CN107233392A - Gold dripping pill and preparation method thereof - Google Patents
Gold dripping pill and preparation method thereof Download PDFInfo
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- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
- A61K36/481—Astragalus (milkvetch)
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- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/35—Caprifoliaceae (Honeysuckle family)
- A61K36/355—Lonicera (honeysuckle)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/53—Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/53—Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
- A61K36/539—Scutellaria (skullcap)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/59—Menispermaceae (Moonseed family), e.g. hyperbaena or coralbead
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/70—Polygonaceae (Buckwheat family), e.g. spineflower or dock
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/20—Pills, tablets, discs, rods
- A61K9/2004—Excipients; Inactive ingredients
- A61K9/2022—Organic macromolecular compounds
- A61K9/2031—Organic macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polyethylene glycol, polyethylene oxide, poloxamers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/333—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using mixed solvents, e.g. 70% EtOH
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/39—Complex extraction schemes, e.g. fractionation or repeated extraction steps
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/50—Methods involving additional extraction steps
- A61K2236/51—Concentration or drying of the extract, e.g. Lyophilisation, freeze-drying or spray-drying
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/50—Methods involving additional extraction steps
- A61K2236/53—Liquid-solid separation, e.g. centrifugation, sedimentation or crystallization
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Abstract
The invention discloses a kind of Chinese medicine gold dripping pill for treating flu, it is characterized in that taking the Radix Astragali, radix scutellariae, herba fibraureae recisae, cymose buckwheat rhizome, desmodium, honeysuckle prescription, through alcohol extracting, water extraction, is concentrated in vacuo, spray drying, nano powder is made, Chinese medicine dripping pills are further made, for treating flu, good result are achieved.
Description
Technical field
The present invention relates to the field of Chinese medicines, and in particular to a kind of gold dripping pill and preparation method thereof.
Background technology
Flu is common disease, frequently-occurring disease, using heating, runny nose, cough, pharyngalgia as main clinic symptoms.Treat the medicine of flu
Although thing is many, most uncertain therapeutic efficacy is cut, and toxic side effect is again very big, and in the market is badly in need of determined curative effect, quality controllable, effect peace
Full treatment cold medicine.I is caught a cold for many years using the Radix Astragali, radix scutellariae, herba fibraureae recisae, cymose buckwheat rhizome, desmodium, honeysuckle prescription therapeutic,
Good result is obtained, a kind of safely and effectively superior drug is provided for numerous cold patients.
The content of the invention
The present invention is, according to my tcm clinical practice experience for many years, sense to be treated there is provided one kind with reference to modern Chinese herbal medicine preparation technique
The gold dripping pill emitted.
Invention embodiment is as follows:
Take 100~300 parts of the Radix Astragali, 100~300 parts of radix scutellariae, 100~300 parts of herba fibraureae recisae, 100~300 parts of cymose buckwheat rhizome, desmodium 100
~300 parts, 100~300 parts of honeysuckle;The Radix Astragali, radix scutellariae, desmodium add 70% alcohol reflux and extract secondary, and 8 are added for the first time
Measure, extract 3 hours again, 6 times of second of addition is measured, and is extracted 2 hours, merges extract solution twice, is reclaimed ethanol, is concentrated in vacuo to phase
It is 1.10 to density, obtains alcohol extract, it is standby;Herba fibraureae recisae, cymose buckwheat rhizome, the honeysuckle refluxing extraction that adds water are secondary, add water for the first time 10 times
Amount, extracts 3 hours, adds water 8 times and measure for the second time, extracts 2 hours, merges extract solution twice, being concentrated in vacuo to relative density is
1.10, obtain Aqueous extracts, add above-mentioned alcohol extract, mix, spray drying, put be ground into high energy nanometer impact grinding particle diameter 100~
200nm nano powder, plus 100~300 parts of Macrogol 6000s mixings, 80 DEG C of control material temperature, 4 DEG C of condensation temperature, drop speed
15 drop per minute, is instilled in atoleine, is taken out after dripping pill shaping, is sucked surface coolant, gold dripping pill is made.
The raw material standards that the embodiment above is previously mentioned is as follows:
The Radix Astragali:The Chinese Pharmacopoeia ministerial standard of version one in 2015;
Radix scutellariae:The Chinese Pharmacopoeia ministerial standard of version one in 2015;
Herba fibraureae recisae:The Chinese Pharmacopoeia ministerial standard of version one in 2015;
Cymose buckwheat rhizome:The Chinese Pharmacopoeia ministerial standard of version one in 2015;
Desmodium:The Chinese Pharmacopoeia ministerial standard of version one in 2015;
Honeysuckle:The Chinese Pharmacopoeia ministerial standard of version one in 2015;
Ethanol:The Chinese Pharmacopoeia ministerial standard of version two in 2015;
Macrogol 6000:The Chinese Pharmacopoeia ministerial standard of version two in 2015;
Paraffin:The Chinese Pharmacopoeia ministerial standard of version two in 2015;
Raw material used in the present invention can be commercially available from pharmaceuticals, can be used to implement this as long as meeting national standard
Scheme of the invention.
In the present invention program involved term unless otherwise specified, with Chinese Pharmacopoeia, state food drug surveilance pipe
The medicine related specifications such as reason office standard, which are explained, to be defined.
" part " in embodiment above refers to parts by weight.
Four embodiments
The specific embodiment 1 of the present invention
Take Radix Astragali 100g, radix scutellariae 100g, herba fibraureae recisae 100g, cymose buckwheat rhizome 100g, desmodium 100g, honeysuckle 100g;The Radix Astragali, radix scutellariae,
Desmodium adds 70% alcohol reflux and extracts secondary, and first time adds 8 times of amounts, extracts 3 hours, second of addition, 6 times of amounts, extracts 2
Hour, merge extract solution twice, reclaim ethanol, it is 1.10 to be concentrated in vacuo to relative density, obtains alcohol extract, standby;Herba fibraureae recisae, Jin Qiao
Wheat, the honeysuckle refluxing extraction that adds water are secondary, add water 10 times and measure for the first time, extract 3 hours, add water 8 times and measure for the second time, extract 2 small
When, merge extract solution twice, it is 1.10 to be concentrated in vacuo to relative density, obtain Aqueous extracts, add above-mentioned alcohol extract, mix, spraying
Dry, put the nano powder that 100~200nm of particle diameter is ground into high energy nanometer impact grinding, plus 100g Macrogol 6000s are mixed, control
80 DEG C of temperature of charge processed, 4 DEG C of condensation temperature, drop speed 15 drop per minute instills in atoleine, takes out, suck after dripping pill shaping
Surface coolant, is made gold dripping pill.
The specific embodiment 2 of the present invention
Take Radix Astragali 200g, radix scutellariae 200g, herba fibraureae recisae 200g, cymose buckwheat rhizome 200g, desmodium 200g, honeysuckle 200g;The Radix Astragali, radix scutellariae,
Desmodium adds 70% alcohol reflux and extracts secondary, and first time adds 8 times of amounts, extracts 3 hours, second of addition, 6 times of amounts, extracts 2
Hour, merge extract solution twice, reclaim ethanol, it is 1.10 to be concentrated in vacuo to relative density, obtains alcohol extract, standby;Herba fibraureae recisae, Jin Qiao
Wheat, the honeysuckle refluxing extraction that adds water are secondary, add water 10 times and measure for the first time, extract 3 hours, add water 8 times and measure for the second time, extract 2 small
When, merge extract solution twice, it is 1.10 to be concentrated in vacuo to relative density, obtain Aqueous extracts, add above-mentioned alcohol extract, mix, spraying
Dry, put the nano powder that 100~200nm of particle diameter is ground into high energy nanometer impact grinding, plus 200g Macrogol 6000s are mixed, control
80 DEG C of temperature of charge processed, 4 DEG C of condensation temperature, drop speed 15 drop per minute instills in atoleine, takes out, suck after dripping pill shaping
Surface coolant, is made gold dripping pill.
The specific embodiment 3 of the present invention
Take Radix Astragali 300g, radix scutellariae 300g, herba fibraureae recisae 300g, cymose buckwheat rhizome 300g, desmodium 300g, honeysuckle 300g;The Radix Astragali, radix scutellariae,
Desmodium adds 70% alcohol reflux and extracts secondary, and first time adds 8 times of amounts, extracts 3 hours, second of addition, 6 times of amounts, extracts 2
Hour, merge extract solution twice, reclaim ethanol, it is 1.10 to be concentrated in vacuo to relative density, obtains alcohol extract, standby;Herba fibraureae recisae, Jin Qiao
Wheat, the honeysuckle refluxing extraction that adds water are secondary, add water 10 times and measure for the first time, extract 3 hours, add water 8 times and measure for the second time, extract 2 small
When, merge extract solution twice, it is 1.10 to be concentrated in vacuo to relative density, obtain Aqueous extracts, add above-mentioned alcohol extract, mix, spraying
Dry, put in high energy nanometer impact grinding and be ground into 100~200nm of particle diameter nano powder, plus 100~300g Macrogol 6000s mix
Even, 80 DEG C of control material temperature, 4 DEG C of condensation temperature, drop speed 15 drop per minute is instilled in atoleine, taken out after dripping pill shaping,
Surface coolant is sucked, gold dripping pill is made.
Upper result shows that the various extreme conditions of embodiment of the present invention can be made into gold dripping pill.
The actual effect of the present invention is investigated with gold dripping pill treatment flu made from embodiment 2 below:
Gold dripping pill clinical observation on the therapeutic effect
1 case scenario
Outpatient service and inpatient are counted, cold patients 180, average age 41 years old are observed altogether.Patient has different degrees of hair
The symptoms such as heat, runny nose, cough, pharyngalgia, flu is diagnosed as by TCM syndrome diagnostic criteria.Patient is randomly divided into three groups, experiment
Group takes gold dripping pill made from embodiment 2, and control group takes commercially available Shuanghuangli dripping pill and Qingkailing dripping pill.
2 efficacy assessment standards
Influenza guideline of clinical investigations tcm syndrome curative effect determinate standard is treated according to new Chinese medicine:
Cure:Tcm clinical practice symptom, sign disappear or basic disappearance, and syndrome integral reduces >=95%.
It is effective:Tcm clinical practice symptom, sign are obviously improved, and syndrome integral reduces >=70%.
Effectively:Tcm clinical practice symptom, sign take a favorable turn, and syndrome integral reduces >=30%.
It is invalid:Tcm clinical practice symptom, sign are not improved or aggravated, and syndrome integral reduces < 30%.
Calculation formula:[(Integrated before treatment after integration-treatment)Integrated before ÷ treatments] × 100%.
3 clinical observation results
Table gold dripping pill and commercially available Shuanghuangli dripping pill, Qingkailing dripping pill clinical efficacy contrast table
Above-mentioned clinical observation on the therapeutic effect result shows, made from the embodiment of the present invention 2 during gold dripping pill treatment flu, height evident in efficacy
In classic treatment cold medicine Shuanghuangli dripping pill and Qingkailing dripping pill, p < 0.01.
Claims (3)
1. the Chinese medicine gold dripping pill of flu is treated a kind of, it is characterized in that taking 100~300 parts of the Radix Astragali, 100~300 parts of radix scutellariae, herba fibraureae recisae
100~300 parts, 100~300 parts of cymose buckwheat rhizome, 100~300 parts of desmodium, 100~300 parts of honeysuckle;The Radix Astragali, radix scutellariae, money
Grass adds 70% alcohol reflux and extracts secondary, and first time adds 8 times of amounts, extracts 3 hours, second of addition, 6 times of amounts, extracts 2 small
When, merge extract solution twice, reclaim ethanol, it is 1.10 to be concentrated in vacuo to relative density, obtains alcohol extract, standby;Herba fibraureae recisae, Jin Qiao
Wheat, the honeysuckle refluxing extraction that adds water are secondary, add water 10 times and measure for the first time, extract 3 hours, add water 8 times and measure for the second time, extract 2 small
When, merge extract solution twice, it is 1.10 to be concentrated in vacuo to relative density, obtain Aqueous extracts, add above-mentioned alcohol extract, mix, spraying
Dry, put the nano powder that 100~200nm of particle diameter is ground into high energy nanometer impact grinding, plus 100~300 parts of Macrogol 6000s
Mix, 80 DEG C of control material temperature, 4 DEG C of condensation temperature, drop speed 15 drop per minute is instilled in atoleine, taken after dripping pill shaping
Go out, suck surface coolant, gold dripping pill is made.
2. the preparation method of Chinese medicine gold dripping pill according to claim 1, it is characterized in that taking 100~300 parts of the Radix Astragali, radix scutellariae
100~300 parts, 100~300 parts of herba fibraureae recisae, 100~300 parts of cymose buckwheat rhizome, 100~300 parts of desmodium, 100~300 parts of honeysuckle;
The Radix Astragali, radix scutellariae, desmodium add 70% alcohol reflux and extract secondary, and first time adds 8 times of amounts, extracts 3 hours, second of addition 6
Measure, extract 2 hours again, merge extract solution twice, reclaim ethanol, it is 1.10 to be concentrated in vacuo to relative density, obtains alcohol extract, standby
With;Herba fibraureae recisae, cymose buckwheat rhizome, the honeysuckle refluxing extraction that adds water are secondary, add water 10 times and measure for the first time, extract 3 hours, add water 8 for the second time
Measure, extract 2 hours again, merge extract solution twice, it is 1.10 to be concentrated in vacuo to relative density, obtain Aqueous extracts, the above-mentioned alcohol extracting of addition
Liquid, is mixed, spray drying, puts the nano powder that 100~200nm of particle diameter is ground into high energy nanometer impact grinding, plus 100~300 parts
Macrogol 6000 is mixed, 80 DEG C of control material temperature, 4 DEG C of condensation temperature, drop speed 15 drop per minute, is instilled in atoleine,
Taken out after dripping pill shaping, suck surface coolant, gold dripping pill is made.
3. the preparation method of Chinese medicine gold dripping pill according to claim 1, it is characterized in that take 200 parts of the Radix Astragali, 200 parts of radix scutellariae,
200 parts of herba fibraureae recisae, 200 parts of cymose buckwheat rhizome, 200 parts of desmodium, 200 parts of honeysuckle;The Radix Astragali, radix scutellariae, desmodium add 70% alcohol reflux
Extract secondary, first time adds 8 times of amounts, extracts 3 hours, second of addition, 6 times of amounts are extracted 2 hours, merge extract solution twice,
Ethanol is reclaimed, it is 1.10 to be concentrated in vacuo to relative density, obtains alcohol extract, standby;The backflow that adds water of herba fibraureae recisae, cymose buckwheat rhizome, honeysuckle is carried
Take secondary, add water 10 times and measure for the first time, extract 3 hours, add water 8 times and measure for the second time, extract 2 hours, merge extract solution twice, very
It is 1.10 that sky, which is concentrated into relative density, obtains Aqueous extracts, adds above-mentioned alcohol extract, is mixed, spray drying, puts high energy nanometer impact grinding
In be ground into 100~200nm of particle diameter nano powder, plus 200 parts of Macrogol 6000s are mixed, 80 DEG C of control material temperature, condensation
4 DEG C of temperature, drop speed 15 drop per minute, instills in atoleine, is taken out after dripping pill shaping, suck surface coolant, gold is made
Dripping pill.
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Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1448174A (en) * | 2003-05-03 | 2003-10-15 | 南通精华制药有限公司 | Application of cymose buckwheat rhizome in preparation of antiviral drug |
CN102068492A (en) * | 2011-01-05 | 2011-05-25 | 湖南时代阳光药业股份有限公司 | Anti-virus Chinese herbal medicine composition, traditional Chinese medicine composition and preparation method thereof |
CN104173926A (en) * | 2014-08-20 | 2014-12-03 | 赵燕翼 | Xinshubao dropping pill and preparation method thereof |
-
2017
- 2017-06-20 CN CN201710471059.2A patent/CN107233392A/en active Pending
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1448174A (en) * | 2003-05-03 | 2003-10-15 | 南通精华制药有限公司 | Application of cymose buckwheat rhizome in preparation of antiviral drug |
CN102068492A (en) * | 2011-01-05 | 2011-05-25 | 湖南时代阳光药业股份有限公司 | Anti-virus Chinese herbal medicine composition, traditional Chinese medicine composition and preparation method thereof |
CN104173926A (en) * | 2014-08-20 | 2014-12-03 | 赵燕翼 | Xinshubao dropping pill and preparation method thereof |
Non-Patent Citations (2)
Title |
---|
《中国民族药志》编委会: "《中国民族药志》", 31 December 2007, 四川民族出版社 * |
张耕等: "《常见中药毒性研究进展及应用》", 30 September 2013, 湖北科学技术出版社 * |
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Application publication date: 20171010 |