CN107488964A - The dyeing of strength after a kind of fire-retardant space-variant dyeing yarn of holding - Google Patents
The dyeing of strength after a kind of fire-retardant space-variant dyeing yarn of holding Download PDFInfo
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- CN107488964A CN107488964A CN201710852028.1A CN201710852028A CN107488964A CN 107488964 A CN107488964 A CN 107488964A CN 201710852028 A CN201710852028 A CN 201710852028A CN 107488964 A CN107488964 A CN 107488964A
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- Prior art keywords
- dyeing
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- fire
- fire resistance
- resistance fibre
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
- D06B21/00—Successive treatments of textile materials by liquids, gases or vapours
-
- D—TEXTILES; PAPER
- D02—YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
- D02J—FINISHING OR DRESSING OF FILAMENTS, YARNS, THREADS, CORDS, ROPES OR THE LIKE
- D02J13/00—Heating or cooling the yarn, thread, cord, rope, or the like, not specific to any one of the processes provided for in this subclass
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
- D06B15/00—Removing liquids, gases or vapours from textile materials in association with treatment of the materials by liquids, gases or vapours
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
- D06B3/00—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating
- D06B3/04—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating of yarns, threads or filaments
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/263—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acids; Salts or esters thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/327—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated alcohols or esters thereof
- D06M15/333—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated alcohols or esters thereof of vinyl acetate; Polyvinylalcohol
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/0032—Determining dye recipes and dyeing parameters; Colour matching or monitoring
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/02—After-treatment
- D06P5/04—After-treatment with organic compounds
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/02—After-treatment
- D06P5/04—After-treatment with organic compounds
- D06P5/08—After-treatment with organic compounds macromolecular
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/02—After-treatment
- D06P5/10—After-treatment with compounds containing metal
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Materials Engineering (AREA)
- Coloring (AREA)
Abstract
The present invention provides a kind of dyeing of strength after fire-retardant space-variant dyeing yarn of holding, is related to colouring art, comprises the following steps：Desizing is handled：Fire resistance fibre is added in 50~60 DEG C of the desizing aqueous solution, 8~10h is placed in insulation, is cleaned after yarn is taken out with cold water, 30~40 DEG C of drying；Setting process：Fire resistance fibre is subjected to presetting technology at 130~150 DEG C；Water bath processing：Fire resistance fibre is added in 45~55 DEG C of bath solution, 10~15min is placed in insulation；Dyeing is handled；Soap technique：After handling 10~15min at 40~50 DEG C of temperature, take out, cleaned, low temperature drying；It is good the invention enables the Color of fire resistance fibre, color fastness meets the series of corresponding requirements, user is avoided the phenomenon that fades occur in washing, carry out reduction cleaning, the post processing such as washing, thoroughly removes loose colour, to improve the dyefastness of dyeing product and vividness, meet user's multiple demand, while this technology also saves water power.
Description
Technical field
The present invention relates to colouring art, and in particular to the dyeing of strength after a kind of fire-retardant space-variant dyeing yarn of holding.
Background technology
Fire resistance fibre, flame retardant abbreviation letters：FR, refer to only glow in flame, fire does not occur in itself
Flame, flame is left, the fiber for the self-extinguish that glows, be widely used in clothes, household, decoration, adhesive-bonded fabric and filler etc..
On some fields such as firefighter uniform, fire resistance fibre is always a more important ring.The fire-retardant of fiber can be seen by combustion process
Go out, exactly try to hinder the thermal decomposition of fiber, suppress imflammable gas generation and dilution imflammable gas, change pyrolysis
Mechanism, block Thermal feedback loop, and air-isolation and thermal environment, come reach eliminate or mitigate burning three elements (combustible,
Temperature, oxygen) influence, and reach fire-retardant purpose.
In recent years, the high temperature resistant durable flame-proof fiber such as aramid fiber, polyvinyl, Powerleader synthetic fibre, Vinyon N emerged in succession, and it is because excellent
Anti-flammability and receive much concern, its be expected to turn into fire resistance fibre in a big emerging market.However, find in actual applications,
Aramid fiber, polyvinyl, Powerleader synthetic fibre, the compact structure of Vinyon N these fibers, and its modulus is higher, and dye or dye are difficult under common process
Color effect is poor.
The content of the invention
In view of the shortcomings of the prior art, the invention provides a kind of dyer of strength after fire-retardant space-variant dyeing yarn of holding
Skill so that the Color of fire resistance fibre is good.
To realize object above, the present invention is achieved by the following technical programs：One kind keeps fire-retardant space-variant dyeing yarn
The dyeing of strength afterwards, comprises the following steps：
Desizing is handled：Fire resistance fibre is added in 50~60 DEG C of the desizing aqueous solution, 8~10h is placed in insulation, and yarn is taken
Cleaned after going out with cold water, 30~40 DEG C of drying；
Setting process：Fire resistance fibre is subjected to presetting technology at 130~150 DEG C；
Water bath processing：Fire resistance fibre is added in 45~55 DEG C of bath solution, 10~15min is placed in insulation；
Dyeing is handled：Dyeing handle, within 60 DEG C, bath solution add coloring agent dyed, with 1~2 DEG C/
Min programming rate, up to 20~40min is incubated at 100 DEG C, continues heating rate and is set in 1.5 to 70~100 DEG C of temperature ranges
~2 DEG C/min is warming up to 100~120 DEG C of temperature ranges, 60~90min of soaking time, and 8~10 DEG C/min cooling rates are answered after dye
It is down to less than 40 DEG C discharge opeings；
Soap technique：Take out fire resistance fibre to be soaped with saponification agent, 10~15min is handled at 40~50 DEG C of temperature
Afterwards, take out, cleaned, low temperature drying.
Preferably, the desizing aqueous solution includes following component in the step 1：3~5 parts of polyvinyl alcohol, polyacrylic acid 5~8
4~6 parts of part, 2~3 parts of softening agent and anti-friction composition.
Preferably, the saponification agent in the step 5 includes following component：10~15 parts of sodium borohydride, polyethylene glycol 60~
70 parts, 2~4 parts of p-methyl benzenesulfonic acid, 10~15 parts of trimethylolpropane, 8~10 parts of sodium hydroxide, 4~6 parts of acetone, fat
2~4 parts of amine APEO bi-quaternary ammonium salt.
The invention provides a kind of dyeing of strength after fire-retardant space-variant dyeing yarn of holding so that the dyeing of fire resistance fibre
Effect is good, and color fastness meets the series of corresponding requirements, avoids user from the phenomenon that fades occur in washing, carries out reduction cleaning,
The post processing such as washing, thoroughly removes loose colour, to improve the dyefastness of dyeing product and vividness, meets user's diversification need
Ask, while this technology also saves water power.
Embodiment
To make the purpose, technical scheme and advantage of the embodiment of the present invention clearer, below by detailed to of the invention real
The technical scheme applied in example is clearly and completely described, it is clear that and described embodiment is part of the embodiment of the present invention,
Rather than whole embodiment.Based on the embodiment in the present invention, those of ordinary skill in the art are not making creative labor
The every other embodiment obtained under the premise of dynamic, belongs to the scope of protection of the invention.
Embodiment 1：
The dyeing of strength, comprises the following steps after a kind of fire-retardant space-variant dyeing yarn of holding：
Desizing is handled：Fire resistance fibre is added in 50~60 DEG C of the desizing aqueous solution, 8~10h is placed in insulation, and yarn is taken
Cleaned after going out with cold water, 30~40 DEG C of drying；
Setting process：Fire resistance fibre is subjected to presetting technology at 130~150 DEG C；
Water bath processing：Fire resistance fibre is added in 45~55 DEG C of bath solution, 10~15min is placed in insulation；
Dyeing is handled：Dyeing handle, within 60 DEG C, bath solution add coloring agent dyed, with 1~2 DEG C/
Min programming rate, up to 20~40min is incubated at 100 DEG C, continues heating rate and is set in 1.5 to 70~100 DEG C of temperature ranges
~2 DEG C/min is warming up to 100~120 DEG C of temperature ranges, 60~90min of soaking time, and 8~10 DEG C/min cooling rates are answered after dye
It is down to less than 40 DEG C discharge opeings；
Soap technique：Take out fire resistance fibre to be soaped with saponification agent, 10~15min is handled at 40~50 DEG C of temperature
Afterwards, take out, cleaned, low temperature drying.
The invention provides a kind of dyeing of strength after fire-retardant space-variant dyeing yarn of holding so that the dyeing of fire resistance fibre
Effect is good, and color fastness meets the series of corresponding requirements, avoids user from the phenomenon that fades occur in washing.
Embodiment 2：
On the basis of embodiment 1, the desizing aqueous solution includes following component in the step 1：3~5 parts of polyvinyl alcohol, gather
4~6 parts of 5~8 parts of acrylic acid, 2~3 parts of softening agent and anti-friction composition；Saponification agent in the step 5 includes following component：Boron hydrogen
Change 10~15 parts of sodium, 60~70 parts of polyethylene glycol, 2~4 parts of p-methyl benzenesulfonic acid, 10~15 parts of trimethylolpropane, hydroxide
8~10 parts of sodium, 4~6 parts of acetone, 2~4 parts of aliphatic amine polyoxyethylene ether biquaternary.
Embodiment 3：
The dyeing of strength, comprises the following steps after a kind of fire-retardant space-variant dyeing yarn of holding：
Desizing is handled：Fire resistance fibre is added in 60 DEG C of the desizing aqueous solution, 10h is placed in insulation, is used after yarn is taken out
Cold water is cleaned, 40 DEG C of drying；
Setting process：Fire resistance fibre is subjected to presetting technology at 150 DEG C；
Water bath processing：Fire resistance fibre is added in 55 DEG C of bath solution, 15min is placed in insulation；
Dyeing is handled：Dyeing is handled, and within 60 DEG C, is added coloring agent in bath solution and is dyed, with 2 DEG C/min's
Programming rate is incubated 40min to 100 DEG C of temperature ranges, during up to 100 DEG C, continues heating rate and be set in 2 DEG C/min to be warming up to 120
DEG C temperature range, soaking time 90min, 10 DEG C/min cooling rates are answered to be down to less than 40 DEG C discharge opeings after dye；
Soap technique：Take out fire resistance fibre to be soaped with saponification agent, after handling 10~15min under temperature 50 C, take
Go out, cleaned, low temperature drying.
Preferably, the desizing aqueous solution includes following component in the step 1：5 parts of polyvinyl alcohol, 5 parts of polyacrylic acid, softness
4 parts of 3 parts of agent and anti-friction composition.
Preferably, the saponification agent in the step 5 includes following component：15 parts of sodium borohydride, 70 parts of polyethylene glycol, to first
4 parts of base benzene sulfonic acid, 15 parts of trimethylolpropane, 10 parts of sodium hydroxide, 6 parts of acetone, aliphatic amine polyoxyethylene ether biquaternary 4
Part.
Experiment
The detection method of light fastness is tested according to G B/T 8426-1 998,
Fire resistance fibre made from the dyeing of embodiment 1,2,3 is tested, and with the common fire resistance fibre row pair in market
Than.Result of the test is as follows：
Good the invention enables the Color of fire resistance fibre, color fastness meets the series of corresponding requirements, avoids user from existing
Occur the phenomenon that fades during washing, carry out the post processing such as reduction cleaning, washing, loose colour is thoroughly removed, to improve the dye of dyeing product
Color fastness and vividness, meet user's multiple demand, while this technology also saves water power.
The post processing such as reduction cleaning, washing is carried out, thoroughly removes loose colour, to improve the dyefastness of dyeing product and bright-coloured
Degree, meets user's multiple demand, while this technology also saves water power.
It should be noted that herein, such as first and second or the like relational terms are used merely to a reality
Body or operation make a distinction with another entity or operation, and not necessarily require or imply and deposited between these entities or operation
In any this actual relation or order.Moreover, term " comprising ", "comprising" or its any other variant are intended to
Nonexcludability includes, so that process, method, article or equipment including a series of elements not only will including those
Element, but also the other element including being not expressly set out, or it is this process, method, article or equipment also to include
Intrinsic key element.In the absence of more restrictions, the key element limited by sentence "including a ...", it is not excluded that
Other identical element also be present in process, method, article or equipment including the key element.
The above embodiments are merely illustrative of the technical solutions of the present invention, rather than its limitations；Although with reference to the foregoing embodiments
The present invention is described in detail, it will be understood by those within the art that：It still can be to foregoing each implementation
Technical scheme described in example is modified, or carries out equivalent substitution to which part technical characteristic；And these modification or
Replace, the essence of appropriate technical solution is departed from the spirit and scope of various embodiments of the present invention technical scheme.
Claims (3)
1. the dyeing of strength after a kind of fire-retardant space-variant dyeing yarn of holding, it is characterised in that comprise the following steps：
(1) desizing is handled：Fire resistance fibre is added in 50~60 DEG C of the desizing aqueous solution, 8~10h is placed in insulation, and yarn is taken
Cleaned after going out with cold water, 30~40 DEG C of drying；
(2) setting process：Fire resistance fibre is subjected to presetting technology at 130~150 DEG C；
(3) water bath processing：Fire resistance fibre is added in 45~55 DEG C of bath solution, 10~15min is placed in insulation；
(4) dyeing is handled：Dyeing is handled, and within 60 DEG C, is added coloring agent in bath solution and is dyed, with 1~2 DEG C/min
Programming rate to 70~100 DEG C of temperature ranges, up to 20~40min is incubated at 100 DEG C, continues heating rate and be set in 1.5~2
DEG C/min is warming up to 100~120 DEG C of temperature ranges, 60~90min of soaking time, answer 8~10 DEG C/min cooling rates to drop after dye
To less than 40 DEG C discharge opeings；
(5) soap technique：Fire resistance fibre is taken out to be soaped with saponification agent, after handling 10~15min at 40~50 DEG C of temperature,
Take out, cleaned, low temperature drying.
2. the dyeing of strength after fire-retardant space-variant dyeing yarn is kept as claimed in claim 1, it is characterised in that the step
The desizing aqueous solution includes following component in 1：3~5 parts of polyvinyl alcohol, 5~8 parts of polyacrylic acid, 2~3 parts of softening agent and anti-friction composition 4
~6 parts.
3. the dyeing of strength after fire-retardant space-variant dyeing yarn is kept as claimed in claim 1, it is characterised in that the step
Saponification agent in 5 includes following component：10~15 parts of sodium borohydride, 60~70 parts of polyethylene glycol, 2~4 parts of p-methyl benzenesulfonic acid,
10~15 parts of trimethylolpropane, 8~10 parts of sodium hydroxide, acetone 4-6 parts, aliphatic amine polyoxyethylene ether biquaternary 2-4 parts.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710852028.1A CN107488964A (en) | 2017-09-19 | 2017-09-19 | The dyeing of strength after a kind of fire-retardant space-variant dyeing yarn of holding |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710852028.1A CN107488964A (en) | 2017-09-19 | 2017-09-19 | The dyeing of strength after a kind of fire-retardant space-variant dyeing yarn of holding |
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| Publication Number | Publication Date |
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| CN107488964A true CN107488964A (en) | 2017-12-19 |
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| CN201710852028.1A Pending CN107488964A (en) | 2017-09-19 | 2017-09-19 | The dyeing of strength after a kind of fire-retardant space-variant dyeing yarn of holding |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109914002A (en) * | 2019-04-03 | 2019-06-21 | 平湖市三禾染整有限公司 | A kind of yarn pre-treating technology |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105714575A (en) * | 2016-04-27 | 2016-06-29 | 杭州卓达染整有限公司 | Dyeing process of fire retardant fibers |
| CN106498709A (en) * | 2016-10-21 | 2017-03-15 | 岳西县桃园服饰有限公司 | A kind of dyeing pretreating process of synthetic fiber fabric |
| CN106592284A (en) * | 2016-11-24 | 2017-04-26 | 张家港市德宝化工有限公司 | Reduction clearing method used for synthetic fiber |
-
2017
- 2017-09-19 CN CN201710852028.1A patent/CN107488964A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105714575A (en) * | 2016-04-27 | 2016-06-29 | 杭州卓达染整有限公司 | Dyeing process of fire retardant fibers |
| CN106498709A (en) * | 2016-10-21 | 2017-03-15 | 岳西县桃园服饰有限公司 | A kind of dyeing pretreating process of synthetic fiber fabric |
| CN106592284A (en) * | 2016-11-24 | 2017-04-26 | 张家港市德宝化工有限公司 | Reduction clearing method used for synthetic fiber |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109914002A (en) * | 2019-04-03 | 2019-06-21 | 平湖市三禾染整有限公司 | A kind of yarn pre-treating technology |
| CN109914002B (en) * | 2019-04-03 | 2022-01-04 | 平湖市三禾染整股份有限公司 | Yarn pretreatment process |
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Application publication date: 20171219 |