CN107245807A - A kind of preparation method of needle-punched geotextiles applied to fire-retarding decorative material - Google Patents

A kind of preparation method of needle-punched geotextiles applied to fire-retarding decorative material Download PDF

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Publication number
CN107245807A
CN107245807A CN201710498423.4A CN201710498423A CN107245807A CN 107245807 A CN107245807 A CN 107245807A CN 201710498423 A CN201710498423 A CN 201710498423A CN 107245807 A CN107245807 A CN 107245807A
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CN
China
Prior art keywords
needle
fire
punched geotextiles
preparation
decorative material
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CN201710498423.4A
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Chinese (zh)
Inventor
叶晓霞
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Individual
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Individual
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Priority to CN201710498423.4A priority Critical patent/CN107245807A/en
Publication of CN107245807A publication Critical patent/CN107245807A/en
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    • DTEXTILES; PAPER
    • D04BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04HMAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H1/00Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
    • D04H1/40Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
    • D04H1/42Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties characterised by the use of certain kinds of fibres insofar as this use has no preponderant influence on the consolidation of the fleece
    • D04H1/4382Stretched reticular film fibres; Composite fibres; Mixed fibres; Ultrafine fibres; Fibres for artificial leather
    • DTEXTILES; PAPER
    • D04BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04HMAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H1/00Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
    • D04H1/40Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
    • D04H1/42Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties characterised by the use of certain kinds of fibres insofar as this use has no preponderant influence on the consolidation of the fleece
    • D04H1/4266Natural fibres not provided for in group D04H1/425
    • DTEXTILES; PAPER
    • D04BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04HMAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H1/00Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
    • D04H1/40Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
    • D04H1/42Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties characterised by the use of certain kinds of fibres insofar as this use has no preponderant influence on the consolidation of the fleece
    • D04H1/4326Condensation or reaction polymers
    • D04H1/435Polyesters
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/73Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof
    • D06M11/76Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof with carbon oxides or carbonates
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/02Natural fibres, other than mineral fibres
    • D06M2101/04Vegetal fibres

Abstract

The invention discloses a kind of preparation method of the needle-punched geotextiles applied to fire-retarding decorative material, comprise the following steps:Micron order magnalium hydrotalcite powder is distributed in grease at a high speed, emulsion is formed;Cattail wool fiber is adsorbed in emulsion;Cattail wool fiber is mixed with polyester fiber, needle-punched geotextiles are made;Needle-punched geotextiles are carried out with cleaning to deoil, dry, you can.The needle-punched geotextiles of the present invention, it is not only cheap, and good flame retardation effect, it can apply to the fire-retarding decorative materials such as fire resisting door, fire resistant decorative board.

Description

A kind of preparation method of needle-punched geotextiles applied to fire-retarding decorative material
Technical field
The present invention relates to fire proofing technical field, more particularly to a kind of acupuncture geotechnique applied to fire-retarding decorative material The preparation method of cloth.
Background technology
Needle-punched geotextiles are divided into two kinds of filament spunbond needling non-woven geotextiles and fibers needlepunched nonwoven geotextiles.
Filament spunbond needling non-woven geotextiles using high-quality polyester slice by high temperature melting, spinneret networking, acupuncture into Cloth is produced, and filament spunbond needling non-woven geotextiles have higher tension strength, tearing strength, anti-bursting strength, Play a part of reinforcement protection in engineering, be generally used for highway, railway, dykes and dams, water construction, tunnel, refuse landfill Etc. in engineering.
Fibers needlepunched nonwoven geotextiles are formed using polyester staple fiber by acupuncture, terylene short fiber needling non-woven Geotextiles have good water filtering performance, and price is more cheap, play a part of reinforcement protection, pad anti-filter, one in engineering As be applied to the isolation of civil engineering, anti-filter, draining position.
Cattail wool alias:Water candle, Calceolaria, wild candle, raupo, hair wax(Shaanxi call)Deng the Gu at the western side of Shandong Weishan Lake Abundant ground.Abounded with lake among the vegetation such as various reeds, the stem or leaf of cattail, wetland shallow water.2 month weather gradually warm up surface, start life It is long, just it is cattail pollen, through being grown to the cattail's spike eight, September, its tiny fine hair is fluffy such as cotton, the cattail's spike parched after the autumn cattail's spike is completely dry Without when must not can touch, even a little scratching, the cattail's spike has been reformed into " Magic wand ", the Pu of a piece consolidation of moment Rod has just popped into a glob of cattail wool, whiffet, and that cattail wool just floats in the air, grab all grab less than.In every late autumn, work as breeze Cross, local tiny fine hair is danced in the air over the sky, as a kind of landscape, make it is many come this poet, singer be all reluctant to leave lyric, Zhong Duoyou People sees all cannot forget for a long time after this scape.
Current cattail wool is applied to pillow and core mostly as filler, compared with silk and eider down, cattail wool is light and short, It is strongly small, it is traditional pillow inserts.Many people both know about《Book on Chinese herbal medicine》In for cattail wool record some benefits, say its pacify God it is relieving convulsion, clearing heat and cooling blood effect is good, most suitable to old man for children, and cattail wool fiber is warming, breathe freely, delicate fragrance and The characteristics of health care is that it turns into the house non-defective unit of the modern life.
Cattail wool fiber has extraordinary absorption property to grease simultaneously, and the present invention utilizes the absorption property system of cattail wool fiber Standby flame retardant type needle-punched geotextiles.
The content of the invention
In order to solve the above technical problems, the present invention provides a kind of preparation of needle-punched geotextiles applied to fire-retarding decorative material Method.
A kind of preparation method of needle-punched geotextiles applied to fire-retarding decorative material, comprises the following steps:
A, by micron order magnalium hydrotalcite powder at a high speed be distributed in grease, formed emulsion;
B, cattail wool fiber adsorbed in emulsion;
C, cattail wool fiber mixed with polyester fiber, needle-punched geotextiles are made;
D, needle-punched geotextiles are carried out with cleaning deoil, dry, you can.
It is preferred that, in described step A, the particle diameter of described micron order magnalium hydrotalcite powder is 0.5-10 μm.
It is preferred that, described grease is vegetable fat, such as olive oil, rapeseed oil, peanut oil, soybean oil;Or day Right mineral grease, such as paraffin oil, oil alkene.
It is preferred that, need to add dispersant and emulsifying agent in the dispersion process in described step A.
It is preferred that, in described step B, cattail wool fiber is carried out in adsorption process in emulsion, ultrasonic wave is carried out auxiliary Help, be so conducive in adsorption process, micron order magnalium hydrotalcite powder enters cattail wool fibrous inside, while micron order magnalium neatly Stone flour after cattail wool fibre frictoin with that can generate nano level magnalium hydrotalcite powder, it is easier to enter cattail wool fibrous inside, and scattered Uniformly.
It is preferred that, in described step C, described polyester fiber is short fine polyester fiber.
It is further preferred that the mass percent of described cattail wool fiber and short fine polyester fiber be respectively 10-40% and 60-90%。
Typical LDHs compounds are magnalium carbonate form hydrotalcites:Mg6Al2(OH)16CO3·4H2O.LDHs structure is non- Often it is similar to shepardite [Mg (OH)2], by MgO6The shared prismatic of octahedron is into elementary layer, the Mg on layer2+Can be certain In the range of by Al3+Same order elements so that laminate is positively charged, interlayer has tradable CO3 2-Balanced with the positive charge on laminate, So that LDHs overall structure is in electroneutral.Because laminate and interlayer anion are connected by hydrogen bond so that LDHs interlayers it is cloudy from Son has interchangeability.In addition, there are intermediary water these hydrones in LDHs can remove under the conditions of layer structure is not destroyed Go.
LDHs is heated to certain temperature and decomposed, and thermal decomposition process includes de- intermediary water, decarburization acid ion, laminate hydroxyl The steps such as base dehydration.When being less than 200 DEG C in atmosphere, interlayer moisture is only lost, on its structure without influence, when being heated to 250 ~ At 450 DEG C, more moisture are lost, while there is CO2Generation, when being heated to 450 ~ 500 DEG C, CO3 2-Disappear, be completely transformed into CO2, Generate bimetal composite oxide(LDO).In heating process, LDHs ordered lamellar structure is destroyed, surface area increase, hole Hold increase.When heating-up temperature is more than 600 DEG C, then the metal oxide formed after decomposing starts sintering, causes surface area to reduce, Pore volume reduces, and is usually formed spinelle MgAl2O4And MgO.This structure has extraordinary resistance to elevated temperatures.
Beneficial effects of the present invention are compared with prior art:The present invention after step B modifications and the Pu that deoils The fire resistance of Down Fiber is very good., will in order to improve the intensity of needle-punched geotextiles but the insufficient strength of cattail wool fiber is preferable Cattail wool fiber is mixed with terylene, obtained needle-punched geotextiles not only good flame retardation effect, and structural strength is high, and cattail wool fiber is with washing Depending on the mass ratio of synthetic fibre is according to different fire-retardant and intensity requirements;The needle-punched geotextiles of the present invention, it is not only cheap, and resistance Fuel efficiency fruit is good, can apply to the fire-retarding decorative materials such as fire resisting door, fire resistant decorative board.
Embodiment
With reference to embodiment, the embodiment to the present invention is described in further detail.Following examples are used for Illustrate the present invention, but be not limited to the scope of the present invention.
Embodiment 1
A kind of preparation method of needle-punched geotextiles applied to fire-retarding decorative material, comprises the following steps:
A, by micron order magnalium hydrotalcite powder at a high speed be distributed in grease, formed emulsion;
B, ultrasonication effect under, cattail wool fiber is adsorbed in emulsion;
C, cattail wool fiber mixed with short fine polyester fiber, needle-punched geotextiles are made;
D, needle-punched geotextiles are carried out with cleaning deoil, dry, you can.
In described step A, the particle diameter of described micron order magnalium hydrotalcite powder is 0.5-10 μm.
Described grease is soybean oil.
Need to add dispersant and emulsifying agent in dispersion process in described step A.
The mass percent of described cattail wool fiber and short fine polyester fiber is respectively 15% and 85%.
Embodiment 2
A kind of preparation method of needle-punched geotextiles applied to fire-retarding decorative material, comprises the following steps:
A, by micron order magnalium hydrotalcite powder at a high speed be distributed in grease, formed emulsion;
B, ultrasonication effect under, cattail wool fiber is adsorbed in emulsion;
C, cattail wool fiber mixed with short fine polyester fiber, needle-punched geotextiles are made;
D, needle-punched geotextiles are carried out with cleaning deoil, dry, you can.
In described step A, the particle diameter of described micron order magnalium hydrotalcite powder is 0.5-10 μm.
Described grease is the mixture of olive oil and rapeseed oil.
Need to add dispersant and emulsifying agent in dispersion process in described step A.
The mass percent of described cattail wool fiber and short fine polyester fiber is respectively 40% and 60%.
Embodiment 3
A kind of preparation method of needle-punched geotextiles applied to fire-retarding decorative material, comprises the following steps:
A, by micron order magnalium hydrotalcite powder at a high speed be distributed in grease, formed emulsion;
B, ultrasonication effect under, cattail wool fiber is adsorbed in emulsion;
C, cattail wool fiber mixed with short fine polyester fiber, needle-punched geotextiles are made;
D, needle-punched geotextiles are carried out with cleaning deoil, dry, you can.
In described step A, the particle diameter of described micron order magnalium hydrotalcite powder is 0.5-10 μm.
Described grease is paraffin oil.
Need to add dispersant and emulsifying agent in dispersion process in described step A.
The mass percent of described cattail wool fiber and short fine polyester fiber is respectively 10% and 90%.
Embodiment 4
A kind of preparation method of needle-punched geotextiles applied to fire-retarding decorative material, comprises the following steps:
A, by micron order magnalium hydrotalcite powder at a high speed be distributed in grease, formed emulsion;
B, ultrasonication effect under, cattail wool fiber is adsorbed in emulsion;
C, cattail wool fiber mixed with short fine polyester fiber, needle-punched geotextiles are made;
D, needle-punched geotextiles are carried out with cleaning deoil, dry, you can.
In described step A, the particle diameter of described micron order magnalium hydrotalcite powder is 0.5-10 μm.
Described grease is oil alkene.
Need to add dispersant and emulsifying agent in dispersion process in described step A.
The mass percent of described cattail wool fiber and short fine polyester fiber is respectively 25% and 75%.
Described above is only the preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art For member, without departing from the technical principles of the invention, some improvement and modification can also be made, these improvement and modification Also it should be regarded as protection scope of the present invention.

Claims (7)

1. the preparation method of a kind of needle-punched geotextiles applied to fire-retarding decorative material, it is characterised in that comprise the following steps:
A, by micron order magnalium hydrotalcite powder at a high speed be distributed in grease, formed emulsion;
B, cattail wool fiber adsorbed in emulsion;
C, cattail wool fiber mixed with polyester fiber, needle-punched geotextiles are made;
D, needle-punched geotextiles are carried out with cleaning deoil, dry, you can.
2. the preparation method of the needle-punched geotextiles of fire-retarding decorative material is applied to as claimed in claim 1, it is characterised in that institute In the step A stated, the particle diameter of described micron order magnalium hydrotalcite powder is 0.5-10 μm.
3. the preparation method of the needle-punched geotextiles of fire-retarding decorative material is applied to as claimed in claim 1, it is characterised in that institute The grease stated is vegetable fat or natural minerals grease.
4. the preparation method of the needle-punched geotextiles of fire-retarding decorative material is applied to as claimed in claim 1, it is characterised in that institute Need to add dispersant and emulsifying agent in dispersion process in the step A stated.
5. the preparation method of the needle-punched geotextiles of fire-retarding decorative material is applied to as claimed in claim 1, it is characterised in that institute In the step B stated, cattail wool fiber is carried out in adsorption process in emulsion, ultrasonic assistant is carried out.
6. the preparation method of the needle-punched geotextiles of fire-retarding decorative material is applied to as claimed in claim 1, it is characterised in that institute In the step C stated, described polyester fiber is short fine polyester fiber.
7. the preparation method of the needle-punched geotextiles of fire-retarding decorative material is applied to as claimed in claim 6, it is characterised in that institute The mass percent of the cattail wool fiber stated and short fine polyester fiber is respectively 10-40% and 60-90%.
CN201710498423.4A 2017-06-27 2017-06-27 A kind of preparation method of needle-punched geotextiles applied to fire-retarding decorative material Pending CN107245807A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110306293A (en) * 2019-05-13 2019-10-08 山东寿光鲁清石化有限公司 A kind of super soft non-woven fabrics and preparation process and the application in baby's diaper

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101307528A (en) * 2008-02-29 2008-11-19 东莞市莲盈棉制品有限公司 Fire retardant cotton nonwoven fabrics and manufacture method thereof
CN101851863A (en) * 2010-06-08 2010-10-06 福建南纺股份有限公司 Environmentally friendly differential fiber non-woven automotive interior trim material and preparation method thereof
CN102936842A (en) * 2012-10-29 2013-02-20 金猴集团威海鞋业有限公司 Nanometer flame retardant shoe insole material
CN105862225A (en) * 2016-05-16 2016-08-17 长兴恒峰纺织有限公司 Manufacturing method of anti-microbial satin fabric
CN106007627A (en) * 2016-05-26 2016-10-12 湖州德海新型建材有限公司 Preparation method of sound and heat insulating block with flame retardant effect
CN106245145A (en) * 2016-07-27 2016-12-21 长兴县金欣服装辅料有限责任公司 A kind of flame-resistant terylene lining cloth and preparation method thereof

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101307528A (en) * 2008-02-29 2008-11-19 东莞市莲盈棉制品有限公司 Fire retardant cotton nonwoven fabrics and manufacture method thereof
CN101851863A (en) * 2010-06-08 2010-10-06 福建南纺股份有限公司 Environmentally friendly differential fiber non-woven automotive interior trim material and preparation method thereof
CN102936842A (en) * 2012-10-29 2013-02-20 金猴集团威海鞋业有限公司 Nanometer flame retardant shoe insole material
CN105862225A (en) * 2016-05-16 2016-08-17 长兴恒峰纺织有限公司 Manufacturing method of anti-microbial satin fabric
CN106007627A (en) * 2016-05-26 2016-10-12 湖州德海新型建材有限公司 Preparation method of sound and heat insulating block with flame retardant effect
CN106245145A (en) * 2016-07-27 2016-12-21 长兴县金欣服装辅料有限责任公司 A kind of flame-resistant terylene lining cloth and preparation method thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110306293A (en) * 2019-05-13 2019-10-08 山东寿光鲁清石化有限公司 A kind of super soft non-woven fabrics and preparation process and the application in baby's diaper
CN110306293B (en) * 2019-05-13 2021-07-23 山东寿光鲁清石化有限公司 Super-soft non-woven fabric, preparation process and application thereof in baby diapers

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Application publication date: 20171013