CN107267008B - A kind of three-dimensional heat preservation and soundproof composite board material and preparation method - Google Patents
A kind of three-dimensional heat preservation and soundproof composite board material and preparation method Download PDFInfo
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D143/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and containing boron, silicon, phosphorus, selenium, tellurium, or a metal; Coating compositions based on derivatives of such polymers
- C09D143/04—Homopolymers or copolymers of monomers containing silicon
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B27/00—Layered products comprising a layer of synthetic resin
- B32B27/06—Layered products comprising a layer of synthetic resin as the main or only constituent of a layer, which is next to another layer of the same or of a different material
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- B32B27/00—Layered products comprising a layer of synthetic resin
- B32B27/12—Layered products comprising a layer of synthetic resin next to a fibrous or filamentary layer
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- B32B27/00—Layered products comprising a layer of synthetic resin
- B32B27/36—Layered products comprising a layer of synthetic resin comprising polyesters
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B33/00—Layered products characterised by particular properties or particular surface features, e.g. particular surface coatings; Layered products designed for particular purposes not covered by another single class
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
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- B32B5/00—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts
- B32B5/02—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by structural features of a fibrous or filamentary layer
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B5/00—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts
- B32B5/16—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by features of a layer formed of particles, e.g. chips, powder or granules
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B9/00—Layered products comprising a layer of a particular substance not covered by groups B32B11/00 - B32B29/00
- B32B9/005—Layered products comprising a layer of a particular substance not covered by groups B32B11/00 - B32B29/00 comprising one layer of ceramic material, e.g. porcelain, ceramic tile
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B9/00—Layered products comprising a layer of a particular substance not covered by groups B32B11/00 - B32B29/00
- B32B9/04—Layered products comprising a layer of a particular substance not covered by groups B32B11/00 - B32B29/00 comprising such particular substance as the main or only constituent of a layer, which is next to another layer of the same or of a different material
- B32B9/045—Layered products comprising a layer of a particular substance not covered by groups B32B11/00 - B32B29/00 comprising such particular substance as the main or only constituent of a layer, which is next to another layer of the same or of a different material of synthetic resin
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
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- C08L11/00—Compositions of homopolymers or copolymers of chloroprene
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L89/00—Compositions of proteins; Compositions of derivatives thereof
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2262/00—Composition or structural features of fibres which form a fibrous or filamentary layer or are present as additives
- B32B2262/10—Inorganic fibres
- B32B2262/108—Rockwool fibres
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2307/00—Properties of the layers or laminate
- B32B2307/10—Properties of the layers or laminate having particular acoustical properties
- B32B2307/102—Insulating
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- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2307/00—Properties of the layers or laminate
- B32B2307/30—Properties of the layers or laminate having particular thermal properties
- B32B2307/304—Insulating
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2307/00—Properties of the layers or laminate
- B32B2307/50—Properties of the layers or laminate having particular mechanical properties
- B32B2307/554—Wear resistance
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
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Abstract
The invention discloses a kind of three-dimensional heat preservation and soundproof composite board material and preparation methods.In the present invention: the raw material including following weight parts: silicone acrylic emulsion 55-60, water-base fluorocarbon emulsion 15-20, thermosetting phenolic resin 0.8-1.0, hollow ceramic particle 15-20；Polyester fiber 55-60, butyl rubber 15-20, aqua type adhesive 8-10；Mineral rock wool 65-70, animal collagen 3-5, synthetic resin 2-3, neoprene 5-7, modified nitrolacquer 12-15.The present invention is to water-base fluorocarbon emulsion, hollow ceramic particle is added in the thermal insulation material of three-dimensional composite plate, the heat preservation for carrying out surface to three composite plates operates, and water-base fluorocarbon emulsion is free of formaldehyde and any heavy metal, does not have any damage to human body.To polyester fiber, butyl rubber is added in the acoustic material of three-dimensional composite board material, polyester fiber, butyl rubber effectively absorb echo and vibration.Mineral rock wool is used to three-dimensional composite board material, so that the supportive of entire three-dimensional composite plate is improved, effectively enhances the effect of resist compression of three-dimensional composite plate.
Description
Technical field
The invention belongs to three-dimensional composite material fields, more particularly to a kind of three-dimensional heat preservation and soundproof composite board material and preparation
Method.
Background technique
Composite material be by inorganic material, organic material, ceramic material or high molecular material etc. two or more
The heterogeneous material that material is prepared by combination process, a variety of materials make up for each other's deficiencies and learn from each other in performance, generate synergistic effect, make
The comprehensive performance of composite material is better than former composition material and meets a variety of different requirements.
With the promotion of Three-dimension process production technology, composite material is towards structure multiplex, the side of function diversification
To development, in the use environment of many three-dimensional composite materials, there is many severe condition elements, more noises, environment
The quick variation of temperature, external pressure, the variation of wind-force etc. are all an important factor for influencing three-dimensional composite plate use process；
In addition, three composite plates can also use in the more environment of personnel, reducing composite material is also to need to solve to the injury of human body
Certainly the problem of, while also to improve the soundproof effect and pressure resistance degree of three-dimensional composite plate.
Summary of the invention
The purpose of the present invention is to provide a kind of three-dimensional heat preservation and soundproof composite board material and preparation methods, pass through, so as to
Enough so that the supportive of entire three-dimensional composite plate is improved, the effect of resist compression of three-dimensional composite plate is effectively enhanced.
In order to solve the above technical problems, the present invention is achieved by the following technical solutions:
The present invention is a kind of three-dimensional heat preservation and soundproof composite board material, it includes the raw material of following weight parts: silicone acrylic emulsion 55-
60, water-base fluorocarbon emulsion 15-20, thermosetting phenolic resin 0.8-1.0, hollow ceramic particle 15-20；Polyester fiber 55-60, fourth
Base rubber 15-20, aqua type adhesive 8-10；Mineral rock wool 65-70, animal collagen 3-5, synthetic resin 2-3, neoprene 5-
7, modified nitrolacquer 12-15.
A kind of preparation method of three-dimensional heat preservation and soundproof composite board material:
By hollow ceramic particle be added silicone acrylic emulsion, water-base fluorocarbon emulsion mixed liquor in, be sufficiently stirred 15-25 minutes,
It adds thermosetting phenolic resin to be solidified, completes the preparation of insulating layer；The extexine of polyester fiber is subjected to cleaning operation,
Add aqua type adhesive again, graininess butyl rubber be finally uniformly laid on to the outside of aqua type adhesive, complete every
The preparation of sound-absorbing layer；Animal collagen, synthetic resin, neoprene are uniformly mixed, are added into mineral rock wool, and by modified nitrocellulose
Paint is sprayed on the surface layer of mineral rock wool, completes the preparation of resistance to compression layer.
Wherein, the preparation method of silicone acrylic emulsion: suitable aqueous molten by being added in the polymer of organosilicon and acrylic compounds
Agent, then polymerization technique is coated by nucleocapsid and is polymerized.
Wherein, the preparation method of water-base fluorocarbon emulsion: esters of acrylic acid, fluororesin copolymer are mixed, are added suitable
Warm water, and the temperature of 40-45 degree is kept, by stirring in 1.5-2.2 hours, reflux, water-base fluorocarbon emulsion can be obtained.
Wherein, it the preparation method of thermosetting phenolic resin: after evenly mixing by excessive formaldehyde and suitable phenol, is added
Suitable NH4OH, NaOH or Na2CO3Basic catalyst keeps 20-25 degree temperature, i.e. generation thermosetting phenolic resin.
Wherein, the preparation method of mineral rock wool: after basalt and other natural crystals are carried out crushing operation, through excessively high
For warm furnace high-temperature fusion at fibre, cured machine is interior to be added suitable binder, completes solidification processing, generation mineral rock wool.
Wherein, the preparation method of modified nitrolacquer: by appropriate alkyd resin, modified rosin resin, acrylic resin, amino
Resin is mixed with nitrocotton, then add dibutyl phthalate, dioctyl ester, blown castor oil to carry out plasticizing operation,
It recycles ketone, alcohol ethers solvent to carry out instant, the preparation of modified nitrolacquer is finally completed using diluents such as benzene classes.
The invention has the following advantages:
1, the present invention is to water-base fluorocarbon emulsion, hollow ceramic particle is added in the thermal insulation material of three-dimensional composite plate, to three
Position composite plate carries out the heat preservation operation on surface, and water-base fluorocarbon emulsion is free of formaldehyde and any heavy metal, does not have any damage to human body
Evil, and water-base fluorocarbon emulsion coating is wear-resistant, and the service life is 2-3 times of common coating.
2, to addition polyester fiber, butyl rubber, polyester fiber, butyl rubber in the acoustic material of three-dimensional composite board material
Echo and vibration effectively are absorbed, improves the soundproof effect of three composite plates.
3, mineral rock wool is used to three-dimensional composite board material, so that the supportive of entire three-dimensional composite plate is improved, had
Effect enhances the effect of resist compression of three-dimensional composite plate.
Certainly, it implements any of the products of the present invention and does not necessarily require achieving all the advantages described above at the same time.
Detailed description of the invention
In order to illustrate the technical solution of the embodiments of the present invention more clearly, will be described below to embodiment required
Attached drawing is briefly described, it should be apparent that, drawings in the following description are only some embodiments of the invention, for ability
For the those of ordinary skill of domain, without creative efforts, it can also be obtained according to these attached drawings other attached
Figure.
Fig. 1 is integral material structural schematic diagram of the invention；
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete
Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on
Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts all other
Embodiment shall fall within the protection scope of the present invention.
It please refers to shown in attached drawing, the present invention is a kind of three-dimensional heat preservation and soundproof composite board material and preparation method, under it includes
State the raw material of parts by weight: silicone acrylic emulsion 55-60, water-base fluorocarbon emulsion 15-20, thermosetting phenolic resin 0.8-1.0, hollow ceramic
Particle 15-20；Polyester fiber 55-60, butyl rubber 15-20, aqua type adhesive 8-10；Mineral rock wool 65-70, animal collagen
3-5, synthetic resin 2-3, neoprene 5-7, modified nitrolacquer 12-15.
A kind of preparation method of three-dimensional heat preservation and soundproof composite board material:
By hollow ceramic particle be added silicone acrylic emulsion, water-base fluorocarbon emulsion mixed liquor in, be sufficiently stirred 15-25 minutes,
It adds thermosetting phenolic resin to be solidified, completes the preparation of insulating layer；The extexine of polyester fiber is subjected to cleaning operation,
Add aqua type adhesive again, graininess butyl rubber be finally uniformly laid on to the outside of aqua type adhesive, complete every
The preparation of sound-absorbing layer；Animal collagen, synthetic resin, neoprene are uniformly mixed, are added into mineral rock wool, and by modified nitrocellulose
Paint is sprayed on the surface layer of mineral rock wool, completes the preparation of resistance to compression layer
Wherein, the preparation method of silicone acrylic emulsion: suitable aqueous molten by being added in the polymer of organosilicon and acrylic compounds
Agent, then polymerization technique is coated by nucleocapsid and is polymerized.
Wherein, the preparation method of water-base fluorocarbon emulsion: esters of acrylic acid, fluororesin copolymer are mixed, are added suitable
Warm water, and the temperature of 40-45 degree is kept, by stirring in 1.5-2.2 hours, reflux, water-base fluorocarbon emulsion can be obtained.
Wherein, it the preparation method of thermosetting phenolic resin: after evenly mixing by excessive formaldehyde and suitable phenol, is added
Suitable NH4OH, NaOH or Na2CO3Basic catalyst keeps 20-25 degree temperature, i.e. generation thermosetting phenolic resin.
Wherein, the preparation method of mineral rock wool: after basalt and other natural crystals are carried out crushing operation, through excessively high
For warm furnace high-temperature fusion at fibre, cured machine is interior to be added suitable binder, completes solidification processing, generation mineral rock wool.
Wherein, the preparation method of modified nitrolacquer: by appropriate alkyd resin, modified rosin resin, acrylic resin, amino
Resin is mixed with nitrocotton, then add dibutyl phthalate, dioctyl ester, blown castor oil to carry out plasticizing operation,
It recycles ketone, alcohol ethers solvent to carry out instant, the preparation of modified nitrolacquer is finally completed using diluents such as benzene classes.
It further illustrates and illustrates:
Silicone acrylic emulsion has water-fast, acidproof, alkaline-resisting, dirt-resistant, is made of pure C silicon, film not yellowing, UV resistant, resists
Aging, the glue film that silicone acrylic emulsion is formed is fine and close, tough and tensile, hardness is high, water whitening resistance is good.
Water-base fluorocarbon emulsion, as the main filmogen of aqueous fluorocarbon coating, have excellent weatherability, water resistance,
Stain resistance, chemical-resistant, it is similar with solvent-based fluorocarbon resin.It is eager to excel very than other conventional acrylic water-based emulsion performances
It is more, and without organic solvent, therefore it is safe from harm to human body, there are no pollution to the environment.
Thermosetting phenolic resin is during the preparation process: under the conditions of basic catalyst, the PH of reaction medium is greater than 7, phenol and
Addition reaction occurs first and generates a hydroxymethylphenol for formaldehyde, is keeping under room temperature, the phenolic alcohol in alkaline medium is stable
, the reaction speed of the hydrogen on methylol and phenol in a hydroxymethylphenol is than the hydrogen on the ortho position and contraposition of formaldehyde and phenol
Reaction speed it is slow, therefore a hydroxymethylphenol is not easy further polycondensation, can be only generated hydroxymethyl-phenol and trihydroxy methyl
Phenol.
In the description of this specification, the description of reference term " one embodiment ", " example ", " specific example " etc. means
Particular features, structures, materials, or characteristics described in conjunction with this embodiment or example are contained at least one implementation of the invention
In example or example.In the present specification, schematic expression of the above terms may not refer to the same embodiment or example.
Moreover, particular features, structures, materials, or characteristics described can be in any one or more of the embodiments or examples to close
Suitable mode combines.
Present invention disclosed above preferred embodiment is only intended to help to illustrate the present invention.There is no detailed for preferred embodiment
All details are described, are not limited the invention to the specific embodiments described.Obviously, according to the content of this specification,
It can make many modifications and variations.These embodiments are chosen and specifically described to this specification, is in order to better explain the present invention
Principle and practical application, so that skilled artisan be enable to better understand and utilize the present invention.The present invention is only
It is limited by claims and its full scope and equivalent.
Claims (1)
1. a kind of three-dimensional heat preservation and soundproof composite board material, it is characterised in that it includes the raw material of following weight parts:
Silicone acrylic emulsion 55-60, water-base fluorocarbon emulsion 15-20, thermosetting phenolic resin 0.8-1.0, hollow ceramic particle 15-20；
Polyester fiber 55-60, butyl rubber 15-20, aqua type adhesive 8-10；
Mineral rock wool 65-70, animal collagen 3-5, synthetic resin 2-3, neoprene 5-7, modified nitrolacquer 12-15；
A kind of preparation method of the three-dimensional heat preservation and soundproof composite board material, comprising the following steps:
By hollow ceramic particle be added silicone acrylic emulsion, water-base fluorocarbon emulsion mixed liquor in, be sufficiently stirred 15-25 minutes, then plus
Enter thermosetting phenolic resin to be solidified, completes the preparation of insulating layer；
The extexine of polyester fiber is subjected to cleaning operation, then adds aqua type adhesive, it is finally that graininess butyl rubber is equal
The even outside for being laid on aqua type adhesive, completes the preparation of puigging；
Animal collagen, synthetic resin, neoprene are uniformly mixed, are added into mineral rock wool, and modified nitrolacquer is sprayed
On the surface layer of mineral rock wool, the preparation of resistance to compression layer is completed；
The preparation method of the silicone acrylic emulsion: will be added suitable aqueous solvent in the polymer of organosilicon and acrylic compounds, then
Polymerization technique is coated by nucleocapsid to be polymerized；
The preparation method of the water-base fluorocarbon emulsion: esters of acrylic acid, fluororesin copolymer being mixed, suitable warm water is added,
And the temperature of 40-45 degree is kept, by stirring in 1.5-2.2 hours, reflux, water-base fluorocarbon emulsion can be obtained；
The preparation method of the thermosetting phenolic resin: it after evenly mixing by excessive formaldehyde and suitable phenol, is added appropriate
NH4OH, NaOH or Na2CO3Basic catalyst keeps 20-25 degree temperature, i.e. generation thermosetting phenolic resin；
The preparation method of the mineral rock wool: after basalt and other natural crystals are carried out crushing operation, by high temperature furnace
For high-temperature fusion at fibre, cured machine is interior to be added suitable binder, completes solidification processing, generation mineral rock wool；
The preparation method of the modified nitrolacquer: by appropriate alkyd resin, modified rosin resin, acrylic resin, amino resins
It is mixed with nitrocotton, then adds dibutyl phthalate, dioctyl ester, blown castor oil and carry out plasticizing operation, recycled
Ketone, the progress of alcohol ethers solvent are instant, and the preparation of modified nitrolacquer is finally completed using diluents such as benzene classes.
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| CN107815071A (en) * | 2017-11-22 | 2018-03-20 | 马鞍山松鹤信息科技有限公司 | One kind insulation special environment protection material and preparation method thereof |
| CN108485449A (en) * | 2018-02-08 | 2018-09-04 | 广州美的华凌冰箱有限公司 | Heat-insulation material and refrigeration equipment |
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| CN106746992A (en) * | 2016-12-16 | 2017-05-31 | 南京倍立达新材料系统工程股份有限公司 | A kind of cement heat preserving wallboard |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106746992A (en) * | 2016-12-16 | 2017-05-31 | 南京倍立达新材料系统工程股份有限公司 | A kind of cement heat preserving wallboard |
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