CN107372671A - A kind of succulent soil fungicides and preparation method thereof - Google Patents
A kind of succulent soil fungicides and preparation method thereof Download PDFInfo
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- CN107372671A CN107372671A CN201710637236.XA CN201710637236A CN107372671A CN 107372671 A CN107372671 A CN 107372671A CN 201710637236 A CN201710637236 A CN 201710637236A CN 107372671 A CN107372671 A CN 107372671A
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- oil
- oil phase
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- succulent
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- 239000002689 soil Substances 0.000 title claims abstract description 27
- 239000000417 fungicide Substances 0.000 title claims abstract description 23
- 238000002360 preparation method Methods 0.000 title claims abstract description 11
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 42
- 239000003921 oil Substances 0.000 claims abstract description 35
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 23
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 22
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 20
- 150000005846 sugar alcohols Polymers 0.000 claims abstract description 20
- 239000004094 surface-active agent Substances 0.000 claims abstract description 20
- TWFZGCMQGLPBSX-UHFFFAOYSA-N Carbendazim Natural products C1=CC=C2NC(NC(=O)OC)=NC2=C1 TWFZGCMQGLPBSX-UHFFFAOYSA-N 0.000 claims abstract description 14
- 229920002101 Chitin Polymers 0.000 claims abstract description 14
- 239000006013 carbendazim Substances 0.000 claims abstract description 14
- JNPZQRQPIHJYNM-UHFFFAOYSA-N carbendazim Chemical compound C1=C[CH]C2=NC(NC(=O)OC)=NC2=C1 JNPZQRQPIHJYNM-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000010647 garlic oil Substances 0.000 claims abstract description 14
- GNVDAZSPJWCIQZ-UHFFFAOYSA-N flusulfamide Chemical compound ClC1=CC([N+](=O)[O-])=CC=C1NS(=O)(=O)C1=CC=C(Cl)C(C(F)(F)F)=C1 GNVDAZSPJWCIQZ-UHFFFAOYSA-N 0.000 claims abstract description 13
- 238000003756 stirring Methods 0.000 claims abstract description 13
- 239000007908 nanoemulsion Substances 0.000 claims abstract description 12
- 230000000740 bleeding effect Effects 0.000 claims abstract description 9
- 230000000149 penetrating effect Effects 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 7
- -1 spreader-sticker Substances 0.000 claims abstract description 7
- 235000019198 oils Nutrition 0.000 claims description 31
- 239000000203 mixture Substances 0.000 claims description 15
- NWGKJDSIEKMTRX-AAZCQSIUSA-N Sorbitan monooleate Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OC[C@@H](O)[C@H]1OC[C@H](O)[C@H]1O NWGKJDSIEKMTRX-AAZCQSIUSA-N 0.000 claims description 12
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 claims description 12
- 229920000053 polysorbate 80 Polymers 0.000 claims description 12
- AHLWZBVXSWOPPL-RGYGYFBISA-N 20-deoxy-20-oxophorbol 12-myristate 13-acetate Chemical compound C([C@]1(O)C(=O)C(C)=C[C@H]1[C@@]1(O)[C@H](C)[C@H]2OC(=O)CCCCCCCCCCCCC)C(C=O)=C[C@H]1[C@H]1[C@]2(OC(C)=O)C1(C)C AHLWZBVXSWOPPL-RGYGYFBISA-N 0.000 claims description 10
- 241001602688 Pama Species 0.000 claims description 10
- 239000004359 castor oil Substances 0.000 claims description 10
- 235000019438 castor oil Nutrition 0.000 claims description 10
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 claims description 10
- 229940051841 polyoxyethylene ether Drugs 0.000 claims description 9
- 229920000056 polyoxyethylene ether Polymers 0.000 claims description 9
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 8
- 210000000481 breast Anatomy 0.000 claims description 6
- 239000002285 corn oil Substances 0.000 claims description 6
- 235000005687 corn oil Nutrition 0.000 claims description 6
- 239000010497 wheat germ oil Substances 0.000 claims description 6
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 5
- 235000011187 glycerol Nutrition 0.000 claims description 4
- 235000008390 olive oil Nutrition 0.000 claims description 4
- 239000004006 olive oil Substances 0.000 claims description 4
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 claims description 3
- 235000004443 Ricinus communis Nutrition 0.000 claims description 2
- SZXQTJUDPRGNJN-UHFFFAOYSA-N dipropylene glycol Chemical compound OCCCOCCCO SZXQTJUDPRGNJN-UHFFFAOYSA-N 0.000 claims description 2
- 241000894006 Bacteria Species 0.000 claims 1
- 244000018633 Prunus armeniaca Species 0.000 claims 1
- 235000009827 Prunus armeniaca Nutrition 0.000 claims 1
- 240000000528 Ricinus communis Species 0.000 claims 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims 1
- 239000005864 Sulphur Substances 0.000 claims 1
- 150000001412 amines Chemical class 0.000 claims 1
- 229960001777 castor oil Drugs 0.000 claims 1
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims 1
- 230000000844 anti-bacterial effect Effects 0.000 abstract description 7
- 239000003899 bactericide agent Substances 0.000 abstract description 7
- 238000013019 agitation Methods 0.000 abstract 1
- 201000010099 disease Diseases 0.000 description 7
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 7
- 241001478750 Chlorophytum comosum Species 0.000 description 4
- 241000196324 Embryophyta Species 0.000 description 4
- 239000001944 prunus armeniaca kernel oil Substances 0.000 description 3
- 230000001954 sterilising effect Effects 0.000 description 3
- 238000004659 sterilization and disinfection Methods 0.000 description 3
- 241000607479 Yersinia pestis Species 0.000 description 2
- 150000001450 anions Chemical class 0.000 description 2
- 210000002615 epidermis Anatomy 0.000 description 2
- 208000015181 infectious disease Diseases 0.000 description 2
- 230000001338 necrotic effect Effects 0.000 description 2
- 229920002401 polyacrylamide Polymers 0.000 description 2
- 206010000234 Abortion spontaneous Diseases 0.000 description 1
- 244000052616 bacterial pathogen Species 0.000 description 1
- 239000010866 blackwater Substances 0.000 description 1
- 238000009395 breeding Methods 0.000 description 1
- 230000001488 breeding effect Effects 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 238000001727 in vivo Methods 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 235000013372 meat Nutrition 0.000 description 1
- 208000015994 miscarriage Diseases 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 230000035755 proliferation Effects 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 239000008159 sesame oil Substances 0.000 description 1
- 235000011803 sesame oil Nutrition 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 208000000995 spontaneous abortion Diseases 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 210000001519 tissue Anatomy 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
- A01N25/04—Dispersions, emulsions, suspoemulsions, suspension concentrates or gels
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/36—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N41/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a sulfur atom bound to a hetero atom
- A01N41/02—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a sulfur atom bound to a hetero atom containing a sulfur-to-oxygen double bond
- A01N41/04—Sulfonic acids; Derivatives thereof
- A01N41/06—Sulfonic acid amides
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/14—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
- A01N43/16—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
- A01N47/10—Carbamic acid derivatives, i.e. containing the group —O—CO—N<; Thio analogues thereof
- A01N47/18—Carbamic acid derivatives, i.e. containing the group —O—CO—N<; Thio analogues thereof containing a —O—CO—N< group, or a thio analogue thereof, directly attached to a heterocyclic or cycloaliphatic ring
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/42—Aloeaceae [Aloe family] or Liliaceae [Lily family], e.g. aloe, veratrum, onion, garlic or chives
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Plant Pathology (AREA)
- Dentistry (AREA)
- Agronomy & Crop Science (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Biotechnology (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Toxicology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention provides a kind of succulent soil fungicides, raw material includes：Carbendazim, flusulfamide, garlic oil, oil phase, emulsifying agent, polyalcohol, water, surfactant, penetrating agent JFC, spreader-sticker, citric acid and chitin.Its preparation method is first to add to carbendazim, flusulfamide and garlic oil in oil phase, and emulsifying agent and polyalcohol are added after stirring, obtains oil phase, then the water droplet of 5/4 dosage is added in oil phase, is cooled down after high-pressure homogeneous, obtains nano-emulsion；Then the water of 1/5 dosage, surfactant, bleeding agent, spreader-sticker, citric acid and chitin are mixed, adds nano-emulsion under agitation, ultrasonic disperse, produce.Bactericide is made after nano-emulsion and nano-emulsion and bleeding agent, spreader-sticker is made into soil fungicides jointly again by the present invention, can not only extend the effective acting time of bactericide, can also promote the holdup time of bactericide.
Description
Technical field
The invention belongs to succulent planting technology field, and in particular to a kind of succulent soil fungicides and its system
Preparation Method.
Background technology
Succulent is also known as succulent, succulent plant, is primarily referred to as certain part such as stem, leaf of vegetable nutritorium
Or root（A few species have 2 parts concurrently）Parenchymal tissue with prosperity, to store moisture and nutrient, seem plump in shape
A kind of plant of succulence.In recent years, succulent because its form uniqueness, extensive management, it is numerous in variety, be easy to breeding, pest and disease damage
Less and purify the advantages that ability of air is strong and liked by people.Although succulent is few famous with pest and disease damage, due to it
Moisture is rich in vivo, if miscarriage, environment discomfort, are highly prone to the infection of germ during transplanting and management, from
And there is undergrowth phenomenon.
Because disease initial stage of succulent results from root infection more, and plant root is hidden in underground, this just give and
Shi Faxian diseases cause the difficulty of a bit.If succulent disease cannot treat in time, when proliferation of germs to axis
Portion, stem's epidermis is showed the water stain sample necrotic plaque of black, cause the soft corruption of succulent stem, be difficult to treatment.Therefore, exist
When preparing succulent matrix, it using the protective effect of bactericide, can effectively prevent the generation of succulent disease, reduce not
Necessary loss.
At present, it is the effective way for controlling soil disease seriously to occur to carry out soil sterilization.
The content of the invention
Present invention aim to address the wetting of existing soil fungicides, the technical problem of spreading ability difference, there is provided Yi Zhongduo
Meat plant soil fungicides and preparation method thereof.
A kind of succulent soil fungicides, raw material include in parts by weight：Carbendazim 2-4 parts, flusulfamide 1-3 parts,
Garlic oil 3-4 parts, oil phase 100-150 parts, emulsifying agent 0.5-1.5 parts, polyalcohol 0.2-0.5 parts, water 50-100 parts, surface-active
Agent 4-10 parts, penetrating agent JFC 2-4 parts, spreader-sticker 1-3 parts, citric acid 0.5-1.2 parts, chitin 0.5-1 parts.
Preferably, the oil phase is one or more of mixtures in corn oil, apricot kernel oil, olive oil, wheat germ oil.
Preferably, the emulsifying agent is Tween80 and Span80 mixture, and Tween80 and Span80 mass ratio are
1：1.
Preferably, the polyalcohol is one kind in glycerine, ethylene glycol, pentaerythrite or dipropylene glycol.
Preferably, the surfactant is the mixture of castor oil polyoxyethylene ether and PAMA, castor
The mass ratio of sesame oil APEO and PAMA is 4：1.
The preparation method of above-mentioned succulent soil fungicides, comprises the following steps：
Step 1, carbendazim, flusulfamide and garlic oil are added in oil phase, emulsifying agent and polyalcohol is added after stirring, obtains oil
Phase；
Step 2, the water droplet of 5/4 dosage is added in step 1 gained oil phase, is cooled to 4-10 DEG C after high-pressure homogeneous, obtains nanometer
Breast；
Step 3, the water of 1/5 dosage, surfactant, bleeding agent, spreader-sticker, citric acid and chitin are mixed, in stirring bar
Step 2 gained nano-emulsion is added under part, ultrasonic disperse, is produced.
Bactericide is made after nano-emulsion and nano-emulsion and bleeding agent, spreader-sticker is made into soil sterilization jointly again by the present invention
It agent, can not only extend the effective acting time of bactericide, the holdup time of bactericide can also be promoted.
Embodiment
Embodiment 1
A kind of succulent soil fungicides, raw material include in parts by weight：2 parts of carbendazim, 1 part of flusulfamide, garlic oil 3
Part, 100 parts of oil phase, 0.5 part of emulsifying agent, 0.2 part of polyalcohol, 50 parts of water, 4 parts of surfactant, 2 parts of penetrating agent JFC, Zhan Zhe
1 part of agent, 0.5 part of citric acid, 0.5 part of chitin.
Wherein, the oil phase is corn oil；The emulsifying agent be Tween80 and Span80 mixture, Tween80 with
Span80 mass ratio is 1：1；The polyalcohol is glycerine；The surfactant is castor oil polyoxyethylene ether and anion
The mass ratio of the mixture of polyacrylamide, castor oil polyoxyethylene ether and PAMA is 4：1.
The preparation method of above-mentioned succulent soil fungicides, comprises the following steps：
Step 1, carbendazim, flusulfamide and garlic oil are added in oil phase, emulsifying agent and polyalcohol is added after stirring, obtains oil
Phase；
Step 2, the water droplet of 5/4 dosage is added in step 1 gained oil phase, is cooled to 4-10 DEG C after high-pressure homogeneous, obtains nanometer
Breast；
Step 3, the water of 1/5 dosage, surfactant, bleeding agent, spreader-sticker, citric acid and chitin are mixed, in stirring bar
Step 2 gained nano-emulsion is added under part, ultrasonic disperse, is produced.
It will be sprayed after 500 times of soil sterilization dilution agent obtained by above-described embodiment in succulent, kind is pearl chlorophytum comosum, right
According to spray clear water.After one month, the growing way of two groups of pearl chlorophytum comosums is contrasted, as a result shows that control group stem epidermis shows black water
Stain sample necrotic plaque, and the soft corruption of stem, and test group pearl chlorophytum comosum green in color, pearl size, spacing are uniform.After two months, it is right
It is completely downright bad according to group pearl chlorophytum comosum, and test group green in color.
Embodiment 2
A kind of succulent soil fungicides, raw material include in parts by weight：3 parts of carbendazim, 2 parts of flusulfamide, garlic oil 3
Part, 120 parts of oil phase, 0.8 part of emulsifying agent, 0.3 part of polyalcohol, 70 parts of water, 7 parts of surfactant, 3 parts of penetrating agent JFC, Zhan Zhe
2 parts of agent, 0.7 part of citric acid, 0.6 part of chitin.
Wherein, the oil phase be apricot kernel oil, olive oil, the mixture of wheat germ oil, apricot kernel oil, olive oil, the matter of wheat germ oil
Amount is than being 1：1：1；The emulsifying agent is Tween80 and Span80 mixture, and Tween80 and Span80 mass ratio are 1：1；
The polyalcohol is pentaerythrite；The surfactant is the mixing of castor oil polyoxyethylene ether and PAMA
The mass ratio of thing, castor oil polyoxyethylene ether and PAMA is 4：1.
The preparation method of above-mentioned succulent soil fungicides, comprises the following steps：
Step 1, carbendazim, flusulfamide and garlic oil are added in oil phase, emulsifying agent and polyalcohol is added after stirring, obtains oil
Phase；
Step 2, the water droplet of 5/4 dosage is added in step 1 gained oil phase, is cooled to 4-10 DEG C after high-pressure homogeneous, obtains nanometer
Breast；
Step 3, the water of 1/5 dosage, surfactant, bleeding agent, spreader-sticker, citric acid and chitin are mixed, in stirring bar
Step 2 gained nano-emulsion is added under part, ultrasonic disperse, is produced.
Embodiment 3
A kind of succulent soil fungicides, raw material include in parts by weight：2 parts of carbendazim, 1 part of flusulfamide, garlic oil 4
Part, 140 parts of oil phase, 1.2 parts of emulsifying agent, 0.4 part of polyalcohol, 80 parts of water, 8 parts of surfactant, 3 parts of penetrating agent JFC, Zhan Zhe
2 parts of agent, 0.9 part of citric acid, 0.8 part of chitin.
Wherein, the oil phase is the mixture of corn oil and wheat germ oil, and the mass ratio of corn oil and wheat germ oil is 1：1；Institute
The mixture that emulsifying agent is Tween80 and Span80 is stated, Tween80 and Span80 mass ratio are 1：1；The polyalcohol is one
Contracting DPG；The surfactant is the mixture of castor oil polyoxyethylene ether and PAMA, castor oil
The mass ratio of APEO and PAMA is 4：1.
The preparation method of above-mentioned succulent soil fungicides, comprises the following steps：
Step 1, carbendazim, flusulfamide and garlic oil are added in oil phase, emulsifying agent and polyalcohol is added after stirring, obtains oil
Phase；
Step 2, the water droplet of 5/4 dosage is added in step 1 gained oil phase, is cooled to 4-10 DEG C after high-pressure homogeneous, obtains nanometer
Breast；
Step 3, the water of 1/5 dosage, surfactant, bleeding agent, spreader-sticker, citric acid and chitin are mixed, in stirring bar
Step 2 gained nano-emulsion is added under part, ultrasonic disperse, is produced.
Embodiment 4
A kind of succulent soil fungicides, raw material include in parts by weight：4 parts of carbendazim, 3 parts of flusulfamide, garlic oil 4
Part, 150 parts of oil phase, 1.5 parts of emulsifying agent, 0.5 part of polyalcohol, 100 parts of water, 10 parts of surfactant, 4 parts of penetrating agent JFC, exhibition
3 parts of agent, 1.2 parts of citric acid, 1 part of chitin.
Wherein, the oil phase is corn oil；The emulsifying agent be Tween80 and Span80 mixture, Tween80 with
Span80 mass ratio is 1：1；The polyalcohol is glycerine；The surfactant is castor oil polyoxyethylene ether and anion
The mass ratio of the mixture of polyacrylamide, castor oil polyoxyethylene ether and PAMA is 4：1.
The preparation method of above-mentioned succulent soil fungicides, comprises the following steps：
Step 1, carbendazim, flusulfamide and garlic oil are added in oil phase, emulsifying agent and polyalcohol is added after stirring, obtains oil
Phase；
Step 2, the water droplet of 5/4 dosage is added in step 1 gained oil phase, is cooled to 4-10 DEG C after high-pressure homogeneous, obtains nanometer
Breast；
Step 3, the water of 1/5 dosage, surfactant, bleeding agent, spreader-sticker, citric acid and chitin are mixed, in stirring bar
Step 2 gained nano-emulsion is added under part, ultrasonic disperse, is produced.
Claims (6)
- A kind of 1. succulent soil fungicides, it is characterised in that：Raw material includes in parts by weight：Carbendazim 2-4 parts, sulphur bacterium Amine 1-3 parts, garlic oil 3-4 parts, oil phase 100-150 parts, emulsifying agent 0.5-1.5 parts, polyalcohol 0.2-0.5 parts, water 50-100 parts, Surfactant 4-10 parts, penetrating agent JFC 2-4 parts, spreader-sticker 1-3 parts, citric acid 0.5-1.2 parts, chitin 0.5-1 parts.
- 2. succulent soil fungicides according to claim 1, it is characterised in that：The oil phase is corn oil, apricot One or more of mixtures in benevolence oil, olive oil, wheat germ oil.
- 3. succulent soil fungicides according to claim 1, it is characterised in that：The emulsifying agent is Tween80 With Span80 mixture, Tween80 and Span80 mass ratio are 1：1.
- 4. succulent soil fungicides according to claim 1, it is characterised in that：The polyalcohol is glycerine, second One kind in glycol, pentaerythrite or dipropylene glycol.
- 5. succulent soil fungicides according to claim 1, it is characterised in that：The surfactant is castor-oil plant The matter of the mixture of oily APEO and PAMA, castor oil polyoxyethylene ether and PAMA Amount is than being 4：1.
- 6. the preparation method of the succulent soil fungicides described in claim 1, it is characterised in that：Comprise the following steps：Step 1, carbendazim, flusulfamide and garlic oil are added in oil phase, emulsifying agent and polyalcohol is added after stirring, obtains oil Phase；Step 2, the water droplet of 5/4 dosage is added in step 1 gained oil phase, is cooled to 4-10 DEG C after high-pressure homogeneous, obtains nanometer Breast；Step 3, the water of 1/5 dosage, surfactant, bleeding agent, spreader-sticker, citric acid and chitin are mixed, in stirring bar Step 2 gained nano-emulsion is added under part, ultrasonic disperse, is produced.
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Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103907649A (en) * | 2014-04-14 | 2014-07-09 | 山东圣鹏科技股份有限公司 | Soil bactericide pesticide composite |
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Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103907649A (en) * | 2014-04-14 | 2014-07-09 | 山东圣鹏科技股份有限公司 | Soil bactericide pesticide composite |
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