CN107418731A - Method for preparing sugar flavor for cigarettes by high-pressure homogenization - Google Patents

Method for preparing sugar flavor for cigarettes by high-pressure homogenization Download PDF

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Publication number
CN107418731A
CN107418731A CN201710353747.9A CN201710353747A CN107418731A CN 107418731 A CN107418731 A CN 107418731A CN 201710353747 A CN201710353747 A CN 201710353747A CN 107418731 A CN107418731 A CN 107418731A
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CN
China
Prior art keywords
sugared
cigarette
pressure
spices
sugared spices
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710353747.9A
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Chinese (zh)
Inventor
林鸿佳
杨晶津
王慧
汪显国
华崑
华一崑
刘继辉
杨洋
高占勇
赵佳成
崔宇翔
马晓龙
王玉真
程倩
翁瑞杰
邱杰斐
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hongyun Honghe Tobacco Group Co Ltd
Original Assignee
Hongyun Honghe Tobacco Group Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hongyun Honghe Tobacco Group Co Ltd filed Critical Hongyun Honghe Tobacco Group Co Ltd
Priority to CN201710353747.9A priority Critical patent/CN107418731A/en
Publication of CN107418731A publication Critical patent/CN107418731A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/0003Compounds of unspecified constitution defined by the chemical reaction for their preparation
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B3/00Preparing tobacco in the factory
    • A24B3/12Steaming, curing, or flavouring tobacco

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Seasonings (AREA)

Abstract

The invention discloses a method for preparing a sugar flavor for cigarettes by high-pressure homogenization, which comprises the following steps: s1, pre-blending sugar and spice, weighing and mixing the required raw materials according to the proportion, and stirring the raw materials at normal pressure until the feed liquid is basically uniform; s2, passing the sugar and spice pre-blended liquid obtained in the step S1 through a high-pressure homogenizing valve, and controlling the temperature of the liquid to be below 50 ℃; adopting a one-stage or multi-stage high-pressure homogenization combined mode; the pressure of the high-pressure homogenizing valve is 60MPa to 100MPa, and the mixture is circulated until the mixture is uniformly mixed; s3, passing the feed liquid through a microporous filter membrane with the aperture of 0.1-5 mu m; and S4, cooling the finished product of the sugar flavor for cigarettes to room temperature, and then sealing and filling. The invention has the beneficial effects that: the sugar flavor for cigarettes can be kept in a uniform suspension state within 12 months of storage time, the phenomena of layered precipitation, barrel expansion, deterioration and the like can not occur, and the quality protection of the sugar flavor is good.

Description

It is a kind of to prepare method of the cigarette with sugared spices using high-pressure homogeneous
Technical field
It is particularly a kind of to prepare side of the cigarette with sugared spices using high-pressure homogeneous the present invention relates to technical field of cigarette processing Method.
Background technology
The defects of cigarette can be effectively improved excitant in tobacco leaf formulation, miscellaneous gas with sugared spices, pleasant impression is not clean, increase is fragrant Gas and assign cigarette it is unique suck style, to improving and stablize cigarette quality, establishment cigarette style has great importance.Cause This, cigarette is to improve cigarette product quality and personalized key technology with sugared spices, and the uniformity of feed liquid directly affects sugar Quality of flavoring and mix with effect, be related to the quality of finished cigarettes.The sugared spice feed liquid prepared using prior art, in storage one After the section time, the phenomenon of layering and precipitating can often occur.Simultaneously as sugared spices allotment workshop is not totally-enclosed, gnotobasis, system The sugared spices got ready is in long-term storage or transportation, easily because microbial fermentation produces the problems such as swollen bucket, sugared spices are rotten.
To solve the problems, such as in prior art, present invention offer is a kind of to prepare side of the cigarette with sugared spices using high-pressure homogeneous Method, cigarette after normal pressure is stirred, by 60~100Mpa high pressure homogeneous valve pressurization homogenizations, can be formed and uniformly divided with sugared spices Dissipate, mixing fully, the fine and smooth sugared spice solution of composition, and the microorganism in feed liquid is occurred clasmatosis under high pressure effect and It is dead;Installation miillpore filter is exported in high pressure homogenizer, the microorganism not partly being effectively broken is realized to filter off and removed, is reached The effect of double sterilization.The method of the invention can realize cigarette with the nanometer of sugared spices is broken, emulsion dispersion and cold kills simultaneously The function of bacterium, reaching improves sugared spices particle diameter and size, realizes the association of high pressure homogenization technique and heat sterilization purification techniques With application, cigarette homogenizing degree and holding time with sugared spices is increased substantially.
The content of the invention
The shortcomings that it is an object of the invention to overcome prior art, there is provided one kind is using the high-pressure homogeneous cigarette for preparing with sugared spices Method.
The purpose of the present invention is achieved through the following technical solutions:It is a kind of to prepare side of the cigarette with sugared spices using high-pressure homogeneous Method, comprise the following steps:
S1, sugared spices are allocated in advance, according to formulary requirements, required raw material are proportionally weighed after mixing, it is sugared to carry out cigarette The pre- allotment of spices, it is substantially uniform to feed liquid using atmospheric agitation;
S2, will in step S1 by allocating sugared spice feed liquid in advance, by high pressure homogeneous valve, feed temperature control 50 DEG C with Under;Can take one or more levels it is high-pressure homogeneous associated with mode;The pressure of high pressure homogeneous valve is 60MPa~100MPa, is recycled to Mixture is well mixed, and makes microorganism in feed liquid that clasmatosis occur under high pressure effect and dead;
Feed liquid after S3, the homogeneous that will be obtained in step S2, by the miillpore filter that aperture is 0.1 μm~5 μm, to remove The microorganism that part is not crushed by high pressure, you can obtain the sugared spices of the cigarette after high-pressure homogeneous and sterilization;
S4, carry out after the tobacco product obtained in step S3 is cooled into room temperature with sugared spices sealing it is filling.
It is described it is filling after tobacco product deposited in sugared spices standby in freezer, temperature of ice house is controlled in 0~10 DEG C of model In enclosing.
It is described it is filling after tobacco product transported with sugared spices using special freezer transport vehicle, the freezer of freezer transport vehicle Temperature control is in the range of 0~10 DEG C.
The present invention has advantages below:
1st, the present invention uses high-pressure homogeneous, high-pressure homogeneous to be used as a kind of physics crushing technology, will not destroy in sugared spices Active ingredient, solution is only become into uniform suspension, avoid solvent in prolonged storage that layering and precipitating occurs, it is fragrant to improve sugar The degree that homogenizes of material.
2nd, using high-pressure homogeneous sterilization and the synergy of milipore filter sterilization technology, smoke abatement can be removed with exhausted in sugared spices Most of microorganism, reach the purpose of low temperature cold sterilization, it is possible to prevente effectively from influence of the microorganism to sugared fragrance-quality, reaches guarantor Protect the effect of sugared fragrance-quality.
3rd, using the cigarette after the inventive method with sugared spices in the storage time of 12 months, even suspension shape can be kept State, phenomena such as layering and precipitating, swollen bucket will not occur, go bad, sugared fragrance-quality protection is good.
Embodiment
With reference to embodiment, the present invention will be further described:
Embodiment 1:
It is a kind of to prepare method of the cigarette with sugared spices using high-pressure homogeneous, comprise the following steps:
S1, sugared spices are allocated in advance, and according to the formulary requirements that brand A tables are fragrant, required raw material is proportionally weighed after mixing, Pre- allotment of the cigarette with sugared spices is carried out, it is substantially uniform to feed liquid using atmospheric agitation;
S2, it will pass through in step S1 and allocate sugared spice feed liquid in advance, it is high-pressure homogeneous using one-level by high pressure homogeneous valve, it is high The pressure of pressure homogenizing valve is arranged to 80MPa, and cycle-index is 3 times, and feed temperature is controlled at 40 DEG C;
Feed liquid after S3, the homogeneous that will be obtained in step S2, by the miillpore filter that aperture is 0.45 μm, to remove part The microorganism not crushed by high pressure, you can obtain the sugared spices of the cigarette after high-pressure homogeneous and sterilization;
S4, carry out after the tobacco product obtained in step S3 is cooled into room temperature with sugared spice feed liquid sealing it is filling.
Tobacco product after will be filling deposited in sugared spices it is standby in cigarette flavor sugar materials freezer, temperature of ice house control 0 In the range of~10 DEG C;Such as need to transport, then transported using special freezer transport vehicle, the temperature control of the freezer of freezer transport vehicle is 0 In the range of~10 DEG C.
Embodiment 2:
It is a kind of to prepare method of the cigarette with sugared spices using high-pressure homogeneous, comprise the following steps:
S1, sugared spices are allocated in advance, and according to the formulary requirements that brand B tables are fragrant, required raw material is proportionally weighed after mixing, Pre- allotment of the cigarette with sugared spices is carried out, it is substantially uniform to feed liquid using atmospheric agitation;
S2, it will pass through in step S1 and allocate sugared spice feed liquid in advance, it is high-pressure homogeneous using two-stage by high pressure homogeneous valve, one The pressure of level high pressure homogeneous valve is arranged to 100MPa, and two level high pressure homogeneous valve pressure is arranged to 60MPa, and cycle-index is 1 time, material Liquid temperature control is at 30 DEG C;
Feed liquid after S3, the homogeneous that will be obtained in step S2, by the miillpore filter that aperture is 1.0 μm, to remove part The microorganism not crushed by high pressure, you can obtain the sugared spices of the cigarette after high-pressure homogeneous and sterilization;
S4, carry out after the tobacco product obtained in step S3 is cooled into room temperature with sugared spice feed liquid sealing it is filling.
Tobacco product after will be filling deposited in sugared spices it is standby in cigarette flavor sugar materials freezer, temperature of ice house control 0 In the range of~10 DEG C;Such as need to transport, then transported using special freezer transport vehicle, the temperature control of the freezer of freezer transport vehicle is 0 In the range of~10 DEG C.
Embodiment 3:
It is a kind of to prepare method of the cigarette with sugared spices using high-pressure homogeneous, comprise the following steps:
S1, sugared spices are allocated in advance, and according to the formulary requirements that brand C tables are fragrant, required raw material is proportionally weighed after mixing, Pre- allotment of the cigarette with sugared spices is carried out, it is substantially uniform to feed liquid using atmospheric agitation;
S2, it will pass through in step S1 and allocate sugared spice feed liquid in advance, it is high-pressure homogeneous using two-stage by high pressure homogeneous valve, one The pressure of level high pressure homogeneous valve is arranged to 80MPa, and two level high pressure homogeneous valve pressure is arranged to 60MPa, and cycle-index is 3 times, material Liquid temperature control is at 49 DEG C;
Feed liquid after S3, the homogeneous that will be obtained in step S2, by the miillpore filter that aperture is 5.0 μm, to remove part The microorganism not crushed by high pressure, you can obtain the sugared spices of the cigarette after high-pressure homogeneous and sterilization;
S4, carry out after the tobacco product obtained in step S3 is cooled into room temperature with sugared spice feed liquid sealing it is filling.
Tobacco product after will be filling deposited in sugared spices it is standby in cigarette flavor sugar materials freezer, temperature of ice house control 0 In the range of~10 DEG C;Such as need to transport, then transported using special freezer transport vehicle, the temperature control of the freezer of freezer transport vehicle is 0 In the range of~10 DEG C.

Claims (3)

1. a kind of prepare method of the cigarette with sugared spices using high-pressure homogeneous, it is characterised in that:Comprise the following steps:
S1, sugared spices are allocated in advance, according to formulary requirements, required raw material are proportionally weighed after mixing, carries out the sugared spices of cigarette Pre- allotment, it is substantially uniform to feed liquid using atmospheric agitation;
S2, it will pass through in step S1 and allocate sugared spice feed liquid in advance, by high pressure homogeneous valve, feed temperature is controlled below 50 DEG C; Take one or more levels it is high-pressure homogeneous associated with mode;The pressure of high pressure homogeneous valve is 60MPa~100MPa, is recycled to mixture It is well mixed;
Feed liquid after S3, the homogeneous that will be obtained in step S2, pass through the miillpore filter that aperture is 0.1 μm~5 μm, you can obtain height Press the sugared spices of the cigarette after homogeneous and sterilization;
S4, carry out after the tobacco product obtained in step S3 is cooled into room temperature with sugared spices sealing it is filling.
2. a kind of method of the cigarette with sugared spices is prepared according to claim 1 using high-pressure homogeneous, it is characterised in that:It is described It is filling after tobacco product deposited in sugared spices it is standby in freezer, temperature of ice house control in the range of 0~10 DEG C.
3. a kind of method of the cigarette with sugared spices is prepared according to claim 2 using high-pressure homogeneous, it is characterised in that:It is described It is filling after tobacco product with sugared spices using special freezer transport vehicle transport, the temperature control of the freezer of freezer transport vehicle is 0 In the range of~10 DEG C.
CN201710353747.9A 2017-05-18 2017-05-18 Method for preparing sugar flavor for cigarettes by high-pressure homogenization Pending CN107418731A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109022150A (en) * 2018-07-04 2018-12-18 红云红河烟草(集团)有限责任公司 High-pressure sterilization filtering method for preventing fermentation of sugar flavor for cigarettes
CN109222215A (en) * 2018-07-04 2019-01-18 红云红河烟草(集团)有限责任公司 Processing method for reducing viscosity of sugar flavor monomer for cigarettes and promoting absorption through high-pressure homogenization
CN110133171A (en) * 2019-05-28 2019-08-16 红云红河烟草(集团)有限责任公司 Method for improving flavor components of natural spice for cigarettes and identification method thereof
CN113876018A (en) * 2021-10-21 2022-01-04 湖北中烟工业有限责任公司 Preparation method of special slice for homogenizing and heating cigarettes

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CN105154226A (en) * 2015-04-14 2015-12-16 湖北中烟工业有限责任公司 Method for preparing tobacco flavor from cane molasses
CN106590932A (en) * 2016-12-14 2017-04-26 江西中烟工业有限责任公司 Preparation method and application of biomacromolecule composite emulsion system

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CN105154226A (en) * 2015-04-14 2015-12-16 湖北中烟工业有限责任公司 Method for preparing tobacco flavor from cane molasses
CN105062675A (en) * 2015-07-27 2015-11-18 湖北中烟工业有限责任公司 Preparation method of beta vulgaris Maillard reactant for tobacco
CN106590932A (en) * 2016-12-14 2017-04-26 江西中烟工业有限责任公司 Preparation method and application of biomacromolecule composite emulsion system

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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109022150A (en) * 2018-07-04 2018-12-18 红云红河烟草(集团)有限责任公司 High-pressure sterilization filtering method for preventing fermentation of sugar flavor for cigarettes
CN109222215A (en) * 2018-07-04 2019-01-18 红云红河烟草(集团)有限责任公司 Processing method for reducing viscosity of sugar flavor monomer for cigarettes and promoting absorption through high-pressure homogenization
CN109222215B (en) * 2018-07-04 2021-07-16 红云红河烟草(集团)有限责任公司 Processing method for reducing viscosity of sugar flavor monomer for cigarettes and promoting absorption through high-pressure homogenization
CN109022150B (en) * 2018-07-04 2021-09-21 红云红河烟草(集团)有限责任公司 High-pressure sterilization filtering method for preventing fermentation of sugar flavor for cigarettes
CN110133171A (en) * 2019-05-28 2019-08-16 红云红河烟草(集团)有限责任公司 Method for improving flavor components of natural spice for cigarettes and identification method thereof
CN113876018A (en) * 2021-10-21 2022-01-04 湖北中烟工业有限责任公司 Preparation method of special slice for homogenizing and heating cigarettes
CN113876018B (en) * 2021-10-21 2023-01-31 湖北中烟工业有限责任公司 Preparation method of special slice for homogenizing and heating cigarettes

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Application publication date: 20171201