CN107412115A - 一种果冻状粉底及其制备方法 - Google Patents

一种果冻状粉底及其制备方法 Download PDF

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CN107412115A
CN107412115A CN201710069243.4A CN201710069243A CN107412115A CN 107412115 A CN107412115 A CN 107412115A CN 201710069243 A CN201710069243 A CN 201710069243A CN 107412115 A CN107412115 A CN 107412115A
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iron oxide
foundation cream
dimethyl silicone
silicone polymer
jelly
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李继承
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Suzhou Ante Cosmetics Ltd By Share Ltd
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Abstract

本发明公开了一种果冻状粉底及其制备方法,该粉底包含以下组分:二氧化钛、氧化铁黄、氧化铁红、氧化铁黑、珍珠粉、氧化锌、一氮化硼、硅石、异壬酸异壬酯、氢化聚异丁烯、聚二甲基硅氧烷、环五聚二甲基硅氧烷、霍霍巴籽油、山梨坦倍半油酸酯、生育酚乙酸酯、甘油、丁二醇、尿囊素、透明质酸钠、丙烯酸酯类/C10‑30 烷醇丙烯酸酯交联聚合物、三乙醇胺、PEG‑240/HDI共聚物双‑癸基十四醇聚醚‑20醚、对羟基苯甲酸甲酯、对羟基苯甲酸丙酯、苯氧乙醇、香精、去离子水余量;本发明的果冻状粉底,通过双重乳化技术实现妆效持久、防水、防油、且无油腻感以及保湿、遮瑕、隔离防晒等多种功能于一体;其制备方法可以实现规模量产。

Description

一种果冻状粉底及其制备方法
技术领域
本发明涉及化妆品领域,具体地说是一种果冻状粉底及其制备方法。
背景技术
目前市场上销售的粉底类产品有多种,主要分以下几类:油包水、水包油、全油、全水剂型;而一般来讲,粉底作为彩妆的底妆产品首先也是最重要的要求必须妆效持久防水防汗,其次是各种护肤作用以及调节肤色、速瑕、防晒隔离等等功效。毋庸置疑,水包油和全水剂类型粉底在持久妆效和防水防汗方面很薄弱,在保湿护肤功效方面表现较好;而油包水、全油体系的粉底其在持久妆效防水方面效果较好,但使用肤后感相对较油腻,消费者体验感欠佳,较多护肤功效材料不易添加。
发明内容
针对上述存在的技术问题,本发明的目的是:提出了一种果冻状粉底及其制备方法。
本发明的技术解决方案是这样实现的:一种果冻状粉底,包含以下按质量分数计算的原料组分:二氧化钛8.0%~15.0%、氧化铁黄0%~4.0%、氧化铁红0%~3.0%、氧化铁黑0%~2.0%、珍珠粉0%~2.0%、氧化锌0%~2.0%、一氮化硼0%~2.0%、硅石0%~2.0%、异壬酸异壬酯3.0%~8.0%、氢化聚异丁烯1.0%~5.0%、聚二甲基硅氧烷1.0%~3.0%、环五聚二甲基硅氧烷1.0%~10.0%、霍霍巴籽油1.0%~5.0%、山梨坦倍半油酸酯0.5%~3.0%、生育酚乙酸酯0%~0.5%、甘油2.0%~10.0%、丁二醇2.0%~10.0%、尿囊素0%~0.3%、透明质酸钠0%~0.05%、丙烯酸酯类/C10-30烷醇丙烯酸酯交联聚合物0.05%~0.4%、三乙醇胺0.05%~0.4%、PEG-240/HDI共聚物双-癸基十四醇聚醚-20醚0.5%~5.0%、对羟基苯甲酸甲酯0.1%~0.2%、对羟基苯甲酸丙酯0.05%~0.1%、苯氧乙醇0.4%~0.8%、香精0%~0.2%、去离子水余量。
所述的果冻状粉底其制备方法,包括以下步骤:
(1)将二氧化钛、氧化铁黄、氧化铁红、氧化铁黑、珍珠粉、氧化锌、一氮化硼、硅石高速搅拌分散30秒,重复3次搅拌至分散均匀;
(2)将异壬酸异壬酯、氢化聚异丁烯、聚二甲基硅氧烷、环五聚二甲基硅氧烷、霍霍巴籽油、山梨坦倍半油酸酯、生育酚乙酸酯加入搅拌设备边搅拌边将步骤(1)制得的混合料投入,均质2800rpm,持续10分钟;
(3)将甘油、丁二醇、尿囊素、透明质酸钠、去离子水加入搅拌设备搅拌溶解加热至75~80℃;
(4)将步骤(2)制得的混合料加热至75-80℃,持续搅拌200~300rpm,慢速将步骤(3)制得的混合料投入;
(5)将丙烯酸酯类/C10-30烷醇丙烯酸酯交联聚合物、三乙醇胺、PEG-240/HDI共聚物双-癸基十四醇聚醚-20醚依次投入到余量的去离子水中搅拌均匀,加热至80~85℃。
(6)将步骤(4)制得半成品慢速投入步骤(5)制得的混合料中,200~300rpm搅拌5分钟,然后加入预先溶解好的对羟基苯甲酸甲酯、对羟基苯甲酸丙酯、苯氧乙醇,再投入香精搅拌800~1000rpm,10分钟。
由于上述技术方案的运用,本发明与现有技术相比具有下列优点:
本发明的果冻状粉底,通过双重乳化技术实现妆效持久、防水、防油、且无油腻感以及保湿、遮瑕、隔离防晒等多种功能于一体;其制备方法可以实现规模量产。
具体实施方式
下面结合实施例来进一步说明本发明。
本发明的果冻状粉底,包含以下质量分数的原料组分:二氧化铁8.0%~15.0%、氧化铁黄0%~4.0%、氧化铁红0%~3.0%、氧化铁黑0%~2.0%、珍珠粉0%~2.0%、氧化锌0%~2.0%、一氮化硼0%~2.0%、硅石0%~2.0%、异壬酸异壬酯3.0%~8.0%、氢化聚异丁烯1.0%~5.0%、聚二甲基硅氧烷1.0%~3.0%、环五聚二甲基硅氧烷1.0%~10.0%、霍霍巴籽油1.0%~5.0%、山梨坦倍半油酸酯0.5%~3.0%、生育酚乙酸酯0%~0.5%、甘油2.0%~10.0%、丁二醇2.0%~10.0%、尿囊素0%~0.3%、透明质酸钠0%~0.05%、丙烯酸(酯)类/C10-30烷醇丙烯酸酯交联聚合物0.05%-0.4%、三乙醇胺0.05%~0.4%、PEG-240/HDI共聚物双-癸基十四醇聚醚-20醚0.5%~5.0%,对羟基苯甲酸甲酯0.1%~0.2%、对羟基苯甲酸丙酯0.05%~0.1%、苯氧乙醇0.4%~0.8%、香精0%~0.2%、去离子水余量。
实施例1-5的组分含量如下表所示:
其中,各组分单位为百分比,每个实施例中的配方各原料总和为100%,组分含量为0即为添加该组分。
上述实施例1-5的果冻状粉底均按照如下方法制备:
(1)将二氧化钛、氧化铁黄、氧化铁红、氧化铁黑、珍珠粉,氧化锌、一氮化硼、硅石高速搅拌分散30秒,重复3次搅拌至分散均匀;
(2)将异壬酸异壬酯、氢化聚异丁烯、聚二甲基硅氧烷、环五聚二甲基硅氧烷、霍霍巴籽油、山梨坦倍半油酸酯、生育酚乙酸酯加入搅拌设备边搅拌边将步骤(1)制得的混合料投入,均质2800rpm,持续10分钟;
(3)将甘油、丁二醇、尿囊素、透明质酸钠、去离子水加入搅拌设备搅拌溶解加热至75=80℃;
(4)将步骤(2)制得的混合料加热至75~80℃,持续搅拌200~300rpm,慢速将步骤(3)制得的混合料投入;
(5)将丙烯酸(酯)类/C10-30烷醇丙烯酸酯交联聚合物、三乙醇胺、PEG-240/HDI共聚物双~癸基十四醇聚醚-20醚依次投入到余量的去离子水中搅拌均匀,加热至80~85℃。
(6)将步骤(4)制得半成品慢速投入步骤(5)制得的混合料中,200~300rpm搅拌5分钟,然后加入预先溶解好的对羟基苯甲酸甲酯、对羟基苯甲酸丙酯、苯氧乙醇,再投入香精搅拌800~1000rpm,10分钟。
上述实施例只为说明本发明的技术构思及特点,其目的在于让熟悉此项技术的人士能够了解本发明的内容并加以实施,并不能以此限制本发明的保护范围,凡根据本发明精神实质所作的等效变化或修饰,都应涵盖在本发明的保护范围内。

Claims (2)

1.一种果冻状粉底,其特征在于,包含以下按质量分数计算的原料组分:二氧化钛8.0%~15.0%、氧化铁黄0%~4.0%、氧化铁红0%~3.0%、氧化铁黑0%~2.0%、珍珠粉0%~2.0%、氧化锌0%~2.0%、一氮化硼0%~2.0%、硅石0%~2.0%、异壬酸异壬酯3.0%~8.0%、氢化聚异丁烯1.0%~5.0%、聚二甲基硅氧烷1.0%~3.0%、环五聚二甲基硅氧烷1.0%~10.0%、霍霍巴籽油1.0%~5.0%、山梨坦倍半油酸酯0.5%~3.0%、生育酚乙酸酯0%~0.5%、甘油2.0%~10.0%、丁二醇2.0%~10.0%、尿囊素0%~0.3%、透明质酸钠 0%~0.05%、丙烯酸酯类/C10-30 烷醇丙烯酸酯交联聚合物0.05%~0.4%、三乙醇胺0.05%~0.4%、PEG-240/HDI 共聚物双-癸基十四醇聚醚-20 醚0.5%~5.0%、对羟基苯甲酸甲酯0.1%~0.2%、对羟基苯甲酸丙酯0.05%~0.1%、苯氧乙醇0.4%~0.8%、香精0%~0.2%、去离子水余量。
2.一种如权利要求1所述的果冻状粉底的制备方法,其特征在于包括以下步骤:
(1)将二氧化钛、氧化铁黄、氧化铁红、氧化铁黑、珍珠粉、氧化锌、一氮化硼、硅石高速搅拌分散30秒,重复3次搅拌至分散均匀;
(2)将异壬酸异壬酯、氢化聚异丁烯、聚二甲基硅氧烷、环五聚二甲基硅氧烷、霍霍巴籽油、山梨坦倍半油酸酯、生育酚乙酸酯加入搅拌设备边搅拌边将步骤(1)制得的混合料投入,均质2800rpm,持续10分钟;
(3)将甘油、丁二醇、尿囊素、透明质酸钠、去离子水加入搅拌设备搅拌溶解加热至75~80℃;
(4)将步骤(2)制得的混合料加热至75~80℃,持续搅拌200~300rpm,慢速将步骤(3)制得的混合料投入;
(5)将丙烯酸酯类/C10-30 烷醇丙烯酸酯交联聚合物、三乙醇胺、PEG-240/HDI 共聚物双-癸基十四醇聚醚-20 醚依次投入到余量的去离子水中搅拌均匀,加热至80~85℃;
(6)将步骤(4)制得半成品慢速投入步骤(5)制得的混合料中,200~300rpm搅拌5分钟,然后加入预先溶解好的对羟基苯甲酸甲酯、对羟基苯甲酸丙酯、苯氧乙醇,再投入香精搅拌800~1000rpm,10分钟。
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