CN107484860A - A kind of method for improving dai medicine kidney tea active ingredient dissolution rate - Google Patents

A kind of method for improving dai medicine kidney tea active ingredient dissolution rate Download PDF

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Publication number
CN107484860A
CN107484860A CN201710909682.1A CN201710909682A CN107484860A CN 107484860 A CN107484860 A CN 107484860A CN 201710909682 A CN201710909682 A CN 201710909682A CN 107484860 A CN107484860 A CN 107484860A
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kidney tea
time
tea
kidney
fixing
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Inventor
李光
李宜航
罗云
马国需
陈德力
吕亚娜
李学兰
陈曦
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Institute of Medicinal Plant Development of CAMS and PUMC
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Institute of Medicinal Plant Development of CAMS and PUMC
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Priority to CN201710909682.1A priority Critical patent/CN107484860A/en
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23FCOFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
    • A23F3/00Tea; Tea substitutes; Preparations thereof
    • A23F3/34Tea substitutes, e.g. matè; Extracts or infusions thereof

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

The invention discloses a kind of method for improving dai medicine kidney tea active ingredient dissolution rate, comprise the following steps:It is that raw material carries out first time fixing that step (1), which chooses folium orthosiphoni leaf or tender stem position,;Spread out and hang in ventilation shady spot after fixing;Kidney tea after drying again is placed on second of fixing of progress;Step (2) is cooled to room temperature by the kidney tea after fixing is cool, carries out pile fermentation;Kidney tea after pile fermentation knead for the first time;Kidney tea Quick uniform after kneading is dismissed, and shady spot, which spreads out, to be hung;Step (3) finishes the kidney tea third time of dismission;Kidney tea booth after fixing is thin uniformly, and shady spot is hung;Kidney tea after hanging is kneaded to aobvious milli for the second time;Kidney tea is rubbed to group or rubbed along vein to strip by step (4);Pot stir-frying is changed, then gradually heating carries out heating, drying, is then down to room temperature, takes the dish out of the pot.Present invention process is simple, easy to operate, the kidney tea tea mouthfeel lifting after processing, and soaked rear its active ingredient dissolution rate increase.

Description

A kind of method for improving dai medicine kidney tea active ingredient dissolution rate
Technical field
The invention belongs to dai medicine kidney tea process technology field, more particularly to a kind of raising dai medicine kidney tea active ingredient dissolution rate Method.
Background technology
Kidney tea [Clerodendranthus spicatus (thunb) C.Y.Wu] also known as Mao Xu Cao, it is Labiatae kidney Camellia Herbaceos perennial, is the conventional antidote kind of Dai Nationality doctor, Confucian classics record can alone decoct soup or boiling water immersion work as tea-drinking, have The usage history of more than 2000 years, there is clearing heat and detoxicating, inducing diuresis for removing edema, diuresis fossil, support kidney and protect the function such as kidney, cooling blood and hemostasis, it is existing Generation research show in kidney tea chemical composition mainly include flavonoids (Tezuka et al., 2000, Stampoulis et al., 1999, Awale et al., 2001), terpene (Tezuka et al., 2000, Stampoulis et al., 1999, Awale Et al., 2001), phenolic acid class (Tezuka et al., 2000, Akowuah et al., 2005), amino acids (Zhang Ping, 2000), vitamin, mineral matter and volatile oil (Hossain et al., 2008).Pharmaceutical research shows, clerodendranthus spicatus extract With diuresis (Beaux et al., 1999, Yuliana et al., 2009, Adam et al., 2009, Ting et al., 2009, Arafat et al., 2008, Du Dat et al., 1992), row's stone (Cai Hua virtue et al., 2008), improve it is chronic Renal failure (Zhang Shaogui, 2008, Jiang Weisheng, 2009), reducing blood sugar and blood lipid (Sriplang et al., 2007, Mohamed et al., 2011), anti-inflammatory (high South-South et al., 1996, Yam et al., 2010), it is anti-oxidant (MATKOWSKI, 2008, Akowuah Et al., 2004) free radical (Akowuah et al., 2005), liver protection (Mohammed, 2011, Maheswari et, are removed Al., 2008) pharmacology such as immunity of organisms (Cen little Bo and Wang Rui are refined, 1997), anti-senile dementia (trip is for army building, 2015), are improved Activity, wherein active component be phenolic acid class and flavonoids (Li Yueting, 2003, Lin Zhimin, 2009, Akowuah et al., 2004), there are wide market prospects.
It is that will be dried after kidney tea aerial part segment in traditional application process, boiling water soaks on behalf of the tea, and its active component is molten Out-degree is not high, and has the blue or green taste of grass, influences mouthfeel, mouthfeel can be adapted to after needing long-term use, although existing market has processing Tea bag afterwards, but sensory issues are still unresolved, and active constituent content is relatively low in kidney tea old stem, influences kidney tea drug effect.
The content of the invention
In view of the shortcomings of the prior art, the present invention provides a kind of method for improving dai medicine kidney tea active ingredient dissolution rate, this It is that raw material passes through active ingredient after processing raising kidney tea mouthfeel and water logging to invent and choose the tender tip position of kidney tea band 2-3 pieces or folium orthosiphoni leaf Dissolution rate.
First aspect present invention, there is provided a kind of method for improving dai medicine kidney tea active ingredient dissolution rate, comprise the following steps:
The tender stem position that step (1) chooses folium orthosiphoni leaf or top tape 2-3 piece leaves carries out first time fixing for raw material;For the first time Kidney tea is spread out in ventilation shady spot and hung after fixing;Kidney tea after drying again is placed on second of fixing of progress;
Step (2) second is finished after kidney tea it is cool be cooled to room temperature, then carry out pile fermentation;Kidney after pile fermentation is placed Tea knead for the first time;Kidney tea Quick uniform after kneading is dismissed, and shady spot, which spreads out, to be hung;
The kidney tea that step (3) scatters solution carries out third time fixing;Kidney tea booth after third time is finished is thin uniformly, in the shade Place is hung;Kidney tea after hanging is kneaded to aobvious milli for the second time;
Step (4) and then heated in pot, kidney tea is rubbed to group or rubbed along vein to strip;Pot is changed to be turned over Fry, shake loose frequently, repeated multiple times, to water content 15~25%, then gradually heating carries out heating, drying again, is then down to room Temperature, take the dish out of the pot.
Further, 250~280 DEG C of step (1) first time fixing temperature, fixation time are 30~60s;Second of fixing 300~350 DEG C of temperature, fixation time are 30~60s,
Further, 1~2h is covered with moistening cotton during step (2) pile fermentation, to reduce fragrance loss;When kneading for the first time Between be 1~2h.
Further, step (3) third time fixing temperature is 120~150 DEG C, and second of time of kneading is 20~40min.
Further, kidney tea is rubbed with the hands under the conditions of 100~120 DEG C to group or rubbed along vein to strip by step (4), so After change pot and stir-fried at a temperature of 50~60 DEG C, shake loose frequently, it is repeated multiple times, to water content 15~25%, then gradually plus Temperature is dried to 120~150 DEG C.
Second aspect of the present invention, there is provided kidney tea made from methods described.
Further, the kidney tea can be mixed to prepare corresponding drink with other teas.
The features of the present invention is as follows:The present invention is processed kidney tea by fixing method three times, by first time fixing mesh Be in order that kidney tea young stem and leaf rapid dehydration, can ensure kidney tea integrality and color and luster, finished product is after bubble after processing, branch Bar is complete, and color and luster is light green, has preferable form;The purpose of second of green removing in high temperature is to destroy kidney tea organelle at high operating temperatures Structure, at the same make kidney tea space between cells increase, ensure active ingredient can rapid dissolution, and improve active ingredient dissolution rate; Third time fixing purpose is the continuous high temperature during kneading, and destroys the original blue or green taste of grass of kidney tea, further improves product Mouthfeel simultaneously lays the foundation for next step product approval.
Compared with prior art, the invention has the advantages that:Present invention process is simple, easy to operate, after processing The lifting of kidney tea mouthfeel, and it is soaked after the increase of its active ingredient dissolution rate, can preferably play the medical value of kidney tea.
Brief description of the drawings
Fig. 1 is the result figure of active ingredient dissolution rate;
Fig. 2 is the content detection of active ingredient;
Embodiment
Technical scheme is described in further details with reference to specific embodiment, but the present invention does not limit to In following technical scheme.
Embodiment 1
(1) it is raw material to choose folium orthosiphoni leaf or top tape 2-3 piece leaf tender stems position, in 260 DEG C of fixings;
(2) kidney tea is spread out in ventilation shady spot and hangs 20h after finishing;
(3) finished at a temperature of 320 DEG C that the kidney tea after drying again is placed on, the time is 40s;
(4) by again finish after kidney tea it is cool be cooled to normal temperature, then carry out pile fermentation, with moistening cotton covering 1h, to subtract Few fragrance is lost in;
(5) the kidney tea after pile fermentation is placed knead for the first time, gently rubs 1h;
(6) the kidney tea Quick uniform after kneading is dismissed, and shady spot, which spreads out, to be hung;
(7) the kidney tea that solution is scattered is finished again at a temperature of 120 DEG C, to deviate from moisture;
(8) the kidney tea booth after fixing is thin uniformly, shady spot is hung, and ensures its color and luster;
(9) the kidney tea after hanging is kneaded again, time of kneading 20min, to aobvious milli.
(10) enter pot heating, 100 DEG C, 35min, kidney tea is rubbed to group or rubbed along vein to strip.
(11) change pot to be stir-fried at a temperature of 50, shake loose frequently, it is repeated multiple times, to water content 15~20%, then 120 DEG C of progress heating, dryings are gradually warmed to again, are then down to room temperature, are taken the dish out of the pot, you can.
Contained using total phenolics and general flavone after kidney tea boiling water bubble after determined by ultraviolet spectrophotometry kidney tea medicinal material and processing Amount, finds the dissolution rate by that can effectively improve active ingredient after the processing of the present embodiment technique, and untreated kidney tea medicinal material passes through After boiling water bubble, total phenolics constituents content is 15.15 ± 3.37%, and total flavonoid component content is 0.82 ± 0.12%;Pass through This technique processing after kidney tea boiling water bubble after total phenolics class be 28.96 ± 4.18%, total flavonoid component content be 1.35 ± 0.16%, as a result as shown in figure 1,1-14 chromatographic peaks peak area increase in Fig. 2 chromatograms, illustrates kidney tea after processing, 1-14 The increase of composition dissolution rate, and kidney tea, by the way that after this PROCESS FOR TREATMENT, mouthfeel is obviously improved, the blue or green taste of grass disappears, and returns sweet effect enhancing, Diuresis is more obvious.
Embodiment 2
(1) it is raw material to choose folium orthosiphoni leaf or top tape 2-3 piece leaf tender stems position, in 260 DEG C of fixings;
(2) kidney tea is spread out in ventilation shady spot and hangs 20h after finishing;
(3) being finished at a temperature of 320 DEG C that the kidney tea after drying again is placed on, the time is 40s, while not carry out The kidney tea medicinal material of second of fixing is control group, and subsequent treatment is identical;
(4) by again finish after kidney tea it is cool be cooled to normal temperature, then carry out pile fermentation, with moistening cotton covering 1h, to subtract Few fragrance is lost in;
(5) the kidney tea after pile fermentation is placed knead for the first time, gently rubs 1h;
(6) the kidney tea Quick uniform after kneading is dismissed, and shady spot, which spreads out, to be hung;
(7) the kidney tea that solution is scattered is finished again at a temperature of 120 DEG C, to deviate from moisture;
(8) the kidney tea booth after fixing is thin uniformly, shady spot is hung, and ensures its color and luster;
(9) the kidney tea after hanging is kneaded again, time of kneading 20min, to aobvious milli.
(10) enter pot heating, 100 DEG C, 35min, kidney tea is rubbed to group or rubbed along vein to strip.
(11) change pot to be stir-fried at a temperature of 50, shake loose frequently, it is repeated multiple times, to water content 15~20%, then 120 DEG C of progress heating, dryings are gradually warmed to again, are then down to room temperature, are taken the dish out of the pot, you can.
According to version in 2015《Chinese Pharmacopoeia》The Extract mensuration of general rule 2201,11 batches of kidney tea medicinal materials and processing are determined respectively Water-soluble extract content, as a result as shown in the table in medicinal material:
Influence of the different disposal method of table 1 to kidney tea dissolubility extract content
As a result finding, the water-soluble extractives content by second of green removing in high temperature kidney tea medicinal material is 33.49 ± 2.76%, And the water-soluble extractives content for not carrying out second of fixing kidney tea medicinal material is 25.40 ± 2.96%, and there is pole between the two Significant difference, illustrate after second finishes, can greatly destroy kidney tea crude drug cell structure, it is molten to be advantageous to water soluble ingredient Go out.
Embodiment 3
(1) it is raw material to choose folium orthosiphoni leaf or top tape 2-3 piece leaf tender stems position, in 260 DEG C of fixings;
(2) kidney tea is spread out in ventilation shady spot and hangs 20h after finishing;
(3) being finished at a temperature of 280 DEG C and 320 DEG C that the kidney tea after drying again is individually placed to, the time is 40s, Subsequent treatment is identical;
(4) by again finish after kidney tea it is cool be cooled to normal temperature, then carry out pile fermentation, with moistening cotton covering 1h, to subtract Few fragrance is lost in;
(5) the kidney tea after pile fermentation is placed knead for the first time, gently rubs 1h;
(6) the kidney tea Quick uniform after kneading is dismissed, and shady spot, which spreads out, to be hung;
(7) the kidney tea that solution is scattered is finished again at a temperature of 120 DEG C, to deviate from moisture;
(8) the kidney tea booth after fixing is thin uniformly, shady spot is hung, and ensures its color and luster;
(9) the kidney tea after hanging is kneaded again, time of kneading 20min, to aobvious milli.
(10) enter pot heating, 100 DEG C, 35min, kidney tea is rubbed to group or rubbed along vein to strip.
(11) change pot to be stir-fried at a temperature of 50, shake loose frequently, it is repeated multiple times, to water content 15~20%, then 120 DEG C of progress heating, dryings are gradually warmed to again, are then down to room temperature, are taken the dish out of the pot, you can.
According to version in 2015《Chinese Pharmacopoeia》The Extract mensuration of general rule 2201,11 batches of kidney tea medicinal materials and processing are determined respectively Water-soluble extract content, as a result as shown in the table in medicinal material:
Influence of second of the fixing different temperatures of table 2 to kidney tea dissolubility extract content
As a result finding, the water-soluble extractives content by 320 DEG C of green removing in high temperature kidney tea medicinal materials is 33.49 ± 2.76%, And the water-soluble extractives content of 280 DEG C of fixing kidney tea medicinal materials is 27.03 ± 1.33%, and there is pole significance difference between the two It is different, illustrate that second of fixing temperature has considerable influence to kidney tea soluble components dissolution rate.
Embodiment 4
(1) it is raw material to choose folium orthosiphoni leaf or top tape 2-3 piece leaf tender stems position, spreads out and hangs in ventilation shady spot after collection 20h;
(2) hang rear kidney tea and carry out pile fermentation processing with moistening cotton covering 1h, to reduce fragrance loss;
(3) the kidney tea after pile fermentation is placed knead for the first time, gently rubs 1h;
(4) the kidney tea Quick uniform after kneading is dismissed, and shady spot, which spreads out, to be hung;
(5) hang rear kidney tea and enter pot heating, 100 DEG C, 35min, kidney tea is rubbed to group or rubbed along vein to strip.
(11) change pot to be stir-fried at a temperature of 50, shake loose frequently, it is repeated multiple times, to water content 15~20%, then 120 DEG C of progress heating, dryings are gradually warmed to again, are then down to room temperature, are taken the dish out of the pot, you can.
As a result find, after kidney tea is kneaded without fixing processing, obtain that finished product powder is more, and soaked rear blade integrity degree is not Height, still there is a small amount of blue or green taste of grass in mouthfeel, and active ingredient dissolution rate is not high.
Embodiment 5
(1) it is raw material to choose folium orthosiphoni leaf or top tape 2-3 piece leaf tender stems position, in 260 DEG C of fixings;
(2) kidney tea is spread out in ventilation shady spot and hangs 20h after finishing;
(3) being finished at a temperature of 280 DEG C and 320 DEG C that the kidney tea after drying again is individually placed to, the time is 40s, Subsequent treatment is identical;
(4) by again finish after kidney tea it is cool be cooled to normal temperature, then carry out pile fermentation, with moistening cotton covering 1h, to subtract Few fragrance is lost in;
(5) the kidney tea after pile fermentation is placed knead for the first time, gently rubs 1h;
(6) the kidney tea Quick uniform after kneading is dismissed, and shady spot, which spreads out, to be hung;
(7) the kidney tea after hanging is kneaded again, time of kneading 20min, to aobvious milli.
(8) enter pot heating, 100 DEG C, 35min, kidney tea is rubbed to group or rubbed along vein to strip.
(9) change pot to be stir-fried at a temperature of 50, shake loose frequently, it is repeated multiple times, to water content in 15~20%, Ran Houzai 120 DEG C of progress heating, dryings are gradually warmed to, room temperature is then down to, takes the dish out of the pot, you can.
As a result find, kidney tea is handled without third time fixing, and final products are not easy to shape, and soaked rear blade integrity degree is not Height, it is attractive in appearance to influence product.

Claims (7)

  1. A kind of 1. method for improving dai medicine kidney tea active ingredient dissolution rate, it is characterised in that the described method comprises the following steps:
    The tender stem position that step (1) chooses folium orthosiphoni leaf or top tape 2-3 piece leaves carries out first time fixing for raw material;Finish for the first time Kidney tea is spread out in ventilation shady spot and hung afterwards;Kidney tea after drying again is placed on second of fixing of progress;
    Step (2) second is finished after kidney tea it is cool be cooled to room temperature, then carry out pile fermentation;Kidney tea after pile fermentation is placed enters Row is kneaded for the first time;Kidney tea Quick uniform after kneading is dismissed, and shady spot, which spreads out, to be hung;
    The kidney tea that step (3) scatters solution carries out third time fixing;Kidney tea booth after third time is finished is thin uniformly, and shady spot enters Row is hung;Kidney tea after hanging is kneaded to aobvious milli for the second time;
    Step (4) and then heated in pot, kidney tea is rubbed to group or rubbed along vein to strip;Change pot to be stir-fried, no When shake loose, repeated multiple times, to water content 15~25%, then gradually heating carries out heating, drying again, is then down to room temperature, goes out Pot.
  2. 2. the method for dai medicine kidney tea active ingredient dissolution rate is improved as claimed in claim 1, it is characterised in that step (1) the 250~280 DEG C of a fixing temperature, fixation time are 30~60s;Second of 300~350 DEG C of fixing temperature, fixation time are 30~60s.
  3. 3. the method for dai medicine kidney tea active ingredient dissolution rate is improved as claimed in claim 1, it is characterised in that step (2) is wet 1~2h is covered with moistening cotton during heap, to reduce fragrance loss;First time time of kneading is 1~2h.
  4. 4. the method for dai medicine kidney tea active ingredient dissolution rate is improved as claimed in claim 1, it is characterised in that step (3) the Fixing temperature is 120~150 DEG C three times, and second of time of kneading is 20~40min.
  5. 5. the method for dai medicine kidney tea active ingredient dissolution rate is improved as claimed in claim 1, it is characterised in that step (4) will Kidney tea is rubbed with the hands to group under the conditions of 100~120 DEG C or rubbed along vein to strip, is then changed pot and is carried out at a temperature of 50~60 DEG C Stir-frying, shakes loose frequently, repeated multiple times, to water content 15~25%, then is gradually warmed to 120~150 DEG C of drying.
  6. A kind of 6. kidney tea made from method as described in Claims 1 to 5 is any.
  7. 7. kidney tea as claimed in claim 6, it is characterised in that the kidney tea can be mixed to prepare corresponding drink with other teas Product.
CN201710909682.1A 2017-09-29 2017-09-29 A kind of method for improving dai medicine kidney tea active ingredient dissolution rate Pending CN107484860A (en)

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Cited By (3)

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Publication number Priority date Publication date Assignee Title
CN109566818A (en) * 2019-01-29 2019-04-05 韩佳妹 A kind of Mao Xu Cao tea preparation technique method
CN111357845A (en) * 2020-04-17 2020-07-03 上海市农业科学院 Processing method of clerodendranthus spicatus
CN111838368A (en) * 2020-06-29 2020-10-30 上海琮益科技有限公司 Method for mechanically frying clerodendranthus spicatus

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CN102669372A (en) * 2012-06-06 2012-09-19 海南大学 Alpinia oxyphylla miq clerodendranthus spicatus
CN106212751A (en) * 2016-08-12 2016-12-14 贵州省贵定县凤凰茶业有限责任公司 A kind of processing technology of green tea

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CN102669372A (en) * 2012-06-06 2012-09-19 海南大学 Alpinia oxyphylla miq clerodendranthus spicatus
CN106212751A (en) * 2016-08-12 2016-12-14 贵州省贵定县凤凰茶业有限责任公司 A kind of processing technology of green tea

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109566818A (en) * 2019-01-29 2019-04-05 韩佳妹 A kind of Mao Xu Cao tea preparation technique method
CN111357845A (en) * 2020-04-17 2020-07-03 上海市农业科学院 Processing method of clerodendranthus spicatus
CN111357845B (en) * 2020-04-17 2023-06-20 上海市农业科学院 Kidney tea processing method
CN111838368A (en) * 2020-06-29 2020-10-30 上海琮益科技有限公司 Method for mechanically frying clerodendranthus spicatus

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