CN107476068A - A kind of use for synthetic leather is molded wear-resisting bright face inorganic agent of scratch resistance and preparation method thereof - Google Patents
A kind of use for synthetic leather is molded wear-resisting bright face inorganic agent of scratch resistance and preparation method thereof Download PDFInfo
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- CN107476068A CN107476068A CN201710710983.1A CN201710710983A CN107476068A CN 107476068 A CN107476068 A CN 107476068A CN 201710710983 A CN201710710983 A CN 201710710983A CN 107476068 A CN107476068 A CN 107476068A
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- resisting
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- wear
- agent
- scratch resistance
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Classifications
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/564—Polyureas, polyurethanes or other polymers having ureide or urethane links; Precondensation products forming them
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/02—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with hydrocarbons
- D06M13/03—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with hydrocarbons with unsaturated hydrocarbons, e.g. alkenes, or alkynes
- D06M13/07—Aromatic hydrocarbons
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/12—Aldehydes; Ketones
- D06M13/127—Mono-aldehydes, e.g. formaldehyde; Monoketones
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/50—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with organometallic compounds; with organic compounds containing boron, silicon, selenium or tellurium atoms
Abstract
The invention discloses a kind of use for synthetic leather to be molded the wear-resisting bright face inorganic agent of scratch resistance, and it is used for the back segment typography of synthetic leather, includes following components：Modified polyurethane, butyl ester, toluene, butanone, wear-resisting scratch-resisting agent, methyl tin heat stabilizer and slipping agent.The invention also discloses the preparation method that above-mentioned use for synthetic leather is molded the wear-resisting bright face inorganic agent of scratch resistance.Each component that present invention composition is molded the wear-resisting bright face inorganic agent of scratch resistance is mutually coordinated, collective effect, the leather gloss made with such a inorganic agent is natural, color clarification, injection effect is good, bright-colored transparent, crystal-feel is strong, there is splendid stereovision, leather surface sense of touch effect is good after processing, and leather surface feel is dry and comfortable, wear-resisting scratch resistance is good, and resultant effect is good.
Description
Technical field
It is more particularly to a kind of bright with the wear-resisting scratch resistance of use for synthetic leather injection the present invention relates to use for synthetic leather surface conditioning agent field
Face inorganic agent and preparation method thereof.
Background technology
Bright face synthesis leather goods are increasingly welcome by consumers in general.But current bright face synthetic leather generally existing
The flimsy shortcoming in surface, friction and scratch lead to the damage in bright face.And at the existing bright face of the wear-resisting scratch resistance of use for synthetic leather
There is the problems such as comprehensive treatment effect is bad in reason agent, can not meet consumer demand.
The content of the invention
In view of the above-mentioned problems, it is an object of the invention to provide one kind with use for synthetic leather be molded the bright face inorganic agent of wear-resisting scratch resistance and
Its preparation method, solve use for synthetic leather and be molded the problems such as comprehensive treatment effect existing for the wear-resisting bright face inorganic agent of scratch resistance is bad.
To achieve the above object, the present invention takes following technical scheme：
A kind of use for synthetic leather is molded the wear-resisting bright face inorganic agent of scratch resistance, and it is used for the back segment typography of synthetic leather, comprising with
Lower component：Modified polyurethane, butyl ester, toluene, butanone, wear-resisting scratch-resisting agent, methyl tin heat stabilizer and slipping agent.
Further, in terms of mass parts, the proportioning for each component being molded in the bright face inorganic agent of wear-resisting scratch resistance is as follows：It is modified poly-
35~38 parts of urethane, 10~12 parts of butyl ester, 20~22 parts of toluene, 28~30 parts of butanone, 1~2 part of wear-resisting scratch-resisting agent, methyl tin heat
1~2 part of stabilizer, 0~1 part of slipping agent.
Further, in terms of mass parts, the proportioning for each component being molded in the bright face inorganic agent of wear-resisting scratch resistance is as follows：It is modified poly-
36~38 parts of urethane, 11.5~12 parts of butyl ester, 20~22 parts of toluene, 28~30 parts of butanone, 1~2 part of wear-resisting scratch-resisting agent, methyl tin
1~2 part of heat stabilizer, 0~1 part of slipping agent.
Further, in terms of mass parts, the proportioning for each component being molded in the bright face inorganic agent of wear-resisting scratch resistance is as follows：It is modified poly-
36 parts of urethane, 11.5 parts of butyl ester, 22 parts of toluene, 28 parts of butanone, 1 part of wear-resisting scratch-resisting agent, 1 part of methyl tin heat stabilizer, slipping agent
0.5 part.
A kind of any of the above-described use for synthetic leather is molded the preparation method of the wear-resisting bright face inorganic agent of scratch resistance, comprises the steps of:
Step 1：By formula by partially modified polyurethane, butyl ester, toluene, butanone, wear-resisting scratch-resisting agent, methyl tin heat stabilizer
Mixture is uniformly mixing to obtain after mixing；
Step 2：It is made being added in the mixture obtained by step 1 after remaining modified polyurethane and slipping agent stir
It is molded the bright face inorganic agent of wear-resisting scratch resistance.
Further, in terms of mass parts, the proportioning of each component is as follows in this method：35~38 parts of modified polyurethane, butyl ester
10~12 parts, it is 20~22 parts of toluene, 28~30 parts of butanone, 1~2 part of wear-resisting scratch-resisting agent, 1~2 part of methyl tin heat stabilizer, smooth
0~1 part of agent.
Further, the raw material proportioning in the step 1 in this method is calculated as with mass parts：Partially modified polyurethane 31~33
Part, 10~12 parts of butyl ester, 20~22 parts of toluene, 28~30 parts of butanone, 1~2 part of wear-resisting scratch-resisting agent, methyl tin heat stabilizer 1~2
Part.
Further, 2~5 parts of the remaining modified polyurethane in step 2, and partially modified polyurethane and step in step 1
The overall control of remaining modified polyurethane in rapid 2 is at 35~38 parts, and 0~1 part of slipping agent.
Further, all steps in this method are carried out at normal temperatures and pressures.
Due to using above technical scheme, the present invention has following advantageous effects compared with prior art：
1. each component of the wear-resisting bright face inorganic agent of scratch resistance of present invention composition injection is mutually coordinated, collective effect, by group
Addition time and addition is divided accurately to be controlled so that the leather gloss made with such a inorganic agent is naturally, color clarification, injection
Effect is good, and bright-colored transparent, crystal-feel is strong, there is splendid stereovision, and leather surface sense of touch effect is good after processing, and leather surface feel is done
Refreshing, wear-resisting scratch resistance is good, and resultant effect is good；
2. the wear-resisting bright face inorganic agent of scratch resistance of injection of the present invention is a kind of new material of back segment printing, can be in existing synthesis
Applied on leather production line, technique is simple and need not change production equipment increase cost.
Brief description of the drawings
The following drawings is only intended to, in doing schematic illustration and explanation to the present invention, not delimit the scope of the invention.Wherein：
Fig. 1 is the flow chart that the use for synthetic leather of the present invention is molded the preparation method of the wear-resisting bright face inorganic agent of scratch resistance.
Embodiment
For the purposes of the present invention, technical scheme and advantage are more clearly understood, and, are below against accompanying drawing in conjunction with the embodiments
The present invention is further elaborated.It should be appreciated that specific embodiment described herein is only to explain the present invention, not
For limiting the present invention.
A kind of use for synthetic leather of the present invention is molded the wear-resisting bright face inorganic agent of scratch resistance, includes following components：Modified polyurethane, fourth
Ester, toluene, butanone, wear-resisting scratch-resisting agent, methyl tin heat stabilizer and slipping agent.
In terms of mass parts, the proportioning of each component is as follows：35~38 parts of modified polyurethane, 10~12 parts of butyl ester, toluene 20~
22 parts, 28~30 parts of butanone, 1~2 part of wear-resisting scratch-resisting agent, 1~2 part of methyl tin heat stabilizer, 0~1 part of slipping agent.
The use for synthetic leather is molded the wear-resisting bright face inorganic agent of scratch resistance and is applied to synthetic leather rear section technique, belongs to innovative back segment material
Material.Each component that composition is molded the wear-resisting bright face inorganic agent of scratch resistance is mutually coordinated, collective effect, the leather light made with such a inorganic agent
Pool is naturally, color clarification, and injection effect is good, and bright-colored transparent, crystal-feel is strong, has splendid stereovision, leather surface touches after processing
Sense effect is good, and leather surface feel is dry and comfortable, and wear-resisting scratch resistance is good, and resultant effect is good.
Embodiment 1
Use for synthetic leather is molded the wear-resisting bright face inorganic agent of scratch resistance and is made up of the following raw material component：On the basis of the gross weight of resin with
Mass parts meter, it includes 35 parts of modified polyurethane, 10 parts of butyl ester, 20 parts of toluene, 29 parts of butanone, 1.5 parts of wear-resisting scratch-resisting agent, methyl
1.5 parts of tin heat stabilizer.
As shown in figure 1, the preparation technology of the wear-resisting bright face inorganic agent of scratch resistance of injection of the present invention is as follows：
Step 1：By formula by partially modified 33 parts of polyurethane, 10 parts of butyl ester, 20 parts of toluene, 29 parts of butanone, wear-resisting scratch-resisting
1.5 parts of agent, 1.5 parts of methyl tin heat stabilizer are uniformly mixing to obtain mixture；
Step 2：Injection is made after remaining 2 parts of modified polyurethane stirs by being added in the mixture obtained by step 1
The wear-resisting bright face inorganic agent of scratch resistance.
Above-mentioned all steps are carried out at normal temperatures and pressures, the technical performance of the obtained wear-resisting bright face inorganic agent of scratch resistance of injection
Index is shown in Table 1.
Embodiment 2：
Use for synthetic leather is molded the wear-resisting bright face inorganic agent of scratch resistance and is made up of the following raw material component：On the basis of the gross weight of resin with
Mass parts meter, it includes 38 parts of modified polyurethane, 12 parts of butyl ester, 21 parts of toluene, 30 parts of butanone, 2 parts of wear-resisting scratch-resisting agent, methyl tin
2 parts of heat stabilizer, 1 part of slipping agent.
As shown in figure 1, the preparation technology of the wear-resisting bright face inorganic agent of scratch resistance of injection of the present invention is as follows：
Step 1：By formula by partially modified 33 parts of polyurethane, 12 parts of butyl ester, 21 parts of toluene, 30 parts of butanone, wear-resisting scratch-resisting
2 parts of agent, 2 parts of methyl tin heat stabilizer are uniformly mixing to obtain mixture；
Step 2：5 parts of remaining modified polyurethane will be added in mixture obtained by step 1 and 1 part of slipping agent stirs
The wear-resisting bright face inorganic agent of scratch resistance of injection is made afterwards.
Above-mentioned all steps are carried out at normal temperatures and pressures, the technical performance of the obtained wear-resisting bright face inorganic agent of scratch resistance of injection
Index is shown in Table 1.
Embodiment 3：
As optimum embodiment, use for synthetic leather is molded the wear-resisting bright face inorganic agent of scratch resistance and is made up of the following raw material component：With tree
On the basis of the gross weight of fat in terms of mass parts, it includes 36 parts of modified polyurethane, 11.5 parts of butyl ester, 22 parts of toluene, 28 parts of butanone, resistance to
Grind 1 part of scratch resistance agent, 1 part of methyl tin heat stabilizer, 0.5 part of slipping agent.
As shown in figure 1, the preparation technology of the wear-resisting bright face inorganic agent of scratch resistance of injection of the present invention is as follows：
Step 1：By formula by partially modified 31 parts of polyurethane, 11.5 parts of butyl ester, 22 parts of toluene, 28 parts of butanone, wear-resisting anti-
Scrape 1 part of agent, 1 part of methyl tin heat stabilizer is uniformly mixing to obtain mixture；
Step 2：5 parts of remaining modified polyurethane will be added in mixture obtained by step 1 and 0.5 part of stirring of slipping agent is equal
The wear-resisting bright face inorganic agent of scratch resistance of injection is made after even.
Above-mentioned all steps are carried out at normal temperatures and pressures, the technical performance of the obtained wear-resisting bright face inorganic agent of scratch resistance of injection
Index is shown in Table 1.
The technical performance index of the above-mentioned bright face inorganic agent of the wear-resisting scratch resistance of injection is shown in Table 1, wherein, the experimental result of embodiment 3
Embodiment 1 and embodiment 2, particularly stability, solid content and viscosity are substantially better than, effect is compared to most during for surface conditioning agent
It is good.
Table 1 is molded the technical performance index of the bright face inorganic agent of wear-resisting scratch resistance
| Project | Index |
| PH value | 5~7 |
| Outward appearance | Opaque white color liquid |
| Viscosity (cps/25 DEG C) | 100~400 |
| Stability | Without precipitation, it is non-discolouring |
| Dicyandiamide solution | Toluene, butanone |
| Solid content (part) | 20±1 |
Implementation described above only expresses embodiments of the present invention, its describe it is more specific and in detail, but can not be because
This and be interpreted as the limitation to the scope of the claims of the present invention.It should be pointed out that for the person of ordinary skill of the art,
On the premise of not departing from present inventive concept, various modifications and improvements can be made, these belong to protection scope of the present invention.
Therefore, the protection domain of patent of the present invention should be determined by the appended claims.
Claims (9)
1. a kind of use for synthetic leather is molded the wear-resisting bright face inorganic agent of scratch resistance, it is used for the back segment typography of synthetic leather, and its feature exists
In including following components：Modified polyurethane, butyl ester, toluene, butanone, wear-resisting scratch-resisting agent, methyl tin heat stabilizer and smooth
Agent.
2. use for synthetic leather as claimed in claim 1 is molded the wear-resisting bright face inorganic agent of scratch resistance, it is characterised in that in terms of mass parts,
The proportioning of each component is as follows：35~38 parts of the modified polyurethane, 10~12 parts of the butyl ester, the toluene 20~22
Part, 28~30 parts of the butanone, 1~2 part of the wear-resisting scratch-resisting agent, 1~2 part of the methyl tin heat stabilizer, the slipping agent 0
~1 part.
3. use for synthetic leather as claimed in claim 2 is molded the wear-resisting bright face inorganic agent of scratch resistance, it is characterised in that in terms of mass parts,
The proportioning of each component is as follows：36~38 parts of the modified polyurethane, 11.5~12 parts of the butyl ester, the toluene 20~22
Part, 28~30 parts of the butanone, 1~2 part of the wear-resisting scratch-resisting agent, 1~2 part of the methyl tin heat stabilizer, the slipping agent 0
~1 part.
4. use for synthetic leather as claimed in claim 2 is molded the wear-resisting bright face inorganic agent of scratch resistance, it is characterised in that in terms of mass parts,
The proportioning of each component is as follows：36 parts of the modified polyurethane, 11.5 parts of the butyl ester, 22 parts of the toluene, the butanone
28 parts, 1 part of the wear-resisting scratch-resisting agent, 1 part of the methyl tin heat stabilizer, 0.5 part of the slipping agent.
5. a kind of any use for synthetic leather as described in above-mentioned claim is molded the preparation method of the wear-resisting bright face inorganic agent of scratch resistance, its
It is characterised by, comprises the steps of:
Step 1：Partially modified polyurethane, butyl ester, toluene, butanone, wear-resisting scratch-resisting agent, methyl tin heat stabilizer are mixed by formula
After be uniformly mixing to obtain mixture；
Step 2：It is made being added in the mixture obtained by step 1 after remaining modified polyurethane and slipping agent stir
The wear-resisting bright face inorganic agent of scratch resistance of injection.
6. use for synthetic leather as claimed in claim 5 is molded the preparation method of the wear-resisting bright face inorganic agent of scratch resistance, it is characterised in that with
Mass parts meter, the proportioning of each component are as follows：35~38 parts of the modified polyurethane, 10~12 parts of the butyl ester, the toluene 20
~22 parts, 28~30 parts of the butanone, 1~2 part of the wear-resisting scratch-resisting agent, 1~2 part of the methyl tin heat stabilizer, the cunning
Refreshing 0~1 part of agent.
7. use for synthetic leather as claimed in claim 5 is molded the preparation method of the wear-resisting bright face inorganic agent of scratch resistance, it is characterised in that step
Raw material proportioning in rapid 1 is calculated as with mass parts：It is 31~33 parts of the partially modified polyurethane, 10~12 parts of the butyl ester, described
20~22 parts of toluene, 28~30 parts of the butanone, 1~2 part of the wear-resisting scratch-resisting agent, 1~2 part of the methyl tin heat stabilizer.
8. use for synthetic leather as claimed in claim 7 is molded the preparation method of the wear-resisting bright face inorganic agent of scratch resistance, it is characterised in that step
Remaining 2~5 parts of the modified polyurethane in rapid 2, and it is described in the partially modified polyurethane and step 2 in step 1
The overall control of remaining modified polyurethane is at 35~38 parts, and 0~1 part of the slipping agent.
9. use for synthetic leather as claimed in claim 5 is molded the preparation method of the wear-resisting bright face inorganic agent of scratch resistance, it is characterised in that institute
There is step to carry out at normal temperatures and pressures.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710710983.1A CN107476068A (en) | 2017-08-18 | 2017-08-18 | A kind of use for synthetic leather is molded wear-resisting bright face inorganic agent of scratch resistance and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710710983.1A CN107476068A (en) | 2017-08-18 | 2017-08-18 | A kind of use for synthetic leather is molded wear-resisting bright face inorganic agent of scratch resistance and preparation method thereof |
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| CN107476068A true CN107476068A (en) | 2017-12-15 |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102154844A (en) * | 2011-04-02 | 2011-08-17 | 江苏国信合成革有限公司 | High-wear-resistant artificial leather and preparation method thereof |
| CN103103777A (en) * | 2011-11-14 | 2013-05-15 | 江苏宝泽高分子材料股份有限公司 | Matte injection-molding waxy-feel treatment agent for synthetic leather and preparation method thereof |
| CN103304769A (en) * | 2013-06-06 | 2013-09-18 | 广东伊诗德新材料科技有限公司 | High-wear-resistant polyurethane resin for synthetic leather and preparation method thereof |
| CN104927366A (en) * | 2015-06-30 | 2015-09-23 | 广州市斯洛柯高分子聚合物有限公司 | Organic silicon anti-wear agent and preparation method thereof |
| CN106498744A (en) * | 2016-10-28 | 2017-03-15 | 江苏宝泽高分子材料股份有限公司 | A kind of use for synthetic leather injection polishing agent and preparation method thereof |
-
2017
- 2017-08-18 CN CN201710710983.1A patent/CN107476068A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102154844A (en) * | 2011-04-02 | 2011-08-17 | 江苏国信合成革有限公司 | High-wear-resistant artificial leather and preparation method thereof |
| CN103103777A (en) * | 2011-11-14 | 2013-05-15 | 江苏宝泽高分子材料股份有限公司 | Matte injection-molding waxy-feel treatment agent for synthetic leather and preparation method thereof |
| CN103304769A (en) * | 2013-06-06 | 2013-09-18 | 广东伊诗德新材料科技有限公司 | High-wear-resistant polyurethane resin for synthetic leather and preparation method thereof |
| CN104927366A (en) * | 2015-06-30 | 2015-09-23 | 广州市斯洛柯高分子聚合物有限公司 | Organic silicon anti-wear agent and preparation method thereof |
| CN106498744A (en) * | 2016-10-28 | 2017-03-15 | 江苏宝泽高分子材料股份有限公司 | A kind of use for synthetic leather injection polishing agent and preparation method thereof |
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