CN107447216A - A kind of dental implant surface processing method and equipment - Google Patents
A kind of dental implant surface processing method and equipment Download PDFInfo
- Publication number
- CN107447216A CN107447216A CN201710669787.4A CN201710669787A CN107447216A CN 107447216 A CN107447216 A CN 107447216A CN 201710669787 A CN201710669787 A CN 201710669787A CN 107447216 A CN107447216 A CN 107447216A
- Authority
- CN
- China
- Prior art keywords
- frock
- acid
- station
- mobile device
- oxidation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23F—NON-MECHANICAL REMOVAL OF METALLIC MATERIAL FROM SURFACE; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL; MULTI-STEP PROCESSES FOR SURFACE TREATMENT OF METALLIC MATERIAL INVOLVING AT LEAST ONE PROCESS PROVIDED FOR IN CLASS C23 AND AT LEAST ONE PROCESS COVERED BY SUBCLASS C21D OR C22F OR CLASS C25
- C23F1/00—Etching metallic material by chemical means
- C23F1/10—Etching compositions
- C23F1/14—Aqueous compositions
- C23F1/16—Acidic compositions
- C23F1/26—Acidic compositions for etching refractory metals
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61C—DENTISTRY; APPARATUS OR METHODS FOR ORAL OR DENTAL HYGIENE
- A61C8/00—Means to be fixed to the jaw-bone for consolidating natural teeth or for fixing dental prostheses thereon; Dental implants; Implanting tools
- A61C8/0012—Means to be fixed to the jaw-bone for consolidating natural teeth or for fixing dental prostheses thereon; Dental implants; Implanting tools characterised by the material or composition, e.g. ceramics, surface layer, metal alloy
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23F—NON-MECHANICAL REMOVAL OF METALLIC MATERIAL FROM SURFACE; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL; MULTI-STEP PROCESSES FOR SURFACE TREATMENT OF METALLIC MATERIAL INVOLVING AT LEAST ONE PROCESS PROVIDED FOR IN CLASS C23 AND AT LEAST ONE PROCESS COVERED BY SUBCLASS C21D OR C22F OR CLASS C25
- C23F1/00—Etching metallic material by chemical means
- C23F1/08—Apparatus, e.g. for photomechanical printing surfaces
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23G—CLEANING OR DE-GREASING OF METALLIC MATERIAL BY CHEMICAL METHODS OTHER THAN ELECTROLYSIS
- C23G1/00—Cleaning or pickling metallic material with solutions or molten salts
- C23G1/02—Cleaning or pickling metallic material with solutions or molten salts with acid solutions
- C23G1/10—Other heavy metals
- C23G1/106—Other heavy metals refractory metals
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23G—CLEANING OR DE-GREASING OF METALLIC MATERIAL BY CHEMICAL METHODS OTHER THAN ELECTROLYSIS
- C23G3/00—Apparatus for cleaning or pickling metallic material
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D11/00—Electrolytic coating by surface reaction, i.e. forming conversion layers
- C25D11/005—Apparatus specially adapted for electrolytic conversion coating
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D11/00—Electrolytic coating by surface reaction, i.e. forming conversion layers
- C25D11/02—Anodisation
- C25D11/26—Anodisation of refractory metals or alloys based thereon
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Mechanical Engineering (AREA)
- Health & Medical Sciences (AREA)
- Electrochemistry (AREA)
- Oral & Maxillofacial Surgery (AREA)
- Orthopedic Medicine & Surgery (AREA)
- Dentistry (AREA)
- Epidemiology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Ceramic Engineering (AREA)
- ing And Chemical Polishing (AREA)
- Dental Tools And Instruments Or Auxiliary Dental Instruments (AREA)
Abstract
The invention discloses a kind of dental implant surface processing method and equipment, acid etching and pickling processes process are combined by a kind of dental implant surface processing method in the present invention, being formed in titanium alloy dental implant surface has nano level rough surface, and rough surface can improve the osseointegration character of tooth implant and bone tissue after titanium alloy tooth implant implantation human body；A kind of dental implant surface processing equipment has the oxidation frock of automatic centering simultaneously, reduce the positioning difficulty of oxidation frock, avoid displacement of the oxidation frock between station movement, being automatically performed for dental implant surface processing method is realized, and ensures the treatment effect on the surface of tooth implant.
Description
Technical field
The invention belongs to oral cavity titanium alloy tooth implant technical field, and in particular to a kind of titanium alloy dental implant surface changes
The processing method of property.
Background technology
Tooth implant, it is to be implanted into by way of surgical operation in the upper mandibular at human body agomphosis position, treats its hand
After art wound healing, the device of artificial tooth is repaired in installation at an upper portion thereof, plants root of the tooth of the body portion equivalent to dermal tooth, therefore Dental implantion
Fixation of the body for whole tooth serves vital effect, because artificial root of the tooth will be implanted in the alveolar bone of people,
So tooth implant must have good bio-compatibility, intensity and manufacturability, in order to which the bone tissue with people is incorporated in one
A bit, enduringly using heavy burden.
Dental implant materials mainly has Metal and Alloy material class (gold, 316L stainless steels (iron-chromium-nickel alloy), casting
Vitallium, titanium and alloy etc.) and two kinds of ceramic material class, generally use is medical pure titanium at present, and titanium has good
Good bio-compatibility, is referred to as biological metal, can be firmly combined together with the bone of people, this characteristic of titanium is claimed
It is to be taught to find 50 years last century by scientist Bu Luonei marks of Sweden for " synosteosis ".Then, titanium is applied to
Tooth implant, and other field is extend to, such as field of orthopaedics etc.；Allow titanium is more preferable, is quickly done with people's synosteosis, people
Substantial amounts of research and practice.The tooth implant of early stage is not surface-treated especially, maintains machining surface, Zhi Houwei
The more preferable bioactivity of tooth implant and osseointegration character are assigned to meet the Treatment need for shortening healing cycle, starts to apply
Surface coated treatment technology, by the material with bioactive properties it is attached to it (such as：Titanium starches sprayed surface and hydroxyl phosphorus ash
Stone coating surface).By this method obtain tooth implant have micron-nanometer multi micro-structural concurrently, solve surface texture with
The problem of base adhesion deficiency；But because planting body preserves Clinical practice to the end from being fabricated into, generally have one intersegmental
Every the time, tooth kind bigger by the chance of hydrocarbon pollution in air with the extension dental implant surface of holding time
The biological activity of implant is lower；Having research surface, newly its ratio of bone contact (BIC) of planting body of the processing without pollution can reach
To more than 90% and the pure titanium implant BIC of aging only less than 60%, and orthopedic implant is in mechanical environment and biofluid
Erosion collective effect under, coating easily comes off, dissolved, cause the bioactivity of material to reduce, service life shorten；In addition
One problem is additional interfaces between coating and matrix be present, makes Integrated implant maintain to complicate for a long time.Therefore, the surface of non-coating
Roughening attracts people's attention, surface texture technology, to obtain certain coarse surface, to increase surface area, can make bone with
Bonded area between planting body greatly increases, for example, patent " CN102232876 " is processed to tooth by way of sandblasting and acid etching
The surface of planting body is handled, and forms the multi level pit reduced step by step, improves the adhesion of tooth implant and alveolus.
The content of the invention
To overcome problems with present in prior art：In dental implant surface coating technology, face coat easily takes off
Fall, dissolve, causing the bioactivity of material reduces, the problem of with alveolar bone contact force difference；The invention provides a kind of Dental implantion
Surface treating method, by carrying out the processing such as acid etching, pickling and cleaning to dental implant surface, there is table so as to obtain one kind
Face is the tooth implant of the coarse structure of nanometer, tooth implant is obtained more preferable hydrophily, protein adsorption ability, has more preferable
Biological activity.
A kind of equipment of dental implant surface processing, including：Aoxidize frock, basic machine, frock mobile device, air draft system
System and automatic control equipment, frock is aoxidized using V-shape, reduces the positioning difficulty of oxidation frock, avoided oxidation frock and exist
Displacement between station movement, realizes being automatically performed for dental implant surface processing method, and ensure the table of tooth implant
The treatment effect in face.
A kind of method of dental implant surface processing：It is comprised the following steps that：
1) tooth implant is arranged in oxidation frock, oxidation frock is placed into preparation station, technological parameter record and reading
Taking equipment scanning bar code inputs corresponding technological parameter；
2) frock mobile device will aoxidize frock and be moved on ultrasonic wave washing station one to tooth implant progress ultrasonic wave
Heated wash, rinse temperature are 30-40 DEG C, scavenging period 1200s, and the power bottom of ultrasonic rinsing is 1000W, front and rear side
Four, face face is respectively 500W, and the station has two supersonic generators, and the frequency of one is 42KHz, the frequency of another
For 86KHz；
3) frock mobile device will aoxidize frock and be moved to acid etching station progress tooth implant outer surface acid etching, acid etching
The solution of station acid etching groove is 60 DEG C -65 DEG C of acid of hydrochloric acid and nitric acid mixed solution, etching time 2100s-2400s；
4) frock mobile device will aoxidize frock and be moved to pure water spray station, and normal temperature pure water spray is carried out to tooth implant
300s, then frock mobile device by aoxidize frock be moved to ultrasonic wave washing station two carry out tooth implant ultrasound Wave heating drift
1200s is washed, ultrasonic rinsing temperature is 30-40 DEG C, and the power bottom of ultrasonic rinsing is 1000W, and four faces of front and back sides are each
For 500W, ultrasonic frequency 62KHz；
5) frock mobile device is moved to pickling station to tooth implant pickling processes, pickling station pickling by frock is aoxidized
Mixed liquor in groove forms for the mixed solution and water of hydrochloric acid oxalic acid, 80 DEG C of temperature, pickling time 1500s-1800s；
6) frock mobile device will aoxidize frock and be moved to pure water spray station two to tooth implant progress normal temperature pure water spray
Drench 300s；Then frock mobile device will aoxidize frock and be moved to the ultrasonic Wave heating rinsing of ultrasonic rinsing spray station progress,
Scavenging period is 1200s, and ultrasonic rinsing temperature is 30-40 DEG C, and the power of ultrasonic rinsing is that bottom is 1000W, front and rear side
Four, face face is respectively 500W, ultrasonic frequency 62KHz；Then frock mobile device will aoxidize frock and be moved to ultrasonic wave cleaning
Station three, scavenging period 1200s, ultrasonic rinsing temperature are 30-40 DEG C, and the power of ultrasonic rinsing is that bottom is 1000W,
Four faces of front and back sides are respectively 500W, the ultrasonic frequency 156KHz of ultrasonic wave cleaning；
7) frock mobile device is moved to drying station by frock is aoxidized, and hot-air drying is carried out to tooth implant.
In such scheme, as a kind of specific embodiment, the redox of acid of hydrochloric acid and nitric acid mixed solution in step 3)
Current potential>280, the ratio of acid of hydrochloric acid and nitric acid is 5.5:1, the mass concentration of hydrochloric acid is 37%, and the mass concentration of nitric acid is 68%.
In such scheme, as a kind of specific embodiment, the concentration of mixed liquor is 16%-18% in step 5), its
The ratio of hydrochloric acid oxalic acid is 3.5 in middle mixed solution:1, the mass concentration of hydrochloric acid is 37%, and the mass concentration of oxalic acid is 15%.
A kind of equipment of dental implant surface processing, including：Aoxidize frock, basic machine, frock mobile device, air draft system
System and automatic control equipment, the frock mobile device, exhaust system and automatic control equipment are arranged on basic machine, described
Frock mobile device is carried oxidation frock and circulated between each station of basic machine, automatic control equipment control oxidation frock,
The operation of basic machine, frock mobile device and exhaust system.
On this basis, the oxidation frock includes acid etching basket and oxidation suspender, and the acid etching basket is frame structure,
The oxidation suspender includes V-type upper arm, and the lumen width of the V-type Breadth Maximum of the V-type upper arm and the acid etching basket is equal,
The oxidation hanger is suspended on the acid etching basket, and the bottom for aoxidizing hanger is located in acid etching basket.
On this basis, the V-type upper arm is made up of two identical V-shape structures, and V-shape structure is respectively positioned at left and right
Both ends, each V-shape structure are made up of two single armeds separated.
On this basis, the oxidation suspender also includes connector, installing plate, fixture, sealing gasket and tooth implant, institute
State installing plate to be connected with upper arm by connector, the tooth implant is connected by fixture and sealing gasket with installing plate.
On this basis, the exhaust system includes thousand grades of μ high efficiency particulate air filters of cleaning 0.3.
On this basis, the automatic control equipment includes technological parameter record and reads equipment, and acidity liquid level is controlled automatically
Control equipment.
On this basis, the acidity liquid automatic control equipment includes level control device and acid concentration control device.
Compared with prior art, the beneficial effects of the invention are as follows：
1st, acid etching and pickling processes process are combined, formed in titanium alloy dental implant surface with nano level
Rough surface, rough surface can improve the Integrated implant of tooth implant and bone tissue after titanium alloy tooth implant implantation human body
Energy.
2nd, the acid carried out by the V-shape oxidation frock cooperation frock mobile device of automatic centering to dental implant surface
The processing such as erosion, pickling and cleaning, the positioning difficulty of oxidation frock is reduced, avoid shifting of the oxidation frock between station movement
Position, realizes being automatically performed for dental implant surface processing method, and ensure the treatment effect on the surface of tooth implant.
Brief description of the drawings
Fig. 1 is the structural representation of the present invention；
Fig. 2 is the side structure schematic diagram of the present invention；
Fig. 3 aoxidizes the structural representation of frock；
Fig. 4 is the structural representation for aoxidizing hanger；
The control logic figure of Fig. 5 concentration control apparatus；
The control logic figure of Fig. 6 controlling pH devices；
The control logic figure of Fig. 7 fluid level control devices.
In figure：1st, frock is aoxidized, 11, oxidation hanger, 111, upper arm, 1111, single armed, 112, connector, 113, installing plate,
114th, fixture, 115, sealing gasket, 116, tooth implant, 12, acid etching basket, 2, basic machine, 21, station, 211, beam worker
Position, 212, ultrasonic wave washing station one, 213, acid etching station, 214, pure water spray station one, 215, ultrasonic wave washing station two,
216th, pickling station, 217, anodic oxidation station, 218, pure water spray station two, 219, ultrasonic rinsing ＆ spray stations,
2110th, ultrasonic wave washing station three, 2111, drying station, 2112, completion waiting station, 22, frame framework, 3, frock movement
Equipment, 4, exhaust system, 5, automatic control equipment, 51, technological parameter record and read equipment, 52, acidity liquid automatic control
Equipment
Embodiment
With reference to embodiments, the present invention will be described in further detail.It is it should be appreciated that described herein specific real
Example is applied only to explain the present invention, is not intended to limit the present invention.
Embodiment 1
Based on the embodiment in the present invention, a kind of dental implant surface processing method is specific as follows:
1) preparation：Tooth implant 116 is arranged in oxidation frock 1, oxidation frock 1, which is placed into, prepares station 211,
The equipment 51 that technological parameter records and read scans the corresponding technological parameter of bar code input；
2) tooth implant cleans：Frock mobile device 3 will aoxidize frock 1 be moved to it is right on ultrasonic wave washing station 1
Tooth implant 116 carries out ultrasonic wave heated wash, and rinse temperature is 35 DEG C, scavenging period 1200s, the power of ultrasonic rinsing
Bottom is 1000W, and four faces of front and back sides are respectively 500W, and the station has two supersonic generators, and the frequency of one is
42KHz, the frequency of another are 86KHz；
3) acid etching of dental implant surface：Oxidation frock 1 is moved to acid etching station 213 and entered by frock mobile device 3
The outer surface acid etching of row tooth implant 116, the solution of the acid etching groove of acid etching station 213 are the mixed solution of acid of hydrochloric acid and nitric acid, mixing
Oxidation reduction potential>280, temperature is 60 DEG C, etching time 2100s, and the acid of hydrochloric acid and nitric acid mixed solution is according to hydrochloric acid and nitre
The ratio of acid is 5.5:1 is made, and wherein the mass concentration of hydrochloric acid is 37%, and the mass concentration of nitric acid is 68%；
4) cleaning of dental implant surface：Frock mobile device 3 will aoxidize frock 1 and be moved to pure water spray station 214, right
Tooth implant 116 carries out normal temperature pure water spray 300s, and then frock mobile device 3 will aoxidize frock 1 and be moved to ultrasonic wave cleaning
Station 2 215 carries out 116 ultrasonic Wave heating of tooth implant rinsing 1200s, and ultrasonic rinsing temperature is 35 DEG C, ultrasonic rinsing
Power bottom is 1000W, and four faces of front and back sides are respectively 500W, ultrasonic frequency 62KHz；
5) pickling processes of dental implant surface：Frock mobile device 3 will aoxidize frock 1, and to be moved to pickling station 216 right
The pickling processes of tooth implant 116, the mixed liquor in the descaling bath of pickling station 216 form for hydrochloric acid oxalic acid mixed solution and water, temperature
80 DEG C, pickling time 1500s of degree, the concentration of mixed liquor is 16%-18%, and hydrochloric acid oxalic acid ratio is wherein in mixed solution
3.5:1, wherein hydrochloric acid mass concentration 37%, oxalic acid mass concentration 15%；
6) cleaning of tooth implant：Frock mobile device 3 will aoxidize frock 1 and be moved to pure water spray 2 218 pairs of teeth of station
Planting body 116 carries out normal temperature pure water spray 300s；Then frock mobile device 3 will aoxidize frock 1 and be moved to ultrasonic rinsing ＆ sprays
Leaching station 219 carries out ultrasonic Wave heating rinsing, scavenging period 1200s, and ultrasonic rinsing temperature is 35 DEG C, ultrasonic rinsing
Power bottom is 1000W, and four faces of front and back sides are respectively 500W, ultrasonic frequency 62KHz；Then frock mobile device 3 will
Oxidation frock 1 is moved to ultrasonic wave washing station 3 2110, scavenging period 1200s, and ultrasonic rinsing temperature is 35 DEG C, ultrasound
The power bottom of ripple rinsing is 1000W, and four faces of front and back sides are respectively 500W, the ultrasonic frequency 156KHz of ultrasonic wave cleaning；
7) drying of tooth implant：Frock mobile device 3 is moved to drying station 2111 by frock 1 is aoxidized, to Dental implantion
Body 116 carries out hot-air drying.
The present embodiment is about the nanometer level microporous of 50nm~100nm in the aperture that dental implant surface generates；The titanium alloy
Be advantageous to after tooth implant implantation human body it is histiocytic quickly stick, breed and mineralising skeletonization, and can effectively strengthen synosteosis
Intensity.
As shown in Fig. 1-Fig. 7, the present invention schematically illustrates a kind of equipment of dental implant surface processing.
A kind of equipment of dental implant surface processing of present disclosure, as shown in Figure 1 and Figure 2：Including oxidation frock 1, machinery
Body 2, frock mobile device 3, exhaust system 4 and automatic control equipment 5, frock mobile device 3, exhaust system 4 and automatic control
Control equipment 5 is arranged on basic machine 2, and frock mobile device 3 is carried oxidation frock 1 and circulated between each station of basic machine 2,
The control of automatic control equipment 5 aoxidizes the operation of frock 1, basic machine 2, frock mobile device 3 and exhaust system 4.
As shown in Figure 3：Aoxidizing frock 1 includes oxidation hanger 11 and acid etching basket 12, and acid etching basket 12 is frame structure, oxygen
Change the bottom of hanger 11 and be located at the centre of acid etching basket 12, and be suspended on acid etching basket 12；In this embodiment of the present invention,
As shown in Figure 4：Aoxidizing hanger 11 includes V-type upper arm 111, connector 112, installing plate 113, fixture 114, the and of sealing gasket 115
Tooth implant 116；Installing plate 113 is connected by connector 112 with V-type upper arm 111, and tooth implant 116 passes through the He of fixture 114
Sealing gasket 115 is connected with installing plate 113, and for fixture 114 with tooth implant 116 to be threadedly coupled, V-type upper arm 111 includes two
Identical V-shape structure, is connected with the right and left of installing plate respectively, and each V-shape is made up of the single armed 1111 of two separation；
Two single armeds 1111 are separately mounted to the both sides of connecting plate 113, form the V-shape structure of V-type upper arm 111, the V of V-type upper arm 111
The Breadth Maximum of font is equal to the lumen width of acid etching basket 12, and the V-shape single armed of upper arm 111 and the angle of horizontal plane are 90 °,
The value is determined by oxidation hanger 11 and the deadweight of the frictional force and oxidation hanger 11 of acid etching basket 12；Fixture 114 is bolt,
Sequentially pass through installing plate 113 and sealing gasket 115 is connected with tooth implant 116, and alternately stretched along former and later two faces of installing plate 113
Go out the both sides that the big plane of installing plate 113, fixture 114 and sealing gasket 115 are located at installing plate 113 with tooth implant 116 respectively,
Fixture 114 is threadedly coupled with tooth implant 116, and when the screw thread of fixture 114 is screwed into bottom, fixture 114 can compel
Sealing gasket 115 is held out against the end face of tooth implant 116, seal up the inner chamber of tooth implant 116, avoid the inner chamber of tooth implant 116 by
To the destruction of acid etching；When oxidation hanger 11 is put into secundly in acid etching basket 12, the V-structure of oxidation hanger upper arm 111
One side contacted with acid etching basket 12, under itself Action of Gravity Field, V-shape of the oxidation hanger 11 along upper arm 111 is to downslide
It is dynamic, so that oxidation hanger 11 automatically returns to the centre of acid etching basket 12, when oxidation hanger 11 is in the centre of acid etching basket 12,
The V-shape both sides of upper arm 111 contact with acid etching basket 12, and stress is identical to cancel each other, and are located at so as to ensure to aoxidize hanger 11
The centre of acid etching basket 12 is motionless.
As shown in figure 1, the basic machine 2 includes station 21 and frame framework 22, the station 21 includes preparing station
211st, ultrasonic wave washing station 1, acid etching station 213, pure water spray station 1, ultrasonic wave washing station 2 215, acid
Wash station 216, anodic oxidation station 217, pure water spray station 2 218, ultrasonic rinsing ＆ sprays station 219, ultrasonic wave cleaning
Station 3 2110, drying station 2111 and completion waiting station 2112, the station 21 is according to dental implant surface processing method
Flow arrangement, the station 21 is arranged in frame framework 22, and frame framework 22 is 304 stainless steel stents and totally-enclosed outer
Frame.
As shown in Fig. 2 the frock mobile device 3 be arranged on frame framework 22 on, frock mobile device 3 include motor,
Ball screw, timing belt, line slideway, position-detection sensor and arm, the motor driving timing belt drive whole frock
Mobile device moves horizontally along line slideway between each station, and when encountering the position sensor of each station, motor stops
Motion, frock mobile device stop motion, the arm move up and down under the driving of ball screw along line slideway, work as photoelectricity
After proximity sensor senses signal, arm can be automatically moved by the program being previously set and lifted or put down oxidation
Frock 1.
As shown in Fig. 2 the exhaust system 4 is arranged in frame framework 22, exhaust system 4 includes air channel, blower fan and thousand
The clean 0.3 μ high efficiency particulate air filters of level, exhaust system 4 can take the acid mist volatilized away in time, prevent from largely gathering in the short time,
Cause pollution, its thousand grades 0.3 clean μ high efficiency particulate air filters can absorb the bigger acid mist of particulate, and road is handled after avoiding air draft
The load of equipment increases.
As shown in Fig. 2 the automatic control equipment 5 includes the automatic running control device of complete machine, technological parameter record and
Equipment 51, acidity liquid automatic control equipment 52 are read, the automatic running control device of complete machine can make complete machine according to set
Technological process is automatically performed the surface treatment of tooth implant, including frock mobile device 3 to oxidation frock 1 lift put down and
Start and stop between station 21, wait and spread；Technological parameter record and read equipment 51 can to the automatic record of technological parameter and
Read, by bar code barcode scanning device automatic identification and read required technological parameter, mistake when avoiding being manually entered parameter
By mistake；The acidity liquid automatic control equipment 52 includes acid concentration control device and fluid level control device, the acid concentration control
Device includes controlling pH device and concentration control apparatus, and the controlling pH device includes oxidation-reduction electrode, automatic to mend acid
System and control system, the controlling pH device are used for the acidity for controlling mixed liquor in acid etching station 213, the redox
Electrode is arranged in acid etching station 213, and for detecting the oxidation reduction potential value of mixed liquor, control logic is as shown in fig. 6, oxidation
Reduction potential value is the value 280 of a setting, then mends acid automatically when oxidation reduction potential value is less than 280, the setting value can be with
Regulation；The concentration control apparatus is popped one's head in including Concentration Testing, mends sour water charging system, warning system and control system, institute automatically
The concentration that concentration control apparatus is used to control hydrochloric acid oxalic acid in pickling station 216 is stated, the Concentration Testing probe is arranged on pickling
In station 216, for detecting the concentration of hydrochloric acid oxalic acid, control logic is as shown in figure 5, hydrochloric acid concentration of oxalic acid is the model of a setting
Parameter 16%~18% is enclosed, warning system starts while is automatically replenished if concentration is reached more than 18%, is reported if less than 16%
Alert system starts and mends acid automatically, and the range parameter can adjust；The fluid level control device includes level monitoring device and alarm
System, level monitoring device are arranged on and need to detected in the station of liquid level, and control logic is as shown in fig. 7, have two values up and down, if low
Lower value in liquid level or the upper value higher than liquid level can start warning system, need operating personnel's on-site manual to control fluid infusion valve,
The amount of convenient control single fluid infusion.
The preferred embodiments of the present invention have shown and described in described above, as previously described, it should be understood that the present invention is not office
Be limited to form disclosed herein, be not to be taken as the exclusion to other embodiment, and available for various other combinations, modification and
Environment, and can be changed in the scope of the invention is set forth herein by the technology or knowledge of above-mentioned teaching or association area
It is dynamic., then all should be appended by the present invention and the change and change that those skilled in the art are carried out do not depart from the spirit and scope of the present invention
In scope of the claims.
Claims (10)
1. a kind of dental implant surface processing method, it is characterised in that comprise the following steps：
Step 1: tooth implant (116) is arranged in oxidation frock (1), oxidation frock (1), which is placed into, prepares station (211),
Technological parameter records and read equipment (51) scanning bar code and inputs corresponding technological parameter；
It is moved to Step 2: frock mobile device (3) will aoxidize frock (1) on ultrasonic wave washing station one (212) to Dental implantion
Body (116) carries out ultrasonic wave heated wash, and rinse temperature is 30-40 DEG C, scavenging period 1200s, the power of ultrasonic rinsing
Bottom is 1000W, and four faces of front and back sides are respectively 500W, and the station has two supersonic generators, and the frequency of one is
42KHz, the frequency of another are 86KHz；
Step 3: frock mobile device (3), which will aoxidize frock (1), is moved to acid etching station (213) progress tooth implant (116) outside
Surface acid etching, the mixed liquor of acid etching station (213) acid etching groove are 60 DEG C -65 DEG C of acid of hydrochloric acid and nitric acid mixed solution, during acid etching
Between be 2100s-2400s；
Step 4: frock mobile device (3), which will aoxidize frock (1), is moved to pure water spray station (214), to tooth implant
(116) normal temperature pure water spray 300s is carried out, then frock mobile device (3) will aoxidize frock (1) and be moved to ultrasonic wave scavenger
Two (215) of position carry out the ultrasonic Wave heating rinsing 1200s of tooth implant (116), and ultrasonic rinsing temperature is 30-40 DEG C, ultrasonic wave
The power bottom of rinsing is 1000W, and four faces of front and back sides are respectively 500W, ultrasonic frequency 62KHz；
Step 5: frock mobile device (3), which will aoxidize frock (1), is moved to pickling station (216) to tooth implant (116) pickling
Handle, the mixed liquor in pickling station (216) descaling bath forms for the mixed solution and water of hydrochloric acid oxalic acid, 80 DEG C of temperature, pickling
Time is 1500s-1800s；
Step 6: frock mobile device (3), which will aoxidize frock (1), is moved to pure water spray station two (218) to tooth implant
(116) normal temperature pure water spray 300s is carried out；Then frock mobile device (3) will aoxidize frock (1) and be moved to ultrasonic rinsing ＆ sprays
Drench station (219) and carry out ultrasonic Wave heating rinsing, scavenging period 1200s, ultrasonic rinsing temperature is 30-40 DEG C, ultrasonic wave
The power bottom of rinsing is 1000W, and four faces of front and back sides are respectively 500W, ultrasonic frequency 62KHz；Then frock movement is set
Standby (3) will aoxidize frock (1) and be moved to ultrasonic wave washing station three (2110), scavenging period 1200s, ultrasonic rinsing temperature
For 30-40 DEG C, the power bottom of ultrasonic rinsing is 1000W, and four faces of front and back sides are respectively 500W, the ultrasound of ultrasonic wave cleaning
Wave frequency rate 156KHz；
Step 7: frock mobile device (3), which will aoxidize frock (1), is moved to drying station (2111), tooth implant (116) is entered
Row hot-air is dried.
A kind of 2. dental implant surface processing method according to claim 1, it is characterised in that：Acid of hydrochloric acid and nitric acid in step 3
Mixed solution oxidation-reduction potential>280；The ratio of hydrochloric acid and nitric acid is 5.5 in the mixed solution of acid of hydrochloric acid and nitric acid:1, hydrochloric acid
Mass concentration be 37%, the mass concentration of nitric acid is 68%.
A kind of 3. dental implant surface processing method according to claim 2, it is characterised in that：Mixed liquor in step 5
Concentration is 16%-18%, and the ratio of hydrochloric acid and oxalic acid is 3.5 wherein in hydrochloric acid oxalic acid mixed solution:1, the mass concentration of hydrochloric acid
For 37%, the mass concentration of oxalic acid is 15%.
A kind of 4. equipment of dental implant surface processing, it is characterised in that：Including oxidation frock (1), basic machine (2), frock
Mobile device (3), exhaust system (4) and automatic control equipment (5), the frock mobile device (3), exhaust system (4) and from
Dynamic control device (5) is arranged on basic machine (2), and frock mobile device (3) carries oxidation frock (1) in basic machine (2)
Each station between circulate, automatic control equipment (5) control oxidation frock (1), basic machine (2), frock mobile device (3) and
The operation of exhaust system (4).
5. the equipment of dental implant surface processing according to claim 4, it is characterised in that：Oxidation frock (1) bag
Acid etching basket (12) and oxidation hanger (11) are included, the acid etching basket (12) is frame structure, and the oxidation hanger (11) includes
Upper arm (111), the upper arm (111) are V-type upper arm, the V-type Breadth Maximum and the acid etching basket (12) of the upper arm (111)
Lumen width it is equal, the oxidation hanger (11) is suspended on the acid etching basket (12), and is aoxidized under hanger (11)
Portion is located in acid etching basket (12).
A kind of 6. equipment of dental implant surface processing according to claim 5, it is characterised in that：The upper arm (111)
It is made up of two identical V-shape structures, V-shape structure is located at left and right ends respectively, and each V-shape structure is by separate two
Single armed (1111) forms.
A kind of 7. equipment of dental implant surface processing according to claim 6, it is characterised in that：The oxidation hanger
(11) connector (112), installing plate (113), fixture (114), sealing gasket (115) and tooth implant (116) are also included, it is described
Installing plate (113) is connected by connector (112) with upper arm (111), the tooth implant (116) by fixture (114) and
Sealing gasket (115) is connected with installing plate (113).
A kind of 8. equipment of dental implant surface processing according to claim 7, it is characterised in that：The exhaust system
(4) thousand grades of μ high efficiency particulate air filters of cleaning 0.3 are included.
A kind of 9. equipment of dental implant surface processing according to claim 8, it is characterised in that：Described automatically control sets
Standby (5) include technological parameter and record and read equipment (51), acidity liquid automatic control equipment (52).
A kind of 10. equipment of dental implant surface processing according to claim 9, it is characterised in that：The acidity liquid level
Automatic control equipment (52) includes level control device and acid concentration control device.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710669787.4A CN107447216B (en) | 2017-08-08 | 2017-08-08 | A kind of dental implant surface processing method and equipment |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710669787.4A CN107447216B (en) | 2017-08-08 | 2017-08-08 | A kind of dental implant surface processing method and equipment |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN107447216A true CN107447216A (en) | 2017-12-08 |
| CN107447216B CN107447216B (en) | 2019-08-06 |
Family
ID=60490930
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710669787.4A Active CN107447216B (en) | 2017-08-08 | 2017-08-08 | A kind of dental implant surface processing method and equipment |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107447216B (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109316261A (en) * | 2018-09-18 | 2019-02-12 | 南京医科大学附属口腔医院 | Easily displacement positioning Totally-enclosed-type acid etching flusher |
| CN111826700A (en) * | 2020-07-27 | 2020-10-27 | 上海市特种设备监督检验技术研究院 | Pickling and passivating combined liquid for anodizing titanium material and pickling and passivating method |
| CN114951133A (en) * | 2022-05-10 | 2022-08-30 | 无锡领缔生物科技有限公司 | Plant surface corrosion cleaning system and cleaning method thereof |
| CN115041462A (en) * | 2022-07-15 | 2022-09-13 | 江苏创英医疗器械有限公司 | Surface cleaning process for dental implant |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101014297A (en) * | 2004-08-06 | 2007-08-08 | 彭特恩临床科技有限公司 | Dental filling material |
| CN101888815A (en) * | 2007-12-11 | 2010-11-17 | 山八齿材工业株式会社 | The manufacture method of implant and artificial dental root |
| CN102113918A (en) * | 2009-12-30 | 2011-07-06 | 沈阳天贺新材料开发有限公司 | Method for preparing porous structure on surface of pure titanium dental implant |
| CN102525826A (en) * | 2012-01-19 | 2012-07-04 | 浙江大学 | Preparation method for superhydrophilic micro-nano composite dental implant surface |
| JP2012143416A (en) * | 2011-01-13 | 2012-08-02 | Gc Corp | Dental implant and surface treatment method of dental implant |
| CN103451602A (en) * | 2012-05-28 | 2013-12-18 | 江苏创英医疗器械有限公司 | Surface treatment process of bioactive metallic titanium implant having multistage micro-pit structure |
-
2017
- 2017-08-08 CN CN201710669787.4A patent/CN107447216B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101014297A (en) * | 2004-08-06 | 2007-08-08 | 彭特恩临床科技有限公司 | Dental filling material |
| CN101888815A (en) * | 2007-12-11 | 2010-11-17 | 山八齿材工业株式会社 | The manufacture method of implant and artificial dental root |
| CN102113918A (en) * | 2009-12-30 | 2011-07-06 | 沈阳天贺新材料开发有限公司 | Method for preparing porous structure on surface of pure titanium dental implant |
| JP2012143416A (en) * | 2011-01-13 | 2012-08-02 | Gc Corp | Dental implant and surface treatment method of dental implant |
| CN102525826A (en) * | 2012-01-19 | 2012-07-04 | 浙江大学 | Preparation method for superhydrophilic micro-nano composite dental implant surface |
| CN103451602A (en) * | 2012-05-28 | 2013-12-18 | 江苏创英医疗器械有限公司 | Surface treatment process of bioactive metallic titanium implant having multistage micro-pit structure |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109316261A (en) * | 2018-09-18 | 2019-02-12 | 南京医科大学附属口腔医院 | Easily displacement positioning Totally-enclosed-type acid etching flusher |
| CN109316261B (en) * | 2018-09-18 | 2024-03-29 | 南京医科大学附属口腔医院 | Easy-to-shift positioning totally-enclosed acid etching flushing device |
| CN111826700A (en) * | 2020-07-27 | 2020-10-27 | 上海市特种设备监督检验技术研究院 | Pickling and passivating combined liquid for anodizing titanium material and pickling and passivating method |
| CN114951133A (en) * | 2022-05-10 | 2022-08-30 | 无锡领缔生物科技有限公司 | Plant surface corrosion cleaning system and cleaning method thereof |
| CN115041462A (en) * | 2022-07-15 | 2022-09-13 | 江苏创英医疗器械有限公司 | Surface cleaning process for dental implant |
| CN115041462B (en) * | 2022-07-15 | 2023-09-01 | 江苏创英医疗器械有限公司 | Tooth implant surface cleaning process |
Also Published As
| Publication number | Publication date |
|---|---|
| CN107447216B (en) | 2019-08-06 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN107447216B (en) | A kind of dental implant surface processing method and equipment | |
| Vinothkumar et al. | Influence of deep dry cryogenic treatment on cutting efficiency and wear resistance of nickel–titanium rotary endodontic instruments | |
| CN106890356A (en) | A kind of degradable zinc-containing alloy implantation material and preparation method and application | |
| CN106902390A (en) | A kind of titanium alloy is implanted into composite material and its preparation and application | |
| CN108478858A (en) | A kind of preparation method of titanium implant nanoscale ultra-hydrophilic surface | |
| CN104233431B (en) | The preparation method of pure magnesium surface ultrasonic microarc oxidation-phytic acid-fibroin albumen multistage composite bioactivity coatings composite | |
| CN109848546A (en) | A kind of titanium or titanium alloy surface micro-nano structure method of modifying | |
| CN106267342A (en) | A kind of dentistry implant and preparation method thereof | |
| CN109731135A (en) | A kind of hydrophilic treatment process of implant surface | |
| CN109259878A (en) | One-part form Immediate prosthesis dental implant of copper-bearing antibacterial titanium alloy and preparation method thereof | |
| CN105803428A (en) | Method for preparing zinc-doped nanometer structure with bacteriostatic action on surface of porous pure titanium | |
| CN109537025A (en) | Metallic composite, degradable magnesium alloy bone screw and application containing corrosion-resistant coating | |
| CN110157948B (en) | Medical titanium alloy special for implant and capable of achieving immediate implantation and preparation method thereof | |
| CN106823001B (en) | A kind of biologic bracket material for dental root regeneration, preparation method and applications | |
| CN105935317B (en) | Plant percutaneous base station and preparation method thereof in a kind of surface carried medicine sustained-release jaw face | |
| CN1451367A (en) | Induction ossified bio-active artificial tooth root implant material and preparing method thereof | |
| CN103833424B (en) | The surface treatment method of zirconium oxide ceramic dental implant | |
| CN205590777U (en) | Hot dipping zinc is with scraping grey device in batches | |
| CN108070900A (en) | Titanium-based nano pipe surface is formed in situ the preparation method of hexagonal flake apatite coating | |
| CN107740103A (en) | A kind of method for activating surface of tooth implant | |
| Fomin et al. | Efficiency of osseointegration properties manifestation in dental implants with hydroxyapatite plasma coating | |
| CN109259879A (en) | Titanium alloy one-part form Immediate prosthesis dental implant and preparation method thereof | |
| CN109431637A (en) | A kind of surface treatment method of dental implant | |
| CN113798678A (en) | Method for inducing high-bioactivity surface of oral titanium alloy implant by laser | |
| CN100467669C (en) | Method of fast growing HA biologically active layer from oxidation film on titanium alloy surface by ultraviolet excitation |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |