CN107384576A - A kind of method that fructus cannabis machine squeezing cake residual oil content is reduced using aqua method - Google Patents
A kind of method that fructus cannabis machine squeezing cake residual oil content is reduced using aqua method Download PDFInfo
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- CN107384576A CN107384576A CN201710766785.7A CN201710766785A CN107384576A CN 107384576 A CN107384576 A CN 107384576A CN 201710766785 A CN201710766785 A CN 201710766785A CN 107384576 A CN107384576 A CN 107384576A
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- machine
- fructus cannabis
- residual oil
- cake
- oil content
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/02—Pretreatment
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/10—Production of fats or fatty oils from raw materials by extracting
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Fats And Perfumes (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention belongs to food processing technology field, more particularly to a kind of method that fructus cannabis machine squeezing cake residual oil content is reduced using aqua method.Comprise the following steps：Weigh a certain amount of fructus cannabis machine and squeeze cake, pulverizer crosses 60 mesh sieves after crushing, and the fructus cannabis machine after sieving squeezes cake powder with deionized water according to 1：46 volume ratio is well mixed, and is heated to 75 85 DEG C, extracts 7.5 8.5h；Fructus cannabis machine after extraction is squeezed into the drying of cake powder, the fructus cannabis machine that residual oil content is 8.1 10.5% is obtained and squeezes cake powder.The present invention reduces the Residual oil of the numb cake of fire using aqua method, have received preferable effect by suitable process conditions and technological effect, greatly reduces residual oil content.
Description
Technical field
It is more particularly to a kind of that fructus cannabis machine squeezing cake Residual oil is reduced using aqua method the invention belongs to food processing technology field
The method of rate.
Background technology
Contain essential fatty acid, phytosterol and chlorophyll, beta carotene, nicotinic acid, folic acid, plant in fiery sesame oil
10 kinds of amino acid necessary to the human body cells such as acid, lecithin.Wherein unsaturated fatty acid content is up to 93%, linoleic acid (ω -6)
Reach 2.4 with the ratio of alpha-linolenic acid (ω -3)：1, it is the grease of great nutrient balance, is assigned " plant docosapentaenoic acid ".Together
When important source material of the fire sesame oil as organic chemical industry, day it is aobvious using it is extensive.Fructus cannabis contains 35% good protein
The human body such as resource, also lecithin, leukotrienes, vitamin and calcium, iron mineral is necessarily micro-.Blood fat can not only be reduced
With cholesterol, pre- preventing thrombosis and treatment heart disease, tonifying middle-Jiao and Qi, relax bowel, improving eyesight liver protection, getting rid of illness lengthens one's life, but also promote
Children and the healthy development of teen-age brain and eyes, also there is very big benefit to the elderly, cardiovascular and cerebrovascular disease can be prevented and treated
And senile dementia and encephalatrophy etc..
The numb cake of fire is as the primary raw material for producing the numb albumen powder of fire, it is desirable to which oil-containing is below 10%, at present using hydraulic cold
Squeezing method takes the fiery numb cake oil-containing of oil to be up to 12.5%, in order to meet the albumen powder export requirement of extraction, it is necessary to without using organic
Oil content is reduced in the case of solvent.
The content of the invention
In order to solve the above-mentioned technical problem, present invention offer is a kind of reduces fructus cannabis machine squeezing cake residual oil content using aqua method
Method, the Residual oil of the numb cake of fire is reduced using aqua method, preferable effect have received by suitable process conditions and technological effect,
Greatly reduce residual oil content.
The present invention is achieved in that a kind of method that fructus cannabis machine squeezing cake residual oil content is reduced using aqua method, including such as
Lower step：
1) weigh a certain amount of fructus cannabis machine and squeeze cake, pulverizer crosses 60 mesh sieves after crushing, and screenings is stand-by；
2) the fructus cannabis machine after being sieved in step 1) is squeezed into cake powder with deionized water according to 1：4-6 volume ratio mixing is equal
It is even, 75-85 DEG C is heated to, extracts 7.5-8.5h；
3) the fructus cannabis machine after being extracted in step 2) is squeezed into the drying of cake powder, obtains the fire fiber crops that residual oil content is 8.1-10.5%
Benevolence machine squeezes cake powder.
Further, the extraction conditions in step 2) is：Fructus cannabis machine after sieving squeeze cake powder and deionized water according to
1：5 volume ratio is well mixed, and is heated to 75 DEG C, extracts 8h, is obtained the fructus cannabis machine that residual oil content is 8.1% and is squeezed cake powder.
Further, the extraction conditions in step 2) is determined by single factor experiment and orthogonal test.
Further, the fructus cannabis machine in step 3) is squeezed cake powder and dried using vacuum drying chamber, 70-80 DEG C of temperature, pressure
Strong 0.08MPa, time 1.8-2.2h.
Further, it is 8.1-10.5% that the fructus cannabis machine prepared by the above method, which squeezes cake powder residual oil content,.
Further, the fructus cannabis machine prepared by the above method squeezes the preparation that cake powder is used for the numb albumen powder of fire.
Compared with prior art, it is an advantage of the current invention that using the aqua method for not adding enzyme, it is situated between without organic solvent
Enter, the feasibility and extraction conditions of the fiery sesame oil of aqua method extraction of being analyzed and researched by experiment of single factor and orthogonal experiment.Operating
On the premise of condition is suitable, aqua method technique can effectively extract grease in cake, the fiery numb cake lighter color of acquisition, and protein contains
Amount is high, and nutritional properties keep good.Orthogonal test obtains optimum process condition：Extraction temperature is 75 DEG C, solid-liquid ratio (body
Product ratio) it is 1：5, extraction times 8hr.
Brief description of the drawings
Fig. 1 represents that residual oil content changes line chart with extraction temperature in single factor experiment；
Fig. 2 represents that residual oil content changes line chart with solid-liquid ratio (volume ratio) in single factor experiment；
Fig. 3 represents that residual oil content changes line chart with extraction time in single factor experiment；
Fig. 4 represents that single factor experiment residual oil content changes line chart with condition.
Embodiment
In order to make the purpose , technical scheme and advantage of the present invention be clearer, with reference to embodiments, to the present invention
It is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not used to
Limit the present invention.
Fiery fiber crops are the oil plants that can be uniquely dissolved in water, and up to more than 90% unrighted acid is contained in fiery sesame oil, is
The grease of great nutrient balance, it is described as " plant docosapentaenoic acid ".In fiery numb cake after fructus cannabis degreasing the content of protein compared with
Height, trace element is abundant, great nutritive value.Fructus cannabis machine squeezes cake and makes fructus cannabis powder at present, and international market demand is very
Greatly.However, albumen powder production requirement raw material machine squeeze cake Residual oil below 10%, and drop Residual oil process must not use it is organic molten
Agent, the press cake Residual oil that domestic fiery sesame oil cold-squeezing obtains at present are usually above 12%.Therefore, in view of fiery sesame oil it is water-soluble
Characteristic, the Residual oil of the numb cake of fire is reduced using aqua method, study suitable process conditions and have received preferable effect with technological effect.
1st, the factor for determining to influence aqua method effect of extracting is with horizontal, and design orthogonal experiment is as shown in the table：
In solid-liquid ratio 1：Under conditions of 4, extraction times 8hr, enter trip temperature single factor experiment, concrete outcome is shown in Fig. 1；
Under conditions of 80 DEG C of temperature, extraction times 8hr, solid-liquid ratio single factor experiment is carried out, concrete outcome is shown in Fig. 2；
In 80 DEG C of temperature, solid-liquid ratio 1：Under conditions of 4, time single factor experiment is stripped, concrete outcome is shown in Fig. 3；
See Fig. 4, by 3 kinds of single factor experiment results in general, residual oil content minimum point is the flex point water of single factor experiment
It is flat, thereby determine that three level values of experiment of single factor.
2nd, orthogonal experiment
2.1, according to experiment of single factor result, find each factor knee-level value, determine the orthogonal side of Three factors-levels
Case, specifically it see the table below：
2.2 range analysis
In range analysis of orthogonal experiment result, aqua method reduce the numb cake of fire residual oil content it is minimum be A1B2C2, residual oil content
8.1%.Corresponding extracting condition is 75 DEG C of temperature, solid-liquid ratio 1：5, extraction time 8 hours.
R values show that aqua method is reduced in the experimentation that fructus cannabis machine squeezes cake residual oil content, the disturbance degree highest (R of solid-liquid ratio
It is worth for 1.04), next to that temperature (R values 0.83), is finally extraction time (R values 0.60).It is indicated above that the water using fiery sesame oil
Molten characteristic is more effective, and solid-liquid ratio directly affects effect of extracting；The influence of temperature is also bigger, the damp and hot denaturation based on protein
Property, high the dropping with protein denaturation and extraction yield of temperature；Influence of the extraction time to technological effect is little, and reaches
Extend time residual oil content after certain effect of extracting no longer to decline.
3rd, conclusion
3.1 find that the water soluble characteristic of fiery sesame oil can by single factor experiment and further orthogonal experiments analysis
So that in terms of it is preferably used in the Residual oil for reducing the numb cake of fire, this process is not destroying the water solubility and trophism of protein
On the basis of effectively carried out, meet fructus cannabis powder make non-solvent method requirement.
3.2 extraction processes are carried out under conditions of normal pressure is without enzyme, and the technological parameter of acquisition is 75 DEG C of temperature, solid-liquid ratio 1：5,
Extraction time 8 hours.Extraction time is partially long in condition, and experiment shows heating to reducing Residual oil with shortening the time without obvious effect
Fruit, this may have certain correlation with the damp and hot denaturation of protein；When increasing solid-liquid ratio (amount of water) to reducing Residual oil and shortening
Between also do not help.
Claims (6)
- A kind of 1. method that fructus cannabis machine squeezing cake residual oil content is reduced using aqua method, it is characterised in that comprise the following steps：1) weigh fructus cannabis machine and squeeze cake, pulverizer crosses 60 mesh sieves after crushing, and screenings is stand-by；2) the fructus cannabis machine after being sieved in step 1) is squeezed into cake powder with deionized water according to 1：4-6 volume ratio is well mixed, 75-85 DEG C is heated to, extracts 7.5-8.5h；3) the fructus cannabis machine after being extracted in step 2) is squeezed into the drying of cake powder, obtains the fructus cannabis machine that residual oil content is 8.1-10.5% Squeeze cake powder.
- 2. the method for fructus cannabis machine squeezing cake residual oil content is reduced using aqua method as claimed in claim 1, it is characterised in that described Extraction conditions in step 2) is：Fructus cannabis machine after sieving squeezes cake powder with deionized water according to 1：5 volume ratio mixing is equal It is even, 75 DEG C are heated to, extracts 8h, the fructus cannabis machine that residual oil content is 8.1% is obtained and squeezes cake powder.
- 3. the method that fructus cannabis machine squeezing cake residual oil content is reduced using aqua method as described in claim 1 or 2 is any, its feature are existed In the extraction conditions in the step 2) is determined by single factor experiment and orthogonal test.
- 4. the method that fructus cannabis machine squeezing cake residual oil content is reduced using aqua method as described in claim 1 or 2 is any, its feature are existed In, the fructus cannabis machine in the step 3) squeezes cake powder is dried using vacuum drying chamber, 70-80 DEG C of temperature, pressure 0.08MPa, Time 1.8-2.2h.
- 5. a kind of method preparation that fructus cannabis machine squeezing cake residual oil content is reduced using any described aqua method of claim 1 or 2 Fructus cannabis machine squeezes cake powder, it is characterised in that it is 8.1-10.5% that the fructus cannabis machine, which squeezes cake powder residual oil content,.
- 6. fructus cannabis machine as claimed in claim 5 squeezes the application of cake powder, it is characterised in that the fructus cannabis machine squeezes cake powder Preparation for the numb albumen powder of fire.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109730288A (en) * | 2019-03-06 | 2019-05-10 | 锦州俏牌生物科技有限公司 | A kind of fire sesame paste production method |
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| CN1561829A (en) * | 2004-03-30 | 2005-01-12 | 云南工业用大麻实业有限公司 | Hemp seed protein powder and its preparing method and use |
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| CN103113460A (en) * | 2013-03-05 | 2013-05-22 | 刘睿 | Extraction process for fructus cannabis globulin |
| CN105994930A (en) * | 2016-05-16 | 2016-10-12 | 黄山普和康生物科技有限公司 | Process for processing high-purity fructus cannabis protein power |
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2017
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Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1561829A (en) * | 2004-03-30 | 2005-01-12 | 云南工业用大麻实业有限公司 | Hemp seed protein powder and its preparing method and use |
| CN101176504A (en) * | 2007-04-18 | 2008-05-14 | 广西巴马常春藤生命科技发展有限公司 | Technique of processing Huoma albumen powder |
| CN103113460A (en) * | 2013-03-05 | 2013-05-22 | 刘睿 | Extraction process for fructus cannabis globulin |
| CN105994930A (en) * | 2016-05-16 | 2016-10-12 | 黄山普和康生物科技有限公司 | Process for processing high-purity fructus cannabis protein power |
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| CN109730288A (en) * | 2019-03-06 | 2019-05-10 | 锦州俏牌生物科技有限公司 | A kind of fire sesame paste production method |
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