CN107485583A - The preparation method of ganoderma spove powder toothpaste - Google Patents
The preparation method of ganoderma spove powder toothpaste Download PDFInfo
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- CN107485583A CN107485583A CN201710538455.2A CN201710538455A CN107485583A CN 107485583 A CN107485583 A CN 107485583A CN 201710538455 A CN201710538455 A CN 201710538455A CN 107485583 A CN107485583 A CN 107485583A
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- liquid
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- ganoderma
- toothpaste
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0241—Containing particulates characterized by their shape and/or structure
- A61K8/0245—Specific shapes or structures not provided for by any of the groups of A61K8/0241
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
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- General Health & Medical Sciences (AREA)
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- Oral & Maxillofacial Surgery (AREA)
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- Birds (AREA)
- Epidemiology (AREA)
- Medicines Containing Plant Substances (AREA)
- Cosmetics (AREA)
Abstract
The invention provides a kind of preparation method of ganoderma spove powder toothpaste, it comprises the following steps：Step 1, ganoderma lucidum is cleaned, ganoderma lucidum is crushed after cleaning, it is standby to crush placement；Step 2, the Reishi sporule in the glossy ganoderma powder crushed in extraction step one；Step 3, broken wall treatment is carried out to the Reishi sporule in step 2；Step 4, the Reishi sporule handled well in step 3 is fermented, ganoderma lucidum fermented liquid is obtained after fermentation；Step 5, is filtered and separation of solid and liquid etc. to the ganoderma lucidum fermented liquid in step 4；Step 6, filtering and the good lucidum liquid of separation of solid and liquid in step 5 are carried out extraction thickening-purification technology, drying forms conidia powder powder；Step 7, by the conidia powder powder in step 6 and toothpaste according to weight ratio 1 200：1000 are sufficiently mixed and are molded.
Description
Technical field
The present invention relates to a kind of toothpaste preparation method, in particular it relates to a kind of preparation side of ganoderma spove powder toothpaste
Method.
Background technology
Ganoderma lucidum is the general name of Basidiomycetes On Polyporaceae red sesame and purple sesame, has and strengthens the body resistance to consolidate the constitution and other effects, ganoderma lucidum spore
Sub- powder is the elite of ganoderma lucidum, and lucidum spore powder has antitumor, hypoglycemic, raising body immunity, strengthens the disease-resistant energy of body
Power, liver protection, anti-inflammation, antipyretic-antalgic, reduce transaminase, reduce after cholesterol, the effect such as calmness, but Reishi sporule are taken not
Easily by human consumption, and ganoderma lucidium spore powder wall breaking method mainly utilizes chemical method broken wall or heating means broken wall now, profit
Chemically broken wall is that lucidum spore powder is added into chemical solvent immersion, other PROCESS FOR TREATMENTs is then carried out again, using chemistry
Method broken wall, the composition difficulty or ease separation of chemical solvent is clean, and when people take with other medicines, the chemical substance of residual may
Reacted with other medicines, or chemical analysis directly causes damage to human body；Using the method for heating, due to heating repeatedly,
Temperature is too high, and spore includes active material and is killed or its ingredient change.Product be present in the lucidum spore powder of these methods extraction
Concentration is not high enough, the problems such as product quality is low.
The content of the invention
For in the prior art the defects of, the technical problem to be solved in the present invention is to provide a kind of ganoderma spove powder tooth
The preparation method of cream, it in the case where not destroying the material of lucidum spore powder, can improve the concentration of lucidum spore powder, improve
Product quality, the utilization rate of product is improved, its capacity is absorbed by human body.
According to an aspect of the present invention, there is provided a kind of preparation method of ganoderma spove powder toothpaste, it includes following
Step：
Step 1, ganoderma lucidum is cleaned, ganoderma lucidum is crushed after cleaning, it is standby to crush placement；
Step 2, the Reishi sporule in the glossy ganoderma powder crushed in extraction step one；
Step 3, broken wall treatment is carried out to the Reishi sporule in step 2；
Step 4, the Reishi sporule handled well in step 3 is fermented, ganoderma lucidum fermented liquid is obtained after fermentation；
Step 5, is filtered and separation of solid and liquid to the ganoderma lucidum fermented liquid in step 4；
Step 6, filtering and the good lucidum liquid of separation of solid and liquid in step 5 are carried out extraction thickening-purification technology, drying forms spore
Sub- powder powder；
Step 7, the conidia powder powder in step 6 and toothpaste are compared into 1-200 according to weight：1000 are sufficiently mixed simultaneously
Shaping.
Preferably, the toothpaste component includes：Calcium carbonate, water, D-sorbite, propane diols, hydrated silica, laruyl alcohol sulfuric acid
Ester sodium, essence, HPG, cellulose gum, saccharin sodium, sodium metasilicate, methyl hydroxybenzoate, Nipasol.
Preferably, the toothpaste component includes：40-50% rubbing agents, 20-30% NMFs, 2-5% foaming agents, 1-2%
Thickener, 0.01-0.l% sweeteners, 1-2% chlorophyll.
Preferably, the filter type in the step 5 is suspension is situated between by a kind of filtering with many pores
Matter, suspension thalline and residual media thing is trapped in above this medium, and reach a kind of operation of Solid-Liquid Separation.
Preferably, the step 6 is to be allowed to be changed into the solution of high concentration from the solution removing water or solvent of low concentration.
Preferably, the step 5 uses a kind of following filter type：Natural filtration, pressure filtration, vacuum filter, centrifugation
Filtering.
Preferably, the step 6 is by the way of a kind of following extraction thickening-purification technology：Atmospheric evaporation purification, thin film evaporation
Purification, dry decontamination.
Compared with prior art, the present invention has following beneficial effect：The present invention can not destroy lucidum spore powder
Material in the case of, improve the concentration of lucidum spore powder, improve product quality, improve the utilization rate of product, make its capacity quilt
Human body is absorbed, and ganoderma spove powder has immunological regulation, hypoglycemic, the anti-ageing effect of waiting for a long time, and broken wall spirit is added in toothpaste
Ganoderma lucidum spore powder, add the health-care effect of toothpaste.
Embodiment
With reference to specific embodiment, the present invention is described in detail.Following examples will be helpful to the technology of this area
Personnel further understand the present invention, but the invention is not limited in any way.It should be pointed out that the ordinary skill to this area
For personnel, without departing from the inventive concept of the premise, various modifications and improvements can be made.These belong to the present invention
Protection domain.
The preparation method of ganoderma spove powder toothpaste of the present invention comprises the following steps：
Step 1, ganoderma lucidum is cleaned, ganoderma lucidum is crushed after cleaning, it is standby to crush placement；
Step 2, the Reishi sporule in the glossy ganoderma powder crushed in extraction step one；
Step 3, broken wall treatment is carried out to the Reishi sporule in step 2；
Step 4, the Reishi sporule handled well in step 3 is fermented, ganoderma lucidum fermented liquid is obtained after fermentation；
Step 5, is filtered and separation of solid and liquid to the ganoderma lucidum fermented liquid in step 4；
Step 6, filtering and the good lucidum liquid of separation of solid and liquid in step 5 are carried out extraction thickening-purification technology, drying forms spore
Sub- powder powder；
Step 7, the conidia powder powder in step 6 and toothpaste are compared into 1-200 according to weight：1000 are sufficiently mixed simultaneously
Shaping.
Preferably, the toothpaste component includes：Calcium carbonate, water, D-sorbite, propane diols, hydrated silica, laruyl alcohol sulfuric acid
Ester sodium, essence, HPG, cellulose gum, saccharin sodium, sodium metasilicate, methyl hydroxybenzoate, Nipasol.
Preferably, the toothpaste component includes：40-50% rubbing agents, 20-30% NMFs, 2-5% foaming agents, 1-2%
Thickener, 0.01-0.l% sweeteners, 1-2% chlorophyll.
Filter type in the step 5 is to make suspension make to hang by a kind of filter medium with many pores
Floating thalline and residual media thing are trapped in above this medium, and reach a kind of operation of Solid-Liquid Separation.
Filter type in the step 5 includes following several：
First, natural filtration, it mainly produces motive force by a filtrate potential difference and causes filtering；
2nd, pressure filtration, it is mainly with the pressure suffered by a compressed gas larger fluid or defeated sample liquid with a pump
Motive force of the hydraulic pressure as filtering is produced when delivering to filter；
3rd, vacuum filter, itself and pressure filtration are on the contrary, be just to be vacuumized under filter medium, to increase on filter medium
Under pressure difference, promote solvent have rotary drum vacuum filter by filter medium, conventional vacuum filter；
4th, centrifugal filtration, by the use of rotary drum, centrifugal force as the motive force of filtering, makes suspension caused by rotation at a high speed for it
Middle thalline separates with liquid；Because caused centrifugal force is larger, the rate of filtration is very fast, most uses in medicinal fungi is produced
Centrifugation apparatus has heavy configuration centrifuge, horizontal centrifuge, tubular-bowl centrifuge, link-suspended basket centrifuge etc.；Wherein 3-foot from
Scheming is a kind of conventional centrifuge of current medicinal fungi production, and it has simple in construction, smooth operation, floor space small, solid
The advantages that scapus does not wear, especially suitable for small lot, the medium bulk crystalline material of multi items and very thin shape material
Dehydration.
The step 6 is to be allowed to be changed into the solution of high concentration, heating and decompression from the solution removing water or solvent of low concentration
One of the most frequently used method of vaporation-type, such convenient use.
The mode of extraction thickening-purification technology in the step 6 includes following several：
First, atmospheric evaporation purifies, and thickening-purification technology liquid to be extracted evaporates at ambient pressure, is steamed using a kind of stainless steel of jacket type
Pot is sent out, this equipment is an open Dumpage type folder evaporation boiler, and chuck pot is fixed in hollow shaft, has pot wheel that pot can be made any on axle
Rotate, steam is passed through from connecting tube, and condensed water flows out from connecting tube, and active ingredient of this equipment suitable for liquid is heat-resisting
's；Product chemical stability is strong, molten coal again without flammability, and it is nontoxic with it is harmless；
2nd, thin film evaporation purifies, and is liquid is formed film, increase gasification surface, accelerates evaporation；Steamed using a film
There is upright heating tube in hair device, heat transfer area is larger, and liquid under reduced pressure, into heating tube, pulls into liquid of evaporation thin
Film runs through the inwall of pipe, continuous evaporation, is the advantages of thin film evaporation：Liquid film surface is very big, and heat transfer is fast and uniform, and liquid exists
Evaporation tube residence time is very short, accordingly even when temperature is slightly higher, material is not easy to destroy；
3rd, dry decontamination, the process that the aqueous solvent in the solid of humidity, paste, concentrate and liquid is evolved；Its mesh
Be improve product stability, it is met defined standard, the thickening-purification technology of Ganoderma lucidum mycelium body fluid zymotic fluid is typically often adopted
With spray dry scrubbing method；Spray drying is that feed liquid (aqueous more than 50% solution, suspension, pulpous state liquid etc.) is sprayed into mist
Drop is scattered in thermal current, moisture is evaporated rapidly and is turned into granular dried product；The effect of spray dry scrubbing is decided by
Droplet size, when fogdrop diameter is 10um or so, the number of drops that every liter of liquid is formed can reach Total face
Product can reach 600m2, for usual fogdrop diameter between 10~50um, surface area is big, and evaporation is exceedingly fast, and drying time is very short, number
Second to number 10 seconds, moisture evaporation, which takes away heat, can also be such that the temperature of drop and surrounding reduces rapidly；Therefore can do at ambient pressure
Dry heat sensitive material, the granularity and water content of product can also be adjusted by changing operating condition, and can be made and hollow be paid spherical production
Product, it is easy to dissolve；Spray dry scrubbing device includes：Spray chamber, liquid sprayer, heat air and it is connected into spraying
The equipment of room, from damp-heat air separate fine powder device；Air filters through a filter frame, and being sent into air by an air blower adds
Hot cell, the air pressure of oven heats pipe maintain 8.5kgcm-2, add 130 DEG C of air themperature；Material by an air compressor or
One high-pressure pump is with 70Kgcm-2Pressure be sprayed into mist, evaporation drying immediately of being met in spray chamber with hot-air, obtain pole
The finished product of fine cleaning；The fine powder of dry decontamination largely falls thin in the bottom of spray chamber, the drying that fraction is taken away by hot-air
Powder is then collected in bag hose, and waste gas is discharged into outdoor through centrifugal exhaust blower air blower；Cooling spray drying principle be
Make air dehydration before heating using hygroscopic agent, reduce air humidity, the temperature of spray drying can be further reduced, so as to carry
The quality of high spray dried products.
The specific embodiment of the present invention is described above.It is to be appreciated that the invention is not limited in above-mentioned
Particular implementation, those skilled in the art can make various deformations or amendments within the scope of the claims, this not shadow
Ring the substantive content of the present invention.
Claims (7)
1. a kind of preparation method of ganoderma spove powder toothpaste, it is characterised in that comprise the following steps：
Step 1, ganoderma lucidum is cleaned, ganoderma lucidum is crushed after cleaning, it is standby to crush placement；
Step 2, the Reishi sporule in the glossy ganoderma powder crushed in extraction step one；
Step 3, broken wall treatment is carried out to the Reishi sporule in step 2；
Step 4, the Reishi sporule handled well in step 3 is fermented, ganoderma lucidum fermented liquid is obtained after fermentation；
Step 5, is filtered and separation of solid and liquid to the ganoderma lucidum fermented liquid in step 4；
Step 6, filtering and the good lucidum liquid of separation of solid and liquid in step 5 are carried out extraction thickening-purification technology, drying forms conidia powder
Powder；
Step 7, the conidia powder powder in step 6 and toothpaste are compared into 1-200 according to weight：1000 be sufficiently mixed and into
Type.
2. preparation method according to claim 1, it is characterised in that the toothpaste component includes：Calcium carbonate, water, sorb
Sugar alcohol, propane diols, hydrated silica, laruyl alcohol sodium sulfovinate, essence, HPG, cellulose gum, saccharin sodium, sodium metasilicate,
Methyl hydroxybenzoate, Nipasol.
3. preparation method according to claim 1, it is characterised in that the toothpaste component includes：40-50% rubbing agents,
20-30% NMFs, 2-5% foaming agents, 1-2% thickeners, 0.01-0.l% sweeteners, 1-2% chlorophyll.
4. the preparation method according to Claims 2 or 3, it is characterised in that the filter type in the step 5 is to make to hang
Supernatant liquid makes suspension thalline and residual media thing be trapped on this medium by a kind of filter medium with many pores
Face, and reach a kind of operation of Solid-Liquid Separation.
5. preparation method according to claim 4, it is characterised in that the step 6 is to remove water from the solution of low concentration
Or solvent is allowed to be changed into the solution of high concentration.
6. preparation method according to claim 5, it is characterised in that the step 5 uses a kind of following filter type：
Natural filtration, pressure filtration, vacuum filter, centrifugal filtration.
7. preparation method according to claim 6, it is characterised in that the step 6 is net using a kind of following extraction concentration
The mode of change：Atmospheric evaporation purification, thin film evaporation purification, dry decontamination.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710538455.2A CN107485583A (en) | 2017-07-04 | 2017-07-04 | The preparation method of ganoderma spove powder toothpaste |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710538455.2A CN107485583A (en) | 2017-07-04 | 2017-07-04 | The preparation method of ganoderma spove powder toothpaste |
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| CN201710538455.2A Pending CN107485583A (en) | 2017-07-04 | 2017-07-04 | The preparation method of ganoderma spove powder toothpaste |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115887308A (en) * | 2022-11-10 | 2023-04-04 | 武夷山元生泰生物科技有限公司 | Ganoderma lucidum toothpaste and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105362155A (en) * | 2015-12-15 | 2016-03-02 | 江苏道诚生物科技有限公司 | Toothpaste composition containing lucid ganoderma component and preparation method of toothpaste composition |
| CN105769667A (en) * | 2016-03-18 | 2016-07-20 | 无限极（中国）有限公司 | Lucid ganoderma fermentation liquor preparation method and application of lucid ganoderma fermentation liquor |
-
2017
- 2017-07-04 CN CN201710538455.2A patent/CN107485583A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105362155A (en) * | 2015-12-15 | 2016-03-02 | 江苏道诚生物科技有限公司 | Toothpaste composition containing lucid ganoderma component and preparation method of toothpaste composition |
| CN105769667A (en) * | 2016-03-18 | 2016-07-20 | 无限极（中国）有限公司 | Lucid ganoderma fermentation liquor preparation method and application of lucid ganoderma fermentation liquor |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115887308A (en) * | 2022-11-10 | 2023-04-04 | 武夷山元生泰生物科技有限公司 | Ganoderma lucidum toothpaste and preparation method thereof |
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Application publication date: 20171219 |