CN107372576A - A kind of spray water mosquito-repellent incense composition and preparation method thereof - Google Patents
A kind of spray water mosquito-repellent incense composition and preparation method thereof Download PDFInfo
- Publication number
- CN107372576A CN107372576A CN201710635708.8A CN201710635708A CN107372576A CN 107372576 A CN107372576 A CN 107372576A CN 201710635708 A CN201710635708 A CN 201710635708A CN 107372576 A CN107372576 A CN 107372576A
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- Prior art keywords
- mosquito
- repellent incense
- spray water
- minutes
- pyrethrins
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N53/00—Biocides, pest repellants or attractants, or plant growth regulators containing cyclopropane carboxylic acids or derivatives thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
- A01N25/04—Dispersions, emulsions, suspoemulsions, suspension concentrates or gels
- A01N25/06—Aerosols
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N31/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic oxygen or sulfur compounds
- A01N31/08—Oxygen or sulfur directly attached to an aromatic ring system
- A01N31/14—Ethers
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Plant Pathology (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- Pest Control & Pesticides (AREA)
- Agronomy & Crop Science (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Toxicology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Catching Or Destruction (AREA)
Abstract
The present invention relates to mosquito repellent technical field, specifically provides a kind of spray water mosquito-repellent incense composition and preparation method thereof, is made up of each component of following percentage by weight：Pyrethrins 0.01 ~ 2%；Pyrethroid 0.01 ~ 2%；Thixotropic agent 5 ~ 20%；Distilled water 70 ~ 95%；The weight of above each component is equal to 100% than sum.Distilled water is added after above pyrethrins, pyrethroid and thixotropic agent are mixed 10 ~ 15 minutes and continues stirring 15 ~ 20 minutes, it can be prepared by a kind of spray water mosquito-repellent incense, the present invention has good repellent effect to mosquito, it is harmless, it is very friendly to environment, and mosquito repelling efficiency time is grown, while preparation method is simple, with the advantages of efficient, environmentally friendly, possess good market prospects.
Description
Technical field
The present invention relates to mosquito repellent technical field, more particularly to a kind of spray water mosquito-repellent incense composition and preparation method thereof.
Background technology
Biting for mosquito brings no small influence, particularly summer and autumn to the life of people, and mosquito is more, mosquito
Various different degrees of influences can be produced to people by biting, and such as reduced sleep quality, influenceed the spirit that works by day, spread disease,
Directly threat is formed to the health of people, at this stage, people are in order to solve the problems, such as bite by mosquitos, commonly using some mosquito repellents
Product, such as mosquito-repellent incense and solid mosquito-dispelling tablet, and it is because being formulated unreasonable the defects of existing mosquito repellant product is common, causes mosquito repellent to be lived
Property composition when starting volatilization it is fast, concentration is high, and repelling effect is good, and later stage volatilization is slow, and repelling effect is substantially deteriorated, and existing drive
Mosquito product often has toxic odor, and the health of people can be affected in the past for a long time, and mosquito also can be simultaneously
Antibody is produced in vivo, and repelling effect is poor, and the mosquito-driving liquid of another kind of liquid type, is typically that with the addition of various chemical agents, such as anti-corruption
Agent, wetting agent, bleeding agent, surfactant etc., it is unfavorable that much time using can cause to the skin of people, feels under the weather.
Also one kind is culicifuge made of natural material, although Nantural non-toxic, prepares material and is not easy to obtain, and preparation method is answered
It is miscellaneous, long preparation period.
The content of the invention
It is an object of the invention to be provided for solution above-mentioned technical problem, a kind of preparation technology is simple, cost is cheap, nothing
Color is tasteless, environment-friendly and low-toxicity, the advantages that not developed immunity to drugs to mosquito spray water mosquito-repellent incense.
For above-mentioned technical problem, technical scheme provided by the invention is specific as follows：A kind of spray water mosquito-repellent incense composition and
Its preparation method, it is made up of each component of following percentage by weight：Pyrethrins 0.01~2%；Pyrethroid 0.01~
2%；Thixotropic agent 5~20%；Distilled water 70~95%.
Preferably, the thixotropic agent is modified hydrogenated castor oil, is advantageous to pyrethrins and pyrethroid preferably hangs
It is floating, there is good anti-settling property and storage stability.
Preferably, the pyrethroid is etrafluorine ethofenprox, fluorine chlorine ether chrysanthemum ester, dimefluthrin or seven fluorine methyl ether chrysanthemums
One kind in ester, repelling effect are more preferable.
Present invention also offers a kind of preparation method of spray water mosquito-repellent incense composition, comprise the following steps：S1, measure spraying
The each component of water mosquito-repellent incense composition, first pyrethrins, pyrethroid and thixotropic agent are mixed 10~15 minutes；S2, general
Continue stirring 15~20 minutes in the mixture that distilled water is added in step S1, that is, a kind of spray water mosquito-repellent incense is made.
Compared with prior art, the beneficial effects of the present invention are：Colorless and odorless, it is harmless；It is environment-friendly and low-toxicity, to ring
Border is very friendly；Mosquito repelling efficiency time is grown, and not developed immunity to drugs；Preparation method is simple, and cost is cheap, has height
The advantages of imitating, be environmentally friendly, possesses good market prospects.
Embodiment
In order that those skilled in the art is better understood from technical scheme, implement below by specific implementation
Technical scheme is further explained, following examples are merely to illustrate the present invention, without restricted.
Embodiment one：A kind of spray water mosquito-repellent incense composition, the percentage by weight of wherein each component are as follows：
Pyrethrins 0.5%；
Etrafluorine ethofenprox 0.3%；
Modified hydrogenated castor oil 8%；
Distilled water 91.2%；
After pyrethrins, etrafluorine ethofenprox and modified hydrogenated castor oil are mixed 10 minutes, add distilled water and continue
Stirring 15 minutes, that is, be made a kind of spray water mosquito-repellent incense.
Embodiment two：A kind of spray water mosquito-repellent incense composition, the percentage by weight of wherein each component are as follows：
Pyrethrins 0.5%；
Fluorine chlorine ether chrysanthemum ester 0.5%；
Modified hydrogenated castor oil 8%；
Distilled water 91%；
After pyrethrins, fluorine chlorine ether chrysanthemum ester and modified hydrogenated castor oil are mixed 12 minutes, add distilled water and continue
Stirring 15 minutes, that is, be made a kind of spray water mosquito-repellent incense.
Embodiment three：A kind of spray water mosquito-repellent incense composition, the percentage by weight of wherein each component are as follows：
Pyrethrins 0.6%；
Dimefluthrin 0.4%；
Modified hydrogenated castor oil 7%；
Distilled water 92%；
By pyrethrins, dimefluthrin and modified hydrogenated castor oil mix 11 minutes after, add distilled water after
Continuous stirring 17 minutes, that is, be made a kind of spray water mosquito-repellent incense.
Example IV：A kind of spray water mosquito-repellent incense composition, the percentage by weight of wherein each component are as follows：
Pyrethrins 0.5%；
Seven fluorine methothrins 0.2%；
Modified hydrogenated castor oil 8%；
Distilled water 91.3%；
By pyrethrins, seven fluorine methothrins and modified hydrogenated castor oil mix 12 minutes after, add distilled water after
Continuous stirring 16 minutes, that is, be made a kind of spray water mosquito-repellent incense.
Test experiments one：
With square 100cmx100cmx100cm lucite square chest four, each 50 of Culex pipiens pallens, each case are respectively put into
Different formulations water mosquito-repellent incense in ultrasonic intelligent eluting device and embodiment one to four is put into, opens normal sustained release program, observation
The state of the Culex pipiens pallens of each hour, test data such as table 1 below:
As can be seen from Table 1, embodiment 1~4 has fine repelling effect, because being sustained moisture content only 0.1 of cold spray
~0.3 micron, mosquito wing in sporting flying can touch cold spray mist, can quickly be knocked down, due to cold spray drug effect
It is not denatured, and incense coil, ant perfume, electric mosquito repellent tablet and mosquito liquid high temperature change its drug effect, dosage is big, compares down,
The dosage of the present invention reduces by the magnitudes such as ten, has reached environmentally friendly, hygienic and safe to use effect.
Test experiments two：
In 53 square metres of mutually synthermal laboratories, the fine and closely woven ventilative of the identical 10x10cm specifications of a size is respectively put
Netted windows platforms be used for place ultrasonic intelligent eluting device, respectively put the identical 40x20cm specifications of a size wicket and
The observation window of 10x10cm specifications.
20 young age small white mouses are pacified into each two of male and female to be put in 5 laboratories, and are divided into 1 control group and 4 tests
Group, test group respectively put different formulations water mosquito-repellent incense in the embodiment of the present invention one to four, and the ultrasonic intelligent sustained release of 4 test groups is set
Standby spray water mosquito-repellent incense amount pharmaceutical quantities are adjusted to 2 times of usual indoor sanitation mosquito repellent dosage, daily 12 hours program intelligence by program
Sustained release, be used continuously 60 days, the cleaning of laboratory one day once, and records young age Mice weight condition daily, to control group and
Body weight, fed state, active degree and the Behavioral change of the young age small white mouse of test group carry out detailed comparison, and its biology is referred to
Mark is detected and examined, and input computer of filing carries out data analysis, and do not note abnormalities situation.5 groups of young age small white mouses are weekly
Blood test contrasts once, and every biochemical indicator is normal, shows that mosquito-repellent incense of the present invention has no toxic side effect to young age small white mouse, obtains
Go out conclusion：Long-term use of present invention is to young age small white mouse without any toxicity.
Test experiments three：
Acute oral toxicity test is carried out to the young age small white mouse in 4 test groups in test experiments two, by the present invention
The water mosquito-repellent incense liquid of embodiment one to four LD50 carried out to the young age small white mouse of test group be more than 5000 mgs/kg of contaminations,
Activities in rats amount increase in ten minutes, continues 40 minutes or so, activity switchs to normally, and diet is normal, 60 days observation periods nothing after contamination
It is dead.
Testing experiment four：
Dermal application experiment is carried out to the young age small white mouse in 4 test groups in test experiments three, by the reality of the present invention
The water mosquito-repellent incense liquid of example one to four is applied to 200 milligrams of Tu foam on the young age mouse skin of test group, is spaced 5 minutes, continuous 3
Secondary, there is not erythema and oedema shape condition in skin after a hour, illustrates that the water mosquito-repellent incense liquid of the present invention is non-stimulated to skin
Effect.
Embodiments of the invention one have carried out a huge sum of money to the spray water mosquito-repellent incense liquid of example IV by GB2750-2011 requirements
Category picks up survey, and testing result is shown in Table 2 and arrives table 5.
Table 2：
Table 3：
Table 4：
Table 5：
The evaluation result of table 2 to table 5 is qualified.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all essences in the present invention
All any modification, equivalent and improvement done within refreshing and principle etc., should be included in the scope of the protection.
Claims (4)
1. a kind of spray water mosquito-repellent incense composition, it is characterised in that be made up of each component of following percentage by weight：Pyrethrins
0.01~2%；Pyrethroid 0.01 ~ 2%；Thixotropic agent 5 ~ 20%；Distilled water 70 ~ 95%, the weight of above each component are equal to than sum
100%。
2. spray water mosquito-repellent incense composition according to claim 1, it is characterised in that：The thixotropic agent is modified hydrogenated castor-oil plant
Oil.
3. spray water mosquito-repellent incense composition according to claim 1, it is characterised in that：The pyrethroid is tetrafluoro ether chrysanthemum
One kind in ester, fluorine chlorine ether chrysanthemum ester, dimefluthrin or seven fluorine methothrins.
4. according to any one of claim 1-3 spray water mosquito-repellent incense combination preparation method, it is characterised in that including with
Lower step：
S1, each component for measuring spray water mosquito-repellent incense composition, pyrethrins, pyrethroid and thixotropic agent are first mixed 10
~ 15 minutes；
Continue stirring 15 ~ 20 minutes in S2, the mixture for adding distilled water in step S1, that is, a kind of spray water mosquito-repellent incense is made.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710635708.8A CN107372576A (en) | 2017-07-31 | 2017-07-31 | A kind of spray water mosquito-repellent incense composition and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710635708.8A CN107372576A (en) | 2017-07-31 | 2017-07-31 | A kind of spray water mosquito-repellent incense composition and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107372576A true CN107372576A (en) | 2017-11-24 |
Family
ID=60342353
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710635708.8A Pending CN107372576A (en) | 2017-07-31 | 2017-07-31 | A kind of spray water mosquito-repellent incense composition and preparation method thereof |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1745635A (en) * | 2005-10-11 | 2006-03-15 | 华中师范大学 | Water-base long-effective sanitary insecticide |
| CN102283242A (en) * | 2011-09-05 | 2011-12-21 | 中山榄菊日化实业有限公司 | Water-based mosquito-repellent incense and preparation method thereof |
| CN102669155A (en) * | 2012-05-14 | 2012-09-19 | 中山榄菊日化实业有限公司 | Alternative drug using mosquito-repellent incense and preparation method thereof |
| CN102742572A (en) * | 2012-07-27 | 2012-10-24 | 广州立白企业集团有限公司 | Water-based electric heating liquid mosquito-repellent incense and preparation method thereof |
| CN105831137A (en) * | 2016-03-31 | 2016-08-10 | 广东新景象生物工程有限公司 | Insecticidal composition containing destruxins and diflubenzuron, and preparation method and application thereof |
-
2017
- 2017-07-31 CN CN201710635708.8A patent/CN107372576A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1745635A (en) * | 2005-10-11 | 2006-03-15 | 华中师范大学 | Water-base long-effective sanitary insecticide |
| CN102283242A (en) * | 2011-09-05 | 2011-12-21 | 中山榄菊日化实业有限公司 | Water-based mosquito-repellent incense and preparation method thereof |
| CN102669155A (en) * | 2012-05-14 | 2012-09-19 | 中山榄菊日化实业有限公司 | Alternative drug using mosquito-repellent incense and preparation method thereof |
| CN102742572A (en) * | 2012-07-27 | 2012-10-24 | 广州立白企业集团有限公司 | Water-based electric heating liquid mosquito-repellent incense and preparation method thereof |
| CN105831137A (en) * | 2016-03-31 | 2016-08-10 | 广东新景象生物工程有限公司 | Insecticidal composition containing destruxins and diflubenzuron, and preparation method and application thereof |
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Application publication date: 20171124 |
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