CN107281263A - A kind of composition and preparation method thereof, sachet and application - Google Patents

A kind of composition and preparation method thereof, sachet and application Download PDF

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Publication number
CN107281263A
CN107281263A CN201710048544.9A CN201710048544A CN107281263A CN 107281263 A CN107281263 A CN 107281263A CN 201710048544 A CN201710048544 A CN 201710048544A CN 107281263 A CN107281263 A CN 107281263A
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China
Prior art keywords
parts
composition
preparation
borneol
eupatorium
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Inventor
陈珍
黄福荣
马春霓
李佳莉
丁重帅
张荷兰
赵有亮
黄文亮
张明
杨先振
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Chuxiong Medical College
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Chuxiong Medical College
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Publication of CN107281263A publication Critical patent/CN107281263A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/54Lauraceae (Laurel family), e.g. cinnamon or sassafras
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K31/00Medicinal preparations containing organic active ingredients
    • A61K31/045Hydroxy compounds, e.g. alcohols; Salts thereof, e.g. alcoholates
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/28Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/28Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
    • A61K36/282Artemisia, e.g. wormwood or sagebrush
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/53Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
    • A61K36/532Agastache, e.g. giant hyssop
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/53Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
    • A61K36/535Perilla (beefsteak plant)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K9/00Medicinal preparations characterised by special physical form
    • A61K9/0012Galenical forms characterised by the site of application
    • A61K9/007Pulmonary tract; Aromatherapy
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K9/00Medicinal preparations characterised by special physical form
    • A61K9/0087Galenical forms not covered by A61K9/02 - A61K9/7023
    • A61K9/009Sachets, pouches characterised by the material or function of the envelope
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/30Extraction of the material
    • A61K2236/33Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
    • A61K2236/331Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation or decoction
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/50Methods involving additional extraction steps
    • A61K2236/51Concentration or drying of the extract, e.g. Lyophilisation, freeze-drying or spray-drying
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/50Methods involving additional extraction steps
    • A61K2236/53Liquid-solid separation, e.g. centrifugation, sedimentation or crystallization

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  • Health & Medical Sciences (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Chemical & Material Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • General Health & Medical Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • Medicinal Chemistry (AREA)
  • Epidemiology (AREA)
  • Alternative & Traditional Medicine (AREA)
  • Mycology (AREA)
  • Microbiology (AREA)
  • Medical Informatics (AREA)
  • Botany (AREA)
  • Biotechnology (AREA)
  • Engineering & Computer Science (AREA)
  • Pulmonology (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

The invention discloses a kind of composition and preparation method thereof, sachet and application, described composition includes parts by weight of raw materials:3 ~ 10 parts of folium artemisiae argyi, 3 ~ 10 parts of wrinkled giant hyssop, 3 ~ 10 parts of cassia twig, 3 ~ 10 parts of purple perilla, 3 ~ 8 parts of eupatorium, 3 ~ 6 parts of borneol;The preparation method of described composition includes pre-treatment, extraction, post processing;The Chinese medicine sachet that described composition is prepared;Application of the described composition in preventing/treating cold in children.

Description

A kind of composition and preparation method thereof, sachet and application
Technical field
The invention belongs to drug preparation technique field, and in particular to a kind of composition and preparation method thereof, sachet and application.
Background technology
Cold in children, is also named acute upper respiratory infection (acute upper res piratory infections), is The most common disease of children, mainly invades nose, nasopharynx and pharyngeal, therefore conventional " acute nasopharyngitis " (flu), " acpuei pharyngitis " " acute tonsillitis " etc. diagnoses noun, also can be collectively referred to as the infection of the upper respiratory tract, referred to as " upper sense ".Nasopharynx infection often may occur in which simultaneously Disease is sent out, is related to adjacent organs such as larynx, tracheae, lung, oral cavity, nasal sinus, middle ear, eye and lymphonodi cervicales etc..Sometimes pharynx nasalis is primary The symptom of disease has taken a turn for the better or disappeared, and its complication can delay or aggravate.In temperature Change too big season, cold in children occurs Probability rise, have in addition falls ill repeatedly.Therefore, it is very necessary to develop a kind of product that can solve above-mentioned health problem 's.
The content of the invention
The first object of the present invention is to provide a kind of composition;Second purpose is the preparation of the composition described in offer Method;3rd purpose is to provide the Chinese medicine sachet being made using described composition;4th purpose is the group described in offer The application of compound.
The first object of the present invention is achieved in that described composition includes parts by weight of raw materials:3 ~ 10 parts of folium artemisiae argyi, the leaves of pulse plants Fragrant 3 ~ 10 parts, 3 ~ 10 parts of cassia twig, 3 ~ 10 parts of purple perilla, 3 ~ 8 parts of eupatorium, 3 ~ 6 parts of borneol.
The second object of the present invention is achieved in that the preparation method of described composition, specifically includes following steps:
A, pre-treatment:Folium artemisiae argyi, wrinkled giant hyssop, cassia twig, purple perilla, eupatorium are pulverized and sieved respectively, is then well mixed and obtains mixture;
B, extraction:Again in the mixture add 3 ~ 10 times of mixture weight water carry out water extraction, then with 3 ~ 10 times amount 75% second Alcoholic solution is precipitated, and extract solution is obtained after filtering;
C, post processing:By extract solution it is concentrated, dry, pulverize and sieve, add that borneol is well mixed to obtain objective composition.
The third object of the present invention is achieved in that the Chinese medicine sachet prepared using described composition, described Chinese medicine sachet be with breathable fabric parcel composition made from sachet.
The fourth object of the present invention is achieved in that application of the described composition in preventing/treating cold in children. There is good opsonic action to cold in children caused by a variety of different reasons.Particularly to children's recurrent exerbation, cureless Cold symptoms, have effects that conditioning and righting.To following symptoms, with significant treatment or improvement result:Nasal obstruction, throat swell Bitterly, fever and chills headache, receive poor, alliteration uncomfortable in chest, chest gastral cavity ruffian, vomiting and diarrhea.
The advanced water-filling of extraction process of the preparation method of the present invention is extracted, and ethanol solution precipitation process is then used again, can Increase substantially product active ingredient concentration;Using folium artemisiae argyi, wrinkled giant hyssop as monarch drug in a prescription in the present composition, Papillary has fragrance Change is turbid, wards off effect of dirty removing toxic substances.Folium artemisiae argyi is pungent, hardship, warm-natured, enters spleen, liver and kidney channel, and fragrance is pure and fresh, can dispel poison gas, except dirt, There is rationale blood, by cold-dampness, Wen Jing, hemostasis, antiabortive work(;Wrinkled giant hyssop is pungent, slightly warm in nature, return lung, spleen, stomach, there is driving away summer heat inducing diaphoresis, changes Effect of wet and stomach.We are with cassia twig, purple perilla, eupatorium altogether for ministerial drug, and cassia twig, purple perilla, the medicine of eupatorium three take its inducing diaphoresis to dispel with using Wet, warming spleen and stomach for dispelling cold effect, cassia twig is pungent sweet, temperature, enters bladder, the heart, lung channel, can expelling cold and relieving exterior syndrome, warming meridian, activating YANG and prormoting functioning of QI;It is purple Soviet Union is pungent, warm-natured.Return lung, the spleen channel, there is inducing sweat and dispelling exogenous evils, regulating the flow of QI to ease the stomach, effect of solving toxin of fish and crab;Eupatorium is pungent, puts down, enters spleen, stomach Through with removing dampness by means of aromatics, appetizing of being amusing delivers effect of relieving summer-heat.Using borneol as adjuvant in prescription, the work(of its radiating of having one's ideas straightened out is taken Effect, plays the curative effect of auxiliary monarch drug in a prescription cold dispelling, borneol is pungent, hardship, is slightly cold, Delicate fragrance a surname dissipate, and with inducing resuscitation of having one's ideas straightened out, heat-clearing dissipates poison is bright Mesh moves back effect of screen.Full side's all medicines share, complements each other, has effects that obvious cold dispelling brings down a fever, delivers relieving summer-heat, can play The effect of preventing/treating cold in children.
Embodiment
With reference to embodiment, the present invention is further illustrated, but the present invention is not any limitation as in any way, Based on present invention teach that any conversion or replacement made, belong to protection scope of the present invention.
Composition of the present invention includes parts by weight of raw materials:3 ~ 10 parts of folium artemisiae argyi, 3 ~ 10 parts of wrinkled giant hyssop, 3 ~ 10 parts of cassia twig, purple 3 ~ 10 parts of Soviet Union, 3 ~ 8 parts of eupatorium, 3 ~ 6 parts of borneol.
Described composition includes parts by weight of raw materials:4 ~ 8 parts of folium artemisiae argyi, 4 ~ 8 parts of wrinkled giant hyssop, 4 ~ 8 parts of cassia twig, 4 ~ 8 parts of purple perilla, pendant Blue 5 ~ 7 parts, 5 ~ 6 parts of borneol.
Described composition includes parts by weight of raw materials:5 ~ 7 parts of folium artemisiae argyi, 5 ~ 7 parts of wrinkled giant hyssop, 5 ~ 7 parts of cassia twig, 5 ~ 7 parts of purple perilla, pendant Blue 5.5 ~ 6.5 parts, 5.5 ~ 6.5 parts of borneol.
The preparation method of described composition, specifically includes following steps:
A, pre-treatment:Folium artemisiae argyi, wrinkled giant hyssop, cassia twig, purple perilla, eupatorium are pulverized and sieved respectively, is then well mixed and obtains mixture;
B, extraction:Again in the mixture add 3 ~ 10 times of mixture weight water carry out water extraction, then with 3 ~ 10 times amount 75% second Alcoholic solution is precipitated, and extract solution is obtained after filtering;
C, post processing:By extract solution it is concentrated, dry, pulverize and sieve, add that borneol is well mixed to obtain objective composition.
The extraction time that described water is extracted is 18 ~ 30 hours.
The Extracting temperature that described water is extracted is 40 ~ 50 DEG C.
Described sieving was 20 mesh sieves.
Described concentration is to be concentrated into the g/ml of relative density 1.9 ~ 2.0.
The Chinese medicine sachet that described composition is prepared, described Chinese medicine sachet is to wrap up composition system with breathable fabric The sachet obtained.
Application of the described composition in preventing/treating cold in children.
With reference to embodiment 1 ~ 10, the invention will be further described.
Embodiment 1
Composition includes parts by weight of raw materials:3 parts of folium artemisiae argyi, 3 parts of wrinkled giant hyssop, 3 parts of cassia twig, 3 parts of purple perilla, 3 parts of eupatorium, 3 parts of borneol.
Embodiment 2
Composition includes parts by weight of raw materials:10 parts of folium artemisiae argyi, 10 parts of wrinkled giant hyssop, 10 parts of cassia twig, 10 parts of purple perilla, 8 parts of eupatorium, 6 parts of borneol.
Embodiment 3
Composition includes parts by weight of raw materials:4 parts of folium artemisiae argyi, 4 parts of wrinkled giant hyssop, 4 parts of cassia twig, 4 parts of purple perilla, 5 parts of eupatorium, 5 parts of borneol.
Embodiment 4
Composition includes parts by weight of raw materials:8 parts of folium artemisiae argyi, 8 parts of wrinkled giant hyssop, 8 parts of cassia twig, 8 parts of purple perilla, 7 parts of eupatorium, 6 parts of borneol.
Embodiment 5
Composition includes parts by weight of raw materials:5 parts of folium artemisiae argyi, 5 parts of wrinkled giant hyssop, 5 parts of cassia twig, 5 parts of purple perilla, 5.5 parts of eupatorium, 5.5 parts of borneol.
Embodiment 6
Composition includes parts by weight of raw materials:7 parts of folium artemisiae argyi, 7 parts of wrinkled giant hyssop, 7 parts of cassia twig, 7 parts of purple perilla, 6.5 parts of eupatorium, 6.5 parts of borneol.
Embodiment 7
The preparation method of described composition, specifically includes following steps:
A, pre-treatment:Folium artemisiae argyi, wrinkled giant hyssop, cassia twig, purple perilla, eupatorium are pulverized and sieved respectively, is then well mixed and obtains mixture;
B, extraction:Again in the mixture add 3 times of mixture weight water carry out water extraction, then with 3 times measure 75% ethanol solutions Precipitation, extract solution is obtained after filtering;
C, post processing:By extract solution it is concentrated, dry, pulverize and sieve, add that borneol is well mixed to obtain objective composition.
Embodiment 8
The preparation method of described composition, specifically includes following steps:
A, pre-treatment:Folium artemisiae argyi, wrinkled giant hyssop, cassia twig, purple perilla, eupatorium are pulverized and sieved respectively, is then well mixed and obtains mixture;
B, extraction:Again in the mixture add 6.5 times of mixture weight water carry out water extraction, then with 6.5 times measure 75% ethanol Solution is precipitated, and extract solution is obtained after filtering;
C, post processing:By extract solution it is concentrated, dry, pulverize and sieve, add that borneol is well mixed to obtain objective composition.
Embodiment 9
The preparation method of described composition, specifically includes following steps:
A, pre-treatment:Folium artemisiae argyi, wrinkled giant hyssop, cassia twig, purple perilla, eupatorium are pulverized and sieved respectively, is then well mixed and obtains mixture;
B, extraction:The water for adding 10 times of mixture weight in the mixture again carries out water extraction, then molten with 75% ethanol of 10 times of amounts Extract solution is obtained after liquid precipitate, filtering;
C, post processing:By extract solution it is concentrated, dry, pulverize and sieve, add that borneol is well mixed to obtain objective composition.
Embodiment 10:Efficacy validation is tested
Subjects:Using the method for chester sampling, extract certain kindergarten it is small, in, the children of the top class in a kindergarten be subjects, Zong Gongxuan 451 people are taken, wherein in the people of test group 243, boy student is 169 people, and female is 74 people, and the people of control group 208, boy student is 132 people, and schoolgirl 76 People;Compare between group through the age, gender comparison, there was no significant difference.
Test method:Test group is worn use Chinese medicine sachet daily, and a sachet is changed per 10d, 20d is continuously worn;Control Group does not wear Chinese medicine sachet, observes 20d;Flu number of the infected is counted respectively.
Evaluation method:The flu incidence of disease of statistical test group and control group, then calculates protective rate by following equation respectively And efficiency index,
The % of protective rate=(the control group incidence of disease test group incidence of disease)/control group incidence of disease × 100;
Efficiency index=control group the incidence of disease/test group incidence of disease, is effective more than 2.
Result of the test is shown in Table 1 ~ 2.
The test group cold in children situation of table 1(Example)
The control group children of table 2 flu situation(Example)
%=51.0% of protective rate=71/139 × 100, efficiency index=139/68=2.04, effect is effective.
From table 1, table 2, test group number of the infected is 68 people, and control group number of the infected is 139 people, is computed, and is protected Rate is 51.0%, and efficiency index is 2.04, shows that the incidence of disease of flu can effectively be reduced by wearing present composition Chinese medicine sachet.

Claims (10)

1. a kind of composition, it is characterised in that described composition includes parts by weight of raw materials:3 ~ 10 parts of folium artemisiae argyi, 3 ~ 10 parts of wrinkled giant hyssop, 3 ~ 10 parts of cassia twig, 3 ~ 10 parts of purple perilla, 3 ~ 8 parts of eupatorium, 3 ~ 6 parts of borneol.
2. composition according to claim 1, it is characterised in that described composition includes parts by weight of raw materials:Folium artemisiae argyi 4 ~ 8 Part, 4 ~ 8 parts of wrinkled giant hyssop, 4 ~ 8 parts of cassia twig, 4 ~ 8 parts of purple perilla, 5 ~ 7 parts of eupatorium, 5 ~ 6 parts of borneol.
3. composition according to claim 1, it is characterised in that described composition includes parts by weight of raw materials:Folium artemisiae argyi 5 ~ 7 Part, 5 ~ 7 parts of wrinkled giant hyssop, 5 ~ 7 parts of cassia twig, 5 ~ 7 parts of purple perilla, 5.5 ~ 6.5 parts of eupatorium, 5.5 ~ 6.5 parts of borneol.
4. the preparation method of a kind of composition as described in claim 1 ~ 3 is any, it is characterised in that specifically include following steps:
A, pre-treatment:Folium artemisiae argyi, wrinkled giant hyssop, cassia twig, purple perilla, eupatorium are pulverized and sieved respectively, is then well mixed and obtains mixture;
B, extraction:Again in the mixture add 3 ~ 10 times of mixture weight water carry out water extraction, then with 3 ~ 10 times amount 75% second Alcoholic solution is precipitated, and extract solution is obtained after filtering;
C, post processing:By extract solution it is concentrated, dry, pulverize and sieve, add that borneol is well mixed to obtain objective composition.
5. the preparation method of composition according to claim 4, it is characterised in that the extraction time that described water is extracted is 18 ~ 30 hours.
6. the preparation method of composition according to claim 4, it is characterised in that the Extracting temperature that described water is extracted is 40~50℃。
7. the preparation method of composition according to claim 4, it is characterised in that described sieving was 20 mesh sieves.
8. the preparation method of composition according to claim 4, it is characterised in that described concentration be concentrated into it is relatively close Spend 1.9 ~ 2.0 g/ml.
9. the Chinese medicine sachet that one kind is prepared using the composition as described in claim 1 ~ 3 is any, described Chinese medicine sachet It is with sachet made from breathable fabric parcel composition.
10. a kind of application of the composition in preventing/treating cold in children as described in claim 1 ~ 3 is any.
CN201710048544.9A 2017-01-23 2017-01-23 A kind of composition and preparation method thereof, sachet and application Pending CN107281263A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108210830A (en) * 2018-03-29 2018-06-29 德阳爱可依生物科技有限公司 A kind of Chinese medicine composition and its application
CN110051766A (en) * 2019-06-04 2019-07-26 吕锦辉 A kind of Chinese medicine composition that treating flu, dipping packet and preparation method thereof

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CN104146014A (en) * 2014-07-18 2014-11-19 李克锋 Preparation method for mosquito-expelling traditional Chinese medicine sachet
CN105477218A (en) * 2015-12-11 2016-04-13 中国人民解放军第二军医大学 Traditional Chinese medicine composition for preventing influenza and application thereof

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Publication number Priority date Publication date Assignee Title
CN101721618A (en) * 2009-11-24 2010-06-09 中国人民解放军第二军医大学 External Chinese medicinal health-care bag for dispelling filth and preventing and treating influenza
CN104146014A (en) * 2014-07-18 2014-11-19 李克锋 Preparation method for mosquito-expelling traditional Chinese medicine sachet
CN105477218A (en) * 2015-12-11 2016-04-13 中国人民解放军第二军医大学 Traditional Chinese medicine composition for preventing influenza and application thereof

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108210830A (en) * 2018-03-29 2018-06-29 德阳爱可依生物科技有限公司 A kind of Chinese medicine composition and its application
CN110051766A (en) * 2019-06-04 2019-07-26 吕锦辉 A kind of Chinese medicine composition that treating flu, dipping packet and preparation method thereof

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Application publication date: 20171024