CN107447553A - A kind of ketone ester class carrier dyeing method of polyimide fiber and fabric - Google Patents
A kind of ketone ester class carrier dyeing method of polyimide fiber and fabric Download PDFInfo
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- CN107447553A CN107447553A CN201710696173.5A CN201710696173A CN107447553A CN 107447553 A CN107447553 A CN 107447553A CN 201710696173 A CN201710696173 A CN 201710696173A CN 107447553 A CN107447553 A CN 107447553A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/653—Nitrogen-free carboxylic acids or their salts
- D06P1/6536—Aromatic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/53—Polyethers
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/651—Compounds without nitrogen
- D06P1/65106—Oxygen-containing compounds
- D06P1/65112—Compounds containing aldehyde or ketone groups
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/02—Material containing basic nitrogen
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/02—After-treatment
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Coloring (AREA)
Abstract
The invention discloses a kind of ketone ester class carrier dyeing method of polyimide fiber and fabric, belong to textile auxiliary and textile dyeing and finishing manufacture field.The present invention uses following technique：(1) polyimide fiber fabric pretreatment with get rid of throwing, weaving and storage during fabric adhere to impurity；(2) carrier dyeing assigns fabric certain tinctorial yield；(3) dyed fabric is washed, soap boiling, washing to be to remove dyeing loose colour.In the present invention, polyimides fabric is dyed under the high temperature conditions using carrier and the dye of positive ion, fabric has certain tinctorial yield, and fabric has higher washing color fastness after dyeing.
Description
Technical field
The present invention relates to a kind of ketone ester class carrier dyeing method of polyimide fiber and fabric, belong to textile auxiliary
With textile dyeing and finishing manufacture field.
Background technology
Polyimides is a kind of more new high-performance fiber, in the same of the excellent properties with various high-performance fibers
When, also with more preferable heat endurance and anti-flammability.But polyimide fiber carries natural golden yellow, color is very fresh
It is gorgeous, and can not remove, so bringing very big difficulty to dyeing, its high glass transition temperature also increases the difficulty of dyeing.
Colouring method main at present is modification of and coloration and carrier dyeing, and wherein modification of and coloration research is relatively broad.Modification of and coloration refers to
Using the not alkali resistance of polyimide fiber, after being handled using alkali lye fiber disengaging, increase the polar group on strand
So as to reach the purpose of dyeing, but the method destroys the cyclic structure on fiber macromolecular chain, can be to other performances of fiber
Impact.Research of the carrier dyeing on other synthetic fibers such as terylene, aramid fiber is more, but in the dyeing of polyimide fiber
Aspect is less, and suitable carrier needs constantly screening, and carrier dyeing is the swelling action to fiber using organic solvent, in fibre
Dimension is internal and fiber surface forms carrier layer, in the dissolubility using dyestuff in a solvent, makes dyestuff constantly into the interior of fiber
Portion is so as to reaching the purpose of dyeing.
The dyeing for polyimides is concentrated mainly on modification poststaining and the carrier dyeing of fiber at present.Its Patent
CN201310493553.0, CN201610393927.5 and CN201510896425.X etc. are that polyimides is carried out at surface
After reason, dye polyimides with the help of certain auxiliary agent.Patent CN201510623413.X (leads dye using only carrier
Agent) polyimides is dyed, are not utilized by theory of solubility parameter, several differences are calculated for fibre modification, its invention
The compounding of organic solvent is identical with the solubility of polyimides, and the method is feasible, but calculating process is cumbersome, and type of solvent is more
Sample, delete choosing and have no basis and can seek.Patent CN201710342615.6 is dyed using the carrier of amide containing class to polyimides, still
It is difficult to contaminate dark.
The content of the invention
Based on problem above, the invention provides a kind of ketone ester class carrier dyeing method of polyimide fiber and fabric,
Such carrier dyeing effect is fairly obvious, and with the help of such carrier, fiber can contaminate dark, and color fastness to washing is good.
Compared with other kinds of carrier, fabric color is very deep after ketone ester class carrier dyeing used in the present invention, especially power
The big dyestuff of part can reach preferable Color using examples of such carriers.The ketone ester class carrier of the present invention, one kind can be used as
Single carrier uses, and can also compound each other, or as needed with the preferable carrier compounding use of other effects.
Shown in the general structure such as formula (1) or formula (2) of a kind of suitable polyimides dyeing provided by the present invention：
Wherein, in formula (1), R1For any one in hydrogen, alkyl, aryl, hydroxyl；R2, R3, R4, R5, R6For hydrogen, alkyl,
Any one in aryl, alkoxy, hydroxyl.
The general structure of another kind of suitable polyimides dyeing is as follows：
Wherein, in formula (2), R1For any one in hydrogen, alkyl, aryl；R2, R3, R4, R5, R6For hydrogen, alkyl, aryl,
Any one in alkoxy, hydroxyl.
The present invention also provides a kind of method dyed to polyimide fiber or fabric, and methods described is to apply this hair
Any one in bright ketone ester class carrier or multiple combinations.
In one embodiment of the invention, the dyestuff of the dyeing is the dye of positive ion.
Methods described, comprise the following steps：
Step 1, remove the oily impurity of polyimides fabric face attachment；
Step 2, the polyimides fabric after the removal of impurity will be gone to be added to containing the dye of positive ion and the ketone ester class carrier
Dye liquor in, dyed；
Step 3, by polyimides fabric washing to remove dyeing loose colour after the completion of dyeing.
In one embodiment of the invention, step 1, polyimide fiber, which adds, contains 2~3g/L non-ionic surfaces
In the solution of surfactant, bath raio is 20~30:1,30~60min is handled at 85~95 DEG C, is fully dried in the air naturally after washing
It is dry.
In one embodiment of the invention, the non-ionic surface surfactant is AEO-7.
In one embodiment of the invention, step 2, polyimide fiber is added to containing carrier and cation
In the dye liquor of dyestuff, the bath raio of dye liquor and fabric is 15:1~30:1；The dye of positive ion is to fabric weight (owf)
For 2.5%~10%.
In one embodiment of the invention, the carrier is the one or more of compounding of the carrier in the present invention, is carried
Bulk concentration is 10~100g/L.
In one embodiment of the invention, step 2, will go the polyimide fiber after the removal of impurity be added to containing
In the dye liquor of carrier and the dye of positive ion, 120~130 DEG C are warming up to 1.5~3 DEG C/min speed, is incubated 40~120min；
After the completion of with 2~3 DEG C/min speed cool to 70~80 DEG C, ensure that dyestuff is fully upper and contaminate.
In one embodiment of the invention, the washing of the step 3 is first to wash, soap, finally wash again.
In one embodiment of the invention, step 3, after the completion of dyeing by polyimide fiber be added to containing from
In the solution of soaping of sub- surfactant, for example, CT-3, bath raio 20:1~30:1, after 85~95 DEG C handle 15~30min
Fully washing.
Embodiment
Embodiment 1
Select benzophenone class carrier, R1For-CH3, R2、R3、R4、R5And R6For-H.
2g polyimides knitted fabrics are taken, are put into the solution containing nonionic surfactant AEO-7 (2g/L), bath raio is
30:1,30min is handled at 95 DEG C, is fully dried after washing.
Deimpurity polyimides fabric will be gone to be put into containing the Cationic Red X-GRL for weighing 5% to fabric and 10g/L carrier
In dye liquor, wherein the bath raio of dye liquor and fabric is 15:1,120 DEG C of insulation 120min are warming up to 1.5 DEG C/min speed.Insulation
After the completion of with 2 DEG C/min cooling rate cool the temperature to 80 DEG C.
After the completion of dyeing, fabric is put into the liquid of soaping of the nonionic surfactant AEO-7 containing 2g/L, bath raio is
20:1, to fully washing, drying after fabric treating 15min at 85 DEG C.
The color parameter of sample and washing fastness are as shown in table 1 after dyeing.
Embodiment 2
Select phenyl ester class carrier, wherein R1For-CH2CH3, R2、R3、R4、R5And R6For-H.
2g polyimides knitted fabrics are taken, are put into the solution containing nonionic surfactant AEO-7 (3g/L), bath raio is
20:1,30min is handled at 85 DEG C, is fully dried after washing.
Deimpurity polyimides fabric is gone to be put into containing the Cationic Red X-GRL and 15g/L for weighing 2.5% to fabric washing
Carrier dye liquor in, wherein the bath raio of dye liquor and fabric be 30:1,130 DEG C of insulation 40min are warming up to 3 DEG C/min speed.
After the completion of insulation 80 DEG C are cooled the temperature to 3 DEG C/min cooling rate.
After the completion of dyeing, fabric is put into the liquid of soaping of the nonionic surfactant CT-3 containing 2g/L, bath raio is
30:1, to fully washing, drying after fabric treating 30min at 95 DEG C.
The color parameter of sample and washing fastness are as shown in table 1 after dyeing.
Embodiment 3
Select phenyl ester class carrier, wherein R1For-CH3, R2For-OH, R3、R4、R5And R6For-H.
2g polyimides knitted fabrics are taken, are put into the solution containing nonionic surfactant AEO-7 (3g/L), bath raio is
30:1,60min is handled at 85 DEG C, is fully dried after washing.
Deimpurity polyimides fabric will be gone to be put into containing weighing 5% cationic blue x-grrl and 100g/L load to fabric
The bath raio of body, wherein dye liquor and fabric is 20:1,125 DEG C of insulation 60min are warming up to 2 DEG C/min speed.After the completion of insulation
80 DEG C are cooled the temperature to 2 DEG C/min cooling rate.
After the completion of dyeing, fabric is put into the nonionic surfactant AEO-7 containing 2g/L and soaped in liquid, bath raio is
20:1, to fully washing, drying after fabric treating 15min at 95 DEG C.
The color parameter of sample and washing fastness are as shown in table 1 after dyeing.
Embodiment 4
Select benzophenone class carrier and the compounding dyeing of phenyl ester class carrier, the wherein R of benzophenone class carrier1For-CH3, R2、R3、R4、
R5And R6For-H, the R of phenyl ester class carrier1For-CH3, R2、R3、R4、R5And R6For~H.
2g polyimides knitted fabrics are taken, are put into the solution containing nonionic surfactant AEO-7 (2g/L), bath raio is
30:1,60min is handled at 95 DEG C, is fully dried after washing.
Deimpurity polyimides fabric will be gone to be put into positive containing weighing 6% Cationic Red X-GRL to fabric and weighing 4% to fabric
Ion Huang X~GL and 50g/L carrier (two kinds of each 25g/L of carrier), the wherein bath raio of dye liquor and fabric are 20:1, with 2 DEG C/
Min speed is warming up to 125 DEG C of insulation 90min.After the completion of insulation 80 DEG C are cooled the temperature to 2 DEG C/min cooling rate.
After the completion of dyeing, fabric is put into the nonionic surfactant AEO-7 containing 3g/L and soaped in liquid, bath raio is
30:1, to fully washing, drying after fabric treating 15min at 85 DEG C.
The color parameter of sample and washing fastness are as shown in table 1 after dyeing.
Comparative example 1
2g polyimides knitted fabrics are taken, are put into the solution containing nonionic surfactant AEO-7 (2g/L), bath raio is
30:1,30min is handled at 95 DEG C, is fully dried after washing.
Deimpurity polyimides fabric will be gone to be put into containing the Cationic Red X-GRL for weighing 5% to fabric, wherein dye liquor is with knitting
The bath raio of thing is 15:1,120 DEG C of insulation 120min are warming up to 1.5 DEG C/min speed.With 2 DEG C/min drop after the completion of insulation
Warm speed cools the temperature to 80 DEG C.
After the completion of dyeing, fabric is put into the liquid of soaping of the nonionic surfactant AEO-7 containing 2g/L, bath raio is
20:1, to fully washing, drying after fabric treating 15min at 85 DEG C.
The color parameter of sample and washing fastness are as shown in table 1 after dyeing.
Comparative example 2
Select N, N- dimethyl methyls anilide (the commercial vectors Cindye of the non-aramid fiber of N, N- dimethyl methyl anilide
Ink) it is used as carrier.
2g polyimides knitted fabrics are taken, are put into the solution containing nonionic surfactant AEO-7 (2g/L), bath raio is
30:1,30min is handled at 95 DEG C, is fully dried after washing.
Deimpurity polyimides fabric will be gone to be put into containing the Cationic Red X-GRL for weighing 5% to fabric and 10g/L carrier
In dye liquor, wherein the bath raio of dye liquor and fabric is 15:1,120 DEG C of insulation 120min are warming up to 1.5 DEG C/min speed.Insulation
After the completion of with 2 DEG C/min cooling rate cool the temperature to 80 DEG C.
After the completion of dyeing, fabric is put into the liquid of soaping of the nonionic surfactant AEO-7 containing 2g/L, bath raio is
20:1, to fully washing, drying after fabric treating 15min at 85 DEG C.
The color parameter of sample and washing fastness are as shown in table 1 after dyeing.
Comparative example 3
1- phenoxy group -2- propyl alcohol is selected as carrier
2g polyimides knitted fabrics are taken, are put into the solution containing nonionic surfactant AEO-7 (2g/L), bath raio is
30:1,30min is handled at 95 DEG C, is fully dried after washing.
Deimpurity polyimides fabric will be gone to be put into containing the Cationic Red X-GRL for weighing 5% to fabric and 10g/L carrier
In dye liquor, wherein the bath raio of dye liquor and fabric is 15:1,120 DEG C of insulation 120min are warming up to 1.5 DEG C/min speed.Insulation
After the completion of with 2 DEG C/min cooling rate cool the temperature to 80 DEG C.
After the completion of dyeing, fabric is put into the liquid of soaping of the nonionic surfactant AEO-7 containing 2g/L, bath raio is
20:1, to fully washing, drying after fabric treating 15min at 85 DEG C.
The color parameter of sample and washing fastness are as shown in table 1 after dyeing.
CIE Lab, K/S, washing fastness series and strength after the dyeing of the polyimides fabric carrier of table 1
Note：Become color fastness, staining fastness determines according to textile color stability testing standard GB/T 3921~2008；Fracture
Intensity is yarn strength, according to textile single yarn ultimate strength and elongation at break bioassay standard GB/T 3916~
2013 measure.
As shown in table 1, the carrier through various concentrations and the different CIE Lab values to the fabric after the dyeing in fabric
It is varied from, such as embodiment 1 and embodiment 2, polyimides fabric is dyed using Cationic Red X-GRL, dyes
Fabric a values increase afterwards is notable, and b values reduce, and illustrate that the color of fabric more deviates yellow, close toward red direction, the reduction of L values
Illustrate on dyestuff that dye makes fabric color dimmed to fabric.The color parameter of other embodiment, comparative example and polyimides fabric
More can be explained under the auxiliary of carrier, on dyestuff contaminate situation obtained significantly being lifted.Fabric is resistance to after dyeing
Color fastness is washed more than 3 grades, and strength has obtained preferable holding.Embodiment 1, comparative example 1,2,3 be respectively ketone ester class carrier,
Carrier-free, amide-type carrier, ether alcoholic vehicle, it can be seen that after being dyed by Cationic Red X-GRL, knitted after ketone ester class carrier dyeing
The a values of thing are maximum, illustrates to show on fabric red the most obvious, and ether alcohol class is taken second place, and amide-type effect is poor, illustrates ketone ester
Class carrier dyeing, better off is contaminated on dyestuff.But due to there is the taste more stimulated, therefore in actual production, ketone ester class carrier
It can be compounded with the good carrier of other effects to suppress penetrating odor and improve Color.
Although the present invention is disclosed as above with preferred embodiment, it is not limited to the present invention, any to be familiar with this skill
The people of art, without departing from the spirit and scope of the present invention, it can all do various change and modification, therefore the protection model of the present invention
Enclose being defined of being defined by claims.
Claims (10)
- A kind of 1. method dyed to polyimide fiber or fabric, it is characterised in that methods described is contaminated using carrier Color method is dyed；Contain any one in ketone ester class carrier or a variety of in the carrier；Shown in the general structure such as formula (1) or formula (2) of the ketone ester class carrier：In formula (1), R1For any one in hydrogen, alkyl, aryl, hydroxyl；R2, R3, R4, R5, R6For hydrogen, alkyl, aryl, alcoxyl Any one in base, hydroxyl；In formula (2), R1For any one in hydrogen, alkyl, aryl；R2, R3, R4, R5, R6For hydrogen, alkyl, aryl, alkoxy, hydroxyl Any one in base.
- 2. according to the method for claim 1, it is characterised in that the dyestuff of the dyeing is the dye of positive ion.
- 3. according to the method for claim 1, it is characterised in that also containing other any prior art reports in the carrier Dyeing carrier.
- 4. according to the method for claim 1, it is characterised in that methods described comprises the following steps：Step 1, remove the oily impurity of polyimides fabric face attachment；Step 2, the polyimides fabric after the removal of impurity will be gone to be added to the dye containing the dye of positive ion and the ketone ester class carrier In liquid, dyed；Step 3, by polyimides fabric washing to remove dyeing loose colour after the completion of dyeing.
- 5. according to the method for claim 1, it is characterised in that step 1, polyimide fiber add non-containing 2~3g/L In the solution of ion surface surfactant, bath raio is 20~30:1,30~60min, fully washing are handled at 85~95 DEG C Naturally dry afterwards.
- 6. according to the method for claim 1, it is characterised in that the non-ionic surface surfactant is AEO-7.
- 7. according to the method for claim 1, it is characterised in that step 2, polyimide fiber is added to containing carrier In the dye liquor of the dye of positive ion, the bath raio of dye liquor and fabric is 15:1~30:1；The dye of positive ion is knitted to fiber Thing weight (owf) is 2.5%~10%.
- 8. according to the method for claim 1, it is characterised in that the carrier concn is 10~100g/L.
- 9. according to the method for claim 1, it is characterised in that step 2, the polyimide fiber after the removal of impurity will be gone to add Enter into the dye liquor containing carrier and the dye of positive ion, be warming up to 120~130 DEG C with 1.5~3 DEG C/min speed, insulation 40 ~120min；After the completion of with 2~3 DEG C/min speed cool to 70~80 DEG C, ensure that dyestuff is fully upper and contaminate.
- 10. according to the method for claim 1, it is characterised in that the washing of the step 3 is first to wash, soap again, most After wash.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108411645A (en) * | 2018-03-16 | 2018-08-17 | 江南大学 | A kind of polyimide fiber black-dyeing method |
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| CN1071717A (en) * | 1990-05-18 | 1993-05-05 | 弹簧实业有限公司 | The colouring method of fibrous material |
| CN1060126A (en) * | 1990-09-28 | 1992-04-08 | 弹簧实业有限公司 | The colouring method of fibrous material |
| CN101029457A (en) * | 2007-03-05 | 2007-09-05 | 浙江理工大学 | Method for improving Fanglun 1313 fibre dyeing fasteness |
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| CN108411645A (en) * | 2018-03-16 | 2018-08-17 | 江南大学 | A kind of polyimide fiber black-dyeing method |
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