CN107356777A - A kind of sampling device - Google Patents

A kind of sampling device Download PDF

Info

Publication number
CN107356777A
CN107356777A CN201710483106.5A CN201710483106A CN107356777A CN 107356777 A CN107356777 A CN 107356777A CN 201710483106 A CN201710483106 A CN 201710483106A CN 107356777 A CN107356777 A CN 107356777A
Authority
CN
China
Prior art keywords
needle
headspace bottle
cartridge heater
air
gear unit
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710483106.5A
Other languages
Chinese (zh)
Inventor
展义胜
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Priority to CN201710483106.5A priority Critical patent/CN107356777A/en
Publication of CN107356777A publication Critical patent/CN107356777A/en
Pending legal-status Critical Current

Links

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N35/00Automatic analysis not limited to methods or materials provided for in any single one of groups G01N1/00 - G01N33/00; Handling materials therefor
    • G01N35/10Devices for transferring samples or any liquids to, in, or from, the analysis apparatus, e.g. suction devices, injection devices

Landscapes

  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

The present invention relates to a kind of sampling device, including ml headspace bottle, air-out needle and the air inlet needle being connected respectively with transmission mechanism, ml headspace bottle is set to the cylinder that vertical cross-section is inverted trapezoidal, the bottle mouth position of ml headspace bottle is provided with sealing catch, air inlet needle is connected with gas source conduit, valve body and fluid velocity meter are provided with gas source conduit, gas source conduit is connected with source of the gas, air-out needle is connected by outtake tube with detecting instrument, transmission mechanism includes downward gear unit and upward gear unit, and the bottom of ml headspace bottle is arranged in cartridge heater;It has testing result precision high, and operating efficiency is high, simple to operate, has a safety feature, disclosure satisfy that actually detected requirements of one's work.

Description

A kind of sampling device
Technical field
The invention belongs to detection device technology field, is related to a kind of sampling device.
Background technology
At present, in headspace analysis operation, the conventional gas by above sample substrate is sent to headspace analysis detection and set Sample is first placed in closed container and heated, reach heat more using sample introduction operation of knocking off by the standby middle sample introduction work detected A certain amount of sample is extracted with syringe after poised state, the sample is taken rapidly on analyzer and tested and analyzed, the party There is the problems such as analysis testing result error is big, and operating efficiency is low in method, for this reason, it may be necessary to which one kind can solve the problem that in the prior art The sampling device of problem is stated, meets actually detected requirements of one's work.
The content of the invention
It is an object of the present invention to provide a kind of sampling device, solving that testing result error is big, and operating efficiency is low etc. asks Topic, greatly reduces its measuring result error, operating efficiency greatly improves, to meet actually detected requirements of one's work.
To achieve the above object, the present invention provides a kind of sampling device, including the head space being connected respectively with transmission mechanism Bottle, air-out needle and air inlet needle, ml headspace bottle are set to the cylinder that vertical cross-section is inverted trapezoidal, and the bottle mouth position of ml headspace bottle is provided with sealing and kept off Piece, air inlet needle are connected with gas source conduit, are provided with valve body at gas source conduit and fluid velocity meter, gas source conduit are connected with source of the gas Connecing, air-out needle is connected by outtake tube with detecting instrument, and transmission mechanism includes downward gear unit and upward gear unit, The bottom of ml headspace bottle is arranged in cartridge heater, and the bottom on the inside of cartridge heater is provided with heat block, and the bottom on the outside of cartridge heater is provided with solid The base being scheduled on upward gear unit, ml headspace bottle are connected by base with upward gear unit, the outer periphery of cartridge heater Be arranged with collet, the outer sheath of ml headspace bottle is provided with constant temperature sleeve, opening position that air inlet needle is connected with gas source conduit, air-out needle with The opening position that outtake tube is connected is equipped with fixture, and fixture is connected by fixed plate with underdrive unit, upper transmission Positioning and locking part is equipped with unit and underdrive unit, air-out needle and air inlet needle include syringe and syringe needle, syringe and syringe needle Junction is provided with seal nipple, and syringe needle is connected by compaction hoop at seal nipple with syringe.
In above scheme preferably, cartridge heater is set to the structure with inner hollow chamber, is provided with hollow chamber Electrical heating wire.
It may also be preferred that the madial wall of the inner hollow chamber of cartridge heater and the top of heat block are exhausted provided with integral type Edge sealant.
It may also be preferred that cartridge heater is interior, the periphery of ml headspace bottle is uniformly provided with water-circulating pipe.
It may also be preferred that cartridge heater uses cylinder of the vertical cross-section for inverted trapezoidal, and with the bottom phase of ml headspace bottle Matching.
It may also be preferred that positioning and locking part uses tight locking button or ring gear keeper.
It may also be preferred that transmission mechanism is using the combined structure of guide rail and motor.
The sampling device of the present invention, can solve the problem that the problems such as testing result error is big, and operating efficiency is low, and it has detection As a result precision is high, and operating efficiency is high, simple to operate, has a safety feature, disclosure satisfy that actually detected requirements of one's work.
Brief description of the drawings
The invention will be further described with embodiment below in conjunction with the accompanying drawings:
Fig. 1 is the structural representation of the sampling device of the present invention.
In figure, 1 is transmission mechanism, and 2 be ml headspace bottle, and 3 be air-out needle, and 4 be air inlet needle, and 5 be sealing catch, and 6 lead for source of the gas Pipe, 7 be source of the gas, and 8 be outtake tube, and 9 be detecting instrument, and 10 be cartridge heater, and 11 be base, and 12 be collet, and 13 be constant temperature sleeve, 14 be fixture, and 15 be fixed plate.
Embodiment
For a better understanding of the present invention, the present invention is explained in detail with reference to specific embodiment.It is clear that Different modifications can be carried out to the present invention with remodeling and without departing from the broader spirit of the invention and model of appended claims Enclose.Therefore, following examples have exemplary without the implication of limitation.
Embodiment 1:
A kind of sampling device, including ml headspace bottle 2, air-out needle 3 and the air inlet needle 4 being connected respectively with transmission mechanism 1, ml headspace bottle 2 The cylinder that vertical cross-section is inverted trapezoidal is set to, the bottle mouth position of ml headspace bottle 2 is provided with sealing catch 5, air inlet needle 4 and gas source conduit 6 It is connected, valve body and fluid velocity meter is provided with gas source conduit 6, gas source conduit 6 is connected with source of the gas 7, and air-out needle 3 passes through outlet Conduit 8 is connected with detecting instrument 9, and transmission mechanism 1 includes downward gear unit and upward gear unit, the bottom of ml headspace bottle 2 Be arranged in cartridge heater 10, the bottom of the inner side of cartridge heater 10 is provided with heat block, the bottom in the outside of cartridge heater 10 provided be fixed on to Base 11 on upper gear unit, ml headspace bottle 2 are connected by base 11 with upward gear unit, the outer periphery of cartridge heater 10 Collet 12 is arranged with, the outer sheath of ml headspace bottle 2 is provided with constant temperature sleeve 13, opening position that air inlet needle 4 is connected with gas source conduit 6, Air-out needle 3 is equipped with fixture 14 with the opening position that outtake tube 8 is connected, and fixture 14 passes through fixed plate 1 and underdrive list Member is connected, and positioning and locking part is equipped with upper gear unit and underdrive unit, and air-out needle 3 and air inlet needle 4 include syringe And syringe needle, syringe and syringe needle junction are provided with seal nipple, syringe needle is connected by compaction hoop at seal nipple with syringe.

Claims (2)

1. a kind of sampling device, including respectively with transmission mechanism(1)The ml headspace bottle being connected(2), air-out needle(3)And air inlet needle (4), it is characterised in that:Ml headspace bottle(2)It is set to the cylinder that vertical cross-section is inverted trapezoidal, ml headspace bottle(2)Bottle mouth position be provided with it is close Block piece(5), air inlet needle(4)With gas source conduit(6)It is connected, gas source conduit(6)Place is provided with valve body and fluid velocity meter, source of the gas Conduit(6)With source of the gas(7)It is connected, air-out needle(3)Pass through outtake tube(8)With detecting instrument(9)It is connected, transmission mechanism (1)Including downward gear unit and upward gear unit, ml headspace bottle(2)Bottom be arranged on cartridge heater(10)In, cartridge heater (10)The bottom of inner side is provided with heat block, cartridge heater(10)The bottom in outside is provided with the base being fixed on upward gear unit (11), ml headspace bottle(2)Pass through base(11)It is connected with upward gear unit, cartridge heater(10)Outer periphery be arranged with it is heat-insulated Set(12), ml headspace bottle(2)Outer sheath be provided with constant temperature sleeve(13), air inlet needle(4)With gas source conduit(6)The opening position that is connected, Air-out needle(3)The opening position being connected with outtake tube (8) is equipped with fixture(14), fixture(14)Pass through fixed plate(1) It is connected with underdrive unit, positioning and locking part, air-out needle is equipped with upper gear unit and underdrive unit(3)And air inlet needle (4)Include syringe and syringe needle, syringe and syringe needle junction are provided with seal nipple, syringe needle by compaction hoop at seal nipple with Syringe connects;Positioning and locking part uses tight locking button or ring gear keeper;Cartridge heater(10)Use circle of the vertical cross-section for inverted trapezoidal Cylinder, and and ml headspace bottle(2)Bottom match;Transmission mechanism(1)Using the structure that guide rail and motor are combined.
2. sampling device as claimed in claim 1, it is characterised in that:Cartridge heater(10)It is set to the knot with inner hollow chamber Structure, electrical heating wire, cartridge heater are provided with hollow chamber(10)The madial wall of inner hollow chamber and the top of heat block be provided with Integral type insulated enclosure layer, cartridge heater(10)Interior, ml headspace bottle periphery is uniformly provided with water-circulating pipe.
CN201710483106.5A 2017-06-23 2017-06-23 A kind of sampling device Pending CN107356777A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710483106.5A CN107356777A (en) 2017-06-23 2017-06-23 A kind of sampling device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710483106.5A CN107356777A (en) 2017-06-23 2017-06-23 A kind of sampling device

Publications (1)

Publication Number Publication Date
CN107356777A true CN107356777A (en) 2017-11-17

Family

ID=60273575

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201710483106.5A Pending CN107356777A (en) 2017-06-23 2017-06-23 A kind of sampling device

Country Status (1)

Country Link
CN (1) CN107356777A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109374770A (en) * 2018-11-15 2019-02-22 杭州邦沃森生物科技有限公司 A kind of detection method of Turtle Oil volatile component

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109374770A (en) * 2018-11-15 2019-02-22 杭州邦沃森生物科技有限公司 A kind of detection method of Turtle Oil volatile component

Similar Documents

Publication Publication Date Title
JP2018500535A (en) Detection device and detection method
MX2007003391A (en) Method and apparatus for blood sampling.
CN103675080A (en) Headspace sampler and ion mobility spectrometry combined system
CN103454125A (en) System and method for measuring hydrogen content in a sample
CN105823820B (en) Catalyst test apparatus
CN103191795A (en) Distillation apparatus
CN106645369B (en) A kind of on-line detector
CN107356777A (en) A kind of sampling device
CN111024483A (en) Chlorosilane pretreatment system and method for detecting impurity content in chlorosilane
CN102323303B (en) Experimental apparatus and method for testing gas-sensitive temperature characteristic of carbon nanotube sensor
CN204088259U (en) A kind of sampling device be separated with parsing for the preheating of ion mobility spectrometry
CN109238794A (en) A kind of automatic sampling apparatus of shock tube pyrolysis product
CN106542600B (en) Simple and accurate laboratory deoxygenation device and method
CN108982397B (en) A kind of gas-detecting device and method
CN103994917A (en) Heating device used on rock pyrolysis instrument
CN201935928U (en) Automatic liquid sample feeder of sampling tube
CN104165875A (en) Support applied to testing of solid-state fluorescence samples
CN106769346B (en) Method for analyzing hydrogen isotopes in water
CN106442091B (en) Device based on volatile organic trace compounds in hot gas blow-off method enrichment aqueous solid
CN204854967U (en) A infrared temperature measurement device for high temperature alloy temperature measurement
CN205080147U (en) Detect and use head space sampling device
CN107449930A (en) Liquid sample-reserving and sampling device
JP4653286B2 (en) Assemblies for detaching sampling vials, adapters and sampling vials explicitly intended for said assemblies, and parts kit for forming said assemblies
CN206862704U (en) A kind of portable sampler
CN102539636A (en) Deodorization performance testing system and operating method thereof

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20171117

WD01 Invention patent application deemed withdrawn after publication