CN107418714A - A kind of method that caryophyllus oil is extracted in the medicinal material from cloves - Google Patents

A kind of method that caryophyllus oil is extracted in the medicinal material from cloves Download PDF

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Publication number
CN107418714A
CN107418714A CN201710295603.2A CN201710295603A CN107418714A CN 107418714 A CN107418714 A CN 107418714A CN 201710295603 A CN201710295603 A CN 201710295603A CN 107418714 A CN107418714 A CN 107418714A
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CN
China
Prior art keywords
minutes
cloves
immersion
extracted
caryophyllus oil
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710295603.2A
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Chinese (zh)
Inventor
李芹
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Food Co Ltd Anhui Nong Ankang
Original Assignee
Food Co Ltd Anhui Nong Ankang
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Food Co Ltd Anhui Nong Ankang filed Critical Food Co Ltd Anhui Nong Ankang
Priority to CN201710295603.2A priority Critical patent/CN107418714A/en
Publication of CN107418714A publication Critical patent/CN107418714A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00Production of fats or fatty oils from raw materials
    • C11B1/02Pretreatment
    • C11B1/04Pretreatment of vegetable raw material
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00Production of fats or fatty oils from raw materials
    • C11B1/12Production of fats or fatty oils from raw materials by melting out
    • C11B1/16Production of fats or fatty oils from raw materials by melting out with steam

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

A kind of method that caryophyllus oil is extracted in medicinal material from cloves, is related to Chinese medicine processing technique field, it is characterised in that:Comprise the following steps, selection material, cleaning material, material processing.The inventive method is reasonable, easy to operate, product content is high.

Description

A kind of method that caryophyllus oil is extracted in the medicinal material from cloves
Technical field
The present invention relates to Chinese medicine processing technique field, and in particular to the side of caryophyllus oil is extracted in a kind of medicinal material from cloves Method.
Background technology
Cloves is also known as clove tree, Myrtaceae Eugenia, is aiphyllium.Main product is in Madagascar, India Ni Xi Asia, Tanzania, Malaysia, Zanzibar, India, Hainan, the Yunnan of Vietnam and China.Be dried flower flower bud using part, Stem, leaf.
And main component is eugenol in orienting, the oil yield of caryophyllus oil is not high when the method for many extractions uses, and And the content of eugenol is also low, it is easy for causing substantial amounts of waste and loss.
The content of the invention
The technical problems to be solved by the invention be to overcome existing technological deficiency provide a kind of method rationally, operation side Just the method that caryophyllus oil, is extracted in a kind of high medicinal material from cloves of product content.
The technical problems to be solved by the invention are realized using following technical scheme:
A kind of method that caryophyllus oil is extracted in the medicinal material from cloves, it is characterised in that:Comprise the following steps,
Step 1: selection material:Select no snake, the rotten plant that grows fine;
Step 2: cleaning material:
I rinses the material chosen with clear water well, then stands and filters off surface moisture;
Material after cutting is put into immersion 10-15 minutes in medical saline by II, then stands 30 minutes;
Material after standing is put into food steamer stifling 15-25 minutes by III, is stood 10 minutes after taking-up, is placed into 50-65 DEG C roasting plant in toast 20-30 minutes;
Material after baking is removed and placed into immersion 10-15 minutes in pure water by IV;
Step 3: material is processed:
I takes out the material after immersion, then the moisture on naturally dry surface, and material is used to pH=1 sulfuric acid solution Middle immersion 2 hours, then removes acid solution;
II distills material using traditional steam distillation.
Beneficial effects of the present invention are:1st, volatile oil oil yield improves about 10%;
2nd, eugenol content improves 3.5-4.5%;
Main component is eugenol in cloves, the cloves medicinal material after acid soak, and eugenol is dissociated by composition, is extracted Oil yield and eugenol content are higher afterwards.
Embodiment
In order that the technical means, the inventive features, the objects and the advantages of the present invention are easy to understand, enter below One step illustrates the present invention.
A kind of method that caryophyllus oil is extracted in the medicinal material from cloves, it is characterised in that:Comprise the following steps,
Step 1: selection material:Select no snake, the rotten plant that grows fine;
Step 2: cleaning material:
I rinses the material chosen with clear water well, then stands and filters off surface moisture;
Material after cutting is put into immersion 10-15 minutes in medical saline by II, then stands 30 minutes;
Material after standing is put into food steamer stifling 15-25 minutes by III, is stood 10 minutes after taking-up, is placed into 50-65 DEG C roasting plant in toast 20-30 minutes;
Material after baking is removed and placed into immersion 10-15 minutes in pure water by IV;
Step 3: material is processed:
I takes out the material after immersion, then the moisture on naturally dry surface, and material is used to pH=1 sulfuric acid solution Middle immersion 2 hours, then removes acid solution;
II distills material using traditional steam distillation.
The general principle and principal character and advantages of the present invention of the present invention has been shown and described above.The technology of the industry Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the simply explanation described in above-described embodiment and specification is originally The principle of invention, without departing from the spirit and scope of the present invention, various changes and modifications of the present invention are possible, these changes Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its Equivalent thereof.

Claims (1)

1. the method for caryophyllus oil is extracted in a kind of medicinal material from cloves, it is characterised in that:Comprise the following steps,
Step 1: selection material:Select no snake, the rotten plant that grows fine;
Step 2: cleaning material:
I rinses the material chosen with clear water well, then stands and filters off surface moisture;
Material after cutting is put into immersion 10-15 minutes in medical saline by II, then stands 30 minutes;
Material after standing is put into food steamer stifling 15-25 minutes by III, is stood 10 minutes after taking-up, is placed into 50-65 DEG C 20-30 minutes are toasted in roasting plant;
Material after baking is removed and placed into immersion 10-15 minutes in pure water by IV;
Step 3: material is processed:
I takes out the material after immersion, then the moisture on naturally dry surface, and material is used in pH=1 sulfuric acid solution and soaked Bubble 2 hours, then removes acid solution;
II distills material using traditional steam distillation.
CN201710295603.2A 2017-04-28 2017-04-28 A kind of method that caryophyllus oil is extracted in the medicinal material from cloves Pending CN107418714A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710295603.2A CN107418714A (en) 2017-04-28 2017-04-28 A kind of method that caryophyllus oil is extracted in the medicinal material from cloves

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710295603.2A CN107418714A (en) 2017-04-28 2017-04-28 A kind of method that caryophyllus oil is extracted in the medicinal material from cloves

Publications (1)

Publication Number Publication Date
CN107418714A true CN107418714A (en) 2017-12-01

Family

ID=60425276

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201710295603.2A Pending CN107418714A (en) 2017-04-28 2017-04-28 A kind of method that caryophyllus oil is extracted in the medicinal material from cloves

Country Status (1)

Country Link
CN (1) CN107418714A (en)

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1857414A (en) * 2006-03-27 2006-11-08 福州屏山制药有限公司 Volatile clove oil and its process for producing medicine composition
CN103819317A (en) * 2014-02-17 2014-05-28 王喜军 Method for preparing eugenol from clove oil plant

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1857414A (en) * 2006-03-27 2006-11-08 福州屏山制药有限公司 Volatile clove oil and its process for producing medicine composition
CN103819317A (en) * 2014-02-17 2014-05-28 王喜军 Method for preparing eugenol from clove oil plant

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
周勰等: "《医药化学实验》", 31 August 2014, 中山大学出版社 *

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Application publication date: 20171201