CN107384740A - The preparation method of golden clock root chrysanthemum stamen health-care vinegar - Google Patents

The preparation method of golden clock root chrysanthemum stamen health-care vinegar Download PDF

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Publication number
CN107384740A
CN107384740A CN201710809128.6A CN201710809128A CN107384740A CN 107384740 A CN107384740 A CN 107384740A CN 201710809128 A CN201710809128 A CN 201710809128A CN 107384740 A CN107384740 A CN 107384740A
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vinegar
liquid
chrysanthemum
fermentation
health
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CN201710809128.6A
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程龙凤
胡伟
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    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12J—VINEGAR; PREPARATION OR PURIFICATION THEREOF
    • C12J1/00—Vinegar; Preparation or purification thereof
    • C12J1/04—Vinegar; Preparation or purification thereof from alcohol
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
    • A61K36/287—Chrysanthemum, e.g. daisy
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/57—Magnoliaceae (Magnolia family)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/79—Schisandraceae (Schisandra family)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/81—Solanaceae (Potato family), e.g. tobacco, nightshade, tomato, belladonna, capsicum or jimsonweed
    • A61K36/815—Lycium (desert-thorn)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/85—Verbenaceae (Verbena family)

Abstract

The invention discloses a kind of preparation method of golden clock root chrysanthemum stamen health-care vinegar, belong to health-care vinegar manufacture field.It is characterized in that：Manufacturing procedure through pretreatment of raw material, grinding emulsification, anaerobic fermentation, acetic fermentation, extraction, clarification, separation concentration and sterilization.The present invention uses Jin Zhonggen, chrysanthemum stamen as raw material, and after respective pretreatment, ground emulsification, anaerobic fermentation, acetic fermentation, extraction, clarification, separation concentration and the manufacturing procedure sterilized, obtained health-care vinegar is nutritious, unique flavor.The health-care efficacy such as also have dispelling wind, soothing the liver, qi-restoratives moistening lung, strengthening tendons active, it is suitable for people of all ages.

Description

The preparation method of golden clock root chrysanthemum stamen health-care vinegar
Technical field
The present invention relates to a kind of preparation method of health-care vinegar, more particularly, to a kind of making side of golden clock root chrysanthemum stamen health-care vinegar Method.
Background technology
Golden clock root alias pig's feet large bamboo hat with a conical crown and broad brim, beautiful millettia root, beautiful millettia root, hang upside down Jin Zhong, energetically potato.Planted for pulse family pulse family Millettia Thing, beautiful millettia Millettia specisoa Champ.Jin Zhonggen is used as medicine with root, and Main Ingredients and Appearance is protein, starchiness And alkaloid etc..Major function：Qi-restoratives moistening lung, strengthening tendons are active.For lumbar muscle strain, rheumatic arthritis, lung heat, deficiency syndrome of the lung cough are controlled Cough, pulmonary tuberculosis, chronic bronchitis, chronic hepatitis, seminal emission, leukorrhea.Be longer than among the deep and secluded valley of remote mountains, the sweet perfume (or spice) of smell, it is warm-natured and, tool There is establishing-Yang, support kidney qi-restoratives, strengthening tendons is active, the effect of soothing the liver, moistening lung.It is adapted to:Kidney deficiency, vim and vigour are not prosperous, treating rheumatic ostealgia, often cough With acute/chronic bronchitis and smoking and suction kitchen fume personage.
The pistil of chrysanthemum stamen, i.e. chrysanthemum, it can be used as medicine and cure the disease, long term usage or drink chrysanthemum tea can make us long-lived.Song Dynasty poet Soviet Union rut： " Nanyang feverfew has outstanding service, and the more old mans of people are occupied on pool ".Chrysanthemum can make the delicacies of fineness." chrysanthemum meat " is by long-felt A kind of chrysanthemum dish being fabricated to, the delicate pork that it is endured slurry processing by one piece of block with sucrose is processed into, exquisitely carved, just like white It is beautiful.Several chrysanthemum valves are affixed on every piece, drink grease sugar sweet tea of satisfying, its golden color is seen, has and be always or usually as specified in mouth in meat or fish, have meat or fish in element, It is fragrant and sweet oiliness, actually famous dish.Also chrysanthemum fish ball, fried chrysanthemum leaf, chrysanthemum fillet congee, chrysanthemum custard, chrysanthemum wine, chrysanthemum tea etc., these Not only color, smell and taste are all good and nutritious for chrysanthemum meal.Beijing famous " chrysanthemum bowl "（A little chrysanthemums are put in Mutton in hot pot Cooking）, it is light delicious, even more have a distinctive flavour.
The species of in the market health-care vinegar is few, can not meet the needs of in the market, and the product of golden clock root is very single on the market One, it is mainly used in being used as medicine, Jin Zhonggen, chrysanthemum stamen is processed into golden clock root chrysanthemum stamen health-care vinegar, has no pertinent literature report and related production Product list, while also provide a new way for Jin Zhonggen deep processing.
The content of the invention
The technical problem to be solved in the present invention is to provide a kind of preparation method of golden clock root chrysanthemum stamen health-care vinegar, make obtained guarantor Strong vinegar is nutritious, and unique flavor, fragrance is pleasant, also with the health-care efficacy such as diuresis kidney tonifying, the relieving summer-heat that reduces phlegm and internal heat.
The technical scheme adopted by the invention to solve the technical problem is that：
A kind of preparation method of golden clock root chrysanthemum stamen health-care vinegar, it is characterised in that：Through pretreatment of raw material, grinding emulsification, anaerobic fermentation, Acetic fermentation, extraction, clarification, separation concentration and the manufacturing procedure of sterilization, concrete operation step are as follows：
（1）Jin Zhonggen is pre-processed：The rhizome of high-quality drying is selected, adds a little fruit of Chinese magnoliavine, matrimony vine, removal of impurities is cleaned, is immersed in and contains 0.65% citric acid, 0.1% vitamin C, 3% honey the aqueous solution in, per 1L aqueous solution soaking 500g raw materials, immersion After 45min, granulating is crushed, golden clock root grain is made；
（2）Chrysanthemum stamen pre-processes：After chrysanthemum stamen is cleaned, enter in stainless steel cask, add the clear water of 15 times of chrysanthemum stamen weight, keep water temperature 35 DEG C, after soaking 3.5 hours, it is incorporated with the beater of 100 mesh mesh screens and beats into rotten gruel, the rotten material of chrysanthemum stamen is made；
（3）Grinding emulsification：Golden clock root grain and the rotten material of chrysanthemum stamen are pressed 1:0.35 ratio is well mixed, using being segmented colloid mill, First ground with backlash 0.1mm corase grind, the rear emulsification with backlash 0.02mm is ground, and carries out ultra-fine emulsification treatment, and breast is made Change liquid；
（4）Anaerobic fermentation：0.65kg brewer yeast and 1.2kg Glucose Liquid are added into emulsion, after stirring, is added Appropriate drinking water, temperature control are 38 DEG C, anaerobic fermentation 4 days, when the alcoholic strength of wine liquid reaches 10%, fermentation ends, are made Karusen；
（5）Acetic fermentation：With the inoculum concentration of volume ratio 6%, acetic acid bacterium solution is accessed into karusen, is stirred, fermentation temperature 42 DEG C, ferment 15 days, until when vinegar fermented grain acidity reaches 6.5g/100ml, stop fermentation；Filtered using duplex, obtain vinegar liquid and material residue；
（6）Extraction：Material residue is added into 3 times of clear water, carries out microwave abstracting, extracts power 650W, extracts 2 times, 10 minutes every time, closes And obtain extract；Extract and vinegar liquid are remerged, health care vinegar liquid is made；
（7）Clarification：By health care vinegar liquid, low tempertaure storage, centrifugation are gone to precipitate, treat liquid clear, distribute vinegar fragrance i.e. at 2 DEG C Can；
（8）Separation concentration：Using nitrogen flotation method, the vinegar liquid after clarification is put into floatation equipment, carries out separation concentration, is set The volume flow percentage of gas-liquid is 85%, time 5min, finished product vinegar；
（9）Sterilization, packaging：Finished product vinegar with vial seal filling, as finished product immediately after ultraviolet sterilization.
Beneficial effect：The present invention uses Jin Zhonggen, chrysanthemum stamen as raw material, after respective pretreatment, ground emulsification, anaerobism hair Ferment, acetic fermentation, extraction, clarification, separation concentration and the manufacturing procedure of sterilization, obtained health-care vinegar is nutritious, unique flavor, Fragrance is pleasant, suitable for people of all ages also with the health-care efficacy such as dispelling wind, soothing the liver, qi-restoratives moistening lung, strengthening tendons be active, is easy to carry.
Embodiment
Embodiment 1：
A kind of preparation method of golden clock root chrysanthemum stamen health-care vinegar, it is characterised in that：Through pretreatment of raw material, grinding emulsification, anaerobic fermentation, Acetic fermentation, extraction, clarification, separation concentration and the manufacturing procedure of sterilization, concrete operation step are：
（1）Jin Zhonggen is pre-processed：The rhizome of high-quality drying is selected, adds the appropriate fruit of Chinese magnoliavine, cassia seed and haw berry, cleans and removes It is miscellaneous, be immersed in containing 0.35% citric acid, 0.1% vitamin C, 3% honey the aqueous solution in, per 1L aqueous solution soaking 500g raw materials, after soaking 45min, granulating is crushed, golden clock root grain is made；
（2）Chrysanthemum stamen pre-processes：After chrysanthemum stamen is cleaned, a little flower of kudzuvine and chrysanthemum brain tender leaf are added, is entered in stainless steel cask, add chrysanthemum stamen The clear water that 20 times of weight, 35 DEG C of water temperature is kept, after soaking 3.5 hours, be incorporated with the beater of 100 mesh mesh screens and beat into rotten Gruel, the rotten material of chrysanthemum stamen is made；
（3）Grinding emulsification：Golden clock root grain and the rotten material of chrysanthemum stamen are pressed 1:0.25 ratio is well mixed, using being segmented colloid mill, First ground with backlash 0.1mm corase grind, the rear emulsification with backlash 0.02mm is ground, and carries out ultra-fine emulsification treatment, and breast is made Change liquid；
（4）Anaerobic fermentation：0.65kg brewer yeast and 1.2kg Glucose Liquid are added into emulsion, after stirring, is added Appropriate drinking water, temperature control are 38 DEG C, anaerobic fermentation 4 days, when the alcoholic strength of wine liquid reaches 10%, fermentation ends, are made Karusen；
（5）Acetic fermentation：With the inoculum concentration of volume ratio 6%, acetic acid bacterium solution is accessed into karusen, is stirred, fermentation temperature 42 DEG C, ferment 15 days, until when vinegar fermented grain acidity reaches 6.5g/100ml, stop fermentation；Filtered using duplex, obtain vinegar liquid and material residue；
（6）Extraction：Material residue is added into 3 times of clear water, carries out microwave abstracting, extracts power 650W, extracts 2 times, 10 minutes every time, closes And obtain extract；Extract and vinegar liquid are remerged, health care vinegar liquid is made；
（7）Clarification：By health care vinegar liquid, low tempertaure storage, centrifugation are gone to precipitate, treat liquid clear, distribute vinegar fragrance i.e. at 2 DEG C Can；
（8）Separation concentration：Using nitrogen flotation method, the vinegar liquid after clarification is put into floatation equipment, carries out separation concentration, is set The volume flow percentage of gas-liquid is 85%, time 5min, finished product vinegar；
（9）Sterilization, packaging：Finished product vinegar with vial seal filling, as finished product immediately after ultraviolet sterilization.
Embodiment 2：
A kind of preparation method of golden clock root chrysanthemum stamen health-care vinegar, it is characterised in that：Through pretreatment of raw material, grinding emulsification, anaerobic fermentation, Acetic fermentation, extraction, clarification, separation concentration and the manufacturing procedure of sterilization, concrete operation step are：
（1）Jin Zhonggen is pre-processed：The rhizome of high-quality drying is selected, adds a little honey raisin tree, thorny elaeagnus, removal of impurities is cleaned, is immersed in and contains 0.5% citric acid, 0.3% vitamin C, 2% honey the aqueous solution in, per 1L aqueous solution soaking 500g raw materials, immersion After 2h, granulating is crushed, golden clock root grain is made；
（2）Chrysanthemum stamen pre-processes：After chrysanthemum stamen are cleaned, appropriate rosemary leave, Leaves of Glycyrrhiza Uralensis Fisch and robiniae,flos are added, is entered in stainless steel cask, The clear water of 25 times of chrysanthemum stamen weight is added, keeps 38 DEG C of water temperature, after soaking 5 hours, is incorporated with the beater of 80 mesh mesh screens and beats Into rotten gruel, the rotten material of chrysanthemum stamen is made；
（3）Grinding emulsification：Golden clock root grain and the rotten material of chrysanthemum stamen are pressed 1:0.5 ratio is well mixed, using colloid mill was segmented, first Ground with backlash 0.25mm corase grind, the rear emulsification with backlash 0.05mm is ground, and carries out ultra-fine emulsification treatment, and emulsification is made Liquid；
（4）Anaerobic fermentation：0.8kg brewer yeast and 2kg Glucose Liquid are added into emulsion, after stirring, is added suitable Drinking water is measured, temperature control is 42 DEG C, anaerobic fermentation 6 days, when the alcoholic strength of wine liquid reaches 12%, fermentation ends, hair is made Ferment wine with dregs；
（5）Acetic fermentation：With the inoculum concentration of volume ratio 8%, acetic acid bacterium solution is accessed into karusen, is stirred, fermentation temperature 42 DEG C, ferment 15 days, until when vinegar fermented grain acidity reaches 6.5g/100ml, stop fermentation；Filtered using duplex, obtain vinegar liquid and material residue；
（6）Extraction：Material residue is added into 2 times of clear water, carries out microwave abstracting, extracts power 350W, extracts 2 times, 15 minutes every time, closes And obtain extract；Extract and vinegar liquid are remerged, health care vinegar liquid is made；
（7）Clarification：By health care vinegar liquid, low tempertaure storage, centrifugation are gone to precipitate, treat liquid clear, distribute vinegar fragrance i.e. at 5 DEG C Can；
（8）Separation concentration：Using nitrogen flotation method, the vinegar liquid after clarification is put into floatation equipment, carries out separation concentration, is set The volume flow percentage of gas-liquid is 75%, time 8min, finished product vinegar；
（9）Sterilization, packaging：Finished product vinegar with vial seal filling, as finished product immediately after ultraviolet sterilization.
Part that the present invention does not relate to is same as the prior art or can be realized using prior art.

Claims (1)

1. a kind of preparation method of golden clock root chrysanthemum stamen health-care vinegar, it is characterised in that sent out through pretreatment of raw material, grinding emulsification, anaerobism Ferment, acetic fermentation, extraction, clarification, separation concentration and the manufacturing procedure of sterilization, concrete operation step are as follows：
（1）Jin Zhonggen is pre-processed：The rhizome of high-quality drying is selected, adds a little fruit of Chinese magnoliavine, matrimony vine, removal of impurities is cleaned, is immersed in and contains 0.65% citric acid, 0.1% vitamin C, 3% honey the aqueous solution in, per 1L aqueous solution soaking 500g raw materials, immersion After 45min, granulating is crushed, golden clock root grain is made；
（2）Chrysanthemum stamen pre-processes：After chrysanthemum stamen is cleaned, enter in stainless steel cask, add the clear water of 15 times of chrysanthemum stamen weight, keep water temperature 35 DEG C, after soaking 3.5 hours, it is incorporated with the beater of 100 mesh mesh screens and beats into rotten gruel, the rotten material of chrysanthemum stamen is made；
（3）Grinding emulsification：Golden clock root grain and the rotten material of chrysanthemum stamen are pressed 1:0.35 ratio is well mixed, using being segmented colloid mill, First ground with backlash 0.1mm corase grind, the rear emulsification with backlash 0.02mm is ground, and carries out ultra-fine emulsification treatment, and breast is made Change liquid；
（4）Anaerobic fermentation：0.65kg brewer yeast and 1.2kg Glucose Liquid are added into emulsion, after stirring, is added Appropriate drinking water, temperature control are 38 DEG C, anaerobic fermentation 4 days, when the alcoholic strength of wine liquid reaches 10%, fermentation ends, are made Karusen；
（5）Acetic fermentation：With the inoculum concentration of volume ratio 6%, acetic acid bacterium solution is accessed into karusen, is stirred, fermentation temperature 42 DEG C, ferment 15 days, until when vinegar fermented grain acidity reaches 6.5g/100ml, stop fermentation；Filtered using duplex, obtain vinegar liquid and material residue；
（6）Extraction：Material residue is added into 3 times of clear water, carries out microwave abstracting, extracts power 650W, extracts 2 times, 10 minutes every time, closes And obtain extract；Extract and vinegar liquid are remerged, health care vinegar liquid is made；
（7）Clarification：By health care vinegar liquid, low tempertaure storage, centrifugation are gone to precipitate, treat liquid clear, distribute vinegar fragrance i.e. at 2 DEG C Can；
（8）Separation concentration：Using nitrogen flotation method, the vinegar liquid after clarification is put into floatation equipment, carries out separation concentration, is set The volume flow percentage of gas-liquid is 85%, time 5min, finished product vinegar；
（9）Sterilization, packaging：Finished product vinegar with vial seal filling, as finished product immediately after ultraviolet sterilization.
CN201710809128.6A 2017-09-10 2017-09-10 The preparation method of golden clock root chrysanthemum stamen health-care vinegar Withdrawn CN107384740A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108865637A (en) * 2018-08-03 2018-11-23 张俊辉 The production method of Yi Zhong Wen Quince honeysuckle health-care vinegar

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107034114A (en) * 2017-05-22 2017-08-11 芜湖市三山区绿色食品产业协会 The preparation method of fruit of Cherokee rose lotus stamen health-care vinegar

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107034114A (en) * 2017-05-22 2017-08-11 芜湖市三山区绿色食品产业协会 The preparation method of fruit of Cherokee rose lotus stamen health-care vinegar

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
敬松: "《中国花膳与花卉》", 31 January 2013 *
柴瑞震: "《中国现代保健药物食物大全》", 31 August 2007 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108865637A (en) * 2018-08-03 2018-11-23 张俊辉 The production method of Yi Zhong Wen Quince honeysuckle health-care vinegar

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Application publication date: 20171124