CN107224937A - A kind of chemical reaction kettle of uniform dropping liquid - Google Patents
A kind of chemical reaction kettle of uniform dropping liquid Download PDFInfo
- Publication number
- CN107224937A CN107224937A CN201710626466.6A CN201710626466A CN107224937A CN 107224937 A CN107224937 A CN 107224937A CN 201710626466 A CN201710626466 A CN 201710626466A CN 107224937 A CN107224937 A CN 107224937A
- Authority
- CN
- China
- Prior art keywords
- kettle
- communicated
- chemical reaction
- dropping liquid
- cooling tube
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000006243 chemical reaction Methods 0.000 title claims abstract description 33
- 239000007788 liquid Substances 0.000 title claims abstract description 28
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 36
- 239000000463 material Substances 0.000 claims abstract description 33
- 238000001816 cooling Methods 0.000 claims abstract description 31
- 238000003756 stirring Methods 0.000 claims abstract description 15
- 238000007790 scraping Methods 0.000 claims abstract description 12
- 239000012530 fluid Substances 0.000 claims description 19
- 238000010030 laminating Methods 0.000 claims 1
- 238000010276 construction Methods 0.000 abstract 1
- 238000005516 engineering process Methods 0.000 description 5
- 239000000376 reactant Substances 0.000 description 3
- 238000009825 accumulation Methods 0.000 description 2
- 238000005039 chemical industry Methods 0.000 description 2
- 230000036632 reaction speed Effects 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000003905 agrochemical Substances 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 239000005060 rubber Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/0013—Controlling the temperature of the process
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/02—Feed or outlet devices; Feed or outlet control devices for feeding measured, i.e. prescribed quantities of reagents
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F28—HEAT EXCHANGE IN GENERAL
- F28D—HEAT-EXCHANGE APPARATUS, NOT PROVIDED FOR IN ANOTHER SUBCLASS, IN WHICH THE HEAT-EXCHANGE MEDIA DO NOT COME INTO DIRECT CONTACT
- F28D7/00—Heat-exchange apparatus having stationary tubular conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall
- F28D7/02—Heat-exchange apparatus having stationary tubular conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall the conduits being helically coiled
- F28D7/024—Heat-exchange apparatus having stationary tubular conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall the conduits being helically coiled the conduits of only one medium being helically coiled tubes, the coils having a cylindrical configuration
Abstract
The invention discloses a kind of chemical reaction kettle of uniform dropping liquid, including kettle, feed pipe is communicated with the right side of the upper end of the kettle, the upper center of kettle is installed with motor, the output shaft of motor is connected with agitating shaft, stirring frame is welded with agitating shaft, the both sides of stirring frame are fixedly connected with material scraping plate, rotary shaft is provided with below agitating shaft, scraper plate is fixedly connected with rotary shaft, cooling device is provided with the outside of kettle, cooling device includes cooling tube, the upper end side of cooling tube is communicated with water inlet pipe, the lower end side of cooling tube is communicated with outlet pipe, water inlet pipe and outlet pipe are connected with water tank, the junction of water inlet pipe and water tank is provided with water pump in water tank, the present invention is simple in construction, it is reasonable in design, accurate dropwise reaction can be carried out, kettle can be cooled simultaneously, the heat of generation can also effectively be utilized, energy-conserving and environment-protective.
Description
Technical field
The present invention relates to a kind of reactor, specifically a kind of chemical reaction kettle of uniform dropping liquid.
Background technology
Answering the broad understanding of kettle has the container physically or chemically reacted, is matched somebody with somebody by the structure design to container and parameter
Put, realize the mixture function of the heating of technological requirement, evaporation, cooling and low high speed, reactor be widely used in oil, chemical industry,
Rubber, agricultural chemicals, dyestuff, medicine, food, for completing to vulcanize, nitrify, hydrogenate, hydrocarbonylation, polymerization, the pressure of the technical process such as condensation
Force container.
With the continuous development of scientific technology, modern reactor production technology is more and more ripe, but modern
Reactor remains more defect, such as modern when chemical reaction is carried out, reactant often adds micro
Reactant, these reactants are either added or add to have lacked can all very big influence to reaction, and modern reactor
Lack effective equipment to carry out often producing substantial amounts of heat during dropwise reaction, simultaneous reactions, more heat is not
Only influence whether that the normal of reactor is used, and these heats are all directly to be radiated in air, it is impossible to obtain effective profit
With.
Therefore, being directed to the problem of being proposed in above-mentioned background technology, those skilled in the art propose a kind of new chemical industry
Reactor.
The content of the invention
It is an object of the invention to provide a kind of chemical reaction kettle of uniform dropping liquid, to solve to propose in above-mentioned background technology
The problem of.
To achieve the above object, the present invention provides following technical scheme：
Connect on the right side of a kind of chemical reaction kettle of uniform dropping liquid, including kettle, cooling device and motor, the upper end of the kettle
It is connected with to be provided with fluid reservoir, fluid reservoir on the left of feed pipe, the upper end of kettle and is vertically arranged with liquid level rod, the lower end of fluid reservoir leads to
Cross drain pipe and be communicated with liquid reserve tank, drain pipe and be provided with valve, liquid reserve tank is fixedly mounted on the inside of the upper end of kettle；The kettle
The upper center of body is installed with motor, and the output shaft of motor is connected with agitating shaft, and agitating shaft is vertically arranged in
Stirring frame is welded with inside kettle, on agitating shaft, the both sides of stirring frame are fixedly connected with material scraping plate；Uniformly opened on the material scraping plate
Provided with multiple sieve material holes, sieve material is fixedly installed cross cutter in hole；Rotary shaft is provided with below the agitating shaft, is rotated
Axle is horizontally set in kettle, and scraper plate is fixedly connected with rotary shaft, and the two ends of rotary shaft pass through clutch shaft bearing and second respectively
Bearing is rotated with kettle and is connected, and one end of rotary shaft passes kettle and is fixedly connected with L-shaped drive rod；The bottom both sides of the kettle
Support column is fixedly connected with, the center bottom of kettle is communicated with discharge nozzle；Cooling device is provided with the outside of the kettle, is cooled down
Device includes cooling tube；The upper end side of the cooling tube is communicated with water inlet pipe, and the lower end side of cooling tube is communicated with outlet pipe,
Water inlet pipe and outlet pipe are connected with water tank, and the junction of water inlet pipe and water tank is provided with water pump in water tank.
Further, the fluid reservoir is made of clear material.
Further, the lower end of the liquid reserve tank is uniformly communicated with multiple fluid holes.
Further, multiple through holes are uniformly offered on the stirring frame.
Further, the material scraping plate is fitted with the madial wall of kettle.
Further, the cooling tube is twist wrapped on the lateral wall of kettle.
Compared with prior art, the present invention adds main reaction material into kettle by feed pipe, and institute is added in fluid reservoir
The micro-reaction material needed, by control valve, so that micro-reaction material is slowly added dropwise into kettle by fluid hole, so that
The purpose accurately controlled is reached, reaction is stirred by stirring frame, the through hole improved on reaction rate, stirring frame is further carried
High reaction speed, while material scraping plate can prevent material sticks on the madial wall of kettle, the cross that sieve material hole is provided with is cut
The material scattering of adhesion can be driven scraper plate to rotate by cutter by L-shaped drive rod, prevent solid accumulation at the bottom of kettle
Cold water can be passed through in portion, course of reaction into cooling tube, so as to cool to kettle, the water for absorbing heat is back to water tank
It inside may be used as domestic water.
Brief description of the drawings
Fig. 1 is the structural representation of the chemical reaction kettle of uniform dropping liquid.
Fig. 2 for uniform dropping liquid chemical reaction kettle in cooling device structural representation.
Fig. 3 for uniform dropping liquid chemical reaction kettle in cooling tube top view.
Embodiment
The technical scheme of this patent is described in more detail with reference to embodiment.
Fig. 1-3, a kind of chemical reaction kettle of uniform dropping liquid, including kettle 7, cooling device and motor 22 are referred to,
It is communicated with the left of feed pipe 23, the upper end of kettle 7 and is provided with fluid reservoir 1, fluid reservoir 1 vertically on the right side of the upper end of the kettle 7
Liquid level rod 2 is provided with, the lower end of fluid reservoir 1 is communicated with liquid reserve tank 5, drain pipe 3 by drain pipe 3 is provided with valve 4, liquid storage
Case 5 is fixedly mounted on the inside of the upper end of kettle 7；The upper center of the kettle 7 is installed with motor 22, motor
22 output shaft is connected with agitating shaft 18, and agitating shaft 18 is vertically arranged in inside kettle 7, and stirring frame is welded with agitating shaft 18
20, the both sides of stirring frame 20 are fixedly connected with material scraping plate 8；Multiple sieve material holes 9, sieve material hole 9 are uniformly offered on the material scraping plate 8
Inside it is fixedly installed cross cutter 10；The lower section of the agitating shaft 18 is provided with rotary shaft 12, and rotary shaft 12 is horizontally set on
In kettle 7, scraper plate 13 is fixedly connected with rotary shaft 12, the two ends of rotary shaft 12 pass through clutch shaft bearing 11 and second bearing respectively
16 are connected with the rotation of kettle 7, and one end of rotary shaft 12 passes kettle 7 and is fixedly connected with L-shaped drive rod 17；The bottom of the kettle 7
End both sides are fixedly connected with support column 14, and the center bottom of kettle 7 is communicated with discharge nozzle 15；The outside of the kettle 7 is provided with
Cooling device, cooling device includes cooling tube 21；The upper end side of the cooling tube 21 is communicated with water inlet pipe 24, cooling tube 21
Lower end side is communicated with outlet pipe 25, and water inlet pipe 24 and outlet pipe 25 are connected with water tank 26, the company of water inlet pipe 24 and water tank 26
Connect to be in water tank 26 and be provided with water pump 27.
Above-mentioned, fluid reservoir 1 is made of clear material.
Above-mentioned, the lower end of liquid reserve tank 5 is uniformly communicated with multiple fluid holes 6.
It is above-mentioned, uniformly offer multiple through holes 19 on stirring frame 20.
Above-mentioned, material scraping plate 8 is fitted with the madial wall of kettle 7.
Above-mentioned, cooling tube 21 is twist wrapped on the lateral wall of kettle 7.
The present invention operation principle be：Main reaction material is added into kettle 2 by feed pipe 23, added in fluid reservoir 1
Required micro-reaction material, by control valve 4, so that micro-reaction thing be slowly added dropwise into kettle 7 by fluid hole 6
Material, so as to reach the purpose accurately controlled, reaction is stirred by stirring frame 20, is improved on reaction rate, stirring frame 20
Through hole 19 further increases reaction speed, while material scraping plate 8 can prevent material sticks on the madial wall of kettle 7, sieve material
The material scattering of adhesion can be driven 13 turns of scraper plate by the cross cutter 10 that hole 9 is provided with by L-shaped drive rod 17
It is dynamic, prevent solid accumulation to be passed through cold water into cooling tube 21 in the bottom of kettle 7, course of reaction, so as to enter to kettle 7
Row cooling, the water of absorption heat, which is back in water tank 26, may be used as domestic water.
The better embodiment to this patent is explained in detail above, but this patent is not limited to above-mentioned embodiment party
, can also be on the premise of this patent objective not be departed from formula, the knowledge that one skilled in the relevant art possesses
Make a variety of changes.
Claims (6)
1. a kind of chemical reaction kettle of uniform dropping liquid, including kettle, cooling device and motor, it is characterised in that the kettle
It is communicated with to be provided with fluid reservoir, fluid reservoir on the left of feed pipe, the upper end of kettle on the right side of the upper end of body and is vertically arranged with liquid level rod,
The lower end of fluid reservoir is communicated with liquid reserve tank, drain pipe by drain pipe and is provided with valve, and liquid reserve tank is fixedly mounted on kettle
On the inside of upper end；The upper center of the kettle is installed with motor, and the output shaft of motor is connected with agitating shaft, stirred
Mix axle to be vertically arranged in inside kettle, stirring frame is welded with agitating shaft, the both sides of stirring frame are fixedly connected with material scraping plate；It is described
Multiple sieve material holes are uniformly offered on material scraping plate, sieve material is fixedly installed cross cutter in hole；Set below the agitating shaft
Rotary shaft is equipped with, rotary shaft is horizontally set in kettle, scraper plate is fixedly connected with rotary shaft, the two ends of rotary shaft pass through respectively
Clutch shaft bearing and second bearing are rotated with kettle to be connected, and one end of rotary shaft passes kettle and is fixedly connected with L-shaped drive rod；It is described
The bottom both sides of kettle are fixedly connected with support column, and the center bottom of kettle is communicated with discharge nozzle；The outside of the kettle is set
There is cooling device, cooling device includes cooling tube；The upper end side of the cooling tube is communicated with water inlet pipe, the lower end one of cooling tube
Side is communicated with outlet pipe, and water inlet pipe and outlet pipe are connected with water tank, and the junction of water inlet pipe and water tank is provided with water tank
Water pump.
2. the chemical reaction kettle of uniform dropping liquid according to claim 1, it is characterised in that the fluid reservoir is by transparent material
It is made.
3. the chemical reaction kettle of uniform dropping liquid according to claim 1, it is characterised in that the lower end of the liquid reserve tank is uniform
It is communicated with multiple fluid holes.
4. the chemical reaction kettle of uniform dropping liquid according to claim 1, it is characterised in that uniformly opened up on the stirring frame
There are multiple through holes.
5. the chemical reaction kettle of uniform dropping liquid according to claim 1, it is characterised in that the material scraping plate and kettle it is interior
Side wall laminating.
6. the chemical reaction kettle of uniform dropping liquid according to claim 1, it is characterised in that the cooling tube is twist twined
It is wound on the lateral wall of kettle.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710626466.6A CN107224937A (en) | 2017-07-27 | 2017-07-27 | A kind of chemical reaction kettle of uniform dropping liquid |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710626466.6A CN107224937A (en) | 2017-07-27 | 2017-07-27 | A kind of chemical reaction kettle of uniform dropping liquid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107224937A true CN107224937A (en) | 2017-10-03 |
Family
ID=59957770
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710626466.6A Pending CN107224937A (en) | 2017-07-27 | 2017-07-27 | A kind of chemical reaction kettle of uniform dropping liquid |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107224937A (en) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108176338A (en) * | 2017-12-30 | 2018-06-19 | 郑州默尔电子信息技术有限公司 | A kind of chemical industry raw material retort |
| CN109053436A (en) * | 2018-09-26 | 2018-12-21 | 郑州睿科生化科技有限公司 | One-step method by biomass ethyl levulinate improvement device |
| CN109107511A (en) * | 2018-08-23 | 2019-01-01 | 管洪化 | A kind of accurately Chemical Manufacture reaction kettle that feeds |
| CN110127775A (en) * | 2019-05-16 | 2019-08-16 | 赣州逸豪优美科实业有限公司 | A kind of reaction kettle for the dropping liquid uniform, controllable being used to prepare cobalt carbonate |
| CN110787757A (en) * | 2019-11-22 | 2020-02-14 | 耒阳金悦科技发展有限公司 | Reaction kettle |
| CN111705215A (en) * | 2020-06-15 | 2020-09-25 | 赣州智晟知识产权咨询服务有限公司 | Fluorescent waste material dissolving reaction device |
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| CN2645759Y (en) * | 2003-07-08 | 2004-10-06 | 中国石油化工股份有限公司齐鲁分公司 | Polymerization kettle with internal cool mixer |
| JP2014223581A (en) * | 2013-05-16 | 2014-12-04 | 株式会社井上製作所 | Low shear type concentric biaxial mixer |
| CN205627929U (en) * | 2016-03-24 | 2016-10-12 | 漯河医学高等专科学校 | Chemical reaction kettle |
| CN205761146U (en) * | 2016-05-26 | 2016-12-07 | 宁波大学 | A kind of rotation frame chemical reaction still |
| CN205761136U (en) * | 2016-05-24 | 2016-12-07 | 江西洪安化工有限公司 | A kind of uniform dropping liquid chemical reaction still of improvement |
-
2017
- 2017-07-27 CN CN201710626466.6A patent/CN107224937A/en active Pending
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Non-Patent Citations (1)
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|---|
| 谭蔚: "《化工设备设计基础（第二版）》", 31 March 2007, 天津大学出版社 * |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108176338A (en) * | 2017-12-30 | 2018-06-19 | 郑州默尔电子信息技术有限公司 | A kind of chemical industry raw material retort |
| CN109107511A (en) * | 2018-08-23 | 2019-01-01 | 管洪化 | A kind of accurately Chemical Manufacture reaction kettle that feeds |
| CN109053436A (en) * | 2018-09-26 | 2018-12-21 | 郑州睿科生化科技有限公司 | One-step method by biomass ethyl levulinate improvement device |
| CN109053436B (en) * | 2018-09-26 | 2021-03-02 | 郑州睿科生化科技有限公司 | Improved device for preparing ethyl levulinate from biomass by one-step method |
| CN110127775A (en) * | 2019-05-16 | 2019-08-16 | 赣州逸豪优美科实业有限公司 | A kind of reaction kettle for the dropping liquid uniform, controllable being used to prepare cobalt carbonate |
| CN110127775B (en) * | 2019-05-16 | 2021-08-31 | 赣州逸豪优美科实业有限公司 | A even controllable reation kettle of dropping liquid for preparing cobalt carbonate |
| CN110787757A (en) * | 2019-11-22 | 2020-02-14 | 耒阳金悦科技发展有限公司 | Reaction kettle |
| CN111705215A (en) * | 2020-06-15 | 2020-09-25 | 赣州智晟知识产权咨询服务有限公司 | Fluorescent waste material dissolving reaction device |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
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| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20171003 |
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