CN107412040A - A kind of cape jasmine facemask powder and preparation method thereof - Google Patents

A kind of cape jasmine facemask powder and preparation method thereof Download PDF

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Publication number
CN107412040A
CN107412040A CN201710320222.5A CN201710320222A CN107412040A CN 107412040 A CN107412040 A CN 107412040A CN 201710320222 A CN201710320222 A CN 201710320222A CN 107412040 A CN107412040 A CN 107412040A
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parts
cape jasmine
powder
extract
gardenia
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CN107412040B (en
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罗联钰
邓立青
刘冰清
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Ningde Rong Hai Aquaculture Co Ltd
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Ningde Rong Hai Aquaculture Co Ltd
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/60—Sugars; Derivatives thereof
    • A61K8/602—Glycosides, e.g. rutin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
    • A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73—Polysaccharides
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/84—Products or compounds obtained by lyophilisation, freeze-drying

Abstract

The present invention provides a kind of cape jasmine facemask powder and preparation method thereof, including following raw material:25 35 parts of Fructus Gardeniae iridoid glycoside powder, 5 10 parts of Folium Rhododendri Simsii extract, 15 parts of cape jasmine flower extract, 5 15 parts of Ramulus et Folium Mussaendae Pubescentis extract, 20 23 parts of konjac glucomannan, 12 16 parts of algin, 10 16 parts of collagen.The material of class containing Fructus Gardeniae iridoid glycoside in the facial mask of the present invention, white tea, konjac glucomannan, algin are pure plant component, preservative free, additive, and injury non-stimulated to skin, and it is fragrant with the distinctive milli of white tea, whelk is suppurated, forming cystic acne has the facial mask of good therapeutic effect.

Description

A kind of cape jasmine facemask powder and preparation method thereof
Technical field
The invention belongs to cosmetic field, and in particular to a kind of cape jasmine facemask powder and preparation method thereof.
Background technology
Cape jasmine is Rubiaceae（Rubiaceae）Plant cape jasmine（Gardenia jasminoides Ellis）Drying and ripening Fruit, cape jasmine is widely distributed in China, and plant origin is complicated, and demand is big, is the medicine-food two-purpose product of first announcement of the Ministry of Public Health Kind.And the active ingredient iridoid glycosides material in cape jasmine fruit, hepatic cholagogic, clearing heat and detoxicating, anti-inflammation can be played Effect.Wherein cape jasmine fruit is used as medicine, and cures mainly excess fire toothache, aphthae, eye conjunctivitis, sore swollen toxin etc..Fuding white tea originates in In Fuding Mount Taimu, have that region is unique, technique is natural and the characteristics such as effect is unique.It does not fry and not rubbed, and white tea remains tealeaves Tea Polyphenols, theanine etc., it is more containing Flavonoid substances, and flavones has anti-oxidation function, and white tea antioxidant content contains Amount than green tea is higher by as many as 3 times, can more effectively neutralize free radical, so far still by be the most strong oxidation resistant plant of nature, its Anti-oxidation function, 200 times are higher by than vitamin E, human detoxification and defense function can be improved.The common people in original producton location just have from ancient times With fiery heat-clearing poison anti-inflammatory disease, Ramulus et Folium Mussaendae Pubescentis extract under white tea to causing the bacterial growths such as staphy lococcus infection, streptococcal infection, pneumonia With prevention effect.
Acne is apt to occur in hebetic men and women, is commonly called as whelk, very big to teen-age psychology and social influence, usually gives Patient brings very big pain, if early prevention, early treatment, and it is avoidable, or injury is preferably minimized degree, now The cosmetics containing various chemical addition agents used on the market, the infringement to skin is larger more, have certain danger with Toxic side effect.There are a variety of facial masks on anti-acne on the market at present.Now there are many mask products on the market, add in products material Add and used different preservatives and the different chemical reagent for thering is certain stimulation skin to endanger, and used non-woven fabrics more, and Consumer is troublesome in poeration, and cost is also higher.
It is less specifically for the facial mask of whelk curative effect, in view of the deficiency of existing product.Now with safely, have no side effect, The cape jasmine of green, white tea, gardenia etc. for natural material exploitation it is a kind of it is cheap, safely, have no side effect, have clearing heat and detoxicating, antibacterial Anti-inflammatory has the facial mask of good therapeutic effect to whelk.
The body anti-inflammation feature of cyclic olefine ether terpinyl side like extractive in cape jasmine is mainly utilized, catechin is anti-in white tea Polyphenol component in oxidisability, white tea improves human detoxification and defence effect performance, the moisture retention of algin, antibiotic property, anti-inflammatory, Improve fat secretion performance, the feature such as regulation fat secretion of azalaic acid in azalea is suppurated to whelk, forms capsule The effect of swollen property acne, has played Synergistic, and without adding the preservative of injury skin, property is gentle, stingless to skin Swash effect, safe to use, convenient facial mask.
Compared with prior art, the facemask powder belongs to pure natural formula, without preservative, to human skin action temperature and, It is non-stimulated, have no toxic side effect, securely and reliably；It is convenient to use and carry, and low-carbon environment-friendly, discarded facial mask biology can drop completely Solution；Can clearing heat and detoxicating, anti-inflammation, it is anti-oxidant, improve human detoxification and defence effect performance, whelk suppurated, form capsule Swollen property acne has good therapeutic effect and with the distinctive milli perfume of white tea.
China's cape jasmine cultivated area is big, aboundresources, therefore further carries out inexpensive, high-quality cape jasmine series of products Study on Preparation, realize that the comprehensive development and utilization of cape jasmine is significant.
The content of the invention
It is an object of the invention to provide a kind of cape jasmine facemask powder and preparation method thereof.
To achieve the above object, the present invention adopts the following technical scheme that：
A kind of cape jasmine facemask powder, including following raw material:Fructus Gardeniae iridoid glycoside powder 25-35 parts, Folium Rhododendri Simsii extract 5- 10 parts, cape jasmine flower extract 1-5 parts, Ramulus et Folium Mussaendae Pubescentis extract 5-15 parts, konjac glucomannan 20-23 parts, algin 12-16 parts, collagen 10-16 parts.
Preferably, the facemask powder includes following raw material:30 parts of Fructus Gardeniae iridoid glycoside powder, azalea extraction 8 parts of thing, 3 parts of cape jasmine flower extract, 10 parts of Ramulus et Folium Mussaendae Pubescentis extract, 22 parts of konjac glucomannan, 14 parts of algin, 13 parts of collagen.
Described Fructus Gardeniae iridoid glycoside powder, preparation method thereof is：
（1）It is lyophilized：High-quality cape jasmine and gardenia are selected, cape jasmine and gardenia are separately immersed in 0.1wt.% food-grade peroxide Change in hydrogen solution, soak 4~6min, drained away the water after being rinsed well with clear water, by pre-treatment good cape jasmine and gardenia Respectively at lyophilized in vacuum freeze drier, it is desirable to which cape jasmine, gardenia moisture are below 10% after lyophilized；
（2）Broken shell：By cape jasmine broken shell, cape jasmine shell is removed；
（3）Ungrease treatment：The cape jasmine after broken shell is taken, by the sieve of 10-18 mesh after crushing, carbon dioxide is then put in and surpasses De-oiling is carried out in critical extraction kettle, carbon dioxide supercritical extraction parameter is：Extracting pressure 25-30MPa, extract preheater temperature 40-45 DEG C, carbon dioxide flow 600-800L/H are set, separating pressure 10MPa, 50-55 DEG C of separation temperature, disengaging time 2 are small When, the crude fat content of the cape jasmine after de-oiling is less than 1.0%；
（4）Ultramicro grinding：Cape jasmine through carbon dioxide supercritical extraction degreasing and lyophilized gardenia together through ultramicro grinding extremely 350-500 mesh, obtains gardenia powder；
（5）Iridoid glycosides extracts：Gardenia powder and the solid-liquid mass ratio of edible ethanol 1：（5~8）, microwave power be 500~ 2000w, 40-50 DEG C of Extracting temperature, extract 40-60min；
（6）Clarification, filtration treatment：The good solution centrifugal filtering of Microwave Extraction, takes supernatant, add final concentration of 0.06~ 0.1wt.% pectases, 0.03~0.05 wt.% chitosans and 1.0~2.0 wt.% honey carry out composite clarification, temperature 40-50 DEG C processing and is filtered 3h；
（7）Concentration：Take step（6）Supernatant, in vacuum 100kPa, the lower concentration of 50~55 DEG C of temperature, density 1.2~1.4, Obtain iridoid glycosides condensed cream；
（8）It is lyophilized：Iridoid glycosides condensed cream is in vacuum pressure 50-100Pa, -45 DEG C of temperature, lyophilized 25h, iridoid glycoside The moisture ＜ 2% of class extract, prepares Fructus Gardeniae iridoid glycoside powder.Extraction rate reached 75~85%.
Facial mask application method is：Often bag is generally 1.0g.Packaging is opened during use, 100ml, 85 DEG C of hot water are taken, while stirring Mix, while facemask powder is slowly uniformly poured into hot water.Then stir to product powder and pour into diaphragm plate after fully dissolving, be cooled to Type is facial mask, and facial mask is applied into note in face, stops 20-30 minutes.
The advantage of the invention is that：
1. the present invention is suppurated to whelk, formation cystic acne is evident in efficacy and its composition is pure plant component, no anti-corrosion Agent, additive, and injury non-stimulated to skin.Cyclic olefine ether terpinyl side like extractive has the function that body anti-inflammation in cape jasmine, can Press down a variety of germs for causing whelk of going out；Azalaic acid in azalea has regulation fat secretion, suppresses seborrheica sebum, dispels Acne, suppress dyskeratosis process and the whitening spot-removing effect of epidermis；Algin has moisture retention, antibiotic property, anti-aging, anti- Synthesis that is scorching, improving fat secretion, suppress melanin in skin, reduces the generation of pigment spot；Catechin has anti-in white tea Oxidisability can strengthen skin resistance, can alleviate aging；Polyphenol component in white tea, human detoxification and defence work(can be improved Effect；Collagen has moisture retention, reparation and skin lightening, improves the metabolism of Skin Cell, alleviates aging.Konjac glucomannan have into Film, it is not required to fruit fibre, non-woven fabrics etc. and does medium, the efficiency factor of facial mask will not lose because of face paper；
3rd, product of the present invention possesses good moisture-keeping function, easy to use, and low-carbon environment-friendly, and discarded facial mask can be completely biological Degraded.
4th, Fructus Gardeniae iridoid glycoside class material is contained in facial mask of the invention, white tea, konjac glucomannan, algin are pure plant Composition, preservative free, and injury non-stimulated to skin, and it is fragrant with the distinctive milli of white tea, whelk is suppurated, formed Cystic Acne has the facial mask of good therapeutic effect.
Embodiment
Embodiment 1
A kind of cape jasmine facemask powder, including following raw material:30 parts of Fructus Gardeniae iridoid glycoside powder, 8 parts of Folium Rhododendri Simsii extract, Cape jasmine Sub- 3 parts of flower extract, 10 parts of Ramulus et Folium Mussaendae Pubescentis extract, 22 parts of konjac glucomannan, 14 parts of algin, 13 parts of collagen.
Described Fructus Gardeniae iridoid glycoside powder, preparation method thereof is：
（1）It is lyophilized：High-quality cape jasmine and gardenia are selected, cape jasmine and gardenia are separately immersed in 0.1wt.% food-grade peroxide Change in hydrogen solution, soak 5min, drained away the water after being rinsed well with clear water, by the good cape jasmine of pre-treatment and gardenia respectively at Freezed in vacuum freeze drier, cape jasmine, gardenia moisture are 8% after freezing；
（2）Broken shell：By cape jasmine broken shell, cape jasmine shell is removed；
（3）Ungrease treatment：The cape jasmine after broken shell is taken, by the sieve of 15 mesh after crushing, is then put in that carbon dioxide is super to be faced De-oiling is carried out in boundary's extraction kettle, carbon dioxide supercritical extraction parameter is：Extracting pressure 28MPa, extraction preheater temperature setting 43 DEG C, carbon dioxide flow 700L/H, separating pressure 10MPa, 53 DEG C of separation temperature, disengaging time 2 hours, the Cape jasmine after de-oiling The crude fat content of son is less than 1.0%；
（4）Ultramicro grinding：Cape jasmine and lyophilized gardenia through carbon dioxide supercritical extraction degreasing are again through ultramicro grinding to 400 Mesh, obtain gardenia powder；
（5）Iridoid glycosides extracts：Gardenia powder and the solid-liquid mass ratio of edible ethanol 1：7, microwave power 1000w, extraction Temperature 45 C, extract 50min；
（6）Clarification, filtration treatment：The good solution centrifugal filtering of Microwave Extraction, takes supernatant, adds final concentration of pectase 0.06%th, chitosan 0.03% and honey 1.0% carry out composite clarification, and temperature 45 C processing 3h is simultaneously filtered；
（7）Concentration：Take step（6）Supernatant, in vacuum 100kPa, the lower concentration of 52 DEG C of temperature, density 1.2, obtain cyclenes Ether terpene glycoside condensed cream；
（8）It is lyophilized：Iridoid glycosides condensed cream carries in vacuum pressure 80Pa, -45 DEG C of temperature, lyophilized 25h, iridoid glycosides The moisture 1% of thing is taken, prepares Fructus Gardeniae iridoid glycoside powder.Extraction rate reached 85%.
Embodiment 2
A kind of cape jasmine facial mask, including following raw material:25 parts of Fructus Gardeniae iridoid glycoside powder, Folium Rhododendri Simsii extract freeze-dried powder 5 Part, 1 part of cape jasmine flower extract, 5 parts of Ramulus et Folium Mussaendae Pubescentis extract, 20 parts of konjac glucomannan, 12 parts of algin, 10 parts of collagen.
Described Fructus Gardeniae iridoid glycoside powder, preparation method thereof is：
（1）It is lyophilized：High-quality cape jasmine and gardenia are selected, cape jasmine and gardenia are separately immersed in 0.1wt.% food-grade peroxide Change in hydrogen solution, soak 4 min, drained away the water after being rinsed well with clear water, the good cape jasmine of pre-treatment and gardenia are distinguished Freezed in vacuum freeze drier, it is desirable to which cape jasmine, gardenia moisture are below 10% after lyophilized；
（2）Broken shell：By cape jasmine broken shell, cape jasmine shell is removed；
（3）Ungrease treatment：The cape jasmine after broken shell is taken, by the sieve of 10 mesh after crushing, is then put in that carbon dioxide is super to be faced De-oiling is carried out in boundary's extraction kettle, carbon dioxide supercritical extraction parameter is：Extracting pressure 25MPa, extraction preheater temperature setting 40 DEG C, carbon dioxide flow 600L/H, separating pressure 10MPa, 50 DEG C of separation temperature, disengaging time 2 hours, the Cape jasmine after de-oiling The crude fat content of son is less than 1.0%；
（4）Ultramicro grinding：Cape jasmine through carbon dioxide supercritical extraction degreasing and lyophilized gardenia together through ultramicro grinding extremely 350 mesh, obtain gardenia powder；
（5）Iridoid glycosides extracts：Gardenia powder and the solid-liquid mass ratio of edible ethanol 1：5, microwave power 500w, extraction temperature 40 DEG C of degree, extract 40min；
（6）Clarification, filtration treatment：The good solution centrifugal filtering of Microwave Extraction, takes supernatant, adds final concentration of pectase 0.8%th, chitosan 0.04% and honey 1.5% carry out composite clarification, and 40 DEG C of processing 3h of temperature are simultaneously filtered；
（7）Concentration：Take step（6）Supernatant, in vacuum 100kPa, the lower concentration of temperature 50 C, density 1.3, obtain cyclenes Ether terpene glycoside condensed cream；
（8）It is lyophilized：Iridoid glycosides condensed cream carries in vacuum pressure 50Pa, -45 DEG C of temperature, lyophilized 25h, iridoid glycosides The moisture 1% of thing is taken, prepares Fructus Gardeniae iridoid glycoside powder.Extraction rate reached 75%.
Embodiment 3
A kind of cape jasmine facial mask, including following raw material:35 parts of Fructus Gardeniae iridoid glycoside powder, Folium Rhododendri Simsii extract freeze-dried powder 10 parts, 5 parts of cape jasmine flower extract, 15 parts of Ramulus et Folium Mussaendae Pubescentis extract, 23 parts of konjac glucomannan, 16 parts of algin, 16 parts of collagen.
Described Fructus Gardeniae iridoid glycoside powder, preparation method thereof is：
（1）It is lyophilized：High-quality cape jasmine and gardenia are selected, cape jasmine and gardenia are separately immersed in 0.1wt.% food-grade peroxide Change in hydrogen solution, soak 6min, drained away the water after being rinsed well with clear water, by the good cape jasmine of pre-treatment and gardenia respectively at Freezed in vacuum freeze drier, it is desirable to which cape jasmine, gardenia moisture are below 10% after lyophilized；
（2）Broken shell：By cape jasmine broken shell, cape jasmine shell is removed；
（3）Ungrease treatment：The cape jasmine after broken shell is taken, by the sieve of 18 mesh after crushing, is then put in that carbon dioxide is super to be faced De-oiling is carried out in boundary's extraction kettle, carbon dioxide supercritical extraction parameter is：Extracting pressure 30MPa, extraction preheater temperature setting 45 DEG C, carbon dioxide flow 800L/H, separating pressure 10MPa, 55 DEG C of separation temperature, disengaging time 2 hours, the Cape jasmine after de-oiling The crude fat content of son is less than 1.0%；
（4）Ultramicro grinding：Cape jasmine through carbon dioxide supercritical extraction degreasing and lyophilized gardenia together through ultramicro grinding extremely 500 mesh, obtain gardenia powder；
（5）Iridoid glycosides extracts：Gardenia powder and the solid-liquid mass ratio of edible ethanol 1：8, microwave power 2000w, extraction Temperature 50 C, extract 60min；
（6）Clarification, filtration treatment：The good solution centrifugal filtering of Microwave Extraction, takes supernatant, adds final concentration of pectase 0.1%th, chitosan 0.05% and honey 2.0% carry out composite clarification, and temperature 50 C processing 3h is simultaneously filtered；
（7）Concentration：Take step（6）Supernatant, in vacuum 100kPa, the lower concentration of 55 DEG C of temperature, density 1.5, obtain cyclenes Ether terpene glycoside condensed cream；
（8）It is lyophilized：Iridoid glycosides condensed cream is in vacuum pressure 100Pa, -45 DEG C of temperature, lyophilized 25h, iridoid glycosides The moisture 1% of extract, prepares Fructus Gardeniae iridoid glycoside powder.Extraction rate reached 80%.
Application Example
Test method：Volunteer trial person 40, the age, mainly student and office civilian, men and women each 20 in 16-25 one full year of life There is different degrees of acne in name, face position, and face has different degrees of acne and inflammation papule, by with the facemask powder of the invention For improving skin of face situation.Every night by 1 bag facemask powder, takes 100ml, 85 DEG C of hot water, side stirring, while facemask powder Slowly uniformly pour into hot water.Then stir to product powder and diaphragm plate is poured into after fully dissolving, it is facial mask to be cooled and shaped, will Facial mask applies note in face, stops 20-30 minutes.Effect criterion refers to effective, effective and invalid Three Standards：It is effective to be Related symptoms are relieved；Effectively alleviate for related symptoms；Invalid is that symptom is unchanged.
Result of the test：After most continuous uses 7 days, related symptoms are eased, and are continuing with 15 days, symptom substantially changes It is kind.In 40 in clinical test, effective 30 people, effective 7 people, invalid 3 people, total effective rate 92.5%.It can be seen that the facemask powder For acne, acne and the inflammation papule patient of face there is certain skin of face that improves to act on
Test typical case
Mr. Wang, male 19 years old, student, severe acne, face have more acne and inflammation papule.Use the facemask powder 10 days, Disease papule and warts are clearly better, and persistently using after 20 days, inflammation papule disappears, as long as a small amount of acne, recovery from illness, have no any pair Effect.
Year certain, female 25 years old, civilian, moderate acne, face have more acne and inflammation papule.The facemask powder 7 is used My god, disease papule and warts are clearly better, and persistently using after 15 days, inflammation papule disappears, as long as a small amount of acne, recovery from illness, have no and appoint What side effect.
Pond, female 18 years old, student, mild acne, face have a small amount of acne and inflammation papule.The facemask powder 5 is used Everyday, disease papule is clearly better, and persistently using after 10 days, inflammation papule is wholly absent, and recovery from illness, has no any side effect.
The foregoing is only presently preferred embodiments of the present invention, all equivalent changes done according to scope of the present invention patent with Modification, it should all belong to the covering scope of the present invention.

Claims (3)

  1. A kind of 1. cape jasmine facemask powder, it is characterised in that：The facemask powder includes following raw material:Fructus Gardeniae iridoid glycoside Powder 25-35 parts, Folium Rhododendri Simsii extract 5-10 parts, cape jasmine flower extract 1-5 parts, Ramulus et Folium Mussaendae Pubescentis extract 5-15 parts, konjac glucomannan 20-23 Part, algin 12-16 parts, collagen 10-16 parts.
  2. A kind of 2. cape jasmine facemask powder according to claim 1, it is characterised in that：It is former that the facial mask includes following parts by weight Material:30 parts of Fructus Gardeniae iridoid glycoside powder, 8 parts of Folium Rhododendri Simsii extract, 3 parts of cape jasmine flower extract, 10 parts of Ramulus et Folium Mussaendae Pubescentis extract, konjaku 22 parts of glue, 14 parts of algin, 13 parts of collagen.
  3. A kind of 3. cape jasmine facemask powder according to claim 1, it is characterised in that：It is prepared by described Fructus Gardeniae iridoid glycoside powder Method is：
    （1）It is lyophilized：High-quality cape jasmine and gardenia are selected, cape jasmine and gardenia are separately immersed in 0.1wt.% food-grade peroxide Change in hydrogen solution, soak 4~6min, drained away the water after being rinsed well with clear water, by pre-treatment good cape jasmine and gardenia Respectively at lyophilized in vacuum freeze drier, it is desirable to which cape jasmine, gardenia moisture are below 10% after lyophilized；
    （2）Broken shell：By cape jasmine broken shell, cape jasmine shell is removed；
    （3）Ungrease treatment：The cape jasmine after broken shell is taken, by the sieve of 10-18 mesh after crushing, carbon dioxide is then put in and surpasses De-oiling is carried out in critical extraction kettle, carbon dioxide supercritical extraction parameter is：Extracting pressure 25-30MPa, extract preheater temperature 40-45 DEG C, carbon dioxide flow 600-800L/H are set, separating pressure 10MPa, 50-55 DEG C of separation temperature, disengaging time 2 are small When, the crude fat content of the cape jasmine after de-oiling is less than 1.0%；
    （4）Ultramicro grinding：Cape jasmine through carbon dioxide supercritical extraction degreasing and lyophilized gardenia together through ultramicro grinding extremely 350-500 mesh, obtains gardenia powder；
    （5）Iridoid glycosides extracts：Gardenia powder and the solid-liquid mass ratio of edible ethanol 1：（5~8）, microwave power be 500~ 2000w, 40-50 DEG C of Extracting temperature, extract 40-60min；
    （6）Clarification, filtration treatment：The good solution centrifugal filtering of Microwave Extraction, takes supernatant, add final concentration of 0.06~ 0.1wt.% pectases, 0.03~0.05 wt.% chitosans and 1.0~2.0 wt.% honey carry out composite clarification, temperature 40-50 DEG C processing and is filtered 3h；
    （7）Concentration：Take step（6）Supernatant, in vacuum 100kPa, the lower concentration of 50~55 DEG C of temperature, density 1.2~1.4, Obtain iridoid glycosides condensed cream；
    （8）It is lyophilized：Iridoid glycosides condensed cream is in vacuum pressure 50-100Pa, -45 DEG C of temperature, lyophilized 25h, iridoid glycoside The moisture ＜ 2% of class extract, prepares Fructus Gardeniae iridoid glycoside powder.
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN117797055A (en) * 2024-02-29 2024-04-02 江西瑞秀朗科技有限公司 Compound essential oil for improving skin aging and skin care product composition containing compound essential oil

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