CN107381983A - A kind of medicament for handling oily sludge and preparation method thereof - Google Patents
A kind of medicament for handling oily sludge and preparation method thereof Download PDFInfo
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- CN107381983A CN107381983A CN201710604774.9A CN201710604774A CN107381983A CN 107381983 A CN107381983 A CN 107381983A CN 201710604774 A CN201710604774 A CN 201710604774A CN 107381983 A CN107381983 A CN 107381983A
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F11/00—Treatment of sludge; Devices therefor
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- Hydrology & Water Resources (AREA)
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- Environmental & Geological Engineering (AREA)
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Abstract
The invention discloses a kind of medicament for handling oily sludge, it is made up of following raw material according to parts by weight：0.5 2 parts of 48 parts of cocoanut shell powder, 5 12 parts of stalk, 10 16 parts of diatomite, 25 parts of peppermint, 1.5 3 parts of the root of Dahurain angelica, 27 parts of radix glycyrrhizae, 48 parts of bean dregs, 12 20 parts of flyash, 25 parts of honeysuckle, 13 parts of selfheal, 0.4 3 parts of sweet wormwood and sodium hypochlorite.The present invention also disclosed the preparation method and application method of the medicament.Raw material sources of the present invention are extensive, and preparation technology is simple, and production cost is low, suitable for large-scale industrial production；Various raw materials are mutually aided in the present invention, and the crude oil concentration in oily sludge is reduced, and are met the requirement of country, can be recycled, have good economic benefit and social benefit.
Description
Technical field
The present invention relates to sludge treatment field, specifically a kind of medicament for handling oily sludge.
Background technology
Oil is a kind of sticky, dark brown liquid.There is petroleum storage upper crustal some areas, and main component is various
Alkane, cycloalkane, the mixture of aromatic hydrocarbon.The sq-km of world ocean area 3.6 hundred million, about the 2.4 of land times.Continental shelf and
Continental slope about fifty-five million sq-km, equivalent to the summation of subaerial deposition basin area.The 1/4 of verified oil resource on the earth
Seabed is all imbedded in the 45% of ultimate recoverable reserves.World oil proved reserves contain center of gravity, progressively will be turned to by land
Ocean.Oil is brought conveniently for our life and production, but many dirts are generated in the exploitation of oil and process
Thing is contaminated, oily sludge is exactly one of which.
Oily sludge is mainly caused greasy filth and oil-sand in petroleum exploration and development industry and petroleum chemical industry production process,
Oily sludge has the features such as yield is big, oil content is high, heavy component is high, comprehensive utilization mode is few, and intractability is big, oil-containing
The presence of sludge exerts an adverse impact to surrounding environment quality, is a bigger problem in current Solid Waste Treatment,
Chemical agent is most common disposal of oily sludge articles for use, but existing chemical agent cost is high, and treatment effect does not reach people
Expection, this just brings inconvenience for the use of people.
The content of the invention
It is an object of the invention to provide a kind of medicament for handling oily sludge, to solve what is proposed in above-mentioned background technology
Problem.
To achieve the above object, the present invention provides following technical scheme：
A kind of medicament for handling oily sludge, is made up of following raw material according to parts by weight：Cocoanut shell powder 4-8 parts, stalk
5-12 parts, diatomite 10-16 parts, peppermint 2-5 parts, root of Dahurain angelica 1.5-3 parts, radix glycyrrhizae 2-7 parts, bean dregs 4-8 parts, flyash 12-20 parts,
Honeysuckle 2-5 parts, selfheal 1-3 parts, sweet wormwood 0.4-3 parts and sodium hypochlorite 0.5-2 parts.
As the further scheme of the present invention：Stalk using soybean stalk, maize straw, broomcorn straw, rice straw and
One or several kinds of mixtures in wheat stalk.
As the further scheme of the present invention：The particle diameter of cocoanut shell powder is 8-20um.
The preparation method of the medicament of the processing oily sludge, is comprised the following steps that：
Step 1, peppermint, the root of Dahurain angelica and radix glycyrrhizae are soaked into 45-70 minutes in the water that temperature is 32-38 degrees Celsius, add it
The decocting of 4-7 times of weight is boiled, and keeps micro-boiling 40-60 minutes for the first time, and 5-6 is added using filtered through gauze, then by the obtained dregs of a decoction
Decocting again is boiled 2 times, decocts 40-50 minutes every time, is merged filtrate three times, is obtained the first mixed solution；
Step 2, by the drying of honeysuckle, selfheal and sweet wormwood and grind into powder, then using mass fraction as 60-75%
Ethanol solution moistening capping 45-60 minutes, make its moistening saturating, it is 60-70%'s to be reloaded into infiltration cylinder and add mass fraction
Ethanol solution soaks 9-14 hours, collects filtrate, ethanol is recovered under reduced pressure, and product is concentrated into relative density for 1.15-1.3 and done
It is dry, obtain the first mixture；
Step 3, cocoanut shell powder, stalk, diatomite and bean dregs are ground and immerse 1-2.5 in the first mixed solution
Hour, then stir, obtain the second mixed solution；
Step 4, flyash and sodium hypochlorite are immersed in 50-75 minutes in hydrochloric acid, then dried, obtains being modified fine coal
Ash and sodium hypochlorite, then the first mixture, the second mixed solution, modified coal ash and sodium hypochlorite are mixed and added appropriate
Water, be mixed evenly, you can obtain finished product.
As the further scheme of the present invention：The mixing speed of step 4 is 90-150rpm.
The application method of the medicament of the processing oily sludge, is comprised the following steps that：Medicament, oily sludge and water are mixed
Uniformly and ferment 10-15 days.
Compared with prior art, the beneficial effects of the invention are as follows：Raw material sources of the present invention are extensive, and preparation technology is simple, raw
It is low to produce cost, suitable for large-scale industrial production；Various raw materials mutually aid in the present invention, by the crude oil in oily sludge
Concentration reduces, and meets the requirement of country, can be recycled, have good economic benefit and social benefit.
Embodiment
The technical scheme of this patent is described in more detail with reference to embodiment.
Embodiment 1
A kind of medicament for handling oily sludge, is made up of following raw material according to parts by weight：4 parts of cocoanut shell powder, stalk 5
Part, 10 parts of diatomite, 2 parts of peppermint, 1.5 parts of the root of Dahurain angelica, 2 parts of radix glycyrrhizae, 4 parts of bean dregs, 12 parts of flyash, 2 parts of honeysuckle, selfheal 1
0.5 part of part, 0.4 part of sweet wormwood and sodium hypochlorite.Stalk is using soybean stalk and the mixture of broomcorn straw.
The preparation method of the medicament of the processing oily sludge, is comprised the following steps that：
Step 1, peppermint, the root of Dahurain angelica and radix glycyrrhizae are soaked 50 minutes in the water that temperature is 32 degrees Celsius, add its weight 5
Times decocting boil, keep micro-boiling 45 minutes for the first time, using filtered through gauze, then the obtained dregs of a decoction added to 5 times of decocting and boil 2
It is secondary, decoct 40 minutes every time, merge filtrate three times, obtain the first mixed solution；
Step 2, by honeysuckle, selfheal and sweet wormwood drying and grind into powder, then using mass fraction as 60% second
Alcoholic solution moistening capping 45 minutes, moistens it saturating, is reloaded into the ethanol solution leaching for adding that mass fraction is 60% in infiltration cylinder
10 hours, filtrate is collected, ethanol is recovered under reduced pressure, product is concentrated into relative density is 1.15 and dries, and obtains the first mixing
Thing；
Step 3, cocoanut shell powder, stalk, diatomite and bean dregs are ground and to immerse in the first mixed solution 1.5 small
When, then stir, obtain the second mixed solution；
Step 4, flyash and sodium hypochlorite are immersed in hydrochloric acid 55 minutes, then dried, obtain modified coal ash and
Sodium hypochlorite, then the first mixture, the second mixed solution, modified coal ash and sodium hypochlorite are mixed and added appropriate
Water, it is mixed evenly, you can obtain finished product.
The application method of the medicament of the processing oily sludge, is comprised the following steps that：Medicament, oily sludge and water are mixed
Uniformly and ferment 12 days.
Embodiment 2
A kind of medicament for handling oily sludge, is made up of following raw material according to parts by weight：6 parts of cocoanut shell powder, stalk 8
Part, 12 parts of diatomite, 3 parts of peppermint, 2 parts of the root of Dahurain angelica, 5 parts of radix glycyrrhizae, 6 parts of bean dregs, 15 parts of flyash, 3 parts of honeysuckle, selfheal 1.5
1 part of part, 1.2 parts of sweet wormwood and sodium hypochlorite.The particle diameter of cocoanut shell powder is 12um.
The preparation method of the medicament of the processing oily sludge, is comprised the following steps that：
Step 1, peppermint, the root of Dahurain angelica and radix glycyrrhizae are soaked 60 minutes in the water that temperature is 35 degrees Celsius, add its weight 6
Times decocting boil, keep micro-boiling 48 minutes for the first time, using filtered through gauze, then the obtained dregs of a decoction added to 6 times of decocting and boil 2
It is secondary, decoct 45 minutes every time, merge filtrate three times, obtain the first mixed solution；
Step 2, by honeysuckle, selfheal and sweet wormwood drying and grind into powder, then using mass fraction as 65% second
Alcoholic solution moistening capping 50 minutes, moistens it saturating, is reloaded into the ethanol solution leaching for adding that mass fraction is 62% in infiltration cylinder
11 hours, filtrate is collected, ethanol is recovered under reduced pressure, product is concentrated into relative density is 1.2 and dries, and obtains the first mixing
Thing；
Step 3, cocoanut shell powder, stalk, diatomite and bean dregs are ground and immersed in the first mixed solution 2 hours,
Then stir, obtain the second mixed solution；
Step 4, flyash and sodium hypochlorite are immersed in hydrochloric acid 58 minutes, then dried, obtain modified coal ash and
Sodium hypochlorite, then the first mixture, the second mixed solution, modified coal ash and sodium hypochlorite are mixed and added appropriate
Water, it is mixed evenly under 120rpm rotating speed, you can obtain finished product.
The application method of the medicament of the processing oily sludge, is comprised the following steps that：Medicament, oily sludge and water are mixed
Uniformly and ferment 14 days.
Embodiment 3
A kind of medicament for handling oily sludge, is made up of following raw material according to parts by weight：7 parts of cocoanut shell powder, stalk 10
Part, 15 parts of diatomite, 4 parts of peppermint, 2.5 parts of the root of Dahurain angelica, 6 parts of radix glycyrrhizae, 7 parts of bean dregs, 18 parts of flyash, 4.5 parts of honeysuckle, selfheal
1.5 parts of 3 parts, 2.6 parts of sweet wormwood and sodium hypochlorite.Stalk uses the mixture of soybean stalk, maize straw and wheat stalk.Coconut
The particle diameter of shell powder is 14um.
The preparation method of the medicament of the processing oily sludge, is comprised the following steps that：
Step 1, peppermint, the root of Dahurain angelica and radix glycyrrhizae are soaked 60 minutes in temperature is the water of 36 degrees Celsius, add its weight 6
Times decocting boil, keep micro-boiling 52 minutes for the first time, using filtered through gauze, then the obtained dregs of a decoction added to 6 times of decocting and boil 2
It is secondary, decoct 48 minutes every time, merge filtrate three times, obtain the first mixed solution；
Step 2, by honeysuckle, selfheal and sweet wormwood drying and grind into powder, then using mass fraction as 72% second
Alcoholic solution moistening capping 55 minutes, moistens it saturating, is reloaded into the ethanol solution leaching for adding that mass fraction is 66% in infiltration cylinder
12 hours, filtrate is collected, ethanol is recovered under reduced pressure, product is concentrated into relative density is 1.24 and dries, and obtains the first mixing
Thing；
Step 3, cocoanut shell powder, stalk, diatomite and bean dregs are ground and immersed in the first mixed solution 2 hours,
Then stir, obtain the second mixed solution；
Step 4, flyash and sodium hypochlorite are immersed in hydrochloric acid 70 minutes, then dried, obtain modified coal ash and
Sodium hypochlorite, then the first mixture, the second mixed solution, modified coal ash and sodium hypochlorite are mixed and added appropriate
Water, it is mixed evenly, you can obtain finished product.
The application method of the medicament of the processing oily sludge, is comprised the following steps that：Medicament, oily sludge and water are mixed
Uniformly and ferment 13 days.
Embodiment 4
A kind of medicament for handling oily sludge, is made up of following raw material according to parts by weight：8 parts of cocoanut shell powder, stalk 11
Part, 16 parts of diatomite, 5 parts of peppermint, 3 parts of the root of Dahurain angelica, 7 parts of radix glycyrrhizae, 8 parts of bean dregs, 20 parts of flyash, 5 parts of honeysuckle, 3 parts of selfheal,
2 parts of 3 parts of sweet wormwood and sodium hypochlorite.Stalk is using soybean stalk, maize straw, broomcorn straw, rice straw and wheat stalk
Mixture.The particle diameter of cocoanut shell powder is 18um.
The preparation method of the medicament of the processing oily sludge, is comprised the following steps that：
Step 1, peppermint, the root of Dahurain angelica and radix glycyrrhizae are soaked 70 minutes in the water that temperature is 38 degrees Celsius, add its weight 7
Times decocting boil, keep micro-boiling 60 minutes for the first time, using filtered through gauze, then the obtained dregs of a decoction added to 6 times of decocting and boil 2
It is secondary, decoct 50 minutes every time, merge filtrate three times, obtain the first mixed solution；
Step 2, by honeysuckle, selfheal and sweet wormwood drying and grind into powder, then using mass fraction as 75% second
Alcoholic solution moistening capping 60 minutes, moistens it saturating, is reloaded into the ethanol solution leaching for adding that mass fraction is 70% in infiltration cylinder
14 hours, filtrate is collected, ethanol is recovered under reduced pressure, product is concentrated into relative density is 1.3 and dries, and obtains the first mixing
Thing；
Step 3, cocoanut shell powder, stalk, diatomite and bean dregs are ground and to immerse in the first mixed solution 2.5 small
When, then stir, obtain the second mixed solution；
Step 4, flyash and sodium hypochlorite are immersed in hydrochloric acid 75 minutes, then dried, obtain modified coal ash and
Sodium hypochlorite, then the first mixture, the second mixed solution, modified coal ash and sodium hypochlorite are mixed and added appropriate
Water, it is mixed evenly under 150rpm rotating speed, you can obtain finished product.
The application method of the medicament of the processing oily sludge, is comprised the following steps that：Medicament, oily sludge and water are mixed
Uniformly and ferment 15 days.
Flyash can reduce the water content of sludge, and the oleaginous material shortened in drying time, with sludge is complexed, and locate
It is good to manage effect；The matrix that cocoanut shell powder, stalk, diatomite and bean dregs are formed immerses first that peppermint, the root of Dahurain angelica and radix glycyrrhizae are formed
In mixed solution, oleaginous material can be purged, then be aided with sodium hypochlorite and honeysuckle, selfheal and sweet wormwood are formed
First mixture, the crude oil concentration in oily sludge can be greatly lowered, meet the requirement of country.
It is obvious to a person skilled in the art that the invention is not restricted to the details of above-mentioned one exemplary embodiment, Er Qie
In the case of without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, embodiment all should be regarded as exemplary, and be nonrestrictive, the scope of the present invention is by appended power
Profit requires rather than described above limits, it is intended that all in the implication and scope of the equivalency of claim by falling
Change is included in the present invention.
Moreover, it will be appreciated that although the present specification is described in terms of embodiments, not each embodiment is only wrapped
Containing an independent technical scheme, this narrating mode of specification is only that those skilled in the art should for clarity
Using specification as an entirety, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
It is appreciated that other embodiment.
Claims (6)
1. a kind of medicament for handling oily sludge, it is characterised in that be made up of following raw material according to parts by weight：Cocoanut shell powder 4-
8 parts, stalk 5-12 parts, diatomite 10-16 parts, peppermint 2-5 parts, root of Dahurain angelica 1.5-3 parts, radix glycyrrhizae 2-7 parts, bean dregs 4-8 parts, flyash
12-20 parts, honeysuckle 2-5 parts, selfheal 1-3 parts, sweet wormwood 0.4-3 parts and sodium hypochlorite 0.5-2 parts.
2. it is according to claim 1 processing oily sludge medicament, it is characterised in that the stalk using soybean stalk,
One or several kinds of mixtures in maize straw, broomcorn straw, rice straw and wheat stalk.
3. the medicament of processing oily sludge according to claim 1 or 2, it is characterised in that the grain of the cocoanut shell powder
Footpath is 8-20um.
4. the preparation method of the medicament of a kind of processing oily sludge as described in claim 1-3 is any, it is characterised in that specific
Step is as follows：
Step 1, peppermint, the root of Dahurain angelica and radix glycyrrhizae are soaked into 45-70 minutes in the water that temperature is 32-38 degrees Celsius, add its weight
4-7 times of decocting is boiled, and keeps micro-boiling 40-60 minutes for the first time, and 5-6 times is added using filtered through gauze, then by the obtained dregs of a decoction
Decocting is boiled 2 times, decocts 40-50 minutes every time, is merged filtrate three times, is obtained the first mixed solution；
Step 2, by the drying of honeysuckle, selfheal and sweet wormwood and grind into powder, then the second using mass fraction as 60-75%
Alcoholic solution moistening capping 45-60 minutes, make its moistening saturating, be reloaded into infiltration cylinder and add the ethanol that mass fraction is 60-70%
Solution soaks 9-14 hours, collects filtrate, ethanol is recovered under reduced pressure, and it is 1.15-1.3 and drying that product is concentrated into relative density,
Obtain the first mixture；
Step 3, cocoanut shell powder, stalk, diatomite and bean dregs are ground and immersed 1-2.5 hours in the first mixed solution,
Then stir, obtain the second mixed solution；
Step 4, flyash and sodium hypochlorite are immersed in 50-75 minutes in hydrochloric acid, then dried, obtain modified coal ash and
Sodium hypochlorite, then the first mixture, the second mixed solution, modified coal ash and sodium hypochlorite are mixed and added appropriate
Water, it is mixed evenly, you can obtain finished product.
5. the preparation method of the medicament of processing oily sludge according to claim 4, it is characterised in that the step 4
Mixing speed is 90-150rpm.
6. the application method of the medicament of the processing oily sludge according to claim 1-3, it is characterised in that specific steps are such as
Under：Medicament, oily sludge and water are well mixed and carry out fermentation 10-15 days.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710604774.9A CN107381983A (en) | 2017-07-24 | 2017-07-24 | A kind of medicament for handling oily sludge and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710604774.9A CN107381983A (en) | 2017-07-24 | 2017-07-24 | A kind of medicament for handling oily sludge and preparation method thereof |
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| CN201710604774.9A Pending CN107381983A (en) | 2017-07-24 | 2017-07-24 | A kind of medicament for handling oily sludge and preparation method thereof |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102373103A (en) * | 2010-08-11 | 2012-03-14 | 金延柱 | Method for producing regenerated fuel by using sludge in urban sewage treatment plant |
| CN104961311A (en) * | 2015-06-11 | 2015-10-07 | 耿跃 | Method for manufacturing biological preparations for treating silt at bottoms of fish ponds |
| CN105217880A (en) * | 2014-06-27 | 2016-01-06 | 南京益佳特科技发展有限公司 | A kind of sewage water treatment method adding Chinese medicine formula |
| CN105253935A (en) * | 2015-11-16 | 2016-01-20 | 范洲卫 | Industrial coking wastewater treatment agent and preparation method thereof |
-
2017
- 2017-07-24 CN CN201710604774.9A patent/CN107381983A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102373103A (en) * | 2010-08-11 | 2012-03-14 | 金延柱 | Method for producing regenerated fuel by using sludge in urban sewage treatment plant |
| CN105217880A (en) * | 2014-06-27 | 2016-01-06 | 南京益佳特科技发展有限公司 | A kind of sewage water treatment method adding Chinese medicine formula |
| CN104961311A (en) * | 2015-06-11 | 2015-10-07 | 耿跃 | Method for manufacturing biological preparations for treating silt at bottoms of fish ponds |
| CN105253935A (en) * | 2015-11-16 | 2016-01-20 | 范洲卫 | Industrial coking wastewater treatment agent and preparation method thereof |
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Application publication date: 20171124 |