CN107324770A - A kind of wear-resistant, high-low temperature resistant ceramic pan and its manufacturing process - Google Patents
A kind of wear-resistant, high-low temperature resistant ceramic pan and its manufacturing process Download PDFInfo
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- CN107324770A CN107324770A CN201710654136.8A CN201710654136A CN107324770A CN 107324770 A CN107324770 A CN 107324770A CN 201710654136 A CN201710654136 A CN 201710654136A CN 107324770 A CN107324770 A CN 107324770A
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- C04B38/00—Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof
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- A—HUMAN NECESSITIES
- A47—FURNITURE; DOMESTIC ARTICLES OR APPLIANCES; COFFEE MILLS; SPICE MILLS; SUCTION CLEANERS IN GENERAL
- A47J—KITCHEN EQUIPMENT; COFFEE MILLS; SPICE MILLS; APPARATUS FOR MAKING BEVERAGES
- A47J27/00—Cooking-vessels
- A47J27/002—Construction of cooking-vessels; Methods or processes of manufacturing specially adapted for cooking-vessels
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- A—HUMAN NECESSITIES
- A47—FURNITURE; DOMESTIC ARTICLES OR APPLIANCES; COFFEE MILLS; SPICE MILLS; SUCTION CLEANERS IN GENERAL
- A47J—KITCHEN EQUIPMENT; COFFEE MILLS; SPICE MILLS; APPARATUS FOR MAKING BEVERAGES
- A47J36/00—Parts, details or accessories of cooking-vessels
- A47J36/02—Selection of specific materials, e.g. heavy bottoms with copper inlay or with insulating inlay
- A47J36/04—Selection of specific materials, e.g. heavy bottoms with copper inlay or with insulating inlay the materials being non-metallic
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
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- C04B33/13—Compounding ingredients
- C04B33/132—Waste materials; Refuse; Residues
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- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3418—Silicon oxide, silicic acids, or oxide forming salts thereof, e.g. silica sol, fused silica, silica fume, cristobalite, quartz or flint
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- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3427—Silicates other than clay, e.g. water glass
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- C04B2235/44—Metal salt constituents or additives chosen for the nature of the anions, e.g. hydrides or acetylacetonate
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- C04B2235/5418—Particle size related information expressed by the size of the particles or aggregates thereof
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- C04B2235/54—Particle size related information
- C04B2235/5418—Particle size related information expressed by the size of the particles or aggregates thereof
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Abstract
The present invention provides a kind of wear-resistant, high-low temperature resistant ceramic pan and its manufacturing process, and the ceramic pan includes base substrate and imposes on the glaze layer of billet surface, and the base substrate is made by the raw material of following parts by weight：30~45 parts of kaolin, 23~30 parts of bone meal, 15~25 parts of silica flour, 10~20 parts of feldspar powder, 8~14 parts of bentonite, waste and old broken 13~20 parts of ceramic powder, 10~15 parts of waterglass, 10~15 parts of land plaster, 5~10 parts of silica flour；The glaze layer is made by the raw material of following parts by weight：10~20 parts of kaolin, 5~12 parts of silica flour, 5~8 parts of bone meal, 5~15 parts of pigment, 1~5 part of silica flour.Using ceramic pan made from the raw material that provides of the present invention and manufacturing process, it has light weight, wear-resistant, high-low temperature resistant, corrosion resistant performance, is available for daily persistently using more than 50 years.
Description
Technical field
The present invention relates to domestic ceramics manufacturing technology field, and in particular to a kind of wear-resistant, high-low temperature resistant ceramic pan and
Its manufacturing process.
Background technology
Compared with metal pan, temperature rising is slower when ceramic pan is heated, and can so allow food uniform and fully heated, can use
In cooking, Baoshang, deep fried foodstuff, and ceramic pan also has weight big, the crisp frangible weakness of matter, and ceramic pan top layer generally has
One layer improve ceramic pan gloss, wearability and corrosion resistance glaze layer, during routine use, if glaze layer is worn, quite
In the protective layer for destroying ceramic pan, its wearability and corrosion resistance are reduced, so that its service life is reduced, with living standard
Increasingly raising, quality, class requirement also more and more higher of the people to domestic ceramics pot.
The content of the invention
Based on above prior art, it is an object of the invention to provide a kind of wear-resistant, high-low temperature resistant ceramic pan, its is heavy
Lighter, convenient use is measured, and with high-wearing feature, be available for daily persistently using more than 50 years.
To achieve these goals, the technical solution adopted by the present invention is：A kind of wear-resistant, high-low temperature resistant ceramic pan,
Including base substrate and the glaze layer for imposing on billet surface, it is characterised in that the base substrate is made by the raw material of following parts by weight：Kaolin
30~45 parts, 23~30 parts of bone meal, 15~25 parts of silica flour, 10~20 parts of feldspar powder, 8~14 parts of bentonite, waste and old broken ceramics
13~20 parts of powder, 10~15 parts of waterglass, 10~15 parts of land plaster, 5~10 parts of silica flour；The glaze layer by following parts by weight original
Material is made：10~20 parts of kaolin, 5~12 parts of silica flour, 5~8 parts of bone meal, 5~15 parts of pigment, 1~5 part of silica flour.
Preferably, the base substrate is made by the raw material of following parts by weight：40 parts of kaolin, 25 parts of bone meal, silica flour 20
Part, 14 parts of feldspar powder, 11 parts of bentonite, waste and old broken 17 parts of ceramic powder, 13 parts of waterglass, 12 parts of land plaster, 8 parts of silica flour；It is described
Glaze layer is manufactured using the following raw material：14 parts of kaolin, 8 parts of silica flour, 6 parts of bone meal, 10 parts of pigment, 4 parts of silica flour.
Preferably, the granularity of the waste and old broken ceramic powder is 100~300 microns, the granularity of the silica flour is 20~200
Nanometer, the granularity of waste and old broken ceramic powder is somewhat larger, relative while ensureing that ceramic pan hardness is made with toughness can reduce it
Weight, the granularity of silica flour is smaller, can be filled up the hole constituted in raw material in ceramics, so as to ensure the hardness of ceramic pan
With wearability.
Present invention also offers a kind of technique for manufacturing wear-resistant, high-low temperature resistant ceramic pan, following steps are included：
Step 1：More than 10 minutes shapes are stirred after kaolin, bone meal, silica flour, feldspar powder, waste and old broken ceramic powder are mixed
Into well mixed ceramic powder；
Step 2：Add to stir after the water for accounting for 8~15 times of its weight into bentonite and expand and formed suspension completely to it
Liquid, continues to stir, is obtained after sequentially adding the ceramic powder obtained in waterglass, land plaster and above-mentioned steps 1 in whipping process
Pug is mixed, mixed soil is anticipated into type and obtains crude green body body, afterwards according to silica flour:Water=1:3~5 weight is than by bad body raw material
In silica flour mixed with water after spraying plating carry out sharp base in crude green body body inner and outer surfaces, after drying in the shade naturally and obtain base substrate；
Step 3：Glaze water is made with accounting in glaze layer raw material after the water of 1.5~3 times of its gross weight is mixed, then to the above-mentioned step of step
Rapid 2 obtained base substrates carry out glazings and simultaneously dried, and the base substrate after finally glazing is dried is placed in nitrogen environment, it is warming up to 1000~
1200 DEG C sinter 30~180 minutes, and then sintering obtains wear-resistant, resistance to for 0.5~2 hour under conditions of 1300 DEG C~1500 DEG C
The ceramic pan of high/low temperature.
The present invention use the principle of raw material and burning process for：Using kaolin, bone meal, silica flour, feldspar powder, waste and old broken
Ceramic powder, land plaster, silica flour as manufacture ceramic body primary raw material, wherein, waste and old broken ceramic powder is will be broken waste and old
Ceramics are ground obtained powder, and ceramic hardness is big, is ground to after powder, its powder granule is larger so that what step 1 was obtained
Hole inside ceramic powder is larger, so that obtaining ceramics in firing is internally formed larger hole, the density of overall reduction ceramic pan.
Hole in the ceramic powder that step 1 is obtained is big, can make the viscosity decline of pug made from step 2, so as to easily make final firing
Obtain ceramic pan excessively matter crisp frangible, thus stirring forms after suspension and adds pottery after first being added water in step 2 into bentonite
Porcelain powder formation pug, bentonite can make the viscosity increase of pug, and the viscous of pug can be then made after being combined with the waterglass of rear addition
Property is bigger, so as to increase its plasticity and toughness, aftershaping after silica flour is mixed with water after spraying plating in crude green body body, appearance
Face, glazing dry after in step 3 in a nitrogen environment in sintering process, the part silicon in ceramic pot reacts with nitrogen to be generated
Silicon nitride, silica has the performances such as excellent high rigidity, wearability, corrosion resistance, inoxidizability, cold-and-heat resistent, thus this
When ceramic pan it is overall there is certain high intensity, obtained after then being sintered under conditions of 1300 DEG C~1500 DEG C
Light weight, wear-resistant, high-low temperature resistant, corrosion resistant ceramic pan.
Preferably, according to silica flour in the step 2:Water=1:4 weight is than by the silica flour and water in bad body raw material
Spraying plating, i.e., will not be because of water on crude green body body after the silica flour under crude green body body inner and outer surfaces, this ratio is mixed with water for spraying plating after mixing
Excessively dry its difficulty, and can also make the silicon of spraying plating uneven because water is very few.
Make preferred, the base substrate after glazing is dried in the step 3 is placed in nitrogen environment, be warming up to 1135 DEG C of sintering 95
Minute, ceramic pan base substrate now has been provided with certain hardness and abrasion resistance, is then sintered 1 hour under conditions of 1455 DEG C
Obtain wear-resistant, high-low temperature resistant ceramic pan, light weight, wear-resistant, high-low temperature resistant, corrosion resistant ceramic pan are obtained under the conditions of this
Best performance is got over, and its service life was up to more than 50 years.
Beneficial effect
The present invention provides a kind of wear-resistant, high-low temperature resistant ceramic pan, and its advantage is as follows：
(1), lightweight, hardness is high, good toughness, and micro-ceramic powder can increase the hole inside ceramics, makes ceramics
Light weight is relatively light, moreover it is possible to make hardness and the toughness increase of ceramics, so as to increase its intensity and service life.
(2), wear-resistant, corrosion-resistant, high-low temperature resistant, base substrate is with adding nanoscale silica flour in glaze layer raw material, inside ceramics
Hole is filled up, and increases its intensity, during sintering, part silica flour and nitrogen reaction generation silicon nitride, so that increase that its is wear-resistant,
Corrosion-resistant, high and low temperature resistance, finally increases its service life.
Embodiment
The present invention is described in further detail with reference to specific embodiment.
Embodiment 1
The present embodiment provides a kind of wear-resistant, high-low temperature resistant ceramic pan, including base substrate and the glaze layer for imposing on billet surface,
The base substrate is made by the raw material of following parts by weight：30 parts of kaolin, 23 parts of bone meal, 15 parts of silica flour, 10 parts of feldspar powder, swelling
8 parts of soil, waste and old broken 13 parts of the ceramic powder that granularity is 150 microns, 10 parts of waterglass, 10~15 parts of land plaster, granularity are 80 nanometers
5 parts of silica flour；The glaze layer is made by the raw material of following parts by weight：12 parts of kaolin, 5 parts of silica flour, 5 parts of bone meal, pigment 5
Part, 2 parts of silica flour.
The present embodiment also provides a kind of technique for manufacturing wear-resistant, high-low temperature resistant ceramic pan, comprises the following steps：
Step 1：Stirring forms mixed for 10 minutes after kaolin, bone meal, silica flour, feldspar powder, waste and old broken ceramic powder are mixed
Close uniform ceramic powder；
Step 2：Add to stir after the water for accounting for 8 times of its weight into bentonite and expand and formed suspension completely to it, after
Mixed soil is obtained after sequentially adding the ceramic powder obtained in waterglass, land plaster and above-mentioned steps 1 in continuous stirring, whipping process
Material, obtains crude green body body, afterwards according to silica flour by pug sizing:Water=1:3 weight is than by the silica flour and water in bad body raw material
Spraying plating carries out sharp base in crude green body body inner and outer surfaces, after drying in the shade naturally and obtains base substrate after mixing；
Step 3：Glaze water is made with accounting in glaze layer raw material after the water of 1.5 times of its gross weight is mixed, then base substrate is carried out
Glaze is simultaneously dried, and the base substrate after finally glazing is dried is placed in nitrogen environment, is warming up to 1200 DEG C and is sintered 170 minutes, then exists
Sintering obtains wear-resistant, high-low temperature resistant ceramic pan for 2 hours under conditions of 1300 DEG C.
Ceramic pan is made using the present embodiment raw material and technique, wearability survey is carried out to its fragment using wearability test machine
Examination, take ceramic pan fragment made from 5 the present embodiment, respectively by potsherd place certain granules level match somebody with somebody grinding steel ball,
No. 80 white fused aluminas and quantitative deionized water or distilled water, carry out spin finishing, to what is had worn away according to the rotary speed of regulation
Potsherd carries out observation contrast with unworn potsherd, by whether appreciable wear vestige can be observed to have evaluated glaze
The wearability of brick, result of this test shows that potsherd increases in rotary speed since 1200 turns, rotating speed reaches 9250~
Start to wear and tear after 9360 turns, its wearability rank is 4 grades, meet the abrasion test method standard GB/T for there are glaze ceramics
3810.7-2006。
The fragment for the present embodiment being made ceramic pan carries out heat stability testing, takes 5 the present embodiment that ceramic pan is made
Fragment, 30 minutes are incubated under the conditions of being placed in 280 DEG C, and insulation is taken out ceramic pan fragment and adjusted after terminating, in 15s rapidly
Temperature is put into 20 DEG C of water, to soak 10min, wherein, weight and the ceramic pan fragment weight ratio of water are 8：1, the water surface is high
Go out ceramic pan fragment 25mm, take out ceramic pan fragment and wipe dry with cloth, colored red ink is checked again after checking for crackle, 24h
Once, its test result is shown, the equal flawless of five potsherds is produced.
Embodiment 2
The present embodiment provides a kind of wear-resistant, high-low temperature resistant ceramic pan, including base substrate and the glaze layer for imposing on billet surface,
The base substrate is made by the raw material of following parts by weight：35 parts of kaolin, 25 parts of bone meal, 17 parts of silica flour, 12 parts of feldspar powder, swelling
10 parts of soil, waste and old broken 15 parts of the ceramic powder that granularity is 200 microns, 10 parts of waterglass, 11~15 parts of land plaster, granularity are 150 to receive
6 parts of the silica flour of rice；The glaze layer is made by the raw material of following parts by weight：15 parts of kaolin, 7 parts of silica flour, 6 parts of bone meal, pigment 5
Part, 5 parts of silica flour.
The present embodiment also provides a kind of technique for manufacturing wear-resistant, high-low temperature resistant ceramic pan, comprises the following steps：
Step 1：Stirring forms mixed for 25 minutes after kaolin, bone meal, silica flour, feldspar powder, waste and old broken ceramic powder are mixed
Close uniform ceramic powder；
Step 2：Add to stir after the water for accounting for 10 times of its weight into bentonite and expand and formed suspension completely to it, after
Mixed soil is obtained after sequentially adding the ceramic powder obtained in waterglass, land plaster and above-mentioned steps 1 in continuous stirring, whipping process
Material, obtains crude green body body, afterwards according to silica flour by pug sizing:Water=1:3 weight is than by the silica flour and water in bad body raw material
Spraying plating carries out sharp base in crude green body body inner and outer surfaces, after drying in the shade naturally and obtains base substrate after mixing；
Step 3：Glaze water is made with accounting in glaze layer raw material after the water of 2 times of its gross weight is mixed, glazing then is carried out to base substrate
And dry, the base substrate after finally glazing is dried is placed in nitrogen environment, is warming up to 1150 DEG C and is sintered 150 minutes, then exists
Sintering obtains wear-resistant, high-low temperature resistant ceramic pan for 1.5 hours under conditions of 1300 DEG C.
Ceramic pan is made using the present embodiment raw material and technique, wearability survey is carried out to its fragment using wearability test machine
Examination, take ceramic pan fragment made from 5 the present embodiment, respectively by potsherd place certain granules level match somebody with somebody grinding steel ball,
No. 80 white fused aluminas and quantitative deionized water or distilled water, carry out spin finishing, to what is had worn away according to the rotary speed of regulation
Potsherd carries out observation contrast with unworn potsherd, by whether appreciable wear vestige can be observed to have evaluated glaze
The wearability of brick, result of this test shows that potsherd increases in rotary speed since 1200 turns, rotating speed reaches 9230~
Start to wear and tear after 9310 turns, its wearability rank is 4 grades, meet the abrasion test method standard GB/T for there are glaze ceramics
3810.7-2006。
The fragment for the present embodiment being made ceramic pan carries out heat stability testing, takes 5 the present embodiment that ceramic pan is made
Fragment, 30 minutes are incubated under the conditions of being placed in 280 DEG C, and insulation is taken out ceramic pan fragment and adjusted after terminating, in 15s rapidly
Temperature is put into 20 DEG C of water, to soak 10 minutes, wherein, weight and the ceramic pan fragment weight ratio of water are 8：1, the water surface is high
Go out ceramic pan fragment 25mm, take out ceramic pan fragment and wipe dry with cloth, colored red ink is checked again after checking for crackle, 24h
Once, its test result is shown, the equal flawless of five potsherds is produced.
Embodiment 3
The present embodiment provides a kind of wear-resistant, high-low temperature resistant ceramic pan, including base substrate and the glaze layer for imposing on billet surface,
The base substrate is made by the raw material of following parts by weight：40 parts of kaolin, 25 parts of bone meal, 20 parts of silica flour, 14 parts of feldspar powder, swelling
11 parts of soil, waste and old broken 17 parts of the ceramic powder that granularity is 100 microns, 13 parts of waterglass, 12 parts of land plaster, the silicon that granularity is 20 nanometers
8 parts of powder；The glaze layer is manufactured using the following raw material：16 parts of kaolin, 8 parts of silica flour, 6 parts of bone meal, 7 parts of pigment, 3 parts of silica flour.
The present embodiment also provides a kind of technique for manufacturing wear-resistant, high-low temperature resistant ceramic pan, comprises the following steps：
Step 1：Stirring forms mixed for 30 minutes after kaolin, bone meal, silica flour, feldspar powder, waste and old broken ceramic powder are mixed
Close uniform ceramic powder；
Step 2：Add to stir after the water for accounting for 12 times of its weight into bentonite and expand and formed suspension completely to it, after
Mixed soil is obtained after sequentially adding the ceramic powder obtained in waterglass, land plaster and above-mentioned steps 1 in continuous stirring, whipping process
Material, obtains crude green body body, afterwards according to silica flour by pug sizing:Water=1:4 weight is than by the silica flour and water in bad body raw material
Spraying plating carries out sharp base in crude green body body inner and outer surfaces, after drying in the shade naturally and obtains base substrate after mixing；
Step 3：Glaze water is made with accounting in glaze layer raw material after the water of 2 times of its gross weight is mixed, glazing then is carried out to base substrate
And dry, the base substrate after finally glazing is dried is placed in nitrogen environment, is warming up to 1135 DEG C and is sintered 95 minutes, then 1455
Sintering obtains wear-resistant, high-low temperature resistant ceramic pan for 1 hour under conditions of DEG C.
Ceramic pan is made using the present embodiment raw material and technique, wearability survey is carried out to its fragment using wearability test machine
Examination, take ceramic pan fragment made from 5 the present embodiment, respectively by potsherd place certain granules level match somebody with somebody grinding steel ball,
No. 80 white fused aluminas and quantitative deionized water or distilled water, carry out spin finishing, to what is had worn away according to the rotary speed of regulation
Potsherd carries out observation contrast with unworn potsherd, by whether appreciable wear vestige can be observed to have evaluated glaze
The wearability of brick, the result of this test shows that potsherd increases in rotary speed since 1200 turns, and rotating speed reaches 11000
Start to wear and tear after~11170 turns, its wearability rank is 4 grades, meet the abrasion test method standard GB/ for there are glaze ceramics
T 3810.7-2006。
The fragment for the present embodiment being made ceramic pan carries out heat stability testing, takes 5 the present embodiment that ceramic pan is made
Fragment, 30 minutes are incubated under the conditions of being placed in 280 DEG C, and insulation is taken out ceramic pan fragment and adjusted after terminating, in 15s rapidly
Temperature is put into 20 DEG C of water, to soak 10min, wherein, weight and the ceramic pan fragment weight ratio of water are 8：1, the water surface is high
Go out ceramic pan fragment 25mm, take out ceramic pan fragment and wipe dry with cloth, colored red ink is checked again after checking for crackle, 24h
Once, its test result is shown, the equal flawless of five potsherds is produced.
Embodiment 4
The present embodiment provides a kind of wear-resistant, high-low temperature resistant ceramic pan, including base substrate and the glaze layer for imposing on billet surface,
The base substrate is made by the raw material of following parts by weight：40 parts of kaolin, 27 parts of bone meal, 23 parts of silica flour, 17 parts of feldspar powder, swelling
12 parts of soil, waste and old broken 17 parts of the ceramic powder that granularity is 250 microns, 13 parts of waterglass, 13 parts of land plaster, granularity are 150 nanometers
9 parts of silica flour；The glaze layer is manufactured using the following raw material：18 parts of kaolin, 9 parts of silica flour, 7 parts of bone meal, 10 parts of pigment, silica flour 4
Part.
The present embodiment also provides a kind of technique for manufacturing wear-resistant, high-low temperature resistant ceramic pan, comprises the following steps：
Step 1：Stirring forms mixed for 35 minutes after kaolin, bone meal, silica flour, feldspar powder, waste and old broken ceramic powder are mixed
Close uniform ceramic powder；
Step 2：Add to stir after the water for accounting for 12 times of its weight into bentonite and expand and formed suspension completely to it, after
Mixed soil is obtained after sequentially adding the ceramic powder obtained in waterglass, land plaster and above-mentioned steps 1 in continuous stirring, whipping process
Material, obtains crude green body body, afterwards according to silica flour by pug sizing:Water=1:5 weight is than by the silica flour and water in bad body raw material
Spraying plating carries out sharp base in crude green body body inner and outer surfaces, after drying in the shade naturally and obtains base substrate after mixing；
Step 3：Glaze water is made with accounting in glaze layer raw material after the water of 2.5 times of its gross weight is mixed, then base substrate is carried out
Glaze is simultaneously dried, and the base substrate after finally glazing is dried is placed in nitrogen environment, is warming up to 1100 DEG C and is sintered 100 minutes, then exists
Sintering obtains wear-resistant, high-low temperature resistant ceramic pan for 0.5 hour under conditions of 1500 DEG C.
Ceramic pan is made using the present embodiment raw material and technique, wearability survey is carried out to its fragment using wearability test machine
Examination, take ceramic pan fragment made from 5 the present embodiment, respectively by potsherd place certain granules level match somebody with somebody grinding steel ball,
No. 80 white fused aluminas and quantitative deionized water or distilled water, carry out spin finishing, to what is had worn away according to the rotary speed of regulation
Potsherd carries out observation contrast with unworn potsherd, by whether appreciable wear vestige can be observed to have evaluated glaze
The wearability of brick, the result of this test shows that potsherd increases in rotary speed since 1200 turns, and rotating speed reaches 10050
Start to wear and tear after~10120 turns, its wearability rank is 4 grades, meet the abrasion test method standard GB/ for there are glaze ceramics
T 3810.7-2006。
The fragment for the present embodiment being made ceramic pan carries out heat stability testing, takes 5 the present embodiment that ceramic pan is made
Fragment, 30 minutes are incubated under the conditions of being placed in 280 DEG C, and insulation is taken out ceramic pan fragment and adjusted after terminating, in 15s rapidly
Temperature is put into 20 DEG C of water, to soak 10min, wherein, weight and the ceramic pan fragment weight ratio of water are 8：1, the water surface is high
Go out ceramic pan fragment 25mm, take out ceramic pan fragment and wipe dry with cloth, colored red ink is checked again after checking for crackle, 24h
Once, its test result is shown, the equal flawless of five potsherds is produced.
Embodiment 5
The present embodiment provides a kind of wear-resistant, high-low temperature resistant ceramic pan, including base substrate and the glaze layer for imposing on billet surface,
The base substrate is made by the raw material of following parts by weight：45 parts of kaolin, 30 parts of bone meal, 25 parts of silica flour, 20 parts of feldspar powder, swelling
14 parts of soil, waste and old broken 20 parts of the ceramic powder that granularity is 300 microns, 15 parts of waterglass, 15 parts of land plaster, granularity are 200 nanometers
10 parts of silica flour；The glaze layer is made by the raw material of following parts by weight：20 parts of kaolin, 11 parts of silica flour, 8 parts of bone meal, pigment 13
Part, 5 parts of the silica flour that granularity is 200 nanometers.
The present embodiment also provides a kind of technique for manufacturing wear-resistant, high-low temperature resistant ceramic pan, comprises the following steps：
Step 1：Stirring forms mixed for 35 minutes after kaolin, bone meal, silica flour, feldspar powder, waste and old broken ceramic powder are mixed
Close uniform ceramic powder；
Step 2：Add to stir after the water for accounting for 15 times of its weight into bentonite and expand and formed suspension completely to it, after
Mixed soil is obtained after sequentially adding the ceramic powder obtained in waterglass, land plaster and above-mentioned steps 1 in continuous stirring, whipping process
Material, obtains crude green body body, afterwards according to silica flour by pug sizing:Water=1:5 weight is than by the silica flour and water in bad body raw material
Spraying plating carries out sharp base in crude green body body inner and outer surfaces, after drying in the shade naturally and obtains base substrate after mixing；
Step 3：Glaze water is made with accounting in glaze layer raw material after the water of 3 times of its gross weight is mixed, glazing then is carried out to base substrate
And dry, the base substrate after finally glazing is dried is placed in nitrogen environment, is warming up to 1100 DEG C and is sintered 40 minutes, then 1500
Sintering obtains wear-resistant, high-low temperature resistant ceramic pan for 0.5 hour under conditions of DEG C.
Ceramic pan is made using the present embodiment raw material and technique, wearability survey is carried out to its fragment using wearability test machine
Examination, take ceramic pan fragment made from 5 the present embodiment, respectively by potsherd place certain granules level match somebody with somebody grinding steel ball,
No. 80 white fused aluminas and quantitative deionized water or distilled water, carry out spin finishing, to what is had worn away according to the rotary speed of regulation
Potsherd carries out observation contrast with unworn potsherd, by whether appreciable wear vestige can be observed to have evaluated glaze
The wearability of brick, result of this test shows that potsherd increases in rotary speed since 1200 turns, rotating speed reaches 9900~
Start to wear and tear after 10050 turns, its wearability rank is 4 grades, meet the abrasion test method standard GB/T for there are glaze ceramics
3810.7-2006。
The fragment for the present embodiment being made ceramic pan carries out heat stability testing, takes 5 the present embodiment that ceramic pan is made
Fragment, 30 minutes are incubated under the conditions of being placed in 280 DEG C, and insulation is taken out ceramic pan fragment and adjusted after terminating, in 15s rapidly
Temperature is put into 20 DEG C of water, to soak 10min, wherein, weight and the ceramic pan fragment weight ratio of water are 8：1, the water surface is high
Go out ceramic pan fragment 25mm, take out ceramic pan fragment and wipe dry with cloth, colored red ink is checked again after checking for crackle, 24h
Once, its test result is shown, the equal flawless of five potsherds is produced.
The potsherd that the raw material provided using above-described embodiment 1 to 5 is obtained with technique, its wearability test result and antibacterial
Test result is as follows：
Wherein, ceramic wear-resisting level standard is 1 to 5 grade, and 5 grades best 1 grade worst, and its criterion is as shown in the table：
| There is the grinding revolution worn and torn | Rank |
| 100 | 0 |
| 150 | 1 |
| 600 | 2 |
| 755,1500 | 3 |
| 2100,6000,12000 | 4 |
| ＞ 12000 | 5 |
Finally it should be noted that：The preferred embodiments of the present invention are the foregoing is only, are not intended to limit the invention,
Although the present invention is described in detail with reference to the foregoing embodiments, for those skilled in the art, it still may be used
To be modified to the technical scheme described in foregoing embodiments, or equivalent substitution is carried out to which part technical characteristic.
Within the spirit and principles of the invention, any modification, equivalent substitution and improvements made etc., should be included in the present invention's
Within protection domain.
Claims (7)
1. a kind of wear-resistant, high-low temperature resistant ceramic pan, including base substrate and the glaze layer for imposing on billet surface, it is characterised in that institute
Base substrate is stated to be made by the raw material of following parts by weight：30~45 parts of kaolin, 23~30 parts of bone meal, 15~25 parts of silica flour, feldspar
10~20 parts of powder, 8~14 parts of bentonite, waste and old broken 13~20 parts of ceramic powder, 10~15 parts of waterglass, 10~15 parts of land plaster,
5~10 parts of silica flour；The glaze layer is made by the raw material of following parts by weight：10~20 parts of kaolin, 5~12 parts of silica flour, bone meal 5
~8 parts, 5~15 parts of pigment, 1~5 part of silica flour.
2. wear-resistant, high-low temperature resistant ceramic pan according to claim 1, it is characterised in that the base substrate by weighing as follows
The raw material for measuring part is made：40 parts of kaolin, 25 parts of bone meal, 20 parts of silica flour, 14 parts of feldspar powder, 11 parts of bentonite, waste and old broken pottery
17 parts of porcelain powder, 13 parts of waterglass, 12 parts of land plaster, 8 parts of silica flour；The glaze layer is manufactured using the following raw material：14 parts of kaolin, stone
8 parts of English powder, 6 parts of bone meal, 10 parts of pigment, 4 parts of silica flour.
3. wear-resistant, high-low temperature resistant ceramic pan according to claim 1 or 2, it is characterised in that the waste and old broken ceramics
The granularity of powder is 100~300 microns.
4. wear-resistant, high-low temperature resistant ceramic pan according to claim 1 or 2, it is characterised in that the granularity of the silica flour
For 20~200 nanometers.
5. the technique of wear-resistant, high-low temperature resistant ceramic pan described in a kind of manufacturing claims 1 to 4, it is characterised in that including with
Lower step：
Step 1：Will kaolin, bone meal, silica flour, feldspar powder, waste and old broken ceramic powder mix after stirring 10 minutes it is formed above mixed
Close uniform ceramic powder；
Step 2：Add to stir after the water for accounting for 8~15 times of its weight into bentonite and expand and formed suspension completely to it, after
Mixed soil is obtained after sequentially adding the ceramic powder obtained in waterglass, land plaster and above-mentioned steps 1 in continuous stirring, whipping process
Material, anticipates type by mixed soil and obtains crude green body body, afterwards according to silica flour:Water=1:3~5 weight is than by the silicon in bad body raw material
Spraying plating carries out sharp base in crude green body body inner and outer surfaces, after drying in the shade naturally and obtains base substrate after powder is mixed with water；
Step 3：Glaze water is made with accounting in glaze layer raw material after the water of 1.5~3 times of its gross weight is mixed, then above-mentioned steps 2 are obtained
To base substrate glazing and dry, the base substrate after finally glazing is dried is placed in nitrogen environment, is warming up to 1000~1200
DEG C sintering 30~180 minutes, then under conditions of 1300 DEG C~1500 DEG C sintering obtain within 0.5~2 hour wear-resistant, resistance to height
The ceramic pan of temperature.
6. a kind of technique for manufacturing wear-resistant, high-low temperature resistant ceramic pan according to claim 5, it is characterised in that institute
State in step 2 according to silica flour:Water=1:4 weight than the silica flour in bad body raw material is mixed with water after spraying plating in crude green body body,
Outer surface.
7. a kind of manufacture according to claim 5 or 6 is wear-resistant, high-low temperature resistant ceramic pan technique, it is characterised in that
Base substrate after glazing is dried in the step 3 is placed in nitrogen environment, is warming up to 1135 DEG C and is sintered 95 minutes, then 1455
Sintering obtains wear-resistant, high-low temperature resistant ceramic pan for 1 hour under conditions of DEG C.
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| CN202011409114.3A CN112479734A (en) | 2017-08-03 | 2017-08-03 | Wear-resistant high-low temperature-resistant ceramic product |
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| CN112479734A (en) | 2021-03-12 |
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Denomination of invention: A ceramic pot with wear resistance, high and low temperature resistance and its manufacturing process Effective date of registration: 20210507 Granted publication date: 20210101 Pledgee: Industrial Commercial Bank of China Ltd. Dehua branch Pledgor: FUJIAN DEHUA HUACHEN CERAMIC Co.,Ltd. Registration number: Y2021980003325 |
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