CN107345084A - A kind of indigo dye made of indigo herb and preparation method thereof - Google Patents
A kind of indigo dye made of indigo herb and preparation method thereof Download PDFInfo
- Publication number
- CN107345084A CN107345084A CN201710642313.0A CN201710642313A CN107345084A CN 107345084 A CN107345084 A CN 107345084A CN 201710642313 A CN201710642313 A CN 201710642313A CN 107345084 A CN107345084 A CN 107345084A
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- indigo
- herb
- pteridophyte
- ethanol
- dye
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0071—Process features in the making of dyestuff preparations; Dehydrating agents; Dispersing agents; Dustfree compositions
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0071—Process features in the making of dyestuff preparations; Dehydrating agents; Dispersing agents; Dustfree compositions
- C09B67/0077—Preparations with possibly reduced vat, sulfur or indigo dyes
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Coloring (AREA)
Abstract
The invention provides a kind of indigo dye made of indigo herb and preparation method thereof; it is by mass percentage; it is made up of indigo 15 30%, the double sodium starch 10 18% of acetylation diacid, pteridophyte ash 10 18%, ethanol 7 17%, water; its each component degree sum is 100%; it is more preferable that dyestuff coloring is made in it; the cloth color and luster dyed is bright and new gorgeous, is not easy to fade.
Description
Technical field
The invention belongs to dyestuff processing technique field, and in particular to a kind of indigo dye made of indigo herb and preparation method thereof.
Background technology
Indigo is a kind of careless art plant, and its cultivation and being produced in Yao nationality people has a long history, the master of indigo
It is to dye cloth to want purposes, also pharmaceutically acceptable.Precious jade man indigo not only oneself uses, and also takes as product and is sold on fairground, is a small number of people
The dyestuff that race special procures.Indigo seed is tiny, is similar to China fir art kind, is collected seed after March is clear and bright, and May, site preparation buried moisture in the soil scaffolding seedling, and seven
Transplanted to August.Transplanting in taro and mountain valley with clumps of trees and bamboo limes marginis, is advisable with the place that soil property is moist mostly.The chi of indigo plant height two to three, school
Leaf bar extraction is green, and its taste fragrance, exclusive characteristic, seven to August tap immersion.
In most of China region, all useful indigo is come the tradition dying cloth, contaminate silk and tailor, in China much
Square is among the people, and particularly dyestuff is made to dye cloth in minority area, all useful indigo, the tradition of sewing clothes, especially position
Black clothing in Guangxi Napo County is strengthened, the Typical Representative for sewing clothes of even more being dyed cloth with indigo, and they are advocated with black for U.S., so far still
The most traditional, the most Zhuang nationality dress of feature and intension is so maintain, is exactly black dress ornament, this cloth made of indigo is dyed cloth
Dress ornament is made, wears with mosquito-proof sting, cool in summer and warm in winter, easy cleaning, it is wear-resisting the effect of.As rural tourism culture is produced
The development of industry, the people are increasingly favored national wind dress ornament, and therefore, carrying out indigo dye made of indigo herb industry has preferable market value,
But traditional indigo dye made of indigo herb and cloth dyeing technology has cumbersome, the cloth color and luster dyed is not bright-coloured, the defects of being particularly easy to fade.
The content of the invention
The present invention is in order to solve the above problems, there is provided a kind of indigo dye made of indigo herb, its by mass percentage, 15- containing indigo
30%th, the double sodium starch 10-18% of acetylation diacid, pteridophyte ash 10-18%, ethanol 7-17%, water are made, its each component hundred
It is 100% to divide than content sum.
Specifically：A kind of indigo dye made of indigo herb, its by mass percentage, the double sodium starch of 20-25% containing indigo, acetylation diacid
13-15%, pteridophyte 13-15%, ethanol 10-14% and water are made, and its each component degree sum is 100%.
Again specifically, a kind of indigo dye made of indigo herb, its by mass percentage, containing indigo 22%, the double sodium starch of acetylation diacid
14%th, pteridophyte 14%, ethanol 12% and water are made, and its each component degree sum is 100%.
Pteridophyte ash described above is that the ashes being fired into is dried by pteridophyte.
Present invention also offers a kind of preparation method of indigo dye made of indigo herb, comprise the following steps：Indigo be put into dye vat is added
Enter 50-60 DEG C, add the double sodium starch of pteridophyte ash, acetylation diacid, ethanol, water and stir, indigo dye made of indigo herb.
Further, the preparation method of described indigo dye made of indigo herb, comprises the following steps：Indigo be put into dye vat is added 55
DEG C, add the double sodium starch of pteridophyte ash, acetylation diacid, ethanol, water and stir, indigo dye made of indigo herb.
Beneficial effects of the present invention are：
More preferably, the cloth color and luster dyed is bright and new gorgeous, is not easy to fade for the dyestuff coloring of the invention obtained.
Embodiment：
The present invention is by the way that below by embodiment and experimental example, the present invention will be further elaborated.It is necessary herein means
What is gone out is that the present embodiment is served only for being described further invention, it is impossible to is interpreted as limiting the scope of the invention.
Embodiment 1：The preparation of indigo dye made of indigo herb：
By mass percentage, will take 15% it is indigo be put into dye vat add 50 DEG C, add 10% pteridophyte ash,
The double sodium starch of 10% acetylation diacid, 7% ethanol, 58% water stir, indigo dye made of indigo herb.
Embodiment 2：The preparation of indigo dye made of indigo herb：
By mass percentage, will take 20% it is indigo be put into dye vat add 50 DEG C, add 13% pteridophyte ash,
The double sodium starch of 13% acetylation diacid, 10% ethanol, 44% water stir, indigo dye made of indigo herb.
Embodiment 3：The preparation of indigo dye made of indigo herb：
By mass percentage, will take 22% it is indigo be put into dye vat add 50 DEG C, add 14% pteridophyte ash,
The double sodium starch of 14% acetylation diacid, 12% ethanol, 38% water stir, indigo dye made of indigo herb.
Embodiment 4：The preparation of indigo dye made of indigo herb：
By mass percentage, will take 25% it is indigo be put into dye vat add 50 DEG C, add 15% pteridophyte ash,
The double sodium starch of 15% acetylation diacid, 14% ethanol, 31% water stir, indigo dye made of indigo herb.
Embodiment 5：The preparation of indigo dye made of indigo herb：
By mass percentage, will take 30% it is indigo be put into dye vat add 50 DEG C, add 18% pteridophyte ash,
The double sodium starch of 18% acetylation diacid, 17% ethanol, 17% water stir, indigo dye made of indigo herb.
Embodiment 6：The preparation of indigo dye made of indigo herb：
By mass percentage, will take 22% it is indigo be put into dye vat add 50 DEG C, add 14% pteridophyte ash,
12% ethanol, 38% water stir, indigo dye made of indigo herb.
Experimental example：Dyestuff produced by the present invention is investigated：
Using by dyestuff made from 1-6 of the embodiment of the present invention with method dyed cloth, control group：Dyed for traditional indigo dye made of indigo herb
Cloth, then cloth is used containing 20% alcohol solution dipping 1h, observe discoloration, experimental result such as table 1 below：
| Experimental group | Cloth color and luster | Cloth color and luster situation is soaked through 20% ethanol |
| Experimental group 1 | It is bright in colour | Ethanol solution is in light blue |
| Experimental group 2 | It is bright in colour, relatively bright | Ethanol solution is in light blue |
| Experimental group 3 | Lovely luster, become clear | Ethanol solution is in micro- light blue |
| Experimental group 4 | It is bright in colour, relatively bright | Ethanol solution is in micro- light blue |
| Experimental group 5 | It is bright in colour, relatively bright | Ethanol solution is in micro- light blue |
| Experimental group 6 | Blueness, color are dark | Blueness |
| Control group | Blueness | Blueness |
Above-mentioned experiment shows：Indigo dye made of indigo herb produced by the present invention is used for dyed cloth, and it is bright in colour, becomes clear, and be not easy
Fade.
Claims (6)
- A kind of 1. indigo dye made of indigo herb, it is characterised in that：By mass percentage, the double sodium starch of 15-30% containing indigo, acetylation diacid 10-18%, pteridophyte ash 10-18%, ethanol 7-17%, water are made, and its each component degree sum is 100%.
- A kind of 2. indigo dye made of indigo herb according to claim 1, it is characterised in that：By mass percentage, 20- containing indigo 25%th, acetylation diacid double sodium starch 13-15%, pteridophyte 13-15%, ethanol 10-14% and water are made, its each component hundred It is 100% to divide than content sum.
- A kind of 3. indigo dye made of indigo herb according to claim 1 or 2, it is characterised in that：By mass percentage, containing indigo 22%th, acetylation diacid double sodium starch 14%, pteridophyte 14%, ethanol 12% and water are made, its each component degree Sum is 100%.
- 4. according to any described indigo dye made of indigo herb of claim 1-3, it is characterised in that：The pteridophyte ash is by pteridophyte Dry the ashes being fired into.
- A kind of 5. preparation method of indigo dye made of indigo herb, it is characterised in that：Comprise the following steps：Indigo be put into dye vat is added into 50- 60 DEG C, add the double sodium starch of pteridophyte ash, acetylation diacid, ethanol, water and stir, indigo dye made of indigo herb.
- 6. the preparation method of indigo dye made of indigo herb according to claim 5, it is characterised in that：Comprise the following steps：Put indigo Enter and 55 DEG C added in dye vat, add the double sodium starch of pteridophyte ash, acetylation diacid, ethanol, water and stir, indigo Dyestuff.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710642313.0A CN107345084A (en) | 2017-07-31 | 2017-07-31 | A kind of indigo dye made of indigo herb and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710642313.0A CN107345084A (en) | 2017-07-31 | 2017-07-31 | A kind of indigo dye made of indigo herb and preparation method thereof |
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| Publication Number | Publication Date |
|---|---|
| CN107345084A true CN107345084A (en) | 2017-11-14 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201710642313.0A Pending CN107345084A (en) | 2017-07-31 | 2017-07-31 | A kind of indigo dye made of indigo herb and preparation method thereof |
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Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20100034757A1 (en) * | 2006-11-24 | 2010-02-11 | Mitsukiyo Fujii | Extract powder of indigo plant, and its preparation and uses |
| CN102918199A (en) * | 2010-03-09 | 2013-02-06 | 科莱恩金融(Bvi)有限公司 | Combined warp sizing and fixing agent and new method for fixing sulfur dyestuffs on warp |
| CN102911516A (en) * | 2012-10-23 | 2013-02-06 | 杨昌标 | Indigo dye and dying method thereof |
| CN103013167A (en) * | 2012-12-25 | 2013-04-03 | 郭瑞 | Preparation method and application of natural plant indigotin dye |
| CN104017436A (en) * | 2014-05-28 | 2014-09-03 | 南昌大学 | Children pigment composed of edible composition |
| CN105064075A (en) * | 2015-09-01 | 2015-11-18 | 莫玉明 | Process for dyeing cloth by using indigo |
| CN105586789A (en) * | 2014-10-24 | 2016-05-18 | 邵杰 | Environmental-friendly type dyeing sizing agent |
-
2017
- 2017-07-31 CN CN201710642313.0A patent/CN107345084A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20100034757A1 (en) * | 2006-11-24 | 2010-02-11 | Mitsukiyo Fujii | Extract powder of indigo plant, and its preparation and uses |
| CN102918199A (en) * | 2010-03-09 | 2013-02-06 | 科莱恩金融(Bvi)有限公司 | Combined warp sizing and fixing agent and new method for fixing sulfur dyestuffs on warp |
| CN102911516A (en) * | 2012-10-23 | 2013-02-06 | 杨昌标 | Indigo dye and dying method thereof |
| CN103013167A (en) * | 2012-12-25 | 2013-04-03 | 郭瑞 | Preparation method and application of natural plant indigotin dye |
| CN104017436A (en) * | 2014-05-28 | 2014-09-03 | 南昌大学 | Children pigment composed of edible composition |
| CN105586789A (en) * | 2014-10-24 | 2016-05-18 | 邵杰 | Environmental-friendly type dyeing sizing agent |
| CN105064075A (en) * | 2015-09-01 | 2015-11-18 | 莫玉明 | Process for dyeing cloth by using indigo |
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Application publication date: 20171114 |