CN107312640A - 一种含黄芩提取物的中药洗衣液的制备方法 - Google Patents

一种含黄芩提取物的中药洗衣液的制备方法 Download PDF

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CN107312640A
CN107312640A CN201710540700.3A CN201710540700A CN107312640A CN 107312640 A CN107312640 A CN 107312640A CN 201710540700 A CN201710540700 A CN 201710540700A CN 107312640 A CN107312640 A CN 107312640A
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单筱慧
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Abstract

一种含黄芩提取物的中药洗衣液的制备方法，属于洗衣液领域，包括：制备黄芩提取物，并加入烷基糖苷、脂肪醇聚氧乙烯醚、脂肪酰胺丙基氧化铵、十二烷基二甲基苄基氯化铵、山梨酸钾、海藻酸钠、壳聚糖、乙二胺四乙酸二钠、柠檬酸、香精、工业盐等，制备洗衣液。本发明的洗衣液具有良好的杀菌效果，且性能温和，健康环保，能保护手部皮肤且制备方法简单，适合规模化生产且去污率高。

Description

一种含黄芩提取物的中药洗衣液的制备方法
技术领域
本发明涉及洗衣液领域，尤其涉及一种含黄芩提取物的中药洗衣液的制备方法。
背景技术
随着环境的污染日益严重，衣物经普通清洗剂清洗后，放置于室内，由于室内环境潮湿，往往容易滋生大量细菌，对人体危害严重，尤其是贴身衣物和内衣。现有技术中多在洗衣液中添加化学杀菌剂，来达到杀菌的效果。这些化学添加剂会对人体皮肤造成一定程度的影响，皮肤经过洗衣液的浸泡后会对皮肤造成一些影响，导致皮肤粗糙、携带细菌或者过敏等，这是传统洗衣液存在的缺陷。中草药具有良好的消毒效果，而且没有副作用。
发明内容
根据现有技术中存在的问题，本发明提供了一种含黄芩提取物的中药洗衣液的制备方法，具有良好的杀菌效果，且不含化学杀菌剂，健康环保。
本发明采用以下技术方案：
一种含黄芩提取物的中药洗衣液的制备方法，包括以下步骤：
步骤一：洗净新鲜的黄芩，将水分晾干；
步骤二：将晾干后的黄芩置于微波炉中，中火干燥2-3min；
步骤三：将干燥后的黄芩，放入粉碎机中粉碎，将粉碎后的黄芩过200目筛，得黄芩粉末；
步骤四：称取黄芩粉末100g，浸泡0.5h，加热煎煮提取3次，第1次加入25倍黄芩重量的水，煎煮提取2h，过滤得滤液1，第2次加入20倍滤渣重量的水，煎煮提取1.5h，过滤得滤液2，第3次加15倍滤渣重量的水，煎煮提取1h，过滤得滤液3，将滤液1、2、3合并，加热浓缩至滤液的体积为黄芩重量的3-6倍，过滤即得黄芩提取物；
步骤五：按重量份称取去离子水90份，分成等量的3份，取其中一份加入搅拌器中，加热至45℃后，边搅拌边加入烷基糖苷10重量份、脂肪醇聚氧乙烯醚12重量份、脂肪酰胺丙基氧化铵8重量份、十二烷基二甲基苄基氯化铵3重量份，继续搅拌，搅拌器转速为100r/min，搅拌35min；
步骤六：按重量份称取的山梨酸钾2份、海藻酸钠1份、壳聚糖1份以及三分之一的去离子水加入搅拌器中，搅拌器转速为80r/min，搅拌20min；
步骤七：按重量份称取黄芩提取物3份以及余量的去离子水加入搅拌器中继续搅拌35min后，转速为50r/min；
步骤八：搅拌器加热升温至80℃，保温20min，降温至40℃，按重量份再加入乙二胺四乙酸二钠0.2份、柠檬酸0.1份、香精0.1份、工业盐0.1份，并加入PH调节剂，调节PH至6-7，即得洗衣液。
优选的，步骤八中所述的香精为柠檬香精或玫瑰香精。
优选的，步骤三中所述的粉碎是采用LD-Y400A高速万能粉碎机。
本发明的有益效果在于：
1)本发明添加黄芩提取物，黄芩具有良好的抑菌杀菌的效果。
2)本发明添加十二烷基二甲基苄基氯化铵，是一种阳离子表面活性剂，同时也是一种非氧化性杀菌剂，具有广谱、高效的杀菌效果。
3)本发明的洗衣液性能温和，健康环保，能保护手部皮肤且制备方法简单，适合规模化生产且去污率高。
具体实施方式
以下将结合具体实施例对本发明做进一步的说明。
实施例1
一种含黄芩提取物的中药洗衣液的制备方法，包括以下步骤：
步骤一：洗净新鲜的黄芩，将水分晾干；
步骤二：将晾干后的黄芩置于微波炉中，中火干燥2-3min；
步骤三：将干燥后的黄芩，放入粉碎机中粉碎，将粉碎后的黄芩过200目筛，得黄芩粉末；
步骤四：称取黄芩粉末100g，浸泡0.5h，加热煎煮提取3次，第1次加入25倍黄芩重量的水，煎煮提取2h，过滤得滤液1，第2次加入20倍滤渣重量的水，煎煮提取1.5h，过滤得滤液2，第3次加15倍滤渣重量的水，煎煮提取1h，过滤得滤液3，将滤液1、2、3合并，加热浓缩至滤液的体积为黄芩重量的3-6倍，过滤即得黄芩提取物；
步骤五：按重量份称取去离子水90份，分成等量的3份，取其中一份加入搅拌器中，加热至45℃后，边搅拌边加入烷基糖苷10重量份、脂肪醇聚氧乙烯醚12重量份、脂肪酰胺丙基氧化铵8重量份、十二烷基二甲基苄基氯化铵3重量份，继续搅拌，搅拌器转速为100r/min，搅拌35min；
步骤六：按重量份称取的山梨酸钾2份、海藻酸钠1份、壳聚糖1份以及三分之一的去离子水加入搅拌器中，搅拌器转速为80r/min，搅拌20min；
步骤七：按重量份称取黄芩提取物3份以及余量的去离子水加入搅拌器中继续搅拌35min后，转速为50r/min；
步骤八：搅拌器加热升温至80℃，保温20min，降温至40℃，按重量份再加入乙二胺四乙酸二钠0.2份、柠檬酸0.1份、香精0.1份、工业盐0.1份，并加入PH调节剂，调节PH至6-7，即得洗衣液。
步骤八中所述的香精为柠檬香精或玫瑰香精。
步骤三中所述的粉碎是采用LD-Y400A高速万能粉碎机。
将本发明实施例1制得的洗衣液和市面上的同类型洗衣液的去污性能对比结果见下表1。
表1
项目 去污率％
实施例1 85以上
同类型洗衣液 70-75

Claims (3)

1.一种含黄芩提取物的中药洗衣液的制备方法，其特征在于，包括以下步骤：
步骤一：洗净新鲜的黄芩，将水分晾干；
步骤二：将晾干后的黄芩置于微波炉中，中火干燥2-3min；
步骤三：将干燥后的黄芩，放入粉碎机中粉碎，将粉碎后的黄芩过200目筛，得黄芩粉末；
步骤四：称取黄芩粉末100g，浸泡0.5h，加热煎煮提取3次，第1次加入25倍黄芩重量的水，煎煮提取2h，过滤得滤液1，第2次加入20倍滤渣重量的水，煎煮提取1.5h，过滤得滤液2，第3次加15倍滤渣重量的水，煎煮提取1h，过滤得滤液3，将滤液1、2、3合并，加热浓缩至滤液的体积为黄芩重量的3-6倍，过滤即得黄芩提取物；
步骤五：按重量份称取去离子水90份，分成等量的3份，取其中一份加入搅拌器中，加热至45℃后，边搅拌边加入烷基糖苷10重量份、脂肪醇聚氧乙烯醚12重量份、脂肪酰胺丙基氧化铵8重量份、十二烷基二甲基苄基氯化铵3重量份，继续搅拌，搅拌器转速为100r/min，搅拌35min；
步骤六：按重量份称取的山梨酸钾2份、海藻酸钠1份、壳聚糖1份以及三分之一的去离子水加入搅拌器中，搅拌器转速为80r/min，搅拌20min；
步骤七：按重量份称取黄芩提取物3份以及余量的去离子水加入搅拌器中继续搅拌35min后，转速为50r/min；
步骤八：搅拌器加热升温至80℃，保温20min，降温至40℃，按重量份再加入乙二胺四乙酸二钠0.2份、柠檬酸0.1份、香精0.1份、工业盐0.1份，并加入PH调节剂，调节PH至6-7，即得洗衣液。
2.根据权利要求1所述的一种含黄芩提取物的中药洗衣液的制备方法，其特征在于：步骤八中所述的香精为柠檬香精或玫瑰香精。
3.根据权利要求1所述的一种含黄芩提取物的中药洗衣液的制备方法，其特征在于：步骤三中所述的粉碎是采用LD-Y400A高速万能粉碎机。
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CN103194341A (zh) * 2013-04-25 2013-07-10 上海巴方精细化工有限公司 黄芩低刺激护肤香皂
CN104178370A (zh) * 2014-08-29 2014-12-03 成都顺发消洗科技有限公司 一种含中药成分的杀菌洗衣液及其制备方法
CN105087189A (zh) * 2015-08-28 2015-11-25 吉林大学 一种植物抗菌复方杀菌皂及其制备方法
CN106244358A (zh) * 2016-08-18 2016-12-21 河南中医学院 一种抗菌消炎的渲染中药手工皂

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103194341A (zh) * 2013-04-25 2013-07-10 上海巴方精细化工有限公司 黄芩低刺激护肤香皂
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