CN107447332A - A kind of preparation technology of soybean fiber selvedge band - Google Patents
A kind of preparation technology of soybean fiber selvedge band Download PDFInfo
- Publication number
- CN107447332A CN107447332A CN201710575838.7A CN201710575838A CN107447332A CN 107447332 A CN107447332 A CN 107447332A CN 201710575838 A CN201710575838 A CN 201710575838A CN 107447332 A CN107447332 A CN 107447332A
- Authority
- CN
- China
- Prior art keywords
- soybean fiber
- spinning
- yarn
- soybean
- temperature
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- D—TEXTILES; PAPER
- D03—WEAVING
- D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
- D03D15/00—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D1/00—Treatment of filament-forming or like material
- D01D1/02—Preparation of spinning solutions
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/09—Addition of substances to the spinning solution or to the melt for making electroconductive or anti-static filaments
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
- D01F1/103—Agents inhibiting growth of microorganisms
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F4/00—Monocomponent artificial filaments or the like of proteins; Manufacture thereof
-
- D—TEXTILES; PAPER
- D02—YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
- D02G—CRIMPING OR CURLING FIBRES, FILAMENTS, THREADS, OR YARNS; YARNS OR THREADS
- D02G3/00—Yarns or threads, e.g. fancy yarns; Processes or apparatus for the production thereof, not otherwise provided for
- D02G3/02—Yarns or threads characterised by the material or by the materials from which they are made
-
- D—TEXTILES; PAPER
- D03—WEAVING
- D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
- D03D13/00—Woven fabrics characterised by the special disposition of the warp or weft threads, e.g. with curved weft threads, with discontinuous warp threads, with diagonal warp or weft
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06C—FINISHING, DRESSING, TENTERING OR STRETCHING TEXTILE FABRICS
- D06C7/00—Heating or cooling textile fabrics
- D06C7/02—Setting
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06L—DRY-CLEANING, WASHING OR BLEACHING FIBRES, FILAMENTS, THREADS, YARNS, FABRICS, FEATHERS OR MADE-UP FIBROUS GOODS; BLEACHING LEATHER OR FURS
- D06L1/00—Dry-cleaning or washing fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods
- D06L1/12—Dry-cleaning or washing fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods using aqueous solvents
- D06L1/14—De-sizing
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
- D06M15/11—Starch or derivatives thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/263—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acids; Salts or esters thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/327—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated alcohols or esters thereof
- D06M15/333—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated alcohols or esters thereof of vinyl acetate; Polyvinylalcohol
-
- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2211/00—Protein-based fibres, e.g. animal fibres
- D10B2211/20—Protein-derived artificial fibres
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacturing & Machinery (AREA)
- Mechanical Engineering (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention discloses a kind of preparation technology of soybean fiber selvedge band, comprise the following steps：Wet spinning, spinning, sizing, weaving, desizing washing and stentering forming.By adding chitosan in spinning solution lasting antibacterial and antistatic property are obtained with soybean fiber strong bonded.Winder, warping in strict control spinning stage, sizing operation reduce the friction dynamics between yarn, the generation of minimizing electrostatic, and remaining electrostatic is neutralized by chitosan, and the generation of filoplume is reduced with this.It is efficiently gentle using enzyme desizing technique, chemical residue is reduced, reduces pollution.Soybean fiber selvedge band of the present invention is not likely to produce filoplume, antistatic, antibacterial effect is well lasting, it is ventilative lead it is wet.
Description
Technical field
The present invention relates to selvedge band technical field, and in particular to a kind of preparation technology of soybean fiber selvedge band.
Background technology
Soybean fiber belongs to aftergrowth azelon, and structure is rough, and surface grooves are led wet, and section is in irregular mute
Bell type, island structure, there is micropore, and breathing freely, it is wet to lead, and applies on yarn, can effectively increase the gloss and toughness of yarn,
And legumin therein is good with human body skin compatibility, adverse reaction will not occur with human contact.Soybean fiber monofilament is thin
Degree is thin, proportion is small, strength and elongation is higher, acid-fast alkali-proof is good, and the fabric being woven into it has the soft feel as cashmere, silk
As sub-dued lustre, better than premium properties such as the warmth retention property of cotton and good skin-friendly, in addition, soybean fiber outer layer is basic
On be all protein, it is self-evident containing several amino acids needed by human, its healthcare function.
The good characteristic of the existing natural silk of soybean fiber, there is the mechanical performance of synthetic fibers again, but processing used
Electrostatic is easily produced in journey, the electrostatic hazard of fiber is determined by the quantity of electric charge remained on fiber, when the electricity remained on fiber
Lotus amount will damage more than a definite limitation to the body even production environment of fabric, people.Generally use starching or coating
Process adds antistatic additive to solve this problem, but this mode has its defect, on the one hand, this can only obtain fabric finished product
Anlistatig ability, preceding spinning is spun after, spun yarn to twist thread, doffing to weaving etc. does not entirely spin and knitted electrostatic caused by process not
To effect, during this, between fiber and fiber, friction can be all produced between yarn and yarn, makes fiber yarn negatively charged
And accumulate, electrostatic negative charge identical charges repel each other and electrostatic field caused by mechanics effect cause the cohesive force between fiber or yarn to reduce
And there is loose twist, the head end of fiber or tail end is stretched out outside main body and is formed substantial amounts of filoplume, have a strong impact on fabric quality；It is another
Aspect, exist antistatic additive combine it is insecure, antistatic effect is difficult to the problem of lasting.In addition, postfinishing process and repeatedly
Cleaning can destroy the antibacterial effect of soybean fiber itself, and how to strengthen its antibacterial effect is also urgent problem to be solved.
The content of the invention
The invention solves above-mentioned technical problem so as to provide a kind of preparation technology of soybean fiber selvedge band, described is big
Beans fiber selvedge band is not likely to produce filoplume, and antistatic and anti-microbial property is well lasting, and breathing freely, it is wet to lead.
To reach above-mentioned purpose, the concrete technical scheme that the present invention uses is as follows：
A kind of preparation technology of soybean fiber selvedge band, comprises the following steps：
（1）Wet spinning：Take soybean fiber spinning solution, add 2~4% chitosans and 1.5~3% Chinese medical extracts, stirring 3~
6h, 20~30min of ultrasonic disperse, 3~5min is stood, add 0.3~1% glutaraldehyde and 0.5~2% dispersant, be stirred at room temperature mixed
It is even, protein spinning solution is made, soybean fiber is made using the mode of wet spinning；
（2）Spinning：By soybean fiber by collecting, twisting, drawing yarn, winding spinning obtains raw yarn, raw yarn carries out winder and warping
Process, winder use metal drum, 6~8cN of influence of winding tension, winder 600~800m/min of speed, and warping uses batch warping
Machine, 500~650m/min of speed, collective's creeling, using segmented configuration warp tension：Preceding 10 cN, in 8 cN, rear 6 cN, side yarn
15 cN；
（3）Sizing：Prepare slurries and carry out starching, the slurries composition is：30~40 parts of polyvinyl alcohol, acrylic size 20~
30 parts, 20~30 parts of converted starch, it is added with water to 6~9s of slurry viscosity；Slurry groove temperature control is at 88~96 DEG C, the temperature of drying room
Control is at 95~100 DEG C, 12~16kN of squeezing pressure, the rate of sizing 7.8~9%, regain 8.6~10%；
（4）Weaving：Yarn is woven on looms in a manner of warp thread and weft yarn are orthogonal and causes fabric, warp tension during weaving
130~150kg, 160~180r/min of speed；
（5）Desizing is washed：Fabric is immersed in 2~4g/L of concentration amylase solution, at 55~60 DEG C, pH's control temperature exists
7.0~8.0,60~80min of reaction time, washing, 80~90 DEG C of temperature；
（6）Stentering forming：Stentering forming is carried out using framing shaping machine, controls 135~150 DEG C of temperature, 25~40m/ of speed
min。
Preferably, the soybean fiber spinning solution is dissolved in by soybean cellulose in the mixed solution of sodium hydroxide and urea
It is formulated.
Preferably, the Chinese medical extract is that the one or more in the coptis, the root of Dahurain angelica, rheum officinale, folium artemisiae argyi, the red sage root are extracted
Arrive.
Preferably, step（5）The amylase solution solvent is phosphate buffer solution, also includes 0.5 in amylase solution
~1g/L bleeding agents, 3~5g/L sodium chloride.
The invention has the advantages that：
1st, by being added in spinning solution, chitosan plays good lasting antibacterial to the present invention and antistatic property, chitosan contain
Amino（NH2 +）, these amino suppress bacterium by combining negatron, while chitosan is adsorbed in albumen and formed in fiber surface
Conductive cortex plays anlistatig effect, and suction-operated and bonding action combine both between chitosan and soybean protein molecule
Firmly, it is of the invention further to have consolidated this combination：Chitosan stirs and evenly mixs after adding soybean fiber spinning solution, using ultrasound
Scattered mode causes chitosan to be equably incorporated into soybean protein molecular surface, then adds glutaraldehyde to realize the friendship between chitosan
Connection,
Postfinishing process and cleaning are difficult to destroy this structure, and adding dispersant prevents from settling, in manufactured soybean fiber respectively into
Divide and be uniformly distributed.Compared to antiseptic and antistatic additive is added in starching or coating process, effect is more lasting, spins in addition
Chinese medical extract is also added in silk liquid, can not only strengthen antibacterial effect, the distinctive delicate fragrance of Chinese medical extract itself can rise
To certain effect of eliminating the unusual smell.
2nd, antistatic effect of the invention is not only embodied on selvedge band finished product, is also embodied in preparation process, is passed through two
Aspect realizes the antistatic property in preparation process so as to reduce the generation of filoplume：（1）Subtracted by the strict control to technique
The friction dynamics between yarn, the generation of electrostatic are reduced less：Metal drum, configuration tension force less than normal, relatively low speed are used during winder
Control, warping are suitably increased using relatively low speed, collective's creeling, tensioner pressurization segmentation, side yarn tension, sizing process car
Between control larger regain.（2）Chitosan in fiber absorbs electrostatic caused by friction, and yarn is due to rubbing action surface band
Negative electrical charge, the free positive charge that chitosan carries can neutralize these negative electrical charges.
3rd, using enzyme desizing technique, in the presence of amylase, starch is hydrolyzed to dextrin, maltose, or even glucose,
Molecular weight and viscosity are greatly lowered, and water solubility increase, can be removed through washing.Whole process is efficiently gentle, to soybean fiber
Damage small, desizing effect is good, and chemical residue is less after washing, smaller to skin irritation, and the pollution to environment is also smaller.
Embodiment
With reference to embodiment, the invention will be further described.
Embodiment 1
A kind of preparation technology of soybean fiber selvedge band is as follows：
（1）Wet spinning：Soybean cellulose, which is dissolved in the mixed solution of sodium hydroxide and urea, obtains soybean fiber spinning solution,
Soybean fiber spinning solution is taken, adds 2% chitosan and 1.5% coptis extract, stirs 3h, ultrasonic disperse 20min, stands 3min,
0.3% glutaraldehyde and 0.5% dispersant are added, mixing is stirred at room temperature, protein spinning solution is made, utilizes the mode system of wet spinning
Into soybean fiber；（2）Spinning：By soybean fiber by collecting, twisting, drawing yarn, winding spinning obtains raw yarn, raw yarn carries out winder
And warping process.Winder uses metal drum, influence of winding tension 6cN, winder speed 600m/min.Warping uses beam warper,
Speed 500m/min, collective's creeling, using segmented configuration warp tension：Preceding 10 cN, in 8 cN, rear 6 cN, the cN of side yarn 15；
（3）Sizing：Prepare slurries and carry out starching, the slurries composition is：30 parts of polyvinyl alcohol, 20 parts of acrylic size, denaturation are formed sediment
25 parts of powder, is added with water to slurry viscosity 7s.Slurry groove temperature control at 88 DEG C, the temperature control of drying room at 95 DEG C, squeezing pressure 16kN,
The rate of sizing 8.2%, regain 9%；（4）Weaving：Yarn is woven on looms in a manner of warp thread and weft yarn are orthogonal and causes base
Cloth, warp tension 130kg, speed 160r/min during weaving；（5）Desizing is washed：Prepare amylase solution：Amylase 2 g/L, oozes
Saturating agent 0.5g/L, sodium chloride 3g/L, phosphate buffer solution is as solvent.Fabric is immersed in amylase solution, control temperature exists
55 DEG C, pH 7.2, reaction time 60min, washing, 80 DEG C of temperature；（6）Stentering forming：Tentering is carried out using framing shaping machine to determine
Type, control 135 DEG C of temperature, speed 25m/min.
Embodiment 2
A kind of preparation technology of soybean fiber selvedge band is as follows：
（1）Wet spinning：Soybean cellulose, which is dissolved in the mixed solution of sodium hydroxide and urea, obtains soybean fiber spinning solution,
Soybean fiber spinning solution is taken, adds 3% chitosan, 1.5% Angelica Dahurica extract, 1.2% Chinese rhubarb extract, stirs 4h, ultrasonic disperse
22min, 3min is stood, add 0.5% glutaraldehyde and 1% dispersant, mixing is stirred at room temperature, protein spinning solution is made, utilization is wet
Soybean fiber is made in the mode of method spinning；（2）Spinning：By soybean fiber by collect, twist, draw yarn, winding spinning obtain original
Yarn, raw yarn carry out winder and warping process.Winder uses metal drum, influence of winding tension 7cN, winder speed 680m/min.Warping
Using beam warper, speed 550m/min, collective's creeling, using segmented configuration warp tension：Preceding 10 cN, in 8 cN, rear 6
CN, the cN of side yarn 15；（3）Sizing：Prepare slurries and carry out starching, the slurries composition is：34 parts of polyvinyl alcohol, acrylic acid plasmoid
25 parts of material, 28 parts of converted starch, is added with water to slurry viscosity 8s.Slurry groove temperature is controlled at 90 DEG C, and the temperature control of drying room is 97
DEG C, squeezing pressure 14kN, the rate of sizing 8.5%, regain 9.2%；（4）Weaving：By yarn in a manner of warp thread and weft yarn are orthogonal
Weave on looms and cause fabric, warp tension 140kg, speed 168r/min during weaving；（5）Desizing is washed：It is molten to prepare amylase
Liquid：Amylase 3g/L, bleeding agent 0.7g/L, sodium chloride 4g/L, phosphate buffer solution is as solvent.It is molten that fabric is immersed into amylase
In liquid, control temperature is at 58 DEG C, and pH is in 7.5, reaction time 70min, washing, 85 DEG C of temperature；（6）Stentering forming：Using tentering
Forming machine carries out stentering forming, controls 140 DEG C of temperature, speed 30m/min.
Embodiment 3
（1）Wet spinning：Soybean cellulose, which is dissolved in the mixed solution of sodium hydroxide and urea, obtains soybean fiber spinning solution,
Soybean fiber spinning solution is taken, adds 4% chitosan, 1% Folium Artemisiae Argyi extract, 1% Salvia root P.E, stirs 4h, ultrasonic disperse 25min,
4min is stood, 0.5% glutaraldehyde and 1.5% dispersant is added, mixing is stirred at room temperature, protein spinning solution is made, utilizes Wet-spinning
Soybean fiber is made in the mode of silk；（2）Spinning：By soybean fiber by collecting, twisting, drawing yarn, winding spinning obtains raw yarn, former
Yarn carries out winder and warping process.Winder uses metal drum, influence of winding tension 8cN, winder speed 700m/min.Warping, which uses, divides
Criticize warping machine, speed 600m/min, collective's creeling, using segmented configuration warp tension：Preceding 10 cN, in 8 cN, rear 6 cN, side
The cN of yarn 15；（3）Sizing：Prepare slurries and carry out starching, the slurries composition is：36 parts of polyvinyl alcohol, acrylic size 25
Part, 30 parts of converted starch, it is added with water to slurry viscosity 8s.Slurry groove temperature control is at 90 DEG C, and the temperature control of drying room is at 98 DEG C, pressure
Starch power 14kN, the rate of sizing 8%, regain 9.6%；（4）Weaving：By yarn in a manner of warp thread and weft yarn are orthogonal on loom
Weave into fabric, warp tension 145kg, speed 170r/min during weaving；（5）Desizing is washed：Prepare amylase solution：Amylase
3.6g/L, bleeding agent 0.8g/L, sodium chloride 4.5g/L, phosphate buffer solution is as solvent.Fabric is immersed in amylase solution,
Controlling temperature, pH is in 7.2, reaction time 70min, washing, 85 DEG C of temperature at 58 DEG C；（6）Stentering forming：Using framing shaping machine
Stentering forming is carried out, controls 142 DEG C of temperature, speed 35m/min.
Embodiment 4
（1）Wet spinning：Soybean cellulose, which is dissolved in the mixed solution of sodium hydroxide and urea, obtains soybean fiber spinning solution,
Soybean fiber spinning solution is taken, adds 4% chitosan, 3% Chinese rhubarb extract, stirs 6h, ultrasonic disperse 30min, stands 5min, is added
1% glutaraldehyde and 2% dispersant, are stirred at room temperature mixing, and protein spinning solution is made, and soybean fibre is made using the mode of wet spinning
Dimension；（2）Spinning：By soybean fiber by collecting, twisting, drawing yarn, winding spinning obtains raw yarn, raw yarn carries out winder and warping work
Sequence.Winder uses metal drum, influence of winding tension 8cN, winder speed 800m/min.Warping uses beam warper, speed 650m/
Min, collective's creeling, using segmented configuration warp tension：Preceding 10 cN, in 8 cN, rear 6 cN, the cN of side yarn 15；（3）Sizing：Match somebody with somebody
Slurrying liquid carries out starching, and the slurries composition is：40 parts of polyvinyl alcohol, 30 parts of acrylic size, 30 parts of converted starch, add water
It is adjusted to slurry viscosity 9s.Slurry groove temperature control is at 96 DEG C, and the temperature control of drying room is at 100 DEG C, squeezing pressure 12kN, the rate of sizing 9%,
Regain 10%；（4）Weaving：Yarn is woven on looms in a manner of warp thread and weft yarn are orthogonal and causes fabric, during weaving on
Machine tension force 150kg, speed 180r/min；（5）Desizing is washed：Prepare amylase solution：Amylase 4g/L, bleeding agent 1g/L, chlorine
Change sodium 5g/L, phosphate buffer solution is as solvent.Fabric is immersed in amylase solution, control temperature at 60 DEG C, pH 7.8,
Reaction time 80min, washing, 90 DEG C of temperature；（6）Stentering forming：Stentering forming is carried out using framing shaping machine, controls temperature
150 DEG C, speed 40m/min.
Comparative example：Soybean fabric lining coated with antistatic additive.
Embodiment 1~4 and comparative example 1 are subjected to antistatic and anti-microbial property test, test result is as shown in table 1.
Table 1 is antistatic and antibacterial effect
As seen from the above table, the selvedge band that the present invention is prepared is antistatic and antibacterial is good, water-fastness, consistency of performance.On in addition,
It is less and submissive in filoplume caused by the yarn being prepared to state embodiment.
Embodiment described above is only explanation of the invention, is not limitation of the present invention, people in the art
The equivalent transformation and modification that member makes according to the present invention, belong to protection scope of the present invention.
Claims (4)
1. a kind of preparation technology of soybean fiber selvedge band, it is characterised in that comprise the following steps：
（1）Wet spinning：Take soybean fiber spinning solution, add 2~4% chitosans and 1.5~3% Chinese medical extracts, stirring 3~
6h, 20~30min of ultrasonic disperse, 3~5min is stood, add 0.3~1% glutaraldehyde and 0.5~2% dispersant, be stirred at room temperature mixed
It is even, protein spinning solution is made, soybean fiber is made using the mode of wet spinning；
（2）Spinning：By soybean fiber by collecting, twisting, drawing yarn, winding spinning obtains raw yarn, raw yarn carries out winder and warping
Process, winder use metal drum, 6~8cN of influence of winding tension, winder 600~800m/min of speed, and warping uses batch warping
Machine, 500~650m/min of speed, collective's creeling, using segmented configuration warp tension：Preceding 10 cN, in 8 cN, rear 6 cN, side yarn
15 cN；
（3）Sizing：Prepare slurries and carry out starching, the slurries composition is：30~40 parts of polyvinyl alcohol, acrylic size 20~
30 parts, 20~30 parts of converted starch, it is added with water to 6~9s of slurry viscosity；Slurry groove temperature control is at 88~96 DEG C, the temperature of drying room
Control is at 95~100 DEG C, squeezing pressure 12-16kN, the rate of sizing 7.8~9%, regain 8.6~10%；
（4）Weaving：Yarn is woven on looms in a manner of warp thread and weft yarn are orthogonal and causes fabric, warp tension during weaving
130~150kg, 160~180r/min of speed；
（5）Desizing is washed：Fabric is immersed in 2~4g/L of concentration amylase solution, at 55~60 DEG C, pH's control temperature exists
7.0~8.0,60~80min of reaction time, washing, 80~90 DEG C of temperature；
（6）Stentering forming：Stentering forming is carried out using framing shaping machine, controls 135~150 DEG C of temperature, 25~40m/ of speed
min。
2. the preparation technology of soybean fiber selvedge band according to claim 1, it is characterised in that：The soybean fiber spinning
Liquid is dissolved in the mixed solution of sodium hydroxide and urea by soybean cellulose and is formulated.
3. the preparation technology of soybean fiber selvedge band according to claim 1, it is characterised in that：The Chinese medical extract is
One or more extractions in the coptis, the root of Dahurain angelica, rheum officinale, folium artemisiae argyi, the red sage root obtain.
4. the preparation technology of soybean fiber selvedge band according to claim 1, it is characterised in that：Step（5）The starch
Enzyme solutions solvent is phosphate buffer solution, also includes 0.5~1g/L bleeding agents, 3~5g/L sodium chloride in amylase solution.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710575838.7A CN107447332A (en) | 2017-07-14 | 2017-07-14 | A kind of preparation technology of soybean fiber selvedge band |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710575838.7A CN107447332A (en) | 2017-07-14 | 2017-07-14 | A kind of preparation technology of soybean fiber selvedge band |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107447332A true CN107447332A (en) | 2017-12-08 |
Family
ID=60488114
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710575838.7A Pending CN107447332A (en) | 2017-07-14 | 2017-07-14 | A kind of preparation technology of soybean fiber selvedge band |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107447332A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109881296A (en) * | 2019-03-12 | 2019-06-14 | 四川大学 | A kind of oxidation resistant plant biomass fiber of antibacterial and preparation method thereof |
| WO2019165751A1 (en) * | 2018-02-28 | 2019-09-06 | 江苏金太阳纺织科技股份有限公司 | Buffering agent for balancing ph value of fabric and preparation method therefor |
| CN110359153A (en) * | 2019-07-26 | 2019-10-22 | 际华三五四二纺织有限公司 | A kind of filled type fabric and its weaving process |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101624743A (en) * | 2009-08-04 | 2010-01-13 | 山西绿洲纺织有限责任公司 | Wet-spinning cordettes and preparation method thereof |
| CN103103663A (en) * | 2012-11-29 | 2013-05-15 | 宁波双盾纺织帆布实业有限公司 | Air spinning method for soybean fibres |
| CN106087415A (en) * | 2016-06-16 | 2016-11-09 | 东莞市联洲知识产权运营管理有限公司 | A kind of lace fabric with metallic luster and preparation method thereof |
| CN106727139A (en) * | 2016-12-28 | 2017-05-31 | 芜湖凯奥尔环保科技有限公司 | A kind of soybean facial mask containing traditional Chinese medicine ingredients and preparation method thereof |
-
2017
- 2017-07-14 CN CN201710575838.7A patent/CN107447332A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101624743A (en) * | 2009-08-04 | 2010-01-13 | 山西绿洲纺织有限责任公司 | Wet-spinning cordettes and preparation method thereof |
| CN103103663A (en) * | 2012-11-29 | 2013-05-15 | 宁波双盾纺织帆布实业有限公司 | Air spinning method for soybean fibres |
| CN106087415A (en) * | 2016-06-16 | 2016-11-09 | 东莞市联洲知识产权运营管理有限公司 | A kind of lace fabric with metallic luster and preparation method thereof |
| CN106727139A (en) * | 2016-12-28 | 2017-05-31 | 芜湖凯奥尔环保科技有限公司 | A kind of soybean facial mask containing traditional Chinese medicine ingredients and preparation method thereof |
Non-Patent Citations (3)
| Title |
|---|
| 施安辉: "《经济微生物》", 30 June 1989, 安徽科学技术出版社 * |
| 赵贵兴: "一种再生蛋白纤维――大豆蛋白纤维 ", 《中国油脂》 * |
| 赵贵兴: "一种再生蛋白纤维――大豆蛋白纤维", 《中国油脂》 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2019165751A1 (en) * | 2018-02-28 | 2019-09-06 | 江苏金太阳纺织科技股份有限公司 | Buffering agent for balancing ph value of fabric and preparation method therefor |
| CN109881296A (en) * | 2019-03-12 | 2019-06-14 | 四川大学 | A kind of oxidation resistant plant biomass fiber of antibacterial and preparation method thereof |
| CN110359153A (en) * | 2019-07-26 | 2019-10-22 | 际华三五四二纺织有限公司 | A kind of filled type fabric and its weaving process |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101736468B (en) | Energy-saving and low-pollution method for processing soft yarns | |
| CN107447332A (en) | A kind of preparation technology of soybean fiber selvedge band | |
| CN108085772B (en) | Cellulose nano-fibril reinforced polyurethane fiber and preparation method and application thereof | |
| CN113290971B (en) | Nano antifouling and antibacterial textile fabric and preparation method thereof | |
| CN101191271A (en) | Corn fibre and polynosic fibre blended fabric and manufacturing technique thereof | |
| CN104726998A (en) | Making method for cuprammouium rayon/viscose fiber antibacterial blended fabric | |
| CN102137964B (en) | Functional cellulosic moldings | |
| CN107385865A (en) | A kind of Sand Wash Process of Modal yarn | |
| CN104695109A (en) | Wool, cashmere/bamboo charcoal fiber blended fabric manufacturing method | |
| JP6504471B2 (en) | Method of producing yarn having compatibility with weaving function | |
| WO2019014968A1 (en) | In-situ-based preparation method for antibacterial ribbon | |
| CN105839408A (en) | Preparation method of bamboo fiber-cotton and ramie blended fabric | |
| CN111663216B (en) | Moisture-conductive quick-drying type composite yarn, preparation method thereof and fabric | |
| CN106544773A (en) | A kind of production technology of aloe cotton blended fabric | |
| CN107604512A (en) | A kind of blending has the fabric of graphene fiber | |
| CN104060358A (en) | Radiation-proof cross-blended yarn and preparation method thereof | |
| CN107012524B (en) | A kind of uvioresistant function fiber producing processes based on organic synthesis | |
| CN1532313A (en) | Ironing-free, washing-free wearable fabric with pure cotton apperance | |
| KR20060040626A (en) | The he manufacturing method of flocked fabrics with elasticity using scrapped leather | |
| CN107237017A (en) | A kind of textile material and preparation method thereof | |
| CN105951268A (en) | Cotton and hemp composite functional fabric | |
| CN109183190B (en) | Functional textile material and preparation method and application thereof | |
| CN110965313A (en) | Pretreatment process of polar fleece knitted fabric gray fabric | |
| CN105544047A (en) | Corn fiber and viscose fiber blending fabric and manufacture method thereof | |
| CN112647143A (en) | Spinning solution and preparation method thereof, and antibacterial cuprammonium fabric and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20171208 |