CN107321277B - A kind of synthetic latex resource recovering system - Google Patents
A kind of synthetic latex resource recovering system Download PDFInfo
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- CN107321277B CN107321277B CN201710663395.7A CN201710663395A CN107321277B CN 107321277 B CN107321277 B CN 107321277B CN 201710663395 A CN201710663395 A CN 201710663395A CN 107321277 B CN107321277 B CN 107321277B
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- container
- collet
- water
- degassing
- water storage
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/0013—Controlling the temperature of the process
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F22—STEAM GENERATION
- F22B—METHODS OF STEAM GENERATION; STEAM BOILERS
- F22B33/00—Steam-generation plants, e.g. comprising steam boilers of different types in mutual association
- F22B33/18—Combinations of steam boilers with other apparatus
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/00094—Jackets
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Mechanical Engineering (AREA)
- General Engineering & Computer Science (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
Abstract
The present invention relates to a kind of synthetic latex resource recovering systems, comprising: steam generator, mixing vessel, synthesising container, container of growing up, degassing container, the first water storage container are connected to the entrance of the outlet of synthesising container collet and degassing container collet；Second water storage container is connected to the outlet of growth vessel jacket and steam generator；Third water storage container is connected to the jacket inlet of the outlet of degassing container collet, container of growing up.Synthetic latex resource recovering system of the invention, store the water of different temperatures respectively by three water storage containers, and the water of three kinds of different temperatures is applied in the heating or cooling of synthesising container, growth container, degassing container or is used to generate steam, water and thermal energy can be made full use of, the effect of energy-saving and emission-reduction is played.
Description
Technical field
The present invention relates to a kind of synthetic latex resource recovering systems, belong to synthetic latex equipment technical field.
Background technique
The reaction vessel and degassing container of synthetic latex commonly use jacketed reaction container, and jacketed reaction container is normal closes
At an outside sandwich more on container outer wall, what is led in interlayer is heat source or coolant, as water, oil or gas etc, lead to heat
When source, by heat transfer effect, reaction vessel can be heated, when coolant can then cool down to reaction vessel.Existing synthesis
In latex, there is soft water in usual raw material, interlayer is flowed through using steam, reaction vessel and degassing container are heated, steam liquefaction
After form water, usually just for live use or cool, water resource therein and thermal energy just slattern, and are one to resource
Kind waste.
Summary of the invention
The technical problem to be solved by the present invention is being provided the technical issues of the wasting of resources when to solve synthetic latex production
One kind being capable of recycle-water and thermal energy synthetic latex resource recovering system.
The technical solution adopted by the present invention to solve the technical problems is:
The present invention provides a kind of synthetic latex resource recovering system, comprising:
Steam generator, for generating steam；
Mixing vessel is used for mixed raw material；
Synthesising container has collet on outer wall, and jacket inlet, which be connected to receive steam and heat with steam generator, synthesizes appearance
Material in device, for carrying out preliminary polymerization；
Grow up container, there is collet, for further being polymerize on outer wall；
Degassing container has collet on outer wall, for deaerating for latex；
First water storage container is connected to the entrance of the outlet of synthesising container collet and degassing container collet, is steamed for storing
High-temperature water after vapour-liquid, and high-temperature water is transported in degassing container collet to degassing when degassing container is de-gassed operation
Material in container is heated and is kept the temperature；
Second water storage container is connected to the outlet of growth vessel jacket and steam generator, for storing growth container clip
The middle warm water of outflow is covered, and warm water in this is used to generate steam in steam generator；
Third water storage container, the jacket inlet and/or mixing vessel of outlet, container of growing up with degassing container collet connect
It is logical, cooling growth container is used for for storing the water at low temperature of degassing container collet outflow, and by the water at low temperature.
Preferably, synthetic latex resource recovering system of the invention, the outlet of the second water storage container also connect with mixing vessel
It is logical.
Preferably, synthetic latex resource recovering system of the invention, grow up container on jacket inlet also with cooling water pipe
Connection, for receiving room temperature cooling water.
Preferably, synthetic latex resource recovering system of the invention, between the first water storage container of synthesising container jacket outlet
Pipeline also pass through the connection of the pipeline between valve and the first water storage container and degassing container jacket inlet.
Preferably, synthetic latex resource recovering system of the invention, the outlet of the first water storage container also with steam generator
Connection.
Preferably, synthetic latex resource recovering system of the invention, synthetic latex resource recovering system are styrene-butadiene latex money
Source recovery system or carboxylic styrene butadiene latex resource recovering system.
The beneficial effects of the present invention are:
Synthetic latex resource recovering system of the invention stores the water of different temperatures by three water storage containers respectively, and
And the water of three kinds of different temperatures is applied in the heating or cooling of synthesising container, growth container, degassing container or is used for
Steam is generated, water and thermal energy can be made full use of, play the effect of energy-saving and emission-reduction.
Detailed description of the invention
Present invention will be further explained below with reference to the attached drawings and examples.
Fig. 1 is the structural schematic diagram of the synthetic latex resource recovering system of the embodiment of the present invention；
Appended drawing reference in figure are as follows:
1- steam generator；2- mixing vessel；3- synthesising container；4- growth container；5- degassing container；The first water storage of 61-
Container；The second water storage container of 62-；63- third water storage container.
Specific embodiment
In conjunction with the accompanying drawings, the present invention is further explained in detail.These attached drawings are simplified schematic diagram, only with
Illustration illustrates basic structure of the invention, therefore it only shows the composition relevant to the invention.
Embodiment
The present embodiment provides a kind of synthetic latex resource recovering systems, as shown in Figure 1, comprising:
Steam generator 1 (steam boiler), for generating steam；
Mixing vessel 2 is used for mixed raw material；
Synthesising container 3, has collet on outer wall, and jacket inlet is connected to reception steam with steam generator 1 and heats synthesis
Material in container, for carrying out preliminary polymerization；
Grow up container 4, there is collet, for further being polymerize on outer wall；
Degassing container 5 has collet on outer wall, for deaerating for latex；
First water storage container 61 is connected to, for depositing with the entrance of 5 collet of the outlet of 3 collet of synthesising container and degassing container
High-temperature water after storing up steam liquefied, and high-temperature water is transported in 5 collet of degassing container when degassing container 5 is de-gassed operation
Material in degassing container 5 is heated and kept the temperature；
Second water storage container 62, outlet and steam generator 1 (can also be with mixing vessel 2) with growth 4 collet of container are even
It is logical, water is provided for storing the middle warm water of growth 4 collet of container outflow, and when steam generator 1 generates steam, or will be low
Warm water be used for as polymerize when raw material -- soft water (is passed through mixing vessel 2)；
Third water storage container 63 is connected to, for storing with the jacket inlet of the outlet of 5 collet of degassing container, container 4 of growing up
The water at low temperature of 5 collet of degassing container outflow, and the water at low temperature is used for the material of cooling growth container 4.
The synthetic latex resource recovering system of the present embodiment is mixed for producing styrene-butadiene latex or carboxylic styrene butadiene latex
Container 2, synthesising container 3, growth container 4, degassing container 5 are sequentially communicated, and complete part material mixing, synthesis in mixing vessel 2
Container 3 carries out preliminary polymerization, needs to heat at this time, and steam generator 1 generates steam and is passed into progress in the collet of synthesising container 3
Heating, initiation reaction, steam form high-temperature water (about 80-90 DEG C) in the collet heat release of synthesising container 3, are stored into the first water storage appearance
In device 61, (show as gas butadiene reaction therein to complete, container inner pressure decline after monomer is completely polymerized into small molecule
It is considered as completion reaction to an atmospheric pressure), it is carried out in material indentation growth container 4 in synthesising container 3；Container 4 of growing up is interior to be relied on
Exothermic polymerization reaction is spontaneous to be polymerize, and due to exothermic heat of reaction in growth container 4, temperature is excessively high in order to prevent, needs to introduce
Cooling water, therefore, the water at low temperature (about 30-50 DEG C) of third water storage container 63 introduce in growth 4 collet of container when absorbing heat at
Temperature required by long container holding technique, water at low temperature warm water (about 50-60 DEG C) in being formed after 4 collet of container of growing up,
It is stored in third water storage container 63；Latex is formed after material reaction in growth container 4, material is pressed into degassing container
In 5, nitrogen blowing degassing is carried out to latex in degassing container 5, nitrogen blowing will lead to the decline of latex temperature, in order to compensate at a temperature of
It drops, the high-temperature water in the first water storage container 61 is introduced in the collet of degassing container 5, for adding for the latex of degassing container 5
Heat, it is generally the case that high-temperature water can be more, therefore the first water storage container 61 can also be connected to steam generator 1, by high temperature water gas
It is melted into steam, becomes water at low temperature storage into third water storage container 63 by the high-temperature water of 5 collet of degassing container.Second water storage
Middle warm water in container 62, which is passed into, to be used to generate steam in steam generator 1, or is passed into and is passed through in mixing vessel 2.
The synthetic latex resource recovering system of above-described embodiment stores different temperatures by three water storage containers respectively
Water, and the water of three kinds of different temperatures is applied in the heating or cooling of synthesising container 3, growth container 4, degassing container 5
Or for generating steam, water and thermal energy can be made full use of, plays the effect of energy-saving and emission-reduction.
As an improvement the jacket inlet on growth container 4 is also connected to cooling water pipe, for receiving room temperature cooling
Water, to prevent 63 water of third water storage container that cooling effect is not enough not achieved.
As a further improvement, the pipeline between 3 the first water storage container of jacket outlet 61 of synthesising container also pass through valve with
The connection of pipeline between 5 jacket inlet of first water storage container 61 and degassing container, 3 jacket outlet of synthesising container when valve is opened
The high-temperature water of outflow flows into 5 collet of degassing container without between the first water storage container 61.
It is worth noting that steam generator 1 and mixing vessel 2 and synthesising container 3 and growth container 4 and de- in attached drawing 1
Connection relationship between gas container 5 does not show, this is the common connection type of synthetic latex equipment, respectively manages in recovery system
Flow control valve is installed, for controlling flow, to guarantee the temperature control of synthesis technology on road.
The synthetic latex resource recovering system of the present embodiment can be used for heat release when any synthesis, and polymerization process is divided into two
The synthetic latex equipment divided.
Taking the above-mentioned ideal embodiment according to the present invention as inspiration, through the above description, relevant staff is complete
Various changes and amendments can be carried out without departing from the scope of the technological thought of the present invention' entirely.The technology of this invention
Property range is not limited to the contents of the specification, it is necessary to which the technical scope thereof is determined according to the scope of the claim.
Claims (6)
1. a kind of synthetic latex resource recovering system characterized by comprising
Steam generator (1), for generating steam；
Mixing vessel (2) is used for mixed raw material；
Synthesising container (3), has collet on outer wall, and jacket inlet is connected to reception steam with steam generator (1) and heats synthesis
Material in container, for carrying out preliminary polymerization；
Grow up container (4), there is collet, for further being polymerize on outer wall；
Degassing container (5) has collet on outer wall, for deaerating for latex；
First water storage container (61) is connected to the entrance of the outlet of synthesising container (3) collet and degassing container (5) collet, is used for
High-temperature water after storing steam liquefied, and high-temperature water is transported to degassing container (5) when degassing container (5) is de-gassed operation
The material in degassing container (5) is heated and kept the temperature in collet；
Second water storage container (62) is connected to, for storing growth with the outlet of growth container (4) collet and steam generator (1)
The middle warm water of container (4) collet outflow, and warm water in this is used to generate steam in steam generator (1)；
Third water storage container (63) is connected to, for depositing with the jacket inlet of the outlet of degassing container (5) collet, growth container (4)
The water at low temperature of degassing container (5) collet outflow is stored up, and the water at low temperature is used for cooling growth container (4).
2. synthetic latex resource recovering system according to claim 1, which is characterized in that the second water storage container (62) goes out
Mouth is also connected to mixing vessel (2).
3. synthetic latex resource recovering system according to claim 1, which is characterized in that the collet in growth container (4)
Entrance is also connected to cooling water pipe, for receiving room temperature cooling water.
4. synthetic latex resource recovering system according to claim 1, which is characterized in that synthesising container (3) jacket outlet
Pipeline between first water storage container (61) also pass through valve and the first water storage container (61) and degassing container (5) jacket inlet it
Between pipeline connection.
5. synthetic latex resource recovering system according to claim 1-4, which is characterized in that the first water storage container
(61) outlet is also connected to steam generator (1).
6. synthetic latex resource recovering system according to claim 1-4, which is characterized in that synthetic latex resource
Recovery system is styrene-butadiene latex resource recovering system or carboxylic styrene butadiene latex resource recovering system.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710663395.7A CN107321277B (en) | 2017-08-05 | 2017-08-05 | A kind of synthetic latex resource recovering system |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710663395.7A CN107321277B (en) | 2017-08-05 | 2017-08-05 | A kind of synthetic latex resource recovering system |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN107321277A CN107321277A (en) | 2017-11-07 |
| CN107321277B true CN107321277B (en) | 2019-01-22 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201710663395.7A Active CN107321277B (en) | 2017-08-05 | 2017-08-05 | A kind of synthetic latex resource recovering system |
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Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108187596A (en) * | 2018-03-14 | 2018-06-22 | 德莱创节能科技（苏州）有限公司 | A kind of synthetic latex production system for recycling heat energy from waste gas |
| CN108380149A (en) * | 2018-03-14 | 2018-08-10 | 德莱创节能科技（苏州）有限公司 | A kind of method of synthetic latex production system recycling heat energy from waste gas |
| CN108467459B (en) * | 2018-04-16 | 2021-04-20 | 德莱创节能科技（苏州）有限公司 | Energy-saving and emission-reducing styrene-butadiene latex production system |
| CN111569808B (en) * | 2020-05-22 | 2022-06-17 | 中石化上海工程有限公司 | Energy integrated utilization bulk drug reaction purification system and process method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN202538754U (en) * | 2012-03-16 | 2012-11-21 | 骏马化纤股份有限公司 | Constant temperature device for preparing glue solution |
| CN105892521A (en) * | 2016-04-19 | 2016-08-24 | 山东豪迈机械制造有限公司 | Efficient temperature control system and temperature control method thereof |
| CN205575993U (en) * | 2016-04-28 | 2016-09-14 | 浙江天晨胶业股份有限公司 | Synthetic latex production system of closed recovery styrene |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6277954B2 (en) * | 1999-09-14 | 2001-08-21 | Kaneka Corporation | Method of stripping for latex of vinyl chloride paste resin, stripping apparatus, and vinyl chloride paste resin latex having low concentration of residual monomer |
-
2017
- 2017-08-05 CN CN201710663395.7A patent/CN107321277B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN202538754U (en) * | 2012-03-16 | 2012-11-21 | 骏马化纤股份有限公司 | Constant temperature device for preparing glue solution |
| CN105892521A (en) * | 2016-04-19 | 2016-08-24 | 山东豪迈机械制造有限公司 | Efficient temperature control system and temperature control method thereof |
| CN205575993U (en) * | 2016-04-28 | 2016-09-14 | 浙江天晨胶业股份有限公司 | Synthetic latex production system of closed recovery styrene |
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| CN107321277A (en) | 2017-11-07 |
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