CN107343861B - 含天然植物精油的长效驱蚊和抗菌喷剂及其制备方法 - Google Patents
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Abstract
含天然植物精油的长效驱蚊和抗菌喷剂及其制备方法,涉及含天然植物精油。提供一种天然香料作为主驱蚊成分,其它天然香料为辅助成份,应用于皮肤表面的长效驱蚊喷剂,解决了现有市场上销售的有毒驱蚊剂对于人体身心健康造成影响,同时可喷出或使用过程中产生让人十分愉悦的香氛气息,有效遮避异味,还具有一定抗菌抑菌功效的含天然植物精油的长效驱蚊和抗菌喷剂及其制备方法。通过提取具有驱蚊功效和抗菌功效的天然精油的有效成份,精心调配其它具有香氛作用的辅助天然香料,最后制成喷雾制剂。
Description
技术领域
本发明涉及含天然植物精油,尤其是涉及含天然植物精油的长效驱蚊和抗菌喷剂及其制备方法。
背景技术
炎热的夏季,蚊虫猖獗,人们经常会受到蚊虫的叮咬,严重影响了人们的正常生活、工作、学习和休息,更为严重的是,蚊虫的叮咬还会传播各种疾病,对人们的身体健康带来了严重的威胁。尽管在室内使用的灭蚊产品有蚊香、电蚊香片、电热蚊香液等不同形式,但其内在杀虫成份都含有天然除虫菊酯或拟除虫菊酯,对于长期使用影响人的身心健康,尤其是小孩,孕妇这类群体更加影响。
由于夏季天气炎热,穿着较少,暴露位置较多,且属于传统的蚊香液以及蚊香片使用的空窗期,往往这是比较容易受到蚊虫叮咬。
气温过高,人体容易出汗,如果不时常擦洗容易产生异味或皮肤过敏等。
中国专利CN103622867A公开一种以天然植物精油为主要活性成份的香水,使用的天然原料包括有:猪笼草、七里香、天竺葵、薄荷、桉叶、番木瓜、缬草根、艾叶、三股筋香、光清香藤、车轴草、土木香、母菊、黄栌。该发明提供的驱蚊香水,采用了天然植物原料,不含有化学合成驱蚊剂,驱蚊时间可以达到6h以上,香味独特,对皮肤不产生刺激。
发明内容
本发明的目的在于提供一种天然香料作为主驱蚊成分,其它天然香料为辅助成份,应用于皮肤表面的长效驱蚊喷剂,解决了现有市场上销售的有毒驱蚊剂对于人体身心健康造成影响,同时可喷出或使用过程中产生让人十分愉悦的香氛气息,有效遮避异味,还具有一定抗菌抑菌功效的含天然植物精油的长效驱蚊和抗菌喷剂及其制备方法。
所述含天然植物精油的长效驱蚊和抗菌喷剂的原料组成按质量比为:
以下给出本发明所述含天然植物精油的长效驱蚊和抗菌喷剂的制备方法:
1)将爪哇香根油、超级藿香油、丙二酸二乙酯、丁酸苄酯、二氢茉莉酮酸甲酯、柳酸苄酯、柳酸叶醇酯、三醋酸甘油酯、乙酸苄酯、乙酸二甲基苄基原酯(DMBCA)、乙酸芳樟酯、乙酸苏合香酯、乙酸叶醇酯、异丁酸苯乙酯、白花醇、苯乙醇、二丙二醇、二氢月桂烯醇、天然芳樟醇、美研醇、乙基芳樟醇、丙位癸内酯环、十五内酯、环十五烯内酯、黄葵内酯、丙位十一内酯、甲基苯基缩水甘油酸乙酯、丙位壬内酯、HCA(甲位己基桂醛)、铃兰醛、兔耳草醛、新洋茉莉醛、丁位突厥酮、环十六烯酮、甲基柏木酮、龙涎酮麝、超级龙涎醚、香烯酮、突厥烯酮2#、乙位紫罗兰酮、异甲基紫罗兰酮、香豆素、香兰素、甜橙油萜、10%呋喃酮(丙二醇)、檀香210、佳乐麝香50(IPM)、麝香T、丁香酚、合成橡苔、天然柠檬醛、香茅油、香叶油按原料组成范围加入第1个搅拌锅,搅拌后,得产物A;
2)将丙二醇、对-薄荷烷-3-8-二醇、去离子水、EDTA-2NA、乙醇、氢化蓖麻油(PEG-40)放入第2个搅拌锅,待固体溶解后加入产物A中搅拌,搅拌后纯化,过滤后即得含天然植物精油的长效驱蚊和抗菌喷剂。
在步骤2)中,所述搅拌的时间可为1~2h,所述纯化的时间可为1~24h,所述过滤可采用滤网过滤,所述滤网可采用120目以上的滤网。
本发明通过提取具有驱蚊功效和抗菌功效的天然精油的有效成份,精心调配其它具有香氛作用的辅助天然香料,最后制成喷雾制剂。
与现有技术相比,本发明具有以下优点:
1)与传统驱蚊制剂如花露水等比较,消除除虫菊酯或拟除虫菊酯的副作用。
2)与单纯的天然驱蚊香料如香茅油、柠檬桉油等比较,驱蚊有效成份含量更高,有工业化生产的原材料质量保证。
3)天然香料的精心调配,保证了产品使用的愉悦香氛;产品以喷雾制剂使用方法,比传统家用蚊香或电蚊香液更方便,也利于携带。
具体实施方式
以下给出具体实施例。
实施例1
所述含天然植物精油的长效驱蚊和抗菌喷剂的原料组成按质量比为表1:
表1
实施例2
所述含天然植物精油的长效驱蚊和抗菌喷剂的原料组成按质量比为表2:表2
实施例3
所述含天然植物精油的长效驱蚊和抗菌喷剂的原料组成按质量比为表3:
表3
实施例4
所述含天然植物精油的长效驱蚊和抗菌喷剂的原料组成按质量比为表4:
表4
实施例5
所述含天然植物精油的长效驱蚊和抗菌喷剂的原料组成按质量比为表5:
表5
本发明通过驱蚊有效时间试验,以及抗菌性能试验。
以下给出驱蚊实验:
1.实验项目
在室内对白纹伊蚊的药效试验。
2.试验根据
GB/T 13917.9-2009.
3.试验虫种
采用实验室饲养的敏感品系标准试虫,白纹伊蚊,羽化后3~5天未吸血雌蚊。
4.试验条件
温度:(26±1)℃,相对湿度:65%±10%。
5.实验设备
蚊笼:长400mm,宽300mm,高300mm。
6.试验方法
A.攻击力试验:
蚊笼内放入300只试虫,测试人员手背暴露40mm×40mm皮肤,其余部分严密遮蔽。将手伸入蚊笼中停留2min,密切观察,发现蚊虫停落,在其口器将刺入皮肤前抖动手臂将其驱离,记为1只试虫停落。前来停落的试虫多于30只的测试人员和试虫为攻击合格,此人及此笼蚊虫可进行驱避试验。
B.驱避试验:
选择至少4名攻击力合格的测试人员(男女各半,且试验前和试验期间不应饮酒、茶或咖啡,不应使用含香精类的产品),在其双手手背各画出50mm×50mm的皮肤面积,其中一只手按1.5μL/cm2的剂量均匀涂抹待测的驱避剂,暴露其中的40mm×40mm皮肤,严密遮蔽其余部分,另一只手为空白对照。涂抹驱避剂2h,将手伸入攻击力合格的蚊虫笼中2min,观察有无蚊虫前来停落吸血。之后每间隔1h测试一次,只要有一只蚊虫前来吸血即判作驱避剂失效。记录驱避剂的有效保护时间(h)。每次对照手先做对照测试,攻击力合格的试虫可继续试验,试虫攻击力不合格则需更换合格试虫进行试验。
C.计算:
将药剂对至少4名受试者的有效保护时间相对,取其平均数(保留1位小数)作为该试剂的有效保护时间(h)
D.试验结果:
案例1(对应实施例5):
驱蚊液按1.5μL/cm2涂于人体手背表面时,在实验室内对白纹伊蚊驱避效果见表6。
表6
案例2(对应实施例3):
驱蚊液按1.5μL/cm2涂于人体手背表面时,在实验室内对白纹伊蚊驱避效果见下表7。
表7
案例3(对应实施例2):
驱蚊液按1.5μL/cm2涂于人体手背表面时,在实验室内对白纹伊蚊驱避效果见下表8。
表8
7.评价
驱蚊液对受试者有效保护时间为≥7h,根据GB/T 13917.9-2009的评价标准,为A级。
8.抗菌检测
使用实施例1的产品作为检测原液。
检测方法:《消毒技术规范》2002年版-2.1.11.3.2,参见表9。
表9
检测项目:抑菌性能。
Claims (6)
2.如权利要求1所述含天然植物精油的长效驱蚊和抗菌喷剂的制备方法,其特征在于包括以下步骤:
1)将爪哇香根油、超级藿香油、丙二酸二乙酯、丁酸苄酯、二氢茉莉酮酸甲酯、柳酸苄酯、柳酸叶醇酯、三醋酸甘油酯、乙酸苄酯、乙酸二甲基苄基原酯、乙酸芳樟酯、乙酸苏合香酯、乙酸叶醇酯、异丁酸苯乙酯、白花醇、苯乙醇、二丙二醇、二氢月桂烯醇、天然芳樟醇、美研醇、乙基芳樟醇、丙位癸内酯、环十五内酯、环十五烯内酯、黄葵内酯、丙位十一内酯、甲基苯基缩水甘油酸乙酯、丙位壬内酯、甲位己基桂醛、铃兰醛、兔耳草醛、新洋茉莉醛、丁位突厥酮、环十六烯酮、甲基柏木酮、龙涎酮、超级龙涎醚、麝香烯酮、突厥烯酮2#、乙位紫罗兰酮、异甲基紫罗兰酮、香豆素、香兰素、甜橙油萜、10%呋喃酮丙二醇溶液、檀香210、佳乐麝香50IPM、麝香T、丁香酚、合成橡苔、天然柠檬醛、香茅油、香叶油按原料组成范围加入第1个搅拌锅,搅拌后,得产物A;
2)将丙二醇、对-薄荷烷-3,8-二醇、去离子水、EDTA-2Na、乙醇、PEG-40氢化蓖麻油放入第2个搅拌锅,待固体溶解后加入产物A中搅拌,搅拌后纯化,过滤后即得含天然植物精油的长效驱蚊和抗菌喷剂。
3.如权利要求2所述含天然植物精油的长效驱蚊和抗菌喷剂的制备方法,其特征在于在步骤2)中,所述搅拌的时间为1~2h。
4.如权利要求2所述含天然植物精油的长效驱蚊和抗菌喷剂的制备方法,其特征在于在步骤2)中,所述纯化的时间为1~24h。
5.如权利要求2所述含天然植物精油的长效驱蚊和抗菌喷剂的制备方法,其特征在于在步骤2)中,所述过滤采用滤网过滤。
6.如权利要求5所述含天然植物精油的长效驱蚊和抗菌喷剂的制备方法,其特征在于所述滤网采用120目以上的滤网。
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