CN107053413A - A kind of method for improving maize peel dyeing rate - Google Patents
A kind of method for improving maize peel dyeing rate Download PDFInfo
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- CN107053413A CN107053413A CN201710226013.4A CN201710226013A CN107053413A CN 107053413 A CN107053413 A CN 107053413A CN 201710226013 A CN201710226013 A CN 201710226013A CN 107053413 A CN107053413 A CN 107053413A
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K9/00—Chemical or physical treatment of reed, straw, or similar material
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K3/00—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
- B27K3/34—Organic impregnating agents
- B27K3/50—Mixtures of different organic impregnating agents
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K5/00—Treating of wood not provided for in groups B27K1/00, B27K3/00
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K5/00—Treating of wood not provided for in groups B27K1/00, B27K3/00
- B27K5/0015—Treating of wood not provided for in groups B27K1/00, B27K3/00 by electric means
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K5/00—Treating of wood not provided for in groups B27K1/00, B27K3/00
- B27K5/02—Staining or dyeing wood; Bleaching wood
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Forests & Forestry (AREA)
- Coloring (AREA)
Abstract
The invention discloses a kind of method for improving maize peel dyeing rate, including：(1) suffocating treatment（2）Immersion treatment：(3) illumination and sided corona treatment.By the processing of each step of the invention so that the dyeing rate of maize peel is significantly improved.
Description
Technical field
The invention belongs to maize peel staining technique field, and in particular to a kind of method of raising maize peel dyeing rate.
Background technology
Maize peel is a kind of important wicker plaiting article raw material, and maize peel has excellent pliability and tensile strength, very suitable
Close and carry out wicker plaiting article, but maize peel is difficult to be dyed, dyeing rate is slow, therefore causes the color of product single, or dyeing
Afterwards, maize peel irregular colour is even, influences the ornamental quality of flax and cornstraw weaving fabric.
The content of the invention
The purpose of the present invention is that there is provided a kind of method for improving maize peel dyeing rate the problem of being directed to existing.
The present invention is achieved by the following technical solutions：
A kind of method for improving maize peel dyeing rate, comprises the following steps：
（1）Suffocating treatment
Maize peel is put into fumatorium, Chinese Toon Leaves are put into burner, stifling indoor humidity is kept with sprayer spraying
For 80%, Chinese Toon Leaves in point burner, closed stifling 2 hours afterburners stop, and stand after 20min, take out maize peel；
（2）Immersion treatment
Will be through step（1）Maize peel after processing carries out immersion treatment at different temperatures using soak, first puts maize peel
Enter in soak, temperature adjustment is incubated 30min to 80-85 DEG C, then by temperature quick regulation to 2-6 DEG C, be incubated 15min, then
By temperature adjustment to 60-62 DEG C, 2 hours are incubated, then by temperature adjustment to 40-44 DEG C, is incubated 1 hour, then dries to aqueous
Measure as 40-50%, the immersion liquid and preparation method thereof is：Red autumnal leaves blade of grass, purple leaf green pepper blade of grass, white arteries and veins green pepper blade of grass, cactus are pressed 1：2：
1：4 mass ratios are admixed together, are subsequently placed in the blanching 15min in 100 DEG C of hot water, after taking-up, 5 times of addition cactus quality
Clear water, mashing, obtains mixed serum, and the sodium carbonate of its quality 2.3%, 1.8% salt and 0.14% are added into mixed serum
Benzene sulfonic acid sodium salt, is incubated 15 min in boiling water bath, is subsequently cooled to room temperature, accesses the lactic acid bacteria of mixed serum quality 0.002%,
Fermented, fermentation temperature is 35 DEG C, and fermentation time is 3h, and separation of solid and liquid is then carried out under high speed centrifugation, mixed liquor is obtained,
The sodium hypochlorite of mixed liquor quality 0.26% is added, after 120r/min rotating speeds stirring 30min, 2 hours is stood at 30 DEG C, obtains
To soak；
（3）Illumination and sided corona treatment
Will be through step（2）Maize peel after processing carries out continuous light 2 hours using the white light of 800lux intensities of illumination, Ran Houzai
Maize peel is placed in corona field and handles 20-22min, corona field field strength is 300KV/m, then dries maize peel to water content
Less than 12%, normal dyeing then can be carried out.
Further, the Chinese toon leaf water content is less than 10%.
Further, the ultracentrifugal speed is 3000r/min.
Further, the maize peel is placed in when being handled in corona field, and environment temperature is 35 DEG C, relative air humidity is
45%。
The present invention has advantages below compared with prior art：, can by using the immersion treatment of soak to maize peel
The motion between maize peel surface molecular is effectively facilitated, molecule diffusion is more uniform, can significantly improve equal after corn leather dyeing
Even property, and can effectively strengthen the toughness and Resisting fractre ability of maize peel surface fiber, improve the use longevity of flax and cornstraw weaving fabric
Life, by the processing of each step of the invention so that the dyeing speed of maize peel is significantly improved, especially by step（3）Light
According to after sided corona treatment so that maize peel surface fiber has very high first dye speed, reaches that the time of dyeing equilibrium also shortens
, especially by the processing of corona so that corn wrapper fibre is easily wetted and is swelled in dyeing, has broken corn leather dyeing
Obstacle is broken, and the processing of corona field causes the specific surface area increase of fiber, and maize peel dyeing rate is improved, particularly in dyeing
Starting stage, but dyeing equilibrium adsorbance is constant.
Embodiment
Embodiment 1
A kind of method for improving maize peel dyeing rate, comprises the following steps：
（1）Suffocating treatment
Maize peel is put into fumatorium, Chinese Toon Leaves are put into burner, stifling indoor humidity is kept with sprayer spraying
For 80%, Chinese Toon Leaves in point burner, closed stifling 2 hours afterburners stop, and stand after 20min, take out maize peel；
（2）Immersion treatment
Will be through step（1）Maize peel after processing carries out immersion treatment at different temperatures using soak, first puts maize peel
Enter in soak, temperature adjustment is incubated 30min to 80 DEG C, then by temperature quick regulation to 2 DEG C, is incubated 15min, then by temperature
Degree regulation is incubated 2 hours to 60 DEG C, then by temperature adjustment to 40 DEG C, is incubated 1 hour, and it is 40%, institute then to dry to water content
Stating immersion liquid and preparation method thereof is：Red autumnal leaves blade of grass, purple leaf green pepper blade of grass, white arteries and veins green pepper blade of grass, cactus are pressed 1：2：1：4 mass ratios are mixed
It is combined together, is subsequently placed in the blanching 15min in 100 DEG C of hot water, after taking-up, adds cactus 5 times of clear water of quality, mashing is obtained
To mixed serum, the sodium carbonate of its quality 2.3%, 1.8% salt and 0.14% benzene sulfonic acid sodium salt are added into mixed serum, in
15 min are incubated in boiling water bath, room temperature is subsequently cooled to, the lactic acid bacteria of access mixed serum quality 0.002% is fermented, sent out
Ferment temperature is 35 DEG C, and fermentation time is 3h, and separation of solid and liquid is then carried out under high speed centrifugation, obtains mixed liquor, adds mixed liquor
The sodium hypochlorite of quality 0.26%, after 120r/min rotating speeds stirring 30min, stands 2 hours at 30 DEG C, obtains soak；
（3）Illumination and sided corona treatment
Will be through step（2）Maize peel after processing carries out continuous light 2 hours using the white light of 800lux intensities of illumination, Ran Houzai
Maize peel is placed in corona field and handles 20min, corona field field strength is 300KV/m, is then dried maize peel low to water content
In 12%, normal dyeing then can be carried out.
The Chinese toon leaf water content is less than 10%.
The ultracentrifugal speed is 3000r/min.
The maize peel is placed in when being handled in corona field, and environment temperature is 35 DEG C, relative air humidity is 45%.
Embodiment 2
A kind of method for improving maize peel dyeing rate, comprises the following steps：
（1）Suffocating treatment
Maize peel is put into fumatorium, Chinese Toon Leaves are put into burner, stifling indoor humidity is kept with sprayer spraying
For 80%, Chinese Toon Leaves in point burner, closed stifling 2 hours afterburners stop, and stand after 20min, take out maize peel；
（2）Immersion treatment
Will be through step（1）Maize peel after processing carries out immersion treatment at different temperatures using soak, first puts maize peel
Enter in soak, temperature adjustment is incubated 30min to 85 DEG C, then by temperature quick regulation to 6 DEG C, is incubated 15min, then by temperature
Degree regulation is incubated 2 hours to 62 DEG C, then by temperature adjustment to 44 DEG C, is incubated 1 hour, and it is 50%, institute then to dry to water content
Stating immersion liquid and preparation method thereof is：Red autumnal leaves blade of grass, purple leaf green pepper blade of grass, white arteries and veins green pepper blade of grass, cactus are pressed 1：2：1：4 mass ratios are mixed
It is combined together, is subsequently placed in the blanching 15min in 100 DEG C of hot water, after taking-up, adds cactus 5 times of clear water of quality, mashing is obtained
To mixed serum, the sodium carbonate of its quality 2.3%, 1.8% salt and 0.14% benzene sulfonic acid sodium salt are added into mixed serum, in
15 min are incubated in boiling water bath, room temperature is subsequently cooled to, the lactic acid bacteria of access mixed serum quality 0.002% is fermented, sent out
Ferment temperature is 35 DEG C, and fermentation time is 3h, and separation of solid and liquid is then carried out under high speed centrifugation, obtains mixed liquor, adds mixed liquor
The sodium hypochlorite of quality 0.26%, after 120r/min rotating speeds stirring 30min, stands 2 hours at 30 DEG C, obtains soak；
（3）Illumination and sided corona treatment
Will be through step（2）Maize peel after processing carries out continuous light 2 hours using the white light of 800lux intensities of illumination, Ran Houzai
Maize peel is placed in corona field and handles 22min, corona field field strength is 300KV/m, is then dried maize peel low to water content
In 12%, normal dyeing then can be carried out.
The Chinese toon leaf water content is less than 10%.
The ultracentrifugal speed is 3000r/min.
The maize peel is placed in when being handled in corona field, and environment temperature is 35 DEG C, relative air humidity is 45%.
Embodiment 3
A kind of method for improving maize peel dyeing rate, comprises the following steps：
（1）Suffocating treatment
Maize peel is put into fumatorium, Chinese Toon Leaves are put into burner, stifling indoor humidity is kept with sprayer spraying
For 80%, Chinese Toon Leaves in point burner, closed stifling 2 hours afterburners stop, and stand after 20min, take out maize peel；
（2）Immersion treatment
Will be through step（1）Maize peel after processing carries out immersion treatment at different temperatures using soak, first puts maize peel
Enter in soak, temperature adjustment is incubated 30min to 82 DEG C, then by temperature quick regulation to 4 DEG C, is incubated 15min, then by temperature
Degree regulation is incubated 2 hours to 61 DEG C, then by temperature adjustment to 42 DEG C, is incubated 1 hour, and it is 42%, institute then to dry to water content
Stating immersion liquid and preparation method thereof is：Red autumnal leaves blade of grass, purple leaf green pepper blade of grass, white arteries and veins green pepper blade of grass, cactus are pressed 1：2：1：4 mass ratios are mixed
It is combined together, is subsequently placed in the blanching 15min in 100 DEG C of hot water, after taking-up, adds cactus 5 times of clear water of quality, mashing is obtained
To mixed serum, the sodium carbonate of its quality 2.3%, 1.8% salt and 0.14% benzene sulfonic acid sodium salt are added into mixed serum, in
15 min are incubated in boiling water bath, room temperature is subsequently cooled to, the lactic acid bacteria of access mixed serum quality 0.002% is fermented, sent out
Ferment temperature is 35 DEG C, and fermentation time is 3h, and separation of solid and liquid is then carried out under high speed centrifugation, obtains mixed liquor, adds mixed liquor
The sodium hypochlorite of quality 0.26%, after 120r/min rotating speeds stirring 30min, stands 2 hours at 30 DEG C, obtains soak；
（3）Illumination and sided corona treatment
Will be through step（2）Maize peel after processing carries out continuous light 2 hours using the white light of 800lux intensities of illumination, Ran Houzai
Maize peel is placed in corona field and handles 21min, corona field field strength is 300KV/m, is then dried maize peel low to water content
In 12%, normal dyeing then can be carried out.
The Chinese toon leaf water content is less than 10%.
The ultracentrifugal speed is 3000r/min.
The maize peel is placed in when being handled in corona field, and environment temperature is 35 DEG C, relative air humidity is 45%.
Comparative example 1：Differed only in embodiment 1 without step（1）Processing.
Comparative example 2：Step is differed only in embodiment 1（2）Soaked in processing using clear water, soaking temperature is 72 DEG C,
Soak time is 2.5 hours.
Comparative example 3：It is with the difference of embodiment 1 without step（3）Processing.
The measure of dye uptake：The accurate maize peel weighed after embodiment and comparative example processing, is 60 DEG C, pH in temperature
It is 1 for 5, bath raio：Under conditions of 150, embodiment and comparative example maize peel are dyed using 2% acid blue, dye liquor is determined and inhales
Luminosity, the dye uptake of sample is calculated using formula：
F=（1-At/A0）× 100%, wherein F are dye uptake, AtTo dye the absorbance of t time dyeing residual liquids, A0For dyeing
The absorbance of stoste；
Table 1
| Dye uptake % | |
| Embodiment 1 | 86.6 |
| Embodiment 2 | 86.3 |
| Embodiment 3 | 86.4 |
| Comparative example 1 | 80.8 |
| Comparative example 2 | 62.7 |
| Comparative example 3 | 46.9 |
As can be seen from Table 1, the maize peel colouring speed of the inventive method processing is significantly improved；
Determine influence of the processing of different corona field field strength in the present invention to maize peel dye uptake（At the method for embodiment 1
Manage maize peel）：
Table 2
| KV/m | Dye uptake % |
| 200 | 80.7 |
| 250 | 83.2 |
| 300 | 86.6 |
| 350 | 86.0 |
| 400 | 85.1 |
As can be seen from Table 2, with the increase of corona field intensity in certain limit, the maize peel dye uptake after processing increases
Plus, corona field intensity reaches maximum when being 300KV/m, after 300KV/m, under the maize peel dye uptake of processing starts
Drop.
Claims (4)
1. a kind of method for improving maize peel dyeing rate, it is characterised in that comprise the following steps：
（1）Suffocating treatment
Maize peel is put into fumatorium, Chinese Toon Leaves are put into burner, stifling indoor humidity is kept with sprayer spraying
For 80%, Chinese Toon Leaves in point burner, closed stifling 2 hours afterburners stop, and stand after 20min, take out maize peel；
（2）Immersion treatment
Will be through step（1）Maize peel after processing carries out immersion treatment at different temperatures using soak, first puts maize peel
Enter in soak, temperature adjustment is incubated 30min to 80-85 DEG C, then by temperature quick regulation to 2-6 DEG C, be incubated 15min, then
By temperature adjustment to 60-62 DEG C, 2 hours are incubated, then by temperature adjustment to 40-44 DEG C, is incubated 1 hour, then dries to aqueous
Measure as 40-50%, the immersion liquid and preparation method thereof is：Red autumnal leaves blade of grass, purple leaf green pepper blade of grass, white arteries and veins green pepper blade of grass, cactus are pressed 1：2：
1：4 mass ratios are admixed together, are subsequently placed in the blanching 15min in 100 DEG C of hot water, after taking-up, 5 times of addition cactus quality
Clear water, mashing, obtains mixed serum, and the sodium carbonate of its quality 2.3%, 1.8% salt and 0.14% are added into mixed serum
Benzene sulfonic acid sodium salt, is incubated 15 min in boiling water bath, is subsequently cooled to room temperature, accesses the lactic acid bacteria of mixed serum quality 0.002%,
Fermented, fermentation temperature is 35 DEG C, and fermentation time is 3h, and separation of solid and liquid is then carried out under high speed centrifugation, mixed liquor is obtained,
The sodium hypochlorite of mixed liquor quality 0.26% is added, after 120r/min rotating speeds stirring 30min, 2 hours is stood at 30 DEG C, obtains
To soak；
（3）Illumination and sided corona treatment
Will be through step（2）Maize peel after processing carries out continuous light 2 hours using the white light of 800lux intensities of illumination, Ran Houzai
Maize peel is placed in corona field and handles 20-22min, corona field field strength is 300KV/m, then dries maize peel to water content
Less than 12%, normal dyeing then can be carried out.
2. a kind of method for improving maize peel dyeing rate as claimed in claim 1, it is characterised in that the Chinese toon leaf water content
Less than 10%.
3. a kind of method for improving maize peel dyeing rate as claimed in claim 1, it is characterised in that the ultracentrifugal speed
Spend for 3000r/min.
4. a kind of method for improving maize peel dyeing rate as claimed in claim 1, it is characterised in that the maize peel is placed in electricity
Have stage fright middle processing when, environment temperature is 35 DEG C, relative air humidity is 45%.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107584603A (en) * | 2017-09-20 | 2018-01-16 | 阜南县中泰工艺品有限公司 | A kind of dyeing treatment of wicker products |
| CN108724395A (en) * | 2018-07-03 | 2018-11-02 | 阜南县大自然工艺品有限公司 | A kind for the treatment of process improving maize peel dyeing property |
| CN108748561A (en) * | 2018-06-06 | 2018-11-06 | 阜南县柳祥工艺品有限公司 | A kind of high-quality colouring method of maize peel |
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| CN107584603A (en) * | 2017-09-20 | 2018-01-16 | 阜南县中泰工艺品有限公司 | A kind of dyeing treatment of wicker products |
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| CN108724395A (en) * | 2018-07-03 | 2018-11-02 | 阜南县大自然工艺品有限公司 | A kind for the treatment of process improving maize peel dyeing property |
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Effective date of registration: 20180824 Address after: 236300 Liu Gang Industrial function area of Huanggang Town, Funan County, Fuyang, Anhui Applicant after: Funan County Shenglong Technology Furniture Co., Ltd. Address before: 236300 Anhui Fuyang Funan County Huanggang town willow weaving function area Applicant before: FUNAN COUNTY YONGSHENG ARTS & CRAFTS CO., LTD. |
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