CN107252406A - A kind of Essence containing Herba Dendrobii extract and preparation method thereof - Google Patents

A kind of Essence containing Herba Dendrobii extract and preparation method thereof Download PDF

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CN107252406A
CN107252406A CN201710391149.0A CN201710391149A CN107252406A CN 107252406 A CN107252406 A CN 107252406A CN 201710391149 A CN201710391149 A CN 201710391149A CN 107252406 A CN107252406 A CN 107252406A
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parts
herba dendrobii
grams
preparation
dendrobii extract
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李维宝
章倩
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Bao Xin Garden Huoshan Stem Of Noble Dendrobium Development Corp Ltd
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Bao Xin Garden Huoshan Stem Of Noble Dendrobium Development Corp Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/60Sugars; Derivatives thereof
    • A61K8/602Glycosides, e.g. rutin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/005Antimicrobial preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
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  • Veterinary Medicine (AREA)
  • Dermatology (AREA)
  • Epidemiology (AREA)
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  • Engineering & Computer Science (AREA)
  • Biotechnology (AREA)
  • Botany (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Gerontology & Geriatric Medicine (AREA)
  • Cosmetics (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

Field is utilized the present invention relates to stem of noble dendrobium product development, a kind of Essence containing Herba Dendrobii extract and preparation method thereof is disclosed.The Essence is made up of following raw material:Herba Dendrobii extract, compound extracted solution, Tea Saponin, plant antimicrobial, propane diols, glycerine, deionized water, the Essence that the present invention is obtained has very strong anti-oxidation function, it can recover and keep the elasticity and gloss of skin, being used for a long time being capable of anti-aging, make one to youthen, and suitable for the crowd of various skin quality.

Description

A kind of Essence containing Herba Dendrobii extract and preparation method thereof
Technical field
Field is utilized the present invention relates to stem of noble dendrobium product development, and in particular to a kind of Essence and its system containing Herba Dendrobii extract Preparation Method.
Background technology
The stem of noble dendrobium also known as dendrobium, generic name Dendrobium is Greek dendron(Trees)With bios(Life)Two word knots Conjunction is formed, and is meant and is grown nonparasitically upon another plant in the tree.Dendrobium is a category maximum in orchid, and original producton location is distributed mainly on Asia heat Band and subtropical zone, Australia and Pacific Islands, the whole world there are about kind more than 1000.China there are about 76 kinds of wherein most distributions In southwest, south China, Taiwan and other places.Dendrobium belongs to for one maximum in orchid family, including about 1500 kinds of plants, about 63 kinds of stones of China Dry measure used in former times platymiscium, is made for 39 kinds of medicinal Dendrobium Sw.The domestic stem of noble dendrobium is distributed in the Qinling Mountains, on the south Huaihe River, for latitude, mostly Several classes are all concentrated between 30 '~25 ° 12 ' of north latitude 15 °, and northwards species is gradually decreased, and most arctogaean realm is no more than 34 ° 24 ' of north latitude. From vertically, the height that 100~3000 meters of height above sea level is all distributed.Dendrobium Sw is towards subtropical zone with tropical southeast subcentre Property weather conditions development monoid, Yunnan of China, Guangxi, Guangdong, Guizhou, the distribution center that Taiwan is domestic platymiscium. Fresh stem of noble dendrobium clearing heat and promoting fluid power is strong, and warm disease and evil is joined the army blood, and hyperpyrexia dysphoria with smothery sensation person is when using, and dendrobium chrysanthum enriching yin is mended clearly as length, the pyreticosis later stage, Yin deficiency abnormal heat person is suitable.Dendrobium candidum, HERBA DENDROBII, the efficacy of a drug are stronger;Dendrobidium huoshanness, suitable for the empty people of old man, YIN-fluid being insufficient person, ear The ring stem of noble dendrobium, promotes the production of body fluid without cold and cool, with generation tea, Appetizing spleen-tonifying.The stem of noble dendrobium and radix polygonati officinalis, there is nourishing Yin and promoting production of body fluid effect, and function is approximate.But The stem of noble dendrobium is sweet salty and cold, and bowl spares has clearly, using the moon of nourishing the stomach kidney as length, the sweet flat matter profit of radix polygonati officinalis, mends and oiliness, to support the moon of lung stomach as two Excellent, two medicines have different with, respectively have partially long, nature and flavor:It is sweet;It is slightly cold.For many years, people focus on its medical value, and have ignored it In the exploitation of cosmetic industry, the stem of noble dendrobium can significantly improve the magnificent enzyme of superoxides discrimination(SOD)Level, reduces lipid peroxide (LPO), brain monoaminergic transmitters level is adjusted, suppresses similar monoamine oxidase(MAO), play a part of anti-aging, because This using the stem of noble dendrobium as cosmetic material by as a kind of application with great potential.
The content of the invention
The invention provides a kind of Essence containing Herba Dendrobii extract and preparation method thereof.
The present invention is achieved by the following technical solutions:
A kind of Essence containing Herba Dendrobii extract and preparation method thereof, the Essence is made up of the raw material of following parts by weight:The stem of noble dendrobium 4.5-4.8 parts of extract, 7.2-7.5 parts of compound extracted solution, 1.2-1.3 parts of Tea Saponin, 5.4-5.6 parts of plant antimicrobial, the third two 1.5-1.7 parts of alcohol, 1.3-1.4 parts of glycerine, 120-130 parts of deionized water, wherein compound extract in parts by weight by with Lower raw material is made:13-15 parts of purslane, 12-14 parts of aloe, 10-12 parts of pomegranate seed, 8-11 parts of rose.
Its preparation method is:
(1)The fresh dendrobium candidum of selection high-quality removes root, cleans, and it is 40-50% to drain to water content, is crushed to 80-100 mesh, plus Enter the ethanol solution that 8-10 times of mass concentration is 80%, normal reflux extraction method is extracted 4-5 hours, filtering removes filter residue, It is concentrated in vacuo at 0.05Mpa-0.08Mpa, 50-60 DEG C and removes alcohol solvent, obtains Herba Dendrobii extract;
(2)The purslane of the parts by weight, aloe, pomegranate seed, Flos Rosae Rugosas pollen are broken to 60-80 mesh, carried using water extraction and alcohol precipitation method Active ingredient is taken, the method extraction effect is good, water extraction temperature is 50-60 DEG C, liquid-solid ratio 10:1, extraction time is 2.5-3 hours, leaching Carry number of times 2-3 times, obtain concentrate cooling and carry out alcohol precipitation, ethanol mass concentration is 80-90%, ethanol and concentrate volume ratio 3: 1, alcohol precipitation temperature is 65-75 DEG C, and 2.0-2.5 hours alcohol precipitation time, filtering reclaims ethanol and obtains the compound extracted solution, has The cold effect of the stem of noble dendrobium, the side effect for thickening cuticula using that will not produce for a long time are neutralized, and with fragrance, eliminates perfume (or spice) The addition of material;
(3)Above-mentioned Herba Dendrobii extract, compound extracted solution are mixed with plant antimicrobial, Tea Saponin, propane diols, glycerine, wherein Tea Saponin belongs to native compound, and with the performance such as emulsification, scattered, gentle, the pharmacology in terms of also impervious, anti-inflammatory, analgesia is made With, and innocuous substance is easily enzymatically decomposed into, do not pollute the environment, deionized water is added while stirring, under 800-900 rotating speeds Stirring 2-3 hours, it is well mixed to produce.
Further described as to such scheme, the plant antimicrobial preparation method is:Weigh 7-8 grams of the coptis, it is white 5-6 grams of father-in-law of head, 4-5 grams of dandelion, 2-3 grams of chrysanthemum indicum, the distilled water that 100 grams are added after smashing to pieces are heated to 120-130 DEG C, dimension Hold 1-1.2 hours, filter 23-5 times while hot, it is the plant antimicrobial to obtain filtrate, the antibacterial antiplaque agent effect is good, and There is the effect nourished to human body skin.
Further described as to such scheme, 1 kilogram of fresh dendrobium candidum can obtain 20-22 grams of the stem of noble dendrobium Extract, preparing 80 grams of compound extracted solution needs purslane, aloe, pomegranate seed, rose total amount to be 1-1.2 kilograms.
Beneficial effects of the present invention:The Essence that the present invention is obtained is compared with existing Essence, significantly improves super oxygen Thing discrimination China enzyme(SOD)Level, reduces lipid peroxide(LPO), brain monoaminergic transmitters level is adjusted, suppresses similar monoamine oxygen Change enzyme(MAO), play a part of anti-aging, and composition health environment-friendly, with very strong anti-oxidation function, and effect is rapid, Skin good absorbing effect, can recover and keep the elasticity and gloss of skin, long-term use can anti-aging, with nutrition flesh Skin, increase skin elasticity, make deep skin moisten, Bearberry Extract, make one to youthen, and suitable for various skin quality people Group.
Embodiment
Embodiment 1
A kind of Essence containing Herba Dendrobii extract and preparation method thereof, the Essence is made up of the raw material of following parts by weight:The stem of noble dendrobium 4.5 parts of extract, 7.2 parts of compound extracted solution, 1.2 parts of Tea Saponin, 5.4 parts of plant antimicrobial, 1.5 parts of propane diols, glycerine 1.3 Part, 120 parts of deionized water, wherein compound extract are made up of following raw material in parts by weight:13 parts of purslane, aloe 12 Part, 10 parts of pomegranate seed, 8 parts of rose.
Its preparation method is:
(1)The fresh dendrobium candidum of selection high-quality removes root, cleans, and it is 40% to drain to water content, is crushed to 80 mesh, adds 8 times of matter The ethanol solution that concentration is 80% is measured, normal reflux extraction method is extracted 4 hours, filtering removes filter residue, at 0.05Mpa, 50 DEG C It is concentrated in vacuo and removes alcohol solvent, obtains Herba Dendrobii extract;
(2)The purslane of the parts by weight, aloe, pomegranate seed, Flos Rosae Rugosas pollen are broken to 60 mesh, being extracted using water extraction and alcohol precipitation method is had Composition is imitated, the method extraction effect is good, water extraction temperature is 50 DEG C, liquid-solid ratio 10:1, extraction time is 2.5 hours, extracting times 2 It is secondary, obtain concentrate cooling and carry out alcohol precipitation, ethanol mass concentration is 80%, ethanol and concentrate volume ratio 3:1, alcohol precipitation temperature is 65 DEG C, 2.0 hours alcohol precipitation time, filtering reclaims ethanol and obtains the compound extracted solution, the effect cold with the stem of noble dendrobium is neutralized, Long-time use will not produce the side effect for thickening cuticula, and with fragrance, eliminate the addition of spices;
(3)Above-mentioned Herba Dendrobii extract, compound extracted solution are mixed with plant antimicrobial, Tea Saponin, propane diols, glycerine, wherein Tea Saponin belongs to native compound, and with the performance such as emulsification, scattered, gentle, the pharmacology in terms of also impervious, anti-inflammatory, analgesia is made With, and innocuous substance is easily enzymatically decomposed into, do not pollute the environment, deionized water is added while stirring, stirred under 800 rotating speeds It is 2 hours, well mixed to produce.
Further described as to such scheme, the plant antimicrobial preparation method is:Weigh 7 grams of the coptis, hoary hair 5 grams of father-in-law, 4 grams of dandelion, 2 grams of chrysanthemum indicum, add 100 grams of distilled water and are heated to 120 DEG C after smashing to pieces, maintain 1 hour, while hot Filter 23, it is the plant antimicrobial to obtain filtrate, and the antibacterial antiplaque agent effect is good, and has nourishing to human body skin Effect.
Further described as to such scheme, the stem of noble dendrobium that 1 kilogram of fresh dendrobium candidum can obtain 20 grams is carried Thing is taken, preparing 80 grams of compound extracted solution needs purslane, aloe, pomegranate seed, rose total amount to be 1 kilogram.
Embodiment 2
A kind of Essence containing Herba Dendrobii extract and preparation method thereof, the Essence is made up of the raw material of following parts by weight:The stem of noble dendrobium 4.6 parts of extract, 7.3 parts of compound extracted solution, 1.25 parts of Tea Saponin, 5.5 parts of plant antimicrobial, 1.6 parts of propane diols, glycerine 1.35 parts, 125 parts of deionized water, wherein compound extract are made up of following raw material in parts by weight:14 parts of purslane, aloe 13 parts, 11 parts of pomegranate seed, 9 parts of rose.
Its preparation method is:
(1)The fresh dendrobium candidum of selection high-quality removes root, cleans, and it is 45% to drain to water content, is crushed to 90 mesh, adds 9 times of matter Measure concentration be 80% ethanol solution, normal reflux extraction method extract 4.5 hours, filtering, remove filter residue, 0.06Mpa, 55 DEG C Lower be concentrated in vacuo removes alcohol solvent, obtains Herba Dendrobii extract;
(2)The purslane of the parts by weight, aloe, pomegranate seed, Flos Rosae Rugosas pollen are broken to 70 mesh, being extracted using water extraction and alcohol precipitation method is had Composition is imitated, the method extraction effect is good, water extraction temperature is 55 DEG C, liquid-solid ratio 10:1, extraction time is 2.8 hours, extracting times 2 It is secondary, obtain concentrate cooling and carry out alcohol precipitation, ethanol mass concentration is 85%, ethanol and concentrate volume ratio 3:1, alcohol precipitation temperature is 70 DEG C, 2.3 hours alcohol precipitation time, filtering reclaims ethanol and obtains the compound extracted solution, the effect cold with the stem of noble dendrobium is neutralized, Long-time use will not produce the side effect for thickening cuticula, and with fragrance, eliminate the addition of spices;
(3)Above-mentioned Herba Dendrobii extract, compound extracted solution are mixed with plant antimicrobial, Tea Saponin, propane diols, glycerine, wherein Tea Saponin belongs to native compound, and with the performance such as emulsification, scattered, gentle, the pharmacology in terms of also impervious, anti-inflammatory, analgesia is made With, and innocuous substance is easily enzymatically decomposed into, do not pollute the environment, deionized water is added while stirring, stirred under 850 rotating speeds It is 2.5 hours, well mixed to produce.
Further described as to such scheme, the plant antimicrobial preparation method is:Weigh 7.5 grams of the coptis, it is white 5.5 grams of father-in-law of head, 4.5 grams of dandelion, 2.5 grams of chrysanthemum indicum, the distilled water that 100 grams are added after smashing to pieces are heated to 125 DEG C, maintenance 1.1 hours, filter 4 times while hot, it is the plant antimicrobial to obtain filtrate, and the antibacterial antiplaque agent effect is good, and to human body Skin has the effect nourished.
Further described as to such scheme, the stem of noble dendrobium that 1 kilogram of fresh dendrobium candidum can obtain 21 grams is carried Thing is taken, preparing 80 grams of compound extracted solution needs purslane, aloe, pomegranate seed, rose total amount to be 1.1 kilograms.
Embodiment 3
A kind of Essence containing Herba Dendrobii extract and preparation method thereof, the Essence is made up of the raw material of following parts by weight:The stem of noble dendrobium 4.8 parts of extract, 7.5 parts of compound extracted solution, 1.3 parts of Tea Saponin, 5.6 parts of plant antimicrobial, 1.7 parts of propane diols, glycerine 1.4 Part, 130 parts of deionized water, wherein compound extract are made up of following raw material in parts by weight:15 parts of purslane, aloe 14 Part, 12 parts of pomegranate seed, 11 parts of rose.
Its preparation method is:
(1)The fresh dendrobium candidum of selection high-quality removes root, cleans, and it is 50% to drain to water content, is crushed to 100 mesh, adds 10 times Mass concentration be 80% ethanol solution, normal reflux extraction method extract 5 hours, filtering, remove filter residue, 0.08Mpa, 60 DEG C Lower be concentrated in vacuo removes alcohol solvent, obtains Herba Dendrobii extract;
(2)The purslane of the parts by weight, aloe, pomegranate seed, Flos Rosae Rugosas pollen are broken to 80 mesh, being extracted using water extraction and alcohol precipitation method is had Composition is imitated, the method extraction effect is good, water extraction temperature is 60 DEG C, liquid-solid ratio 10:1, extraction time is 3 hours, extracting times 3 times, Obtain concentrate cooling and carry out alcohol precipitation, ethanol mass concentration is 90%, ethanol and concentrate volume ratio 3:1, alcohol precipitation temperature is 75 DEG C, 2.5 hours alcohol precipitation time, filtering reclaims ethanol and obtains the compound extracted solution, and the effect cold with the stem of noble dendrobium is neutralized is long Time thickens the side effect of cuticula using that will not produce, and with fragrance, eliminates the addition of spices;
(3)Above-mentioned Herba Dendrobii extract, compound extracted solution are mixed with plant antimicrobial, Tea Saponin, propane diols, glycerine, wherein Tea Saponin belongs to native compound, and with the performance such as emulsification, scattered, gentle, the pharmacology in terms of also impervious, anti-inflammatory, analgesia is made With, and innocuous substance is easily enzymatically decomposed into, do not pollute the environment, deionized water is added while stirring, stirred under 900 rotating speeds It is 3 hours, well mixed to produce.
Further described as to such scheme, the plant antimicrobial preparation method is:Weigh 8 grams of the coptis, hoary hair 6 grams of father-in-law, 5 grams of dandelion, 3 grams of chrysanthemum indicum, the distilled water that 100 grams are added after smashing to pieces are heated to 130 DEG C, maintain 1.2 hours, take advantage of Heat filtering 5 times, it is the plant antimicrobial to obtain filtrate, and the antibacterial antiplaque agent effect is good, and has taste to human body skin Foster effect.
Further described as to such scheme, the stem of noble dendrobium that 1 kilogram of fresh dendrobium candidum can obtain 22 grams is carried Thing is taken, preparing 80 grams of compound extracted solution needs purslane, aloe, pomegranate seed, rose total amount to be 1.2 kilograms.
Comparative example
A kind of Essence, is made up of the raw material of following parts by weight:7.2 parts of compound extracted solution, 1.2 parts of Tea Saponin, plant antimicrobial 5.4 parts, 1.5 parts of propane diols, 1.3 parts of glycerine, 120 parts of deionized water, wherein compound extract is in parts by weight by following Raw material is made:13 parts of purslane, 12 parts of aloe, 10 parts of pomegranate seed, 8 parts of rose, except without Herba Dendrobii extract, its remaining part Point and preparation method thereof be the same as Example 1.
Contrast test
100 citizeness are randomly selected as experiencer, it is front and rear using Essence made from embodiment and comparative example respectively, make It is 3 months with duration, rear result feedback will be used to arrange statistics, it is as shown in the table:
Project Use 15 days Use 1 month Use 3 months Comprehensive marking(10 points of full marks)
Embodiment Skin moistens, and Flexible change is obvious Chloasma is desalinated, and obscure, problem of aging mitigates, and skin gloss exquisiteness is flexible It is turgor, plentiful, flexible, it appears that young 2-3 Sui 9.5 point
Comparative example Skin moistens, and Flexible change is not obvious Effect is not significantly improved Solve the problems, such as scaly dry skin 7.5 point
By contrast test it can be found that:The present invention is more obvious for the improvement result of the various problems of skin, especially Antioxidation effect obtains the consistent favorable comment of user, and the maximum effect of the present invention is exactly to have to mitigate the skin age, makes flesh The vigorous and graceful effect of skin.

Claims (4)

1. a kind of Essence containing Herba Dendrobii extract, it is characterised in that the Essence is made up of the raw material of following parts by weight:The stem of noble dendrobium 4.5-4.8 parts of extract, 7.2-7.5 parts of compound extracted solution, 1.2-1.3 parts of Tea Saponin, 5.4-5.6 parts of plant antimicrobial, the third two 1.5-1.7 parts of alcohol, 1.3-1.4 parts of glycerine, 120-130 parts of deionized water, wherein compound extract in parts by weight by with Lower raw material is made:13-15 parts of purslane, 12-14 parts of aloe, 10-12 parts of pomegranate seed, 8-11 parts of rose.
2. a kind of preparation method of Essence containing Herba Dendrobii extract according to claim 1, it is characterised in that the plant Thing Antibacterial agent preparation method is:7-8 grams of the coptis, 5-6 grams of the Chinese bulbul, 4-5 grams of dandelion, 2-3 grams of chrysanthemum indicum are weighed, after smashing to pieces The distilled water for adding 100 grams is heated to 120-130 DEG C, maintains 1-1.2 hours, filter 23-5 times while hot, and it is described to obtain filtrate Plant antimicrobial.
3. a kind of preparation method of the Essence containing Herba Dendrobii extract described in claim 1, it is characterised in that its preparation method For:
(1)The fresh dendrobium candidum of selection high-quality removes root, cleans, and it is 40-50% to drain to water content, is crushed to 80-100 mesh, plus Enter the ethanol solution that 8-10 times of mass concentration is 80%, normal reflux extraction method is extracted 4-5 hours, filtering removes filter residue, It is concentrated in vacuo at 0.05Mpa-0.08Mpa, 50-60 DEG C and removes alcohol solvent, obtains Herba Dendrobii extract;
(2)The purslane of the parts by weight, aloe, pomegranate seed, Flos Rosae Rugosas pollen are broken to 60-80 mesh, carried using water extraction and alcohol precipitation method Active ingredient is taken, water extraction temperature is 50-60 DEG C, liquid-solid ratio 10:1, extraction time is 2.5-3 hours, and extracting times 2-3 times are obtained Alcohol precipitation is carried out to concentrate cooling, ethanol mass concentration is 80-90%, ethanol and concentrate volume ratio 3:1, alcohol precipitation temperature is 65- 75 DEG C, 2.0-2.5 hours alcohol precipitation time, filtering reclaims ethanol and obtains the compound extracted solution;
(3)Above-mentioned Herba Dendrobii extract, compound extracted solution are mixed with plant antimicrobial, Tea Saponin, propane diols, glycerine, while stirring Mix side and add deionized water, stirred 2-3 hours under 800-900 rotating speeds, it is well mixed to produce.
4. the preparation method of a kind of Essence containing Herba Dendrobii extract according to claim 3, it is characterised in that 1 kilogram Fresh dendrobium candidum can obtain 20-22 grams of Herba Dendrobii extract, preparing 80 grams of compound extracted solution needs purslane, reed Luxuriant growth, pomegranate seed, rose total amount are 1-1.2 kilograms.
CN201710391149.0A 2017-05-27 2017-05-27 A kind of Essence containing Herba Dendrobii extract and preparation method thereof Pending CN107252406A (en)

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CN108392456A (en) * 2018-04-23 2018-08-14 皖西学院 A kind of natural skin-care dendrobium candidum surfactant and preparation method thereof
CN111265430A (en) * 2020-02-19 2020-06-12 中国热带农业科学院海口实验站 Camellia oleifera facial mask essence and camellia oleifera facial mask thereof
CN111825536A (en) * 2018-01-10 2020-10-27 中国科学院昆明植物研究所 Dendrobium candidum compound and cosmetics and application thereof
CN112294738A (en) * 2020-11-12 2021-02-02 厦门鹰君药业有限公司 Essence water composition and preparation method thereof

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CN108392456A (en) * 2018-04-23 2018-08-14 皖西学院 A kind of natural skin-care dendrobium candidum surfactant and preparation method thereof
CN111265430A (en) * 2020-02-19 2020-06-12 中国热带农业科学院海口实验站 Camellia oleifera facial mask essence and camellia oleifera facial mask thereof
CN112294738A (en) * 2020-11-12 2021-02-02 厦门鹰君药业有限公司 Essence water composition and preparation method thereof

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