CN107287904A - A kind of yellowing-proof finish method of real silk fabric - Google Patents
A kind of yellowing-proof finish method of real silk fabric Download PDFInfo
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- CN107287904A CN107287904A CN201710492752.8A CN201710492752A CN107287904A CN 107287904 A CN107287904 A CN 107287904A CN 201710492752 A CN201710492752 A CN 201710492752A CN 107287904 A CN107287904 A CN 107287904A
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- yellowing
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
- D06B3/00—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating
- D06B3/10—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating of fabrics
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/02—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with hydrocarbons
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/244—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
- D06M13/248—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing sulfur
- D06M13/256—Sulfonated compounds esters thereof, e.g. sultones
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/15—Proteins or derivatives thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/10—Animal fibres
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/25—Resistance to light or sun, i.e. protection of the textile itself as well as UV shielding materials or treatment compositions therefor; Anti-yellowing treatments
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention discloses a kind of yellowing-proof finish method of real silk fabric, comprise the following steps：After yellowing-proof finish dilution agent, real silk fabric is bakeed in 5min preheatings, the dilution that yellowing-proof finish agent is impregnated in afterwards under the conditions of 50 DEG C, two leachings two are rolled, and pick-up rate is 80%, dried under the conditions of 50 70 DEG C, 8 15min are bakeed under the conditions of 80 DEG C.The method for sorting uses new yellowing-proof finish agent, after Silk Fabric Finishing, and real silk fabric can have lasting yellowing resistance energy, and yellowing is still difficult by repeatedly washing.And the method for sorting is simple to operate, the pliability of fabric is not influenceed, can effectively improve the commercial value of fabric.
Description
Technical field：
The present invention relates to field of textiles, the yellowing-proof finish method of more particularly to a kind of real silk fabric.
Background technology
In use, easily photooxidation occurs for real silk fabric so that fabric yellowing, embrittlement, have a strong impact on fabric
Aesthetics and comfort level.Real silk fabric yellowing is primarily due to tryptophan, tyrosine in silk protein etc. and absorbs ultraviolet
After line, occur dehydrogenation oxidation reaction to produce yellow substance.
Early in the sixties in last century, ultra-violet absorber is to be handled by the more anti-yellowing applied to real silk fabric,
Ultra-violet absorber BP-4 (HMBS) can be effectively absorption ultraviolet.And have experiment
Point out that HMBS is applied to that in real silk fabric good anti-yellowing effect can be played, but HMBS washability is poor, and be not suitable for
It is used as the persistence yellowing-proof finish of real silk fabric.Had at present using more extensive yellowing-proof finish method：Ultraviolet radiation absorption
Agent arrangement, antioxidant are arranged and resin finishing.Although the notable still washability of anti-yellowing effect is poor for first two method, fabric
It can be remarkably decreased in repeatedly washing rear defence yellowing performance.Although preferable still its anti-yellowing performance of resin finishing wash durability is not
Good, the anti-yellowing effect of fabric can weaken under the irradiation of prolonged sunlight.
Chinese patent 201410443885.2 discloses a kind of yellowing-proof finish method of silk fabric, including following step
Suddenly：Prepare the yellowing-proof finish agent of silk fabric；Silk fabric is immersed in above-mentioned yellowing-proof finish agent, then normal temperature two soaks
Two prick, and pick-up is 100%；Silk fabric is taken out, 40-60 DEG C is dried 10-20min, and then 120-150 DEG C bakes 5-10min.Its
Middle yellowing-proof finish agent includes 2- hydroxyl -4- methoxy benzophenone -5- sulfonic acid, thiourea resin and ammonium acetate.The method for sorting
Persistence applied to the anti-yellowing performance of real silk fabric still needs further raising.Therefore, study a kind of efficient, water-fastness
Real silk fabric yellowing-proof finish method is extremely necessary.
The content of the invention
It is an object of the invention to provide a kind of yellowing-proof finish method of real silk fabric, the method for sorting is prevented using new
Yellowing finishing agent, after Silk Fabric Finishing, real silk fabric can have lasting yellowing resistance energy, by repeatedly washing still not
Easy yellowing.And the method for sorting is simple to operate, the pliability of fabric is not influenceed, can effectively improve the commercial value of fabric.
To achieve the above object, the present invention uses following technical scheme：
A kind of yellowing-proof finish method of real silk fabric, it is characterised in that, comprise the following steps：
(1) after, BTA modified polyorganosiloxane is mixed with emulsifying agent, add homogenizer in it is fully emulsified, then with silk
Protein solution, chitosan, dispersant and water are well mixed, are configured as yellowing-proof finish agent；
(2), by after yellowing-proof finish dilution agent, real silk fabric is bakeed to 5min preheatings under the conditions of 50 DEG C, impregnated afterwards
In the dilution of yellowing-proof finish agent, two leachings two are rolled, and pick-up rate is 80%, are dried under the conditions of 50-70 DEG C, in 80 DEG C of conditions
Lower baking 8-15min；
Wherein, the structural formula of the BTA modified polyorganosiloxane is shown below：
It is preferred that, m in the BTA modified polyorganosiloxane structural formula:N=5:2.
It is preferred that, the yellowing-proof finish agent includes following components, in terms of parts by weight：
70-90 parts of BTA modified polyorganosiloxane, 2-4 parts of fibroin solutions, 20-40 parts of chitosan, dispersant 1-
2 parts, 2-5 parts of emulsifying agent, 20-30 parts of water.
It is preferred that, the fibroin solutions are the solution that concentration containing fibroin is 30%, are prepared by discarded silk
Form.
It is preferred that, the dispersant is one kind in atoleine, Arlacel-60 or Tween-80.
It is preferred that, the emulsifying agent is neopelex, sodium laurate or ethoxylated dodecyl alcohol
In one or more mixtures.
It is preferred that, the dilution ratio of yellowing-proof finish agent is 1 in the step 2:40-60.
The invention has the advantages that, the present invention uses new yellowing-proof finish agent, and the finishing agent is with benzo three
Azoles modified polyorganosiloxane is main component, and the composition can be very good to be attached to silk fiber surface, and with stronger anti-general
Yellow performance.BTA modified polyorganosiloxane interacts with other components so that adhesive force of the finishing agent in fabric face
By force, fabric can still keep higher yellowing resistance energy after repeatedly washing.Fabric through the method for sorting after arranging simultaneously, still
Excellent feel can be kept, the pliability of fabric will not have an impact, and can keep higher commercial value.
Embodiment
In order to be better understood from the present invention, below by embodiment, the present invention is further described, and embodiment is served only for solution
The present invention is released, any restriction will not be constituted to the present invention.
Embodiment 1
(1) after, 70 parts of BTA modified polyorganosiloxanes are mixed with 2 parts of neopelexes, homogenizer is added
In it is fully emulsified, then be well mixed, be configured to 2 parts of silk protein solutions, 30 parts of chitosans, 1 part of atoleine and 20 parts of water
For yellowing-proof finish agent；
(2), by after 50 times of yellowing-proof finish dilution agent, real silk fabric is bakeed to 5min preheatings under the conditions of 50 DEG C, afterwards
In the dilution for being impregnated in yellowing-proof finish agent, two leachings two are rolled, and pick-up rate is 80%, are dried under the conditions of 60 DEG C, in 80 DEG C of bars
15min is bakeed under part；
Real silk fabric after yellowing-proof finish is with after carbon arc light irradiation 20h, whiteness retention after being detected using leucometer
For 97.2%；After scrubbed 10 times of fabric after arrangement, after carbon arc light irradiation 20h, whiteness is protected after being detected using leucometer
It is 94.3% to stay rate.
Embodiment 2
(1) after, 75 parts of BTA modified polyorganosiloxanes are mixed with 3 parts of sodium laurates, add in homogenizer
It is fully emulsified, then be well mixed with 4 parts of silk protein solutions, 35 parts of chitosans, 1 part of atoleine and 20 parts of water, it is configured as
Yellowing-proof finish agent；
(1), by after 50 times of yellowing-proof finish dilution agent, real silk fabric is bakeed to 5min preheatings under the conditions of 50 DEG C, afterwards
In the dilution for being impregnated in yellowing-proof finish agent, two leachings two are rolled, and pick-up rate is 80%, are dried under the conditions of 60 DEG C, in 80 DEG C of bars
15min is bakeed under part；
Real silk fabric after yellowing-proof finish is with after carbon arc light irradiation 20h, whiteness retention after being detected using leucometer
For 98.3%；After scrubbed 10 times of fabric after arrangement, after carbon arc light irradiation 20h, whiteness is protected after being detected using leucometer
It is 95.2% to stay rate.
Embodiment 3
(1) after, 80 parts of BTA modified polyorganosiloxanes are mixed with 3 parts of sodium laurates, add in homogenizer
It is fully emulsified, then be well mixed with 2 parts of silk protein solutions, 25 parts of chitosans, 1 part of Arlacel-60 and 20 parts of water, it is configured as
Yellowing-proof finish agent；
(2), by after 50 times of yellowing-proof finish dilution agent, real silk fabric is bakeed to 5min preheatings under the conditions of 50 DEG C, afterwards
In the dilution for being impregnated in yellowing-proof finish agent, two leachings two are rolled, and pick-up rate is 80%, are dried under the conditions of 60 DEG C, in 80 DEG C of bars
15min is bakeed under part；
Real silk fabric after yellowing-proof finish is with after carbon arc light irradiation 20h, whiteness retention after being detected using leucometer
For 98.8%；After scrubbed 10 times of fabric after arrangement, after carbon arc light irradiation 20h, whiteness is protected after being detected using leucometer
It is 93.4% to stay rate.
Embodiment 4
(1) after, 85 parts of BTA modified polyorganosiloxanes are mixed with 4 parts of ethoxylated dodecyl alcohols, homogenizer is added
In it is fully emulsified, then be well mixed, be configured to 4 parts of silk protein solutions, 20 parts of chitosans, 2 parts of Tween-80s and 20 parts of water
For yellowing-proof finish agent；
(2), by after 50 times of yellowing-proof finish dilution agent, real silk fabric is bakeed to 5min preheatings under the conditions of 50 DEG C, afterwards
In the dilution for being impregnated in yellowing-proof finish agent, two leachings two are rolled, and pick-up rate is 80%, are dried under the conditions of 60 DEG C, in 80 DEG C of bars
15min is bakeed under part；
Real silk fabric after yellowing-proof finish is with after carbon arc light irradiation 20h, whiteness retention after being detected using leucometer
For 97.8%；After scrubbed 10 times of fabric after arrangement, after carbon arc light irradiation 20h, whiteness is protected after being detected using leucometer
It is 92.8% to stay rate.
Embodiment 5
(1) after, 90 parts of BTA modified polyorganosiloxanes are mixed with 5 parts of ethoxylated dodecyl alcohols, homogenizer is added
In it is fully emulsified, then be well mixed, be configured to 3 parts of silk protein solutions, 40 parts of chitosans, 2 parts of Tween-80s and 20 parts of water
For yellowing-proof finish agent；
(2), by after 50 times of yellowing-proof finish dilution agent, real silk fabric is bakeed to 5min preheatings under the conditions of 50 DEG C, afterwards
In the dilution for being impregnated in yellowing-proof finish agent, two leachings two are rolled, and pick-up rate is 80%, are dried under the conditions of 60 DEG C, in 80 DEG C of bars
15min is bakeed under part；
Real silk fabric after yellowing-proof finish is with after carbon arc light irradiation 20h, whiteness retention after being detected using leucometer
For 99.1%；After scrubbed 10 times of fabric after arrangement, after carbon arc light irradiation 20h, whiteness is protected after being detected using leucometer
It is 95.7% to stay rate.
Claims (7)
1. a kind of yellowing-proof finish method of real silk fabric, it is characterised in that comprise the following steps：
(1) after, BTA modified polyorganosiloxane is mixed with emulsifying agent, add homogenizer in it is fully emulsified, then with silk-fibroin
Solution, chitosan, dispersant and water are well mixed, are configured as yellowing-proof finish agent；
(2), by after yellowing-proof finish dilution agent, real silk fabric is bakeed to 5min preheatings under the conditions of 50 DEG C, is impregnated in afterwards anti-
In the dilution of yellowing finishing agent, two leachings two are rolled, and pick-up rate is 80%, are dried under the conditions of 50-70 DEG C, are dried under the conditions of 80 DEG C
Roast 8-15min；
Wherein, the structural formula of the BTA modified polyorganosiloxane is shown below.
2. the yellowing-proof finish method of real silk fabric according to claim 1, it is characterised in that the BTA is modified
M in polysiloxane structure formula:N=5:2.
3. the yellowing-proof finish method of real silk fabric according to claim 1, it is characterised in that the yellowing-proof finish agent
Comprising following components, in terms of parts by weight：
70-90 parts of BTA modified polyorganosiloxane, 2-4 parts of fibroin solutions, 20-40 parts of chitosan, 1-2 parts of dispersant,
2-5 parts of emulsifying agent, 20-30 parts of water.
4. the yellowing-proof finish method of the real silk fabric according to claim 1 or 3, it is characterised in that the fibroin
Solution is the solution that concentration containing fibroin is 30%, is prepared from by discarded silk.
5. the yellowing-proof finish method of the real silk fabric according to claim 1 or 3, it is characterised in that the dispersant is
One kind in atoleine, Arlacel-60 or Tween-80.
6. the yellowing-proof finish method of the real silk fabric according to claim 1 or 3, it is characterised in that the emulsifying agent is
One or more mixtures in neopelex, sodium laurate or ethoxylated dodecyl alcohol.
7. the yellowing-proof finish method of real silk fabric according to claim 1, it is characterised in that prevent in the step 2 general
The dilution ratio of yellow finishing agent is 1:40-60.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201710492752.8A CN107287904A (en) | 2017-06-26 | 2017-06-26 | A kind of yellowing-proof finish method of real silk fabric |
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| CN201710492752.8A CN107287904A (en) | 2017-06-26 | 2017-06-26 | A kind of yellowing-proof finish method of real silk fabric |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108486899A (en) * | 2018-04-21 | 2018-09-04 | 湖南辰砾新材料有限公司 | A kind of fabric softener and preparation method thereof |
| CN111172740A (en) * | 2020-03-05 | 2020-05-19 | 南通大学 | Anti-yellowing antibacterial real silk fabric and preparation method thereof |
| CN112921660A (en) * | 2021-01-26 | 2021-06-08 | 江红丽 | Antibacterial comfortable underwear knitted fabric and preparation method thereof |
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|---|---|---|---|---|
| CN1057304A (en) * | 1991-07-22 | 1991-12-25 | 浙江进出口商品检验技术研究所 | Anti-yellowing finishing agent of novel silk and preparation method thereof |
| CN104233788A (en) * | 2014-09-28 | 2014-12-24 | 苏州印丝特纺织数码科技有限公司 | Finishing technology for yellowing prevention of silk fabric |
| CN104233808A (en) * | 2014-09-03 | 2014-12-24 | 苏州印丝特纺织数码科技有限公司 | Anti-yellowing finishing method for silk fabric |
-
2017
- 2017-06-26 CN CN201710492752.8A patent/CN107287904A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1057304A (en) * | 1991-07-22 | 1991-12-25 | 浙江进出口商品检验技术研究所 | Anti-yellowing finishing agent of novel silk and preparation method thereof |
| CN104233808A (en) * | 2014-09-03 | 2014-12-24 | 苏州印丝特纺织数码科技有限公司 | Anti-yellowing finishing method for silk fabric |
| CN104233788A (en) * | 2014-09-28 | 2014-12-24 | 苏州印丝特纺织数码科技有限公司 | Finishing technology for yellowing prevention of silk fabric |
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| 田俊荣等: "《纺织品功能整理》", 31 October 2015, 中国纺织出版社 * |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108486899A (en) * | 2018-04-21 | 2018-09-04 | 湖南辰砾新材料有限公司 | A kind of fabric softener and preparation method thereof |
| CN108486899B (en) * | 2018-04-21 | 2020-08-07 | 上海鑫妙纺织助剂有限公司 | Fabric softening finishing agent and preparation method thereof |
| CN111172740A (en) * | 2020-03-05 | 2020-05-19 | 南通大学 | Anti-yellowing antibacterial real silk fabric and preparation method thereof |
| CN112921660A (en) * | 2021-01-26 | 2021-06-08 | 江红丽 | Antibacterial comfortable underwear knitted fabric and preparation method thereof |
| CN112921660B (en) * | 2021-01-26 | 2022-09-20 | 金发拉比妇婴童用品股份有限公司 | Antibacterial comfortable underwear knitted fabric and preparation method thereof |
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