CN111705215A - Fluorescent waste material dissolving reaction device - Google Patents
Fluorescent waste material dissolving reaction device Download PDFInfo
- Publication number
- CN111705215A CN111705215A CN202010540419.1A CN202010540419A CN111705215A CN 111705215 A CN111705215 A CN 111705215A CN 202010540419 A CN202010540419 A CN 202010540419A CN 111705215 A CN111705215 A CN 111705215A
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- China
- Prior art keywords
- gear
- tank cover
- drip irrigation
- threaded
- fluorescent
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- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B7/00—Working up raw materials other than ores, e.g. scrap, to produce non-ferrous metals and compounds thereof; Methods of a general interest or applied to the winning of more than two metals
- C22B7/006—Wet processes
- C22B7/007—Wet processes by acid leaching
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- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B59/00—Obtaining rare earth metals
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
Abstract
The invention relates to the technical field of dissolution reaction devices, in particular to a fluorescence waste dissolution reaction device, a plurality of drip irrigation pipes are fixedly arranged on the outer surface of the round barrel along the circumferential direction, each drip irrigation pipe is communicated with the inside of the round barrel, and each drip irrigation pipe is provided with a plurality of drip irrigation holes along the length direction, the surface of the bottom of the drum is fixedly provided with a connecting disc through screws, the lower surface of the connecting disc is fixedly provided with a stirring shaft, the shaft body of the stirring shaft is fixedly provided with a plurality of groups of stirring blades along the length direction, an acid liquor injection mechanism corresponding to the drum is fixedly arranged on the tank cover, a top plate is fixedly arranged at the top ends of the two supporting plates, a transverse plate is fixedly arranged between the two top plates, the transverse plate is provided with a moving module corresponding to the tank cover, and the tail end of the outer side of any one of the rotating shafts is fixedly provided with a limiting mechanism. The invention has the advantages of accurate control of acid liquor injection amount, no violent reaction and more uniform reaction.
Description
Technical Field
The invention relates to the technical field of dissolution reaction devices, in particular to a fluorescence waste dissolution reaction device.
Background
Fluorescent powder, commonly known as noctilucent powder, is generally classified into photo-induced energy storage noctilucent powder and noctilucent powder with radioactivity. The light-induced energy storage luminous powder is prepared by irradiating fluorescent powder with natural light, daylight lamp light, ultraviolet light and the like, storing light energy, and slowly releasing the light energy in a fluorescent mode after the light irradiation is stopped, so that the luminous powder can still see luminescence at night or in a dark place for a duration of several hours to dozens of hours.
At present, China is in the stage of rapid development of science and technology, the production technology is rapidly improved, the product is rapidly updated, due to factors of production and use, domestic fluorescent powder waste reaches dozens of thousands of tons every year, the fluorescent powder waste contains rare earth elements, and the method has great recycling value. One of the recycling processes is to dissolve the phosphor waste, and if too much acid is added at one time during the process of dissolving the phosphor waste, the reaction is too violent, so that workers are easily harmed. Therefore, a dissolution reaction apparatus capable of slowly adding an acid solution is required to solve the above problems.
Disclosure of Invention
The invention aims to solve the problem that the reaction is violent and unsafe due to excessive addition of acid liquor in the prior art, and provides a fluorescent waste material dissolving reaction device.
In order to achieve the purpose, the invention adopts the following technical scheme:
the design is a fluorescent waste dissolution reaction device, which comprises a base, wherein two supporting plates which are correspondingly arranged are fixedly arranged on the base in a surface fixing manner, a rotating shaft is rotatably arranged on each supporting plate, the two rotating shafts are correspondingly arranged, a tank body is fixedly arranged between the two inner ends of the rotating shafts, a tank cover which is matched with the tank body is arranged at the opening at the top end of the tank body, a first motor is fixedly arranged at the center of the tank cover, an output shaft of the first motor penetrates through the tank cover and then is fixedly connected to the inner bottom of a barrel, a plurality of drip irrigation pipes are fixedly arranged on the outer surface of the barrel along the circumferential direction, each drip irrigation pipe is communicated with the inside of the barrel, a plurality of drip irrigation holes are formed in each drip irrigation pipe along the length direction, a connecting disc is fixedly arranged on the surface of the bottom of the barrel through screws, the fixed stirring vane of a plurality of groups of along length direction on the axis body of (mixing) shaft, the fixed acidizing fluid injection mechanism that is equipped with corresponding with the cask on the jar lid, two equal fixed mounting in backup pad top has a roof, two fixed mounting has the diaphragm between the roof, install the removal module corresponding with the cover on the diaphragm, arbitrary one fixed stop gear that is equipped with on the outside tip of pivot.
Preferably, the moving module comprises a threaded sleeve, a threaded rod, a driving mechanism and a guiding mechanism, the threaded sleeve is rotatably mounted on the transverse plate, the threaded rod matched with the threaded sleeve is mounted in the threaded sleeve in a threaded mode, the bottom end of the threaded rod is connected with the tank cover through the guiding mechanism, and the driving mechanism is connected to the threaded sleeve in a transmission mode.
Preferably, the driving mechanism comprises a first gear, a second gear and a second motor, the transverse plate is fixedly provided with the second motor corresponding to the threaded sleeve, the tail end of an output shaft of the second motor is fixedly provided with the second gear, the wall of the threaded sleeve is fixedly provided with the first gear, and the first gear is meshed with the second gear.
Preferably, guiding mechanism includes spliced pole, dead lever, sliding sleeve, guide arm, fixed mounting has two corresponding spliced poles on the bonnet, fixed mounting has the dead lever between the spliced pole top, the both ends of dead lever are all fixed and are equipped with a sliding sleeve, can overlap in the sliding sleeve and be equipped with the guide arm of a looks adaptation with it, the equal fixed connection in top of guide arm is on the diaphragm, the bottom fixed connection of threaded rod is at the dead lever upper surface.
Preferably, the threaded rod top end is threadedly provided with a limiting block.
Preferably, the limiting mechanism comprises a rotary table, a handle, a bolt and a cylinder, the rotary table is fixedly mounted at the tail end of the outer side of the rotary shaft, the handle is fixedly mounted on the outer surface of the rotary table, the bolt penetrates through the handle, the cylinder corresponding to the bolt is fixedly mounted on the base, and the bottom end of the thread is mounted at the top end of the cylinder.
Preferably, the surface of the handle is provided with anti-skid grains.
Preferably, the acid liquor injection mechanism comprises a drainage tube and a connecting hose, the drainage tube is arranged on the tank cover in a penetrating mode, the bottom end of the drainage tube penetrates through the tank cover and then extends into the round barrel, one end of the connecting hose is installed at the bottom end of the drainage tube in a threaded mode, and the other end of the connecting hose is connected with the output end of the acid liquor supply device.
Preferably, the inner surface of the tank cover is coated with a rubber layer, and the rest tank body of the tank cover is in interference fit.
The invention provides a fluorescent waste dissolving reaction device, which has the beneficial effects that: by arranging the drum, the drip irrigation pipe, the stirring shaft, the stirring blade and the like, after acid liquor is injected into the drum through the acid liquor injection mechanism, the first motor is started; acidizing fluid is in getting into the cask back, through drip irrigation the even slow fluorescent waste material that drips into in the jar body of driping into of the hole on the pipe to the rotatory output shaft drive cask of first motor is rotatory, thereby drives the (mixing) shaft rotation, and rotatory epaxial stirring vane that stirs is continuous stirs the waste material, makes more even abundant of reaction like this.
Drawings
FIG. 1 is a first schematic structural diagram of a fluorescent waste dissolution reaction apparatus according to the present invention;
FIG. 2 is a schematic structural diagram of a fluorescent waste dissolution reaction apparatus according to the present invention;
FIG. 3 is a schematic structural diagram III of a fluorescent waste dissolution reaction apparatus according to the present invention;
FIG. 4 is a schematic diagram of a first structure of a moving module of a fluorescent waste dissolution reaction apparatus according to the present invention;
FIG. 5 is a schematic diagram of a second structure of a moving module of the fluorescent waste dissolution reaction apparatus according to the present invention;
FIG. 6 is a schematic cross-sectional view of a fluorescent waste dissolution reaction apparatus according to the present invention;
FIG. 7 is a schematic view of a portion of the structure of FIG. 2 at A;
FIG. 8 is a schematic view of a portion of the structure of FIG. 5 at B;
fig. 9 is a partial structural view at C of fig. 6.
In the figure: the drip irrigation device comprises a base 1, a supporting plate 2, a rotating shaft 3, a tank body 4, a top plate 5, a transverse plate 6, a tank cover 7, a first motor 8, a rotating shaft 9, a barrel 10, a drip irrigation pipe 11, a drip irrigation hole 12, a connecting disc 13, a stirring shaft 14, a stirring blade 15, a connecting column 16, a fixing rod 17, a sliding sleeve 18, a guide rod 19, a threaded sleeve 20, a threaded rod 21, a first gear 22, a second gear 23, a second motor 24, a limiting block 25, a rotating disc 26, a handle 27, a bolt 28, a cylinder 29, a drainage pipe 30 and a connecting hose 31.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments.
Example 1
Referring to fig. 1-9, a fluorescent waste material dissolving reaction device comprises a base 1, two corresponding supporting plates 2 are fixedly mounted on the upper surface of the base 1, a rotating shaft 3 is rotatably mounted on each supporting plate 2, the two rotating shafts 3 are correspondingly arranged, a tank body 4 is fixedly mounted between the inner ends of the two rotating shafts 3, a tank cover 7 matched with the tank body is mounted at the opening at the top end of the tank body 4, a rubber layer is sprayed on the inner surface of the tank cover 7, and the tank cover 7 is in interference fit with the tank body 4.
A first motor 8 is fixedly arranged at the center of the tank cover 7, an output shaft of the first motor 8 penetrates through the tank cover 7 and then is fixedly connected with the bottom in the drum 10, a plurality of drip irrigation pipes 11 are fixedly arranged on the outer surface of the drum 10 along the circumferential direction, each drip irrigation pipe 10 is communicated with the inside of the drum 10, and all open along length direction on every drip irrigation pipe 11 and have a plurality of drip irrigation holes 12, there is connection pad 13 on the surface of cask 10 bottom through screw fixed mounting, the fixed surface is equipped with (mixing) shaft 14 under connection pad 13, it is equipped with a plurality of stirring vane 15 of group to fix along length direction on the axis body of (mixing) shaft 14, fixed being equipped with the acidizing fluid injection mechanism corresponding with cask 10 on the cover 7, 2 equal fixed mounting in top of two backup pads has a roof 5, fixed mounting has diaphragm 6 between two roofs 5, install the removal module corresponding with cover 7 on the diaphragm 6, fixed being equipped with stop gear on the outside tip of arbitrary pivot 3.
The acid liquor injection mechanism comprises a drainage tube 30 and a connecting hose 31, the drainage tube 30 penetrates through the tank cover 7, the bottom end of the drainage tube 30 penetrates through the tank cover 7 and then extends into the barrel 10, one end of the connecting hose 31 is installed at the bottom end of the drainage tube 30 in a threaded mode, and the other end of the connecting hose 31 is connected with the output end of the acid liquor supply device.
When the fluorescent waste-adding device is used, a user firstly lifts the tank cover 7 by using the moving module so as to add fluorescent waste into the net tank body 4 conveniently; after the addition is finished, the mobile module is controlled to close the tank cover 7, acid liquor is injected into the barrel 10 through the acid liquor injection mechanism, and the first motor 8 is started; acid liquor is in getting into cask 10 back, through driping irrigation the even slow fluorescent waste material that drips into in jar body 4 of driping into of 12 drip irrigation hole on the pipe 11 to the rotatory output shaft drive cask 10 of first motor 8 is rotatory, thereby drives the (mixing) shaft 14 rotation, and stirring vane 15 on the rotatory (mixing) shaft 14 is continuous stirs the waste material, makes more even abundant of reaction like this.
Example 2
Referring to fig. 1-7, as another preferred embodiment of the present invention, the difference from embodiment 1 is that the moving module includes a threaded sleeve 20, a threaded rod 21, a driving mechanism, and a guiding mechanism, the threaded sleeve 20 is rotatably mounted on the transverse plate 6, the threaded rod 21 adapted to the threaded sleeve 20 is mounted in the threaded sleeve 20, the bottom end of the threaded rod 21 is connected with the can lid 7 through the guiding mechanism, and the driving mechanism is connected to the threaded sleeve 21 in a transmission manner.
The driving mechanism comprises a first gear 22, a second gear 23 and a second motor 24, the transverse plate 6 is fixedly provided with the second motor 24 corresponding to the threaded sleeve 20, the tail end of an output shaft of the second motor 24 is fixedly provided with the second gear 23, the cylinder wall of the threaded sleeve 20 is fixedly provided with the first gear 22, and the first gear 22 is meshed with the second gear 23.
The guide mechanism comprises connecting columns 16, a fixing rod 17, sliding sleeves 18 and guide rods 19, two corresponding connecting columns 16 are fixedly mounted on the tank cover 7, the fixing rod 17 is fixedly mounted between the top ends of the connecting columns 16, the sliding sleeves 18 are fixedly arranged at two ends of the fixing rod 17, the guide rods 19 matched with the sliding sleeves 18 can be sleeved in the sliding sleeves 18, the top ends of the guide rods 19 are fixedly connected to the transverse plate 6, and the bottom ends of the threaded rods 21 are fixedly connected to the upper surface of the fixing rod 17. The bottom end of the threaded rod 21 is provided with a limiting block 25 in a threaded manner.
The threaded rod 20 is driven by the driving mechanism in a gear transmission mode to move up and down in the threaded sleeve 20, so that the fixed rod 17 moves up and down, the tank cover 7 moves up and down along with the fixed rod 17, and the tank cover 7 can be opened and closed; two guide rods 19 may limit the threaded rod 20.
Example 3
Referring to fig. 1-3, as another preferred embodiment of the present invention, the difference from embodiment 1 is that the limiting mechanism includes a rotating disc 26, a handle 27, a bolt 28, and a cylinder 29, the rotating disc 26 is fixedly mounted at the outer end of any one of the rotating shafts 3, the handle 27 is fixedly mounted on the outer surface of the rotating disc 26, the bolt 28 is disposed on the handle 27 in a threaded manner, the cylinder 29 corresponding to the bolt 28 is fixedly mounted on the base 1, and the bottom end of the thread 28 is threadedly mounted on the top end of the cylinder 29. The surface of the grip 27 is provided with anti-skid lines.
After the fluorescent fertilizer in the tank body 4 is fully reacted, the mobile module is controlled to lift the tank cover 7, the drum 10, the stirring shaft 14 and other mechanisms below the tank cover 7 are taken out of the tank body 4, then a collecting vessel is placed on one side of the base 1, then the bolt 28 is detached, the handle 28 is held, the rotary disc 26 is rotated, so that the tank body 4 is inclined to the side of the collecting vessel, and the material which is reacted in the tank body 4 is poured into the collecting vessel.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.
Claims (9)
1. The utility model provides a fluorescence waste material dissolves reaction unit, includes base (1), its characterized in that, fixed surface installs two backup pads (2) that correspond the setting on base (1), every all can rotate on backup pad (2) and install a pivot (3), and two pivot (3) correspond the setting, two fixed mounting has a jar body (4) between pivot (3) inboard end, jar body (4) top opening part is installed and is had cover (7) of looks adaptation with it, positive department fixed mounting has first motor (8) on cover (7), fixed connection is in cask (10) bottom after the output shaft of first motor (8) passes cover (7), cask (10) outer surface is driped irrigation along circumference fixed and is equipped with a plurality of pipe (11), every drip irrigation pipe (10) all are linked together with cask (10) inside, and every it has a plurality of drip irrigation holes (12) all to open along length direction on drip irrigation pipe (11), there are connection pad (13) on cask (10) bottom surface through screw fixed mounting, connection pad (13) lower fixed surface is equipped with (mixing) shaft (14), be equipped with a plurality of stirring vane (15) of group along length direction is fixed on the axis body of (mixing) shaft (14), fixed acidizing fluid injection mechanism corresponding with cask (10), two of being equipped with on cover (7) backup pad (2) top is equal fixed mounting has a roof (5), two fixed mounting has diaphragm (6) between roof (5), install the removal module corresponding with cover (7) on diaphragm (6), arbitrary one fixed stop gear that is equipped with on the outside tip of pivot (3).
2. The fluorescent waste dissolving reaction device according to claim 1, wherein the moving module comprises a threaded sleeve (20), a threaded rod (21), a driving mechanism and a guiding mechanism, the threaded sleeve (20) is rotatably mounted on the transverse plate (6), the threaded rod (21) matched with the threaded sleeve (20) is mounted in the threaded sleeve (20) in a threaded manner, the bottom end of the threaded rod (21) is connected with the tank cover (7) through the guiding mechanism, and the driving mechanism is in transmission connection with the threaded sleeve (21).
3. The fluorescent waste dissolving reaction device according to claim 2, wherein the driving mechanism comprises a first gear (22), a second gear (23) and a second motor (24), the transverse plate (6) is fixedly provided with the second motor (24) corresponding to the threaded sleeve (20), the tail end of the output shaft of the second motor (24) is fixedly provided with the second gear (23), the wall of the threaded sleeve (20) is fixedly provided with the first gear (22), and the first gear (22) is meshed with the second gear (23).
4. The fluorescent waste dissolving reaction device according to claim 2, wherein the guiding mechanism comprises connecting columns (16), fixing rods (17), sliding sleeves (18) and guide rods (19), two corresponding connecting columns (16) are fixedly installed on the tank cover (7), the fixing rods (17) are fixedly installed between the top ends of the connecting columns (16), the sliding sleeves (18) are fixedly arranged at two ends of the fixing rods (17), the guide rods (19) matched with the sliding sleeves (18) are sleeved in the sliding sleeves (18), the top ends of the guide rods (19) are fixedly connected to the transverse plate (6), and the bottom ends of the threaded rods (21) are fixedly connected to the upper surfaces of the fixing rods (17).
5. The fluorescent waste dissolution reaction unit as set forth in claim 2, wherein a stopper (25) is threadedly mounted on a top end of the threaded rod (21).
6. The fluorescent waste dissolving reaction device according to claim 1, wherein the limiting mechanism comprises a rotary table (26), a handle (27), a bolt (28) and a cylinder (29), the rotary table (26) is fixedly installed at the outer end of the rotating shaft (3), the handle (27) is fixedly installed on the outer surface of the rotary table (26), the bolt (28) is arranged on the handle (27) in a penetrating manner through threads, the cylinder (29) corresponding to the bolt (28) is fixedly installed on the base (1), and the bottom end of the thread (28) is installed at the top end of the cylinder (29) in a threaded manner.
7. The fluorescent waste dissolution reaction apparatus as set forth in claim 6, wherein the surface of the handle (27) is provided with anti-slip lines.
8. The fluorescent waste dissolution reaction device as set forth in claim 1, wherein the acid solution injection mechanism comprises a drainage tube (30) and a connection hose (31), the drainage tube (30) is disposed through the tank cover (7), the bottom end of the drainage tube (30) extends into the drum (10) after passing through the tank cover (7), one end of the connection hose (31) is threadedly mounted at the bottom end of the drainage tube (30), and the other end of the connection hose (31) is connected with the output end of the acid solution supply device.
9. The fluorescent waste dissolving reaction device as claimed in claim 1, wherein the inner surface of the tank cover (7) is coated with a rubber layer, and the tank cover (7) is in interference fit with the tank body (4).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010540419.1A CN111705215A (en) | 2020-06-15 | 2020-06-15 | Fluorescent waste material dissolving reaction device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010540419.1A CN111705215A (en) | 2020-06-15 | 2020-06-15 | Fluorescent waste material dissolving reaction device |
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| CN111705215A true CN111705215A (en) | 2020-09-25 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN202010540419.1A Pending CN111705215A (en) | 2020-06-15 | 2020-06-15 | Fluorescent waste material dissolving reaction device |
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| CN (1) | CN111705215A (en) |
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| CN210736704U (en) * | 2019-10-17 | 2020-06-12 | 珠海横琴新区御峰沉香产业有限公司 | Supercritical extraction device for agilawood essential oil |
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| CN206762819U (en) * | 2016-11-24 | 2017-12-19 | 东莞市源岭硅胶科技有限公司 | New and effective mixer |
| CN206415124U (en) * | 2017-01-20 | 2017-08-18 | 赣州齐畅新材料有限公司 | A kind of fluorescent powder scrap is dissolved with sour molten retort |
| CN107224937A (en) * | 2017-07-27 | 2017-10-03 | 杨旦群 | A kind of chemical reaction kettle of uniform dropping liquid |
| CN208244574U (en) * | 2018-04-16 | 2018-12-18 | 南雄市瑞晟化学工业有限公司 | A kind of resin agitating reaction kettle |
| CN208465888U (en) * | 2018-05-18 | 2019-02-05 | 嘉善东大树脂有限公司 | A kind of unsaturated polyester resin reaction kettle of adjustable autoclave body angle |
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Application publication date: 20200925 |
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