polyoxyethylene polyoxy propyl alcohol amidogen ether, polypropylene glycerol aether and polyoxyethylene polyoxypropylene glycerin ether At least one of.
- 4. the fine nonwoven fabric base wall paper of seamless length according to claim 1, wherein, the long fibre is selected from polyester fiber, nitrile At least one of synthetic fibre fiber, nylon fibre, polypropylene fiber, vinylon fibre and polyvinyl chloride fibre fiber.
- 5. the seamless length fine nonwoven fabric base wall paper according at least one in claim 1-4, wherein, the nonwoven layer Thickness is 20-30 silks, and the thickness of the adhesive layer is 25-40 silks, and the thickness of long fibre layer is 10-15 silks.
- 6. the fine nonwoven fabric base wall paper of seamless length according to claim 5, wherein, the coverage density of fiber in the adhesive layer For 20-30 areas %.
- 7. the seamless length fine nonwoven fabric base wall paper according at least one in claim 1-4, wherein, it is described nano oxidized Silicon, the average grain diameter of nano diatomite are 15-25nm.
- 8. a kind of preparation method of the fine nonwoven fabric base wall paper of seamless length in 1-7 such as claim as described in any one, its feature It is, the preparation method includes：1) described adhesive is coated on to the surface of the nonwoven layer, then carries out preliminarily dried；2) long fibre is laid in the surface of described adhesive, then carries out redrying so that head product is made；3) head product is subjected to compaction treatment so that the seamless fine nonwoven fabric base wall paper of length is made.
- 9. preparation method according to claim 8, wherein, in step 1), the preliminarily dried at least meets following bar Part：Drying temperature is 50-70 DEG C, drying time 0.5-1h.
- 10. preparation method according to claim 8, wherein, in step 2), the redrying at least meets following bar Part：Drying temperature is 80-100 DEG C, drying time 12-24h；Preferably, in step 3), the compaction treatment at least meets following condition：Compaction pressure is 2-4MPa, is compacted the time For 8-12h.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710722137.1A CN107503164A (en) | 2017-08-22 | 2017-08-22 | Seamless fine nonwoven fabric base wall paper of length and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710722137.1A CN107503164A (en) | 2017-08-22 | 2017-08-22 | Seamless fine nonwoven fabric base wall paper of length and preparation method thereof |
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| CN107503164A true CN107503164A (en) | 2017-12-22 |
Family
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Application publication date: 20171222 |
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| RJ01 | Rejection of invention patent application after publication |