CN107494622A - A kind of solid insecticide for green vegetables and preparation method thereof - Google Patents

A kind of solid insecticide for green vegetables and preparation method thereof Download PDF

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Publication number
CN107494622A
CN107494622A CN201710727403.XA CN201710727403A CN107494622A CN 107494622 A CN107494622 A CN 107494622A CN 201710727403 A CN201710727403 A CN 201710727403A CN 107494622 A CN107494622 A CN 107494622A
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China
Prior art keywords
parts
green vegetables
solid
preparation
solid insecticide
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Pending
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CN201710727403.XA
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Chinese (zh)
Inventor
包伟强
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Suzhou Antek Industrial Co Ltd
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Suzhou Antek Industrial Co Ltd
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Priority to CN201710727403.XA priority Critical patent/CN107494622A/en
Publication of CN107494622A publication Critical patent/CN107494622A/en
Pending legal-status Critical Current

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    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
    • A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
    • A01N43/22—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom rings with more than six members
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08—Magnoliopsida [dicotyledons]
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08—Magnoliopsida [dicotyledons]
    • A01N65/20—Fabaceae or Leguminosae [Pea or Legume family], e.g. pea, lentil, soybean, clover, acacia, honey locust, derris or millettia
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08—Magnoliopsida [dicotyledons]
    • A01N65/26—Meliaceae [Chinaberry or Mahogany family], e.g. mahogany, langsat or neem
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08—Magnoliopsida [dicotyledons]
    • A01N65/36—Rutaceae [Rue family], e.g. lime, orange, lemon, corktree or pricklyash
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Zoology (AREA)
  • Agronomy & Crop Science (AREA)
  • Environmental Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Plant Pathology (AREA)
  • Dentistry (AREA)
  • Mycology (AREA)
  • Biotechnology (AREA)
  • Microbiology (AREA)
  • Pest Control & Pesticides (AREA)
  • Botany (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Cosmetics (AREA)
  • Disinfection, Sterilisation Or Deodorisation Of Air (AREA)

Abstract

The invention discloses a kind of solid insecticide for green vegetables, it is made up of the raw material of following mass parts：0.9 1.1 parts of tangerine peel, 0.5 0.8 parts of kuh-seng, hardship remonstrate with 0.9 1.1 parts of skin, 1.8 2.2 parts of macleaya cordata, 35 parts of the basal part of the ear of folding, wear vertical 13 parts, 23 parts of multiple killing teichomycin, 57 parts of agar powder, 1.5 2.5 parts of lemon, 50 70 parts of 35 parts of pectin and alcohol, the invention also discloses the preparation method of the solid insecticide, it is an advantage of the invention that：First, it is made up from natural herbs extract of raw material, can effectively plays a part of deinsectization, environmental protection and public nuisance free；Secondly, solid insecticide of the present invention, the active ingredient of release desinsection that can be steadily in the long term, so as to give play to the sharpest edges of solid deinsectization.

Description

A kind of solid insecticide for green vegetables and preparation method thereof
Technical field
The present invention relates to a kind of insecticide, more particularly to it is a kind of for the solid insecticide of green vegetables and its preparation side Method.
Background technology
In daily life, the transport of vegetables is more prevalent, and expelling parasite processing of the vegetables in transportation becomes particularly important, Today of green and environmental protection is early advocated, a variety of high poisons and high residue chemicals are limited the quantity or stopped production, organophosphor, intend deinsectization The agricultural chemicals such as chrysanthemum ester, benzoyl area kind and biochemistry have made original toxicity decrease to a certain extent through compounded combination, but by In the result used year after year, polypide drug resistance and the resistance to the action of a drug is caused to strengthen year by year, the effect being used alternatingly is also undesirable, and agricultural chemicals removes The actual amount of dilution of worm agent limits the use of scope far beyond it, and agricultural product chemicals residual does not reach non-harmful requirement far, by Year, increased agricultural chemicals demand caused the aggravation of rural environmental pollution, and harm of its residue to human body more can not be ignored.
The content of the invention
Goal of the invention：The first object of the present invention is to provide one kind and is used for green made of natural herbs extract The solid insecticide of vegetables；Second purpose is to provide the preparation method of above-mentioned insecticide.
Technical scheme：Solid insecticide of the present invention for green vegetables is made up of the raw material of following mass parts：Tangerine Skin 0.9-1.1 parts, kuh-seng 0.5-0.8 parts, hardship remonstrate with skin 0.9-1.1 parts, macleaya cordata 1.8-2.2 parts, folding basal part of the ear 3-5 parts, wear vertical 1-3 Part, multiple killing teichomycin 2-3 parts, agar powder 5-7 parts, lemon 1.5-2.5 parts, pectin 3-5 parts and alcohol 50-70 parts.
The preparation method of the solid insecticide for green vegetables, which comprises the following steps, to be prepared：
(1) by the tangerine peel, kuh-seng, hardship of above mass parts remonstrate with skin, macleaya cordata, the folding basal part of the ear, Pei Li and multiple killing teichomycin grind it is mixed Merge refrigeration, obtain active material coarse powder；
(2) with the 0.4-0.6% methanol hydrochloride solutions active material coarse powder in cold soaking step (1), and being concentrated to give repeatedly Active material total extract；
(3) total extract obtained in step (2) is dissolved in NaOH solution, alkalizes to pH8-9, add in the solution Ammonium hydrogen sulfate, distill while stirring to moisture content and be less than 1%, obtain mixture A；
(4) mixture A is mixed into alcohol to seal after lucifuge stores 20-30 days and adds agar powder, pectin and lemon, After stirring, air-dry to moisture content and be less than 0.5% gelatinous solid, be the solid deinsectization that the present invention is used for green vegetables Agent.
Wherein, refrigerated storage temperature is 0-2 DEG C in step (1).
The step (2) cold soaking repeatedly is with methanol hydrochloride solution cold soaking active material coarse powder 4-6 times repeatedly, every time 8-12 days.
Step (2) concentration is to be concentrated under reduced pressure at 20-30 DEG C.
The concentration of NaOH solution is 8-10% described in the step (3).
The concentration of alcohol is 65-85% in the step (4).
Beneficial effect：Compared with prior art, the advantages of of the invention notable is：(1) extracted from natural herbs Thing is made up of raw material, can effectively play a part of deinsectization, environmental protection and public nuisance free；(2) solid insecticide of the present invention, can be long-term The active ingredient of stable release desinsection, so as to give play to the sharpest edges of solid deinsectization.
Embodiment
Embodiment 1
A kind of solid insecticide for green vegetables, it is made up of the raw material of following mass parts：0.9 part of tangerine peel, kuh-seng 0.5 Part, hardship remonstrate with 0.9 part of skin, 1.8 parts of macleaya cordata, 3 parts of the basal part of the ear of folding, wear vertical 1 part, 2 parts of multiple killing teichomycin, 5 parts of agar powder, lemon 50 parts of 1.5 parts, 3 parts of pectin and alcohol.
The preparation method of the described solid insecticide for green vegetables, comprises the following steps and is prepared：
(1) by the tangerine peel, kuh-seng, hardship of above mass parts remonstrate with skin, macleaya cordata, the folding basal part of the ear, Pei Li and multiple killing teichomycin grind it is mixed Merge refrigeration, obtain active material coarse powder；
(2) with the active material coarse powder in 0.4% methanol hydrochloride solution repeatedly cold soaking step (1), and it is concentrated to give activity Material total extract；
(3) total extract obtained in step (2) is dissolved in NaOH solution, alkalizes to pH8, add sulphur in the solution Sour hydrogen ammonium, it is 0.5% to distill while stirring to moisture content, obtains mixture A；
(4) mixture A is mixed into alcohol to seal after lucifuge stores 20 days and adds agar powder, pectin and lemon, stirred After mixing uniformly, air-dry to the gelatinous solid that moisture content is 0, be the solid insecticide that the present invention is used for green vegetables.
Wherein, refrigerated storage temperature is 0 DEG C in step (1).
Step (2) cold soaking repeatedly is 8 days every time with methanol hydrochloride solution cold soaking active material coarse powder 4 times repeatedly.
Step (2) concentration is to be concentrated under reduced pressure at 20 DEG C.
The concentration of NaOH solution described in step (3) is 8%.
The concentration of alcohol is 65% in step (4).
Embodiment 2
A kind of solid insecticide for green vegetables, it is made up of the raw material of following mass parts：1 part of tangerine peel, kuh-seng 0.7 Part, hardship remonstrate with 1 part of skin, 2 parts of macleaya cordata, 4 parts of the basal part of the ear of folding, wear vertical 2 parts, 2.5 parts of multiple killing teichomycin, 6 parts of agar powder, lemon 25 60 parts of part, 4 parts of pectin and alcohol.
The preparation method of the solid insecticide for green vegetables, comprises the following steps and is prepared：
(1) by the tangerine peel, kuh-seng, hardship of above mass parts remonstrate with skin, macleaya cordata, the folding basal part of the ear, Pei Li and multiple killing teichomycin grind it is mixed Merge refrigeration, obtain active material coarse powder；
(2) with the active material coarse powder in 0.5% methanol hydrochloride solution repeatedly cold soaking step (1), and it is concentrated to give activity Material total extract；
(3) total extract obtained in step (2) is dissolved in NaOH solution, alkalizes to pH8.5, add in the solution Ammonium hydrogen sulfate, it is 0.7% to distill while stirring to moisture content, obtains mixture A；
(4) mixture A is mixed into alcohol to seal after lucifuge stores 250 days and adds agar powder, pectin and lemon, stirred After mixing uniformly, air-dry to the gelatinous solid that moisture content is 0.2%, be the solid insecticide that the present invention is used for green vegetables.
Wherein, refrigerated storage temperature is 1 DEG C in step (1).
Step (2) cold soaking repeatedly is 10 days every time with methanol hydrochloride solution cold soaking active material coarse powder 5 times repeatedly.
Step (2) concentration is to be concentrated under reduced pressure at 25 DEG C.
The concentration of NaOH solution described in step (3) is 9%.
The concentration of alcohol is 75% in step (4).
Embodiment 3
A kind of solid insecticide for green vegetables, it is made up of the raw material of following mass parts：1.1 parts of tangerine peel, kuh-seng 0.8 Part, hardship remonstrate with 1.1 parts of skin, 2.2 parts of macleaya cordata, 5 parts of the basal part of the ear of folding, wear vertical 3 parts, 3 parts of multiple killing teichomycin, 7 parts of agar powder, lemon 70 parts of 2.5 parts, 5 parts of pectin and alcohol.
The preparation method of the solid insecticide for green vegetables, comprises the following steps and is prepared：
(1) by the tangerine peel, kuh-seng, hardship of above mass parts remonstrate with skin, macleaya cordata, the folding basal part of the ear, Pei Li and multiple killing teichomycin grind it is mixed Merge refrigeration, obtain active material coarse powder；
(2) with the active material coarse powder in 0.6% methanol hydrochloride solution repeatedly cold soaking step (1), and it is concentrated to give activity Material total extract；
(3) total extract obtained in step (2) is dissolved in NaOH solution, alkalizes to pH9, add sulphur in the solution Sour hydrogen ammonium, it is 0.8% to distill while stirring to moisture content, obtains mixture A；
(4) mixture A is mixed into alcohol to seal after lucifuge stores 20-30 days and adds agar powder, pectin and lemon, After stirring, air-dry to the gelatinous solid that moisture content is 0.4%, be the solid deinsectization that the present invention is used for green vegetables Agent.
Wherein, refrigerated storage temperature is 2 DEG C in the step (1).
Step (2) cold soaking repeatedly is 12 days every time with methanol hydrochloride solution cold soaking active material coarse powder 6 times repeatedly.
Step (2) concentration is to be concentrated under reduced pressure at 30 DEG C.
The concentration of NaOH solution described in step (3) is 10%.
The concentration of alcohol is 85% in step (4).
Test example 1
To the tangerine peel of same concentrations, kuh-seng, bitter skin of remonstrating with, macleaya cordata, the folding basal part of the ear, wear stand the methanolic extracts of 6 kinds of plants with And embodiment 1, embodiment 2 and solid insecticide made from embodiment 3 carry out insect killing effect test, result of the test is shown in Table 1：
The killing in vitro effect of 16 kinds of plant methanolic extracts of table and insecticide of the present invention to cabbageworm
Experiment shows：Tangerine peel, kuh-seng, bitter skin of remonstrating with, macleaya cordata, the folding basal part of the ear, vertical extract of wearing can kill entirely in 6h Worm is tested in portion, and the embodiment of the present invention 1, embodiment 2 and the desinsection of embodiment 3 take up to 1.2h, it can be seen that of the invention removes The insecticidal effect of worm agent is splendid.

Claims (7)

  1. A kind of 1. solid insecticide for green vegetables, it is characterised in that：It is made up of the raw material of following mass parts：Tangerine peel 0.9- 1.1 parts, kuh-seng 0.5-0.8 parts, hardship remonstrate with skin 0.9-1.1 parts, macleaya cordata 1.8-2.2 parts, folding basal part of the ear 3-5 parts, vertical 1-3 parts of wearing, more Killing teichomycin 2-3 parts, agar powder 5-7 parts, lemon 1.5-2.5 parts, pectin 3-5 parts and alcohol 50-70 parts.
  2. 2. the preparation method of the solid insecticide for green vegetables described in claim 1, it is characterised in that：Including following step Suddenly it is prepared：
    (1) tangerine peel, kuh-seng, hardship of above mass parts are remonstrated with into skin, macleaya cordata, the folding basal part of the ear, Pei Li and multiple killing teichomycin grinding mixing simultaneously Refrigeration, obtains active material coarse powder；
    (2) with the 0.4-0.6% methanol hydrochloride solutions active material coarse powder in cold soaking step (1), and be concentrated to give activity repeatedly Material total extract；
    (3) total extract obtained in step (2) is dissolved in NaOH solution, alkalizes to pH8-9, add sulfuric acid in the solution Hydrogen ammonium, distill while stirring to moisture content and be less than 1%, obtain mixture A；
    (4) mixture A is mixed into alcohol to seal and agar powder, pectin and lemon, stirring is added after lucifuge stores 20-30 days After uniformly, air-dry to moisture content and be less than 0.5% gelatinous solid, be the solid insecticide that the present invention is used for green vegetables.
  3. 3. the preparation method of the solid insecticide according to claim 2 for green vegetables, it is characterised in that：Step (1) refrigerated storage temperature is 0-2 DEG C in.
  4. 4. the preparation method of the solid insecticide according to claim 2 for green vegetables, it is characterised in that：Step (2) cold soaking repeatedly is each 8-12 days with methanol hydrochloride solution cold soaking active material coarse powder 4-6 times repeatedly.
  5. 5. the preparation method of the solid insecticide according to claim 2 for green vegetables, it is characterised in that：Step (2) concentration is to be concentrated under reduced pressure at 20-30 DEG C.
  6. 6. the preparation method of the solid insecticide according to claim 2 for green vegetables, it is characterised in that：Step (3) concentration of NaOH solution described in is 8-10%.
  7. 7. the preparation method of the solid insecticide according to claim 2 for green vegetables, it is characterised in that：Step (4) concentration of alcohol is 65-85% in.
CN201710727403.XA 2017-08-23 2017-08-23 A kind of solid insecticide for green vegetables and preparation method thereof Pending CN107494622A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710727403.XA CN107494622A (en) 2017-08-23 2017-08-23 A kind of solid insecticide for green vegetables and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710727403.XA CN107494622A (en) 2017-08-23 2017-08-23 A kind of solid insecticide for green vegetables and preparation method thereof

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CN107494622A true CN107494622A (en) 2017-12-22

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109302960A (en) * 2018-11-29 2019-02-05 邵阳市钲淇农业综合开发有限公司 A kind of implantation methods of point green pepper

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109302960A (en) * 2018-11-29 2019-02-05 邵阳市钲淇农业综合开发有限公司 A kind of implantation methods of point green pepper

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Application publication date: 20171222