CN107456941A - A kind of chemical reaction kettle for being easy to temperature adjustment - Google Patents

A kind of chemical reaction kettle for being easy to temperature adjustment Download PDF

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Publication number
CN107456941A
CN107456941A CN201710854818.3A CN201710854818A CN107456941A CN 107456941 A CN107456941 A CN 107456941A CN 201710854818 A CN201710854818 A CN 201710854818A CN 107456941 A CN107456941 A CN 107456941A
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CN
China
Prior art keywords
heat
kettle
fin
conducting seat
cooling water
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Granted
Application number
CN201710854818.3A
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Chinese (zh)
Other versions
CN107456941B (en
Inventor
刘毅
刘国强
李玉玲
丁克富
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Anhui Futai fine chemical industry limited liability company
Original Assignee
Anqing Zeyuan Chemical Co Ltd
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Priority to CN201710854818.3A priority Critical patent/CN107456941B/en
Publication of CN107456941A publication Critical patent/CN107456941A/en
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Publication of CN107456941B publication Critical patent/CN107456941B/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006Controlling or regulating processes
    • B01J19/0013Controlling the temperature of the process
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0066Stirrers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00074Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00092Tubes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00132Controlling the temperature using electric heating or cooling elements
    • B01J2219/00135Electric resistance heaters

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Accessories For Mixers (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

The present invention relates to a kind of reactor, specially a kind of chemical reaction kettle for being easy to temperature adjustment, the inwall of kettle is provided with multiple adjustment modules, adjustment module can be used for the heating to industrial chemicals, radiating and stirring, adjustment module is included along the heat-conducting seat arranged vertically, for the fin for radiating and heating and the motor to be swung back and forth for fin, heat-conducting seat is provided with the cooling water hole through heat-conducting seat, when adding thermal resistance heats to chemical reaction, one end of fin is hinged on heat-conducting seat, fin is provided with multiple, multiple fins are evenly arranged along the length direction of heat-conducting seat;Motor is arranged on the top of heat-conducting seat, and motor drives fin to swing by connecting rod.The present invention can be achieved the stirring of reactant and the quick transmission of heat, reactant can either be heated, and can is enough to cool to reactant, while reactant can also be stirred, and the control to temperature of charge can be achieved by shuttle-type fin of setting.

Description

A kind of chemical reaction kettle for being easy to temperature adjustment
Technical field
The present invention relates to a kind of reactor, specially a kind of chemical reaction kettle for being easy to temperature adjustment, belong to chemical reaction Kettle applied technical field.
Background technology
The broad understanding of reactor has the container physically or chemically reacted, is matched somebody with somebody by the structure design to container with parameter Put, realize the mixture function of the heating of technological requirement, evaporation, cooling and low high speed, reactor is by kettle, kettle cover, chuck, stirring Device, transmission device, gland seal device, supporting etc. form.Whipped form typically has anchor formula, paddle, turbine type, push type or frame Deng agitating device can use multiple impellers leaf when ratio of height to diameter is larger, also can arbitrarily be matched according to the requirement of user.And in kettle Chuck is set outside wall, or heat-transfer surface is set in device, can also be exchanged heat by outer circulation.Mode of heating has electrical heating, hot water Heating, the heating of conduction oil circulating-heating, Far-infrared Heating, outer inner coil pipe etc., the type of cooling are that chuck cooling and kettle inner coil pipe are cold But, form of stirrer paddle etc..Fulcrum bearing has supporting type or hanging support etc..Rotating speed is preferably subtracted more than more than 160 turns using gear Fast machine.
At present therefore domestic medium and small chemical plant unconditionally fills the higher chemical industry equipment of each reaction temperature, can not also produce The higher chemical products of reaction temperature.It is and slowly difficult using temperature adjustment be present for steam-heated chemical industry equipment.Chemical plant Sometimes to be separately provided pyroreaction kettle, tank, using line-frequency induction electric heater unit, make the cost of equipment and investment very big, no With insulation jacket and heating system, it is impossible to which effectively to the timely heating of reactor and temperature adjusting, and optional equipment occupies factory Room sky asks the capital intensives such as big and tank kettle, pump valve, pipeline, and electric-thermal conversion efficiency is low and temperature is difficult to control.
The content of the invention
The purpose of the present invention is that to solve the above problems and provides a kind of chemical reaction kettle for being easy to temperature adjustment, Shuttle-type fin of the invention by setting, the stirring of reactant and the quick transmission of heat can be achieved, can either be to reaction Thing heats, and and can is enough to cool to reactant, while reactant can also be stirred.
The present invention is achieved through the following technical solutions above-mentioned purpose, a kind of chemical reaction kettle for being easy to temperature adjustment, bag Kettle is included, reaction chamber is provided with kettle, chuck is provided with the outside of kettle, top cover is additionally provided with the upside of kettle, base is provided with the downside of kettle, The base lower end is provided with supporting leg, and base end is provided with drainage conduit, and drainage conduit is provided with discharge electromagnetic valve, is provided with reaction chamber Rotary shaft, the rotary shaft downside are movably attached to inside kettle by rotary shaft support, and multigroup stirring is provided with the outside of rotary shaft Leaf, rotary shaft upside are connected with decelerator, and decelerator is arranged on top cover upper end, and the top cover upper left side is provided with charging aperture, top cover There is upside to be provided with pressure valve, decelerator upper end is connected with motor, and inner wall of kettle is provided with multiple temperature sensors, set on the outside of kettle There is a control cabinet, the control cabinet is provided with touch screen, and the inwall of kettle is provided with multiple adjustment modules, and adjustment module can be used for pair Heating, radiating and the stirring of industrial chemicals, adjustment module are included along the heat-conducting seat arranged vertically, the fin for radiating and heating With the motor to be swung back and forth for fin, the heat-conducting seat is provided with the cooling water hole through heat-conducting seat, adding thermal resistance pair Chemical reaction is when being heated, can be by cooling water hole if the actual temperature of chemical reaction is more than required reaction temperature Injection cooling water is cooled, and the cooling water in cooling water hole can block adding thermal resistance to continue to heat to chemical reaction rapidly, Ensure the security of chemical reaction, further, cooling water hole is bellmouth, the small end water inlet of cooling water hole, brings out water greatly, cold But when water flows to big end by small end, in the presence of negative pressure, the increase of the distance between cooling water hydrone, cooling water can be inhaled More heat is received, is advantageous to the fast cooling to reactant, one end of the fin is hinged on heat-conducting seat, and fin is provided with Multiple, multiple fins are evenly arranged along the length direction of heat-conducting seat;The motor is arranged on the top of heat-conducting seat, driving electricity Machine drives fin to swing by connecting rod, in use, motor drives fin to swing back and forth by connecting rod, realizes to reactant Stirring, while fin can carry out the transmission of heat between heat-conducting seat, be advantageous to the radiating or heating of reactant.
As a kind of technical scheme of the present invention, triangle open mouth groove is provided with the heat-conducting seat, the one of the fin End is arranged in open slot, can be contacted when fin upwardly or downwardly rotates with the side wall of open slot, fin and open slot Side wall be in contact, the contact area between fin and heat-conducting seat can be improved, so as to be advantageous to increase between fin and heat-conducting seat The transmission efficiency of heat.
The spiral shape cooling water wound along kettle outer wall is provided with as a kind of technical scheme of the present invention, on the inside of the chuck Road and spiral shape adding thermal resistance, the back of the heat-conducting seat are provided with the groove being engaged with cooling water channel and adding thermal resistance, led It is tightly connected between hot seat and kettle, the chemical reaction that can be radiated by cooling water channel to needs radiates, by heating electricity The chemical reaction that resistance can heat to needs heats.Cooling water channel and adding thermal resistance directly contact with heat-conducting seat, can improve and lead The transmission speed of hot seat heat, is advantageous to quick heat radiating or heating.
The beneficial effects of the invention are as follows:
1. the present invention can be coordinated paddle to be stirred reactant, be made chemical anti-by shuttle-type fin of setting Should be able to fully it react, while the triangle open mouth groove for passing through design so that the contact area increase between fin and heat-conducting seat, The transmission area of heat is increased, quick heat radiating or heating can be carried out to reactant, so as to realize the fast of reaction cavity temperature Speed control.
2. the present invention can realize that the chemical reaction cooled down to needs cools down by the spiral shape cooling water channel of setting, lead to The spiral adding thermal resistance set is crossed, can be achieved to heat the chemical reaction that needs heat, by setting on heat-conducting seat Put cooling water hole, can the chemical reaction too high to heating-up temperature cool, the transmission of the heat of adding thermal resistance is blocked, so as to have Beneficial to the rapid cooling of chemical reaction, so as to ensure the security of chemical reaction.
Brief description of the drawings
Fig. 1 is the sectional view of the present invention;
Fig. 2 is the sectional view of the heat-conducting seat of the present invention;
In figure:1st, kettle, 2, reaction chamber, 3, chuck, 4, top cover, 5, base, 6, cooling water channel, 8, adding thermal resistance, 9, enter Water pipe, 10, outlet pipe, 11, water pump, 12, supporting leg, 13, drainage conduit, 14, rotary shaft, 15, paddle, 16, rotary shaft support, 17th, motor, 18, decelerator, 19, charge door, 20, pressure valve, 21, temperature sensor, 22, control cabinet, 23, touch screen, 24, Heat-conducting seat, 241, cooling water hole, 242, open slot, 25, fin, 26, motor, 27, connecting rod.
Embodiment
Below in conjunction with the accompanying drawing in the embodiment of the present invention, the technical scheme in the embodiment of the present invention is carried out clear, complete Site preparation describes, it is clear that described embodiment is only part of the embodiment of the present invention, rather than whole embodiments.It is based on Embodiment in the present invention, those of ordinary skill in the art are obtained every other under the premise of creative work is not made Embodiment, belong to the scope of protection of the invention.
Refer to shown in Fig. 1-2, a kind of chemical reaction kettle for being easy to temperature adjustment, including kettle 1, kettle 1 is interior to be provided with instead Answer chamber 2, the outside of kettle 1 is provided with chuck 3, and the upside of kettle 1 is additionally provided with top cover 4, is provided with base 5 on the downside of kettle 1, under the base 5 End is provided with supporting leg 12, and the end of base 5 is provided with drainage conduit 13, and drainage conduit 13 is provided with discharge electromagnetic valve, rotation is provided with reaction chamber 2 Rotating shaft 14, the downside of rotary shaft 14 are movably attached to inside kettle 1 by rotary shaft support 16, and the outside of rotary shaft 14 is provided with more Group paddle 15, the upside of rotary shaft 14 are connected with decelerator 18, and decelerator 18 is arranged on the upper end of top cover 4, the upper left side of top cover 4 Provided with charging aperture 19, top cover 4 has upside to be provided with pressure valve 20, and the upper end of decelerator 18 is connected with motor 17, and the inwall of kettle 1 is provided with Multiple temperature sensors 21, the outside of kettle 1 are provided with control cabinet 22, and the control cabinet 22 is provided with touch screen 23, the inwall of kettle 1 Multiple adjustment modules are installed, adjustment module can be used for heating, radiating and the stirring to industrial chemicals, and adjustment module is included along perpendicular The heat-conducting seat 24 directly arranged, for the fin 25 for radiating and heating and the motor 26 to be swung back and forth for fin 25, it is described Heat-conducting seat 24 is provided with the cooling water hole 241 through heat-conducting seat 24, when adding thermal resistance 8 heats to chemical reaction, if changed When learning the actual temperature of reaction more than required reaction temperature, it can be cooled by injecting cooling water to cooling water hole 241, be cooled down Cooling water in water hole 241 can block adding thermal resistance 8 to continue to heat to chemical reaction rapidly, ensure the safety of chemical reaction Property, further, cooling water hole 241 is bellmouth, the small end water inlet of cooling water hole 241, brings out water greatly, cooling water is by small end stream During to big end, in the presence of negative pressure, the increase of the distance between cooling water hydrone, cooling water can be caused to absorb more heat Amount, is advantageous to the fast cooling to reactant, one end of the fin 25 is hinged on heat-conducting seat 24, and fin 25 is provided with more Individual, length direction of multiple fins 25 along heat-conducting seat 24 is evenly arranged;The motor 26 is arranged on the top of heat-conducting seat 24, Motor 26 drives fin 25 to swing by connecting rod 27, in use, motor 26 drives fin 25 back and forth by connecting rod 27 Swing, realize the stirring to reactant, while fin 25 can carry out the transmission of heat between heat-conducting seat 24, be advantageous to react The radiating or heating of thing.
As one embodiment of the present invention, triangle open mouth groove 242, the fin are provided with the heat-conducting seat 24 25 one end is arranged in open slot 242, can be connect when fin 25 upwardly or downwardly rotates with the side wall of open slot 242 Touch, fin 25 is in contact with the side wall of open slot 242, can improve the contact area between fin 25 and heat-conducting seat 24, so as to have Beneficial to the transmission efficiency of heat between increase fin 25 and heat-conducting seat 24.
As one embodiment of the present invention, the inner side of chuck 3, which is provided with along the spiral shape of the outer wall of kettle 1 winding, to be cooled down Water channel 6 and spiral shape adding thermal resistance 8, the back of the heat-conducting seat 24 are provided with what is be engaged with cooling water channel 6 and adding thermal resistance 8 Groove, it is tightly connected between heat-conducting seat 24 and kettle 1, the chemical reaction that can be radiated by cooling water channel 6 to needs radiates, The chemical reaction that can be heated by adding thermal resistance 8 to needs heats.Cooling water channel 6 and adding thermal resistance 8 are directly and heat-conducting seat 24 contacts, can improve the transmission speed of the heat of heat-conducting seat 24, be advantageous to quick heat radiating or heating.
In the use of the present invention, the material for needing to be chemically reacted is added in kettle 1 successively by charge door 19, Then reaction dissolvent is added, opens motor 17, motor 17 drives rotary shaft 14 to be rotated according to certain speed, passes through control Case 22 can control the rotating speed of motor 17, while rotary shaft 14 drives paddle 15 to be rotated, and passes through the rotation of paddle 15 Reaction mass can sufficiently be stirred, while motor 26 can drive fin 25 to swing back and forth, fin 25, which coordinates, to be stirred Mix leaf 15 and realize stirring to reactant jointly so that reaction mass mixing is more uniform, and reaction is more rapid and thoroughly, simultaneously During reaction, the reaction temperature in reaction chamber 2 is monitored in real time by temperature sensor 21, when real-time in reaction chamber 2 When temperature is more than optimal reaction temperature, water pump 11 is started by control cabinet 22, from water pump 11 by water inlet pipe 9 to cooling water hole Cooling water is pumped into 241, by the cooling water in cooling water hole 241 and the alternating action of adding thermal resistance 8, chemical reaction can be protected Hold in optimum temperature, be advantageous to improve the speed and quality of chemical reaction;Need to dissipate when chemical reaction gives out substantial amounts of heat When hot, chemical reaction can be cooled comprehensively by injecting cooling water into cooling water channel 6.
The basic principles, principal features and advantages of the present invention have been shown and described above.The technical staff of the industry should Understand, the present invention is not limited to the above embodiments, and the description in above-described embodiment and specification simply illustrates the present invention Principle, without departing from the spirit and scope of the present invention, various changes and modifications of the present invention are possible, and these change and changed Enter all fall within the protetion scope of the claimed invention.The claimed scope of the invention is by appended claims and its equivalent Define.

Claims (4)

1. a kind of chemical reaction kettle for being easy to temperature adjustment, including kettle (1), it is characterised in that:Reaction chamber is provided with kettle (1) (2) chuck (3), is provided with the outside of kettle (1), top cover (4) is additionally provided with the upside of kettle (1), base (5), institute are provided with the downside of kettle (1) State base (5) lower end and be provided with supporting leg (12), base (5) end is provided with drainage conduit (13), and drainage conduit (13) is provided with discharge electromagnetism Valve, reaction chamber (2) is interior to be provided with rotary shaft (14), and rotary shaft (14) downside supports (16) to be movably attached to by rotary shaft Kettle (1) is internal, and multigroup paddle (15) is provided with the outside of rotary shaft (14), decelerator (18) is connected with the upside of rotary shaft (14), Decelerator (18) is arranged on top cover (4) upper end, and top cover (4) upper left side is provided with charging aperture (19), and top cover (4) has upside to be provided with Pressure valve (20), decelerator (18) upper end are connected with motor (17), and kettle (1) inwall is provided with multiple temperature sensors (21), Control cabinet (22) is provided with the outside of kettle (1), the control cabinet (22) is provided with touch screen (23), and the inwall of kettle (1) is provided with Multiple adjustment modules, adjustment module can be used for heating, radiating and the stirring to industrial chemicals, and adjustment module is included along vertical arrangement Heat-conducting seat (24), for the fin (25) for radiating and heating and the motor (26) to be swung back and forth for fin (25), institute State heat-conducting seat (24) and be provided with the cooling water hole (241) for running through heat-conducting seat (24), one end of the fin (25) is hinged on heat conduction On seat (24), fin (25) is provided with multiple, and length direction of multiple fins (25) along heat-conducting seat (24) is evenly arranged;The drive Dynamic motor (26) is arranged on the top of heat-conducting seat (24), and motor (26) drives fin (25) to swing by connecting rod (27).
A kind of 2. chemical reaction kettle for being easy to temperature adjustment according to claim 1, it is characterised in that:The heat-conducting seat (24) triangle open mouth groove (242) is provided with, one end of the fin (25) is arranged in open slot (242), fin (25) It can be contacted when upwardly or downwardly rotating with the side wall of open slot (242).
A kind of 3. chemical reaction kettle for being easy to temperature adjustment according to claim 1, it is characterised in that:The chuck (3) Inner side is provided with spiral shape cooling water channel (6) and spiral shape adding thermal resistance (8) along the winding of kettle (1) outer wall, the heat-conducting seat (24) back is provided with the groove being engaged with cooling water channel (6) and adding thermal resistance (8), heat-conducting seat (24) and kettle (1) it Between be tightly connected.
A kind of 4. chemical reaction kettle for being easy to temperature adjustment according to claim 1, it is characterised in that:The cooling water hole (241) it is bellmouth, the small end water inlet of cooling water hole (241), brings out water greatly.
CN201710854818.3A 2017-09-20 2017-09-20 A kind of chemical reaction kettle adjusted convenient for temperature Active CN107456941B (en)

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CN107456941B CN107456941B (en) 2018-09-25

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110923672A (en) * 2019-12-17 2020-03-27 Tcl华星光电技术有限公司 Heating device and chemical vapor deposition equipment
WO2024033187A1 (en) * 2022-08-09 2024-02-15 Shell Internationale Research Maatschappij B.V. An electrically heated apparatus and a method of heating a fluid

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4752640A (en) * 1984-07-27 1988-06-21 Kanegafuchi Chemical Industry Co., Ltd. Temperature controlling method for polymerization reactors
CN201921686U (en) * 2010-12-07 2011-08-10 李建英 Reaction kettle
CN204891874U (en) * 2015-08-13 2015-12-23 河南莱帕克化工设备制造有限公司 Semi -physical simulation's chlorination reaction kettle
CN205042480U (en) * 2015-10-23 2016-02-24 临沂大学 Chemical synthesis device
CN205413035U (en) * 2016-04-06 2016-08-03 河南工程学院 Rapid reaction kettle system adjusts temperature
CN206249216U (en) * 2016-11-08 2017-06-13 东莞市澍华五金制品有限公司 A kind of electronic heat sink

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4752640A (en) * 1984-07-27 1988-06-21 Kanegafuchi Chemical Industry Co., Ltd. Temperature controlling method for polymerization reactors
CN201921686U (en) * 2010-12-07 2011-08-10 李建英 Reaction kettle
CN204891874U (en) * 2015-08-13 2015-12-23 河南莱帕克化工设备制造有限公司 Semi -physical simulation's chlorination reaction kettle
CN205042480U (en) * 2015-10-23 2016-02-24 临沂大学 Chemical synthesis device
CN205413035U (en) * 2016-04-06 2016-08-03 河南工程学院 Rapid reaction kettle system adjusts temperature
CN206249216U (en) * 2016-11-08 2017-06-13 东莞市澍华五金制品有限公司 A kind of electronic heat sink

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110923672A (en) * 2019-12-17 2020-03-27 Tcl华星光电技术有限公司 Heating device and chemical vapor deposition equipment
WO2024033187A1 (en) * 2022-08-09 2024-02-15 Shell Internationale Research Maatschappij B.V. An electrically heated apparatus and a method of heating a fluid

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